CN106337299A - Dyeing method of wool fiber top - Google Patents

Dyeing method of wool fiber top Download PDF

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Publication number
CN106337299A
CN106337299A CN201610709898.9A CN201610709898A CN106337299A CN 106337299 A CN106337299 A CN 106337299A CN 201610709898 A CN201610709898 A CN 201610709898A CN 106337299 A CN106337299 A CN 106337299A
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weight portion
weight
wool top
wool
dye vat
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CN201610709898.9A
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陈金涛
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Changshu Xinhuayuan Colored Tops Factory
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Changshu Xinhuayuan Colored Tops Factory
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Priority to CN201610709898.9A priority Critical patent/CN106337299A/en
Publication of CN106337299A publication Critical patent/CN106337299A/en
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    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/52—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing synthetic macromolecular substances
    • D06P1/5207—Macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • D06P1/5214—Polymers of unsaturated compounds containing no COOH groups or functional derivatives thereof
    • D06P1/5242—Polymers of unsaturated N-containing compounds
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/60—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing polyethers
    • D06P1/613—Polyethers without nitrogen
    • D06P1/6131—Addition products of hydroxyl groups-containing compounds with oxiranes
    • D06P1/6135—Addition products of hydroxyl groups-containing compounds with oxiranes from aromatic alcohols or from phenols, naphthols
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/62—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds with sulfate, sulfonate, sulfenic or sulfinic groups
    • D06P1/621—Compounds without nitrogen
    • D06P1/622—Sulfonic acids or their salts
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
    • D06P1/642—Compounds containing nitrogen
    • D06P1/645—Aliphatic, araliphatic or cycloaliphatic compounds containing amino groups
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
    • D06P1/642—Compounds containing nitrogen
    • D06P1/647—Nitrogen-containing carboxylic acids or their salts
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
    • D06P1/642—Compounds containing nitrogen
    • D06P1/649—Compounds containing carbonamide, thiocarbonamide or guanyl groups
    • D06P1/6495—Compounds containing carbonamide -RCON= (R=H or hydrocarbons)
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/673—Inorganic compounds
    • D06P1/67333—Salts or hydroxides
    • D06P1/6735—Salts or hydroxides of alkaline or alkaline-earth metals with anions different from those provided for in D06P1/67341
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
    • D06P3/02—Material containing basic nitrogen
    • D06P3/04—Material containing basic nitrogen containing amide groups
    • D06P3/14—Wool

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Coloring (AREA)

Abstract

The invention discloses a dyeing method of wool fiber top, comprising the following steps: 1) successively adding tristyrylphenol polyoxyelhylene ether sulfonate, acryloyloxyethyltrimethyl ammonium chloride, polyvinylpyrrolidone, dimethyl formamide and vegetable dye into a dye vat and successively pouring deionized water, uniformly stirring and heating to 45 DEG C; 2) successively pouring N-methyldiethanolamine, linear alklybezene sulfonates, magnesium sulfate and nitrilotriacetic acid, continuously stirring until the materials are fully and uniformly mixed, and heating to 60 DEG C; 3) immersing top into the dye vat for 50 min; 4) drying the immersed top at 85 DEG C; 5) immersing the dried top in clear water and rinsing for 50 min; and 6) taking the rinsed top out of the clear water and naturally airing. The top dyed by the above method has excellent color fastness and has good dyeing uniformity and has no dyeing defect.

Description

The colouring method of wool fiber top
Technical field
The present invention relates to the colouring method of wool fiber top.
Background technology
The colouring method of existing wool fiber top, the color fastness of dyeing wool top is not high, and dyeing uniformity is bad, and easily Produce color flower.
Content of the invention
It is an object of the invention to provide a kind of colouring method of wool fiber top, the wool top after its dyeing has excellent Weathering color fastness, Washing, dry-cleaning color fastness, colorfastness to rubbing, PERSPIRATION COLOR FASTNESS, colour fastness to water, chlorine drift color jail Degree, non-chlorine drift color fastness, and dyeing uniformity is good, colourless flower.
For achieving the above object, the technical scheme is that and design a kind of colouring method of wool fiber top, including Following steps:
1) 1～2 weight portion tristyrylphenol polyoxyethylene ether sulfonate, 0.7 weight portion are sequentially added in dye vat Acrylyl oxy-ethyl-trimethyl salmiac, 1.3 weight account polyethylene ketopyrrolidines, 0.7 weight portion dimethylformamide, 30 weight Part vegetable colour puts into 100 parts by weight of deionized water successively, stirs, and is heated to 45 DEG C；
2) put into successively again 1.4 weight portion n- methyl diethanolamines, 0.7 weight portion 2-Sulfosuccinic acid Diisooctyl sodium, 0.4 Parts sulfuric acid magnesium, 4.3 weight portion nitrilotriacetic acid(NTA), continue stirring, uniform to being sufficiently mixed, and are heated to 60 DEG C；
3) wool top is immersed in 50 minutes in dye vat；
4) wool top after soaking is dried at 85 DEG C；
5) rinse 50 minutes in the wool top immersion clear water after drying；
6) take out the wool top after rinsing naturally to dry.
Preferably, the colouring method of wool fiber top, comprises the steps:
1) 1 weight portion tristyrylphenol polyoxyethylene ether sulfonate, 0.7 parts by weight propylene are sequentially added in dye vat Acyloxyethyl trimethyl ammonium chloride, 1.3 weight account polyethylene ketopyrrolidines, 0.7 weight portion dimethylformamide, 30 weight portions are planted Thing dyestuff puts into 100 parts by weight of deionized water successively, stirs, and is heated to 45 DEG C；
2) put into successively again 1.4 weight portion n- methyl diethanolamines, 0.7 weight portion 2-Sulfosuccinic acid Diisooctyl sodium, 0.4 Parts sulfuric acid magnesium, 4.3 weight portion nitrilotriacetic acid(NTA), continue stirring, uniform to being sufficiently mixed, and are heated to 60 DEG C；
3) wool top is immersed in 50 minutes in dye vat；
4) wool top after soaking is dried at 85 DEG C；
5) rinse 50 minutes in the wool top immersion clear water after drying；
6) take out the wool top after rinsing naturally to dry.
Preferably, the colouring method of wool fiber top, comprises the steps:
1) 2 weight portion tristyrylphenol polyoxyethylene ether sulfonate, 0.7 parts by weight propylene are sequentially added in dye vat Acyloxyethyl trimethyl ammonium chloride, 1.3 weight account polyethylene ketopyrrolidines, 0.7 weight portion dimethylformamide, 30 weight portions are planted Thing dyestuff puts into 100 parts by weight of deionized water successively, stirs, and is heated to 45 DEG C；
2) put into successively again 1.4 weight portion n- methyl diethanolamines, 0.7 weight portion 2-Sulfosuccinic acid Diisooctyl sodium, 0.4 Parts sulfuric acid magnesium, 4.3 weight portion nitrilotriacetic acid(NTA), continue stirring, uniform to being sufficiently mixed, and are heated to 60 DEG C；
3) wool top is immersed in 50 minutes in dye vat；
4) wool top after soaking is dried at 85 DEG C；
5) rinse 50 minutes in the wool top immersion clear water after drying；
6) take out the wool top after rinsing naturally to dry.
Preferably, the colouring method of wool fiber top, comprises the steps:
1) 1.2 weight portion tristyrylphenol polyoxyethylene ether sulfonate, 0.7 weight portion third are sequentially added in dye vat Alkene acyloxyethyl trimethyl ammonium chloride, 1.3 weight account polyethylene ketopyrrolidines, 0.7 weight portion dimethylformamide, 30 weight portions Vegetable colour puts into 100 parts by weight of deionized water successively, stirs, and is heated to 45 DEG C；
2) put into successively again 1.4 weight portion n- methyl diethanolamines, 0.7 weight portion 2-Sulfosuccinic acid Diisooctyl sodium, 0.4 Parts sulfuric acid magnesium, 4.3 weight portion nitrilotriacetic acid(NTA), continue stirring, uniform to being sufficiently mixed, and are heated to 60 DEG C；
3) wool top is immersed in 50 minutes in dye vat；
4) wool top after soaking is dried at 85 DEG C；
5) rinse 50 minutes in the wool top immersion clear water after drying；
6) take out the wool top after rinsing naturally to dry.
Advantages of the present invention and having the beneficial effects that: provide a kind of colouring method of wool fiber top, after its dyeing Wool top has excellent weathering color fastness, Washing, dry-cleaning color fastness, colorfastness to rubbing, PERSPIRATION COLOR FASTNESS, water stain color jail Degree, chlorine drift color fastness, non-chlorine drift color fastness, and dyeing uniformity is good, colourless flower.
The Color of wool top is to be largely to be determined by dyestuff, the component of auxiliary agent and proportioning in dye vat, and Processing step, technological parameter (time, temperature etc.) also function to pivotal role.
In dye vat, the different component of " dyestuff, auxiliary agent " can influence each other, the synthesis of various ingredients and its proportioning, can very great Cheng The final Color of wool top is determined on degree, if the component of " dyestuff, auxiliary agent " and proportioning be not mutually coordinated, single component is carried The beneficial effect come, even can be eliminated by other components abatement, when serious, different component is mutually conflicted, and does not have entirety Comprehensive function, produces negative interaction and substandard products.The present invention passes through a large amount of creative works, repeatedly verifies, obtains " dyestuff, auxiliary agent " Optimal component and proportioning so that various ingredients combine, mutually coordinated and produce positive comprehensive effect.
The present invention, more on the basis of the optimal component and proportioning of above-mentioned " dyestuff, auxiliary agent ", is equipped with and is somebody's turn to do " dyestuff, auxiliary agent " phase Supporting optimum process step, technological parameter is so that the final Color of wool top reaches optimum.
Specific embodiment
With reference to embodiment, the specific embodiment of the present invention is further described.Following examples are only used for more Plus clearly demonstrate technical scheme, and can not be limited the scope of the invention with this.
The technical scheme that the present invention is embodied as is:
Embodiment 1
The colouring method of wool fiber top, comprises the steps:
1) 1～2 weight portion tristyrylphenol polyoxyethylene ether sulfonate, 0.7 weight portion are sequentially added in dye vat Acrylyl oxy-ethyl-trimethyl salmiac, 1.3 weight account polyethylene ketopyrrolidines, 0.7 weight portion dimethylformamide, 30 weight Part vegetable colour puts into 100 parts by weight of deionized water successively, stirs, and is heated to 45 DEG C；
2) put into successively again 1.4 weight portion n- methyl diethanolamines, 0.7 weight portion 2-Sulfosuccinic acid Diisooctyl sodium, 0.4 Parts sulfuric acid magnesium, 4.3 weight portion nitrilotriacetic acid(NTA), continue stirring, uniform to being sufficiently mixed, and are heated to 60 DEG C；
3) wool top is immersed in 50 minutes in dye vat；
4) wool top after soaking is dried at 85 DEG C；
5) rinse 50 minutes in the wool top immersion clear water after drying；
6) take out the wool top after rinsing naturally to dry.
Embodiment 2
The colouring method of wool fiber top, comprises the steps:
1) 1 weight portion tristyrylphenol polyoxyethylene ether sulfonate, 0.7 parts by weight propylene are sequentially added in dye vat Acyloxyethyl trimethyl ammonium chloride, 1.3 weight account polyethylene ketopyrrolidines, 0.7 weight portion dimethylformamide, 30 weight portions are planted Thing dyestuff puts into 100 parts by weight of deionized water successively, stirs, and is heated to 45 DEG C；
2) put into successively again 1.4 weight portion n- methyl diethanolamines, 0.7 weight portion 2-Sulfosuccinic acid Diisooctyl sodium, 0.4 Parts sulfuric acid magnesium, 4.3 weight portion nitrilotriacetic acid(NTA), continue stirring, uniform to being sufficiently mixed, and are heated to 60 DEG C；
3) wool top is immersed in 50 minutes in dye vat；
4) wool top after soaking is dried at 85 DEG C；
5) rinse 50 minutes in the wool top immersion clear water after drying；
6) take out the wool top after rinsing naturally to dry.
Embodiment 3
The colouring method of wool fiber top, comprises the steps:
1) 2 weight portion tristyrylphenol polyoxyethylene ether sulfonate, 0.7 parts by weight propylene are sequentially added in dye vat Acyloxyethyl trimethyl ammonium chloride, 1.3 weight account polyethylene ketopyrrolidines, 0.7 weight portion dimethylformamide, 30 weight portions are planted Thing dyestuff puts into 100 parts by weight of deionized water successively, stirs, and is heated to 45 DEG C；
2) put into successively again 1.4 weight portion n- methyl diethanolamines, 0.7 weight portion 2-Sulfosuccinic acid Diisooctyl sodium, 0.4 Parts sulfuric acid magnesium, 4.3 weight portion nitrilotriacetic acid(NTA), continue stirring, uniform to being sufficiently mixed, and are heated to 60 DEG C；
3) wool top is immersed in 50 minutes in dye vat；
4) wool top after soaking is dried at 85 DEG C；
5) rinse 50 minutes in the wool top immersion clear water after drying；
6) take out the wool top after rinsing naturally to dry.
Embodiment 4
The colouring method of wool fiber top, comprises the steps:
1) 1.2 weight portion tristyrylphenol polyoxyethylene ether sulfonate, 0.7 weight portion third are sequentially added in dye vat Alkene acyloxyethyl trimethyl ammonium chloride, 1.3 weight account polyethylene ketopyrrolidines, 0.7 weight portion dimethylformamide, 30 weight portions Vegetable colour puts into 100 parts by weight of deionized water successively, stirs, and is heated to 45 DEG C；
2) put into successively again 1.4 weight portion n- methyl diethanolamines, 0.7 weight portion 2-Sulfosuccinic acid Diisooctyl sodium, 0.4 Parts sulfuric acid magnesium, 4.3 weight portion nitrilotriacetic acid(NTA), continue stirring, uniform to being sufficiently mixed, and are heated to 60 DEG C；
3) wool top is immersed in 50 minutes in dye vat；
4) wool top after soaking is dried at 85 DEG C；
5) rinse 50 minutes in the wool top immersion clear water after drying；
6) take out the wool top after rinsing naturally to dry.
Through the various embodiments described above dyeing after wool top have excellent weathering color fastness, Washing, dry-cleaning color fastness, Colorfastness to rubbing, PERSPIRATION COLOR FASTNESS, colour fastness to water, chlorine drift color fastness, non-chlorine drift color fastness, and dyeing uniformity is good, colourless Flower.
The above is only the preferred embodiment of the present invention it is noted that ordinary skill people for the art For member, on the premise of without departing from the technology of the present invention principle, some improvements and modifications can also be made, these improvements and modifications Also should be regarded as protection scope of the present invention.

Claims (4)

1. the colouring method of wool fiber top is it is characterised in that comprise the steps:
1) 1～2 weight portion tristyrylphenol polyoxyethylene ether sulfonate, 0.7 parts by weight propylene are sequentially added in dye vat Acyloxyethyl trimethyl ammonium chloride, 1.3 weight account polyethylene ketopyrrolidines, 0.7 weight portion dimethylformamide, 30 weight portions are planted Thing dyestuff puts into 100 parts by weight of deionized water successively, stirs, and is heated to 45 DEG C；
2) 1.4 weight portion n- methyl diethanolamines, 0.7 weight portion 2-Sulfosuccinic acid Diisooctyl sodium, 0.4 weight are put into again successively Part magnesium sulfate, 4.3 weight portion nitrilotriacetic acid(NTA), continue stirring, uniform to being sufficiently mixed, and are heated to 60 DEG C；
3) wool top is immersed in 50 minutes in dye vat；
4) wool top after soaking is dried at 85 DEG C；
5) rinse 50 minutes in the wool top immersion clear water after drying；
6) take out the wool top after rinsing naturally to dry.
2. the colouring method of wool fiber top according to claim 1 is it is characterised in that comprise the steps:
1) 1 weight portion tristyrylphenol polyoxyethylene ether sulfonate, 0.7 parts by weight propylene acyl-oxygen are sequentially added in dye vat Ethyl-trimethyl salmiac, 1.3 weight account polyethylene ketopyrrolidines, 0.7 weight portion dimethylformamide, 30 weight portion plant dyes Material puts into 100 parts by weight of deionized water successively, stirs, and is heated to 45 DEG C；
2) 1.4 weight portion n- methyl diethanolamines, 0.7 weight portion 2-Sulfosuccinic acid Diisooctyl sodium, 0.4 weight are put into again successively Part magnesium sulfate, 4.3 weight portion nitrilotriacetic acid(NTA), continue stirring, uniform to being sufficiently mixed, and are heated to 60 DEG C；
3) wool top is immersed in 50 minutes in dye vat；
4) wool top after soaking is dried at 85 DEG C；
5) rinse 50 minutes in the wool top immersion clear water after drying；
6) take out the wool top after rinsing naturally to dry.
3. the colouring method of wool fiber top according to claim 1 is it is characterised in that comprise the steps:
1) 2 weight portion tristyrylphenol polyoxyethylene ether sulfonate, 0.7 parts by weight propylene acyl-oxygen are sequentially added in dye vat Ethyl-trimethyl salmiac, 1.3 weight account polyethylene ketopyrrolidines, 0.7 weight portion dimethylformamide, 30 weight portion plant dyes Material puts into 100 parts by weight of deionized water successively, stirs, and is heated to 45 DEG C；
2) 1.4 weight portion n- methyl diethanolamines, 0.7 weight portion 2-Sulfosuccinic acid Diisooctyl sodium, 0.4 weight are put into again successively Part magnesium sulfate, 4.3 weight portion nitrilotriacetic acid(NTA), continue stirring, uniform to being sufficiently mixed, and are heated to 60 DEG C；
3) wool top is immersed in 50 minutes in dye vat；
4) wool top after soaking is dried at 85 DEG C；
5) rinse 50 minutes in the wool top immersion clear water after drying；
6) take out the wool top after rinsing naturally to dry.
4. the colouring method of wool fiber top according to claim 1 is it is characterised in that comprise the steps:
1) 1.2 weight portion tristyrylphenol polyoxyethylene ether sulfonate, 0.7 parts by weight propylene acyl are sequentially added in dye vat Oxy-ethyl-trimethyl salmiac, 1.3 weight account polyethylene ketopyrrolidines, 0.7 weight portion dimethylformamide, 30 weight portion plants Dyestuff puts into 100 parts by weight of deionized water successively, stirs, and is heated to 45 DEG C；
2) 1.4 weight portion n- methyl diethanolamines, 0.7 weight portion 2-Sulfosuccinic acid Diisooctyl sodium, 0.4 weight are put into again successively Part magnesium sulfate, 4.3 weight portion nitrilotriacetic acid(NTA), continue stirring, uniform to being sufficiently mixed, and are heated to 60 DEG C；
3) wool top is immersed in 50 minutes in dye vat；
4) wool top after soaking is dried at 85 DEG C；
5) rinse 50 minutes in the wool top immersion clear water after drying；
6) take out the wool top after rinsing naturally to dry.
CN201610709898.9A 2016-08-24 2016-08-24 Dyeing method of wool fiber top Pending CN106337299A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106894247A (en) * 2017-02-16 2017-06-27 山东如意科技集团有限公司 A kind of method that wool top is locally dyeed
CN106893640A (en) * 2017-03-15 2017-06-27 张太平 A kind of surface cleaner of thread
CN108755198A (en) * 2018-06-20 2018-11-06 界首市旭派服饰有限公司 A method of improving reactive blue level-dyeing property on cotton fabric

Citations (5)

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Application publication date: 20170118