CN106336742A - Preparing method of thermal insulation antirust paint - Google Patents

Preparing method of thermal insulation antirust paint Download PDF

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Publication number
CN106336742A
CN106336742A CN201610753876.2A CN201610753876A CN106336742A CN 106336742 A CN106336742 A CN 106336742A CN 201610753876 A CN201610753876 A CN 201610753876A CN 106336742 A CN106336742 A CN 106336742A
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CN
China
Prior art keywords
parts
antirust paint
paint
aluminium silicate
hermetic container
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610753876.2A
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Chinese (zh)
Inventor
徐超
马浩亮
胡飞
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Anhui Huizhishang Electromechanical Technology Co Ltd
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Anhui Huizhishang Electromechanical Technology Co Ltd
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Application filed by Anhui Huizhishang Electromechanical Technology Co Ltd filed Critical Anhui Huizhishang Electromechanical Technology Co Ltd
Priority to CN201610753876.2A priority Critical patent/CN106336742A/en
Publication of CN106336742A publication Critical patent/CN106336742A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D125/00Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an aromatic carbocyclic ring; Coating compositions based on derivatives of such polymers
    • C09D125/02Homopolymers or copolymers of hydrocarbons
    • C09D125/04Homopolymers or copolymers of styrene
    • C09D125/08Copolymers of styrene
    • C09D125/14Copolymers of styrene with unsaturated esters
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/08Anti-corrosive paints
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00Specific properties of additives
    • C08K2201/011Nanostructured additives
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00Specific properties of additives
    • C08K2201/014Additives containing two or more different additives of the same subgroup in C08K
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2201/00Properties
    • C08L2201/08Stabilised against heat, light or radiation or oxydation
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2203/00Applications
    • C08L2203/18Applications used for pipes
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/03Polymer mixtures characterised by other features containing three or more polymers in a blend
    • C08L2205/035Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Application Of Or Painting With Fluid Materials (AREA)
  • Paints Or Removers (AREA)

Abstract

The invention relates to the field of antirust paint, in particular to a preparing method of a thermal insulation antirust paint. The antirust paint is prepared from, by weight, 8-10 parts of calder lai resin, 6-9 parts of mica iron oxide, 38-42 parts of styrene-acrylic emulsion, 11-16 parts of amylopectin, 5-7 parts of zinc borate, 3-4 parts of polymethyl methacrylate, 1-2 parts of simethicone, 3-6 parts of dimethyl benzyl carbonyl butylate, 6-8 parts of ceramic hollow microspheres, 1-2 parts of sodium fluosilicate, 3-5 parts of nano aluminium silicate, 0.5-1.5 parts of 5, 8-dyhydroxy-1, 4-naphthoquinone, 7-10 parts of deionized water. The thermal insulation antirust paint has good cohesiveness and the property can stabilize under the temperature of 43-55 DEG C. The antirust paint has a strong waterproof ability after being dried, and bubbling phenomena will not happen under high temperature of 300 DEG C. The antirust paint has a very good heat-insulating property, and is especially suitable for rust-proof treatment of heating pipelines; in addition, the antirust paint has very good inoxidizability.

Description

A kind of preparation method of insulating anti-rust paint
Technical field
The present invention relates to antirust paint field is and in particular to a kind of preparation method of insulating anti-rust paint.
Background technology
Antirust paint substantially oiliness and two kinds of aqueouss.Oily antirust varniss makes the greasy removal of material surface difficult, seldom makes With.Oily antirust varniss is easy to use, cheap, but because containing noxious substances such as nitrite, chromate, endangering to operator Evil is larger, and country limits use, and such properties of product are single.
Aqueous antirust paint uses more and more extensively, but current antirust paint does not have heat-proof quality, will prevent at some It is very inconvenient that occasion heat-insulated again of becoming rusty uses.
Content of the invention
The technical problem to be solved is to provide a kind of preparation method of insulating anti-rust paint.
The technical problem to be solved employs the following technical solutions to realize:
A kind of preparation method of insulating anti-rust paint, comprises the following steps:
(1) prepare each raw material of following weight portion: Ka get Lai resin 8-10 part, micaceous iron oxide 6-9 part, styrene-acrylic emulsion 38-42 part, amylopectin 11-16 part, Firebrake ZB 5-7 part, polymethyl methacrylate 3-4 part, dimethicone 1-2 part, fourth Sour dimethylbenzyl base ester 3-6 part, ceramic hollow microballon 6-8 part, prodan 1-2 part, nanometer aluminium silicate 3-5 part, 5,8- bis- Hydroxyl -1,4- two naphthoquinone 0.5-1.5 part, deionized water 7-10 part;
(2) by Ka get Lai resin, polymethyl methacrylate, the melting of butanoic acid dimethylbenzyl base ester, then add thereto Enter micaceous iron oxide, nanometer aluminium silicate, and dispersed with stirring is uniform;
(3) step (2) gained compound is put into expanded in bulking machine, expanded after material put in hermetic container and process 30 minutes;
(4) step (3) resulting material and amylopectin, Firebrake ZB, ceramic hollow microballon, fluorine are added in styrene-acrylic emulsion Sodium silicate, nanometer aluminium silicate, 5,8- dihydroxy-Isosorbide-5-Nitrae-two naphthoquinone, deionized water, stir under 2500-2800 rev/min of rotating speed 10 minutes;
(5) it is mixed into dimethicone in step (4) resulting material, be cooled to room temperature and obtain final product antirust paint.
It is filled with mixed gas in hermetic container, in hermetic container, pressure is 2.4mpa, mixed gas composition group in step (3) Become and by its accounting be: carbon dioxide 23%, nitrogen 47%, vapor 15%, carboxylic acid steam 15%.
In step (4), mixing speed is 2600 revs/min.
The invention has the beneficial effects as follows: antirust paint caking property of the present invention is good, stable in properties at a temperature of -43 DEG C~55 DEG C Constant, antirust paint has extremely strong antiseepage outlet capacity after being dried, and does not produce bubbling phenomenon under 300 DEG C of high temperature, antirust The heat-proof quality of paint is very good, is particularly suitable for the antirust treatment in heating pad pipe road, antirust paint also has extraordinary non-oxidizability.
Specific embodiment
In order that technological means, creation characteristic, reached purpose and effect that the present invention realizes are easy to understand, tie below Close specific embodiment, the present invention is expanded on further.
Embodiment 1
A kind of preparation method of insulating anti-rust paint, comprises the following steps:
(1) prepare each raw material of following weight portion: 9 parts of Ka get Lai resin, 8 parts of micaceous iron oxide, styrene-acrylic emulsion 40 part, 14 parts of chain starch, 6 parts of Firebrake ZB, 3 parts of polymethyl methacrylate, 1 part of dimethicone, 4 parts of butanoic acid dimethylbenzyl base ester, 7 parts of ceramic hollow microballon, 1 part of prodan, 4 parts of nanometer aluminium silicate, 1 part of 5,8- dihydroxy -1,4- two naphthoquinone, deionized water 8 Part;
(2) by Ka get Lai resin, polymethyl methacrylate, the melting of butanoic acid dimethylbenzyl base ester, then add thereto Enter micaceous iron oxide, nanometer aluminium silicate, and dispersed with stirring is uniform;
(3) step (2) gained compound is put into expanded in bulking machine, expanded after material put in hermetic container and process 30 minutes;
(4) step (3) resulting material and amylopectin, Firebrake ZB, ceramic hollow microballon, fluorine are added in styrene-acrylic emulsion Sodium silicate, nanometer aluminium silicate, 5,8- dihydroxy-Isosorbide-5-Nitrae-two naphthoquinone, deionized water, stir 10 points under 2600 revs/min of rotating speeds Clock;
(5) it is mixed into dimethicone in step (4) resulting material, be cooled to room temperature and obtain final product antirust paint.
It is filled with mixed gas in hermetic container, in hermetic container, pressure is 2.4mpa, mixed gas composition group in step (3) Become and by its accounting be: carbon dioxide 23%, nitrogen 47%, vapor 15%, carboxylic acid steam 15%.
Embodiment 2
A kind of preparation method of insulating anti-rust paint, comprises the following steps:
(1) prepare each raw material of following weight portion: 8 parts of Ka get Lai resin, 6 parts of micaceous iron oxide, styrene-acrylic emulsion 38 part, 11 parts of chain starch, 5 parts of Firebrake ZB, 3 parts of polymethyl methacrylate, 1 part of dimethicone, 3 parts of butanoic acid dimethylbenzyl base ester, 6 parts of ceramic hollow microballon, 1 part of prodan, 3 parts of nanometer aluminium silicate, 0.5 part of 5,8- dihydroxy -1,4- two naphthoquinone, deionized water 7 parts;
(2) by Ka get Lai resin, polymethyl methacrylate, the melting of butanoic acid dimethylbenzyl base ester, then add thereto Enter micaceous iron oxide, nanometer aluminium silicate, and dispersed with stirring is uniform;
(3) step (2) gained compound is put into expanded in bulking machine, expanded after material put in hermetic container and process 30 minutes;
(4) step (3) resulting material and amylopectin, Firebrake ZB, ceramic hollow microballon, fluorine are added in styrene-acrylic emulsion Sodium silicate, nanometer aluminium silicate, 5,8- dihydroxy-Isosorbide-5-Nitrae-two naphthoquinone, deionized water, stir 10 points under 2500 revs/min of rotating speeds Clock;
(5) it is mixed into dimethicone in step (4) resulting material, be cooled to room temperature and obtain final product antirust paint.
It is filled with mixed gas in hermetic container, in hermetic container, pressure is 2.4mpa, mixed gas composition group in step (3) Become and by its accounting be: carbon dioxide 23%, nitrogen 47%, vapor 15%, carboxylic acid steam 15%.
Embodiment 3
A kind of preparation method of insulating anti-rust paint, comprises the following steps:
(1) prepare following weight portion each raw material: 10 parts of Ka get Lai resin, 9 parts of micaceous iron oxide, 42 parts of styrene-acrylic emulsion, 16 parts of amylopectin, 7 parts of Firebrake ZB, 4 parts of polymethyl methacrylate, 2 parts of dimethicone, butanoic acid dimethylbenzyl base ester 6 Part, 8 parts of ceramic hollow microballon, 2 parts of prodan, 5 parts of nanometer aluminium silicate, 1.5 parts of 5,8- dihydroxy -1,4- two naphthoquinone, go from 10 parts of sub- water;
(2) by Ka get Lai resin, polymethyl methacrylate, the melting of butanoic acid dimethylbenzyl base ester, then add thereto Enter micaceous iron oxide, nanometer aluminium silicate, and dispersed with stirring is uniform;
(3) step (2) gained compound is put into expanded in bulking machine, expanded after material put in hermetic container and process 30 minutes;
(4) step (3) resulting material and amylopectin, Firebrake ZB, ceramic hollow microballon, fluorine are added in styrene-acrylic emulsion Sodium silicate, nanometer aluminium silicate, 5,8- dihydroxy-Isosorbide-5-Nitrae-two naphthoquinone, deionized water, stir 10 points under 2800 revs/min of rotating speeds Clock;
(5) it is mixed into dimethicone in step (4) resulting material, be cooled to room temperature and obtain final product antirust paint.
It is filled with mixed gas in hermetic container, in hermetic container, pressure is 2.4mpa, mixed gas composition group in step (3) Become and by its accounting be: carbon dioxide 23%, nitrogen 47%, vapor 15%, carboxylic acid steam 15%.
Ultimate principle and principal character and the advantages of the present invention of the present invention have been shown and described above.The technology of the industry , it should be appreciated that the present invention is not restricted to the described embodiments, the simply explanation described in above-described embodiment and description is originally for personnel The principle of invention, without departing from the spirit and scope of the present invention, the present invention also has various changes and modifications, these changes Change and improvement both falls within scope of the claimed invention.Claimed scope by appending claims and its Equivalent thereof.

Claims (3)

1. a kind of preparation method of insulating anti-rust paint is it is characterised in that comprise the following steps:
(1) prepare each raw material of following weight portion: Ka get Lai resin 8-10 part, micaceous iron oxide 6-9 part, styrene-acrylic emulsion 38-42 Part, amylopectin 11-16 part, Firebrake ZB 5-7 part, polymethyl methacrylate 3-4 part, dimethicone 1-2 part, butanoic acid diformazan Base benzyl former ester 3-6 part, ceramic hollow microballon 6-8 part, prodan 1-2 part, nanometer aluminium silicate 3-5 part, 5,8- dihydroxy -1, 4- bis- naphthoquinone 0.5-1.5 part, deionized water 7-10 part;
(2) by Ka get Lai resin, polymethyl methacrylate, the melting of butanoic acid dimethylbenzyl base ester, then it is added thereto to cloud Female ferrum oxide, nanometer aluminium silicate, and dispersed with stirring is uniform;
(3) step (2) gained compound is put into expanded in bulking machine, expanded after material put in hermetic container and process 30 points Clock;
(4) step (3) resulting material and amylopectin, Firebrake ZB, ceramic hollow microballon, hexafluosilicic acid are added in styrene-acrylic emulsion Sodium, nanometer aluminium silicate, 5,8- dihydroxy-Isosorbide-5-Nitrae-two naphthoquinone, deionized water, stir 10 points under 2500-2800 rev/min of rotating speed Clock;
(5) it is mixed into dimethicone in step (4) resulting material, be cooled to room temperature and obtain final product antirust paint.
2. as claimed in claim 1 a kind of preparation method of insulating anti-rust paint it is characterised in that hermetic container in step (3) Inside it is filled with mixed gas, in hermetic container, pressure is 2.4mpa, mixed gas composition composition by its accounting is: carbon dioxide 23%th, nitrogen 47%, vapor 15%, carboxylic acid steam 15%.
3. as claimed in claim 1 a kind of preparation method of insulating anti-rust paint it is characterised in that mixing speed in step (4) For 2600 revs/min.
CN201610753876.2A 2016-08-29 2016-08-29 Preparing method of thermal insulation antirust paint Pending CN106336742A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106928782A (en) * 2017-03-14 2017-07-07 天津千岛汽车配件有限公司 A kind of bicycle electric light paint

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103819989A (en) * 2014-02-24 2014-05-28 浙江大学 Aqueous anticorrosive heat-insulation paint and preparation method
CN104845473A (en) * 2015-04-29 2015-08-19 广德嘉宝莉化工有限公司 High-strength, shock-resistant and abrasion-resistant mechanical paint
CN104877484A (en) * 2015-06-18 2015-09-02 常州益和节能科技有限公司 Water-borne energy-saving heat insulation and preservation coating for petrochemical engineering oil tank and preparation method thereof
CN105623400A (en) * 2014-11-04 2016-06-01 赵燕 Thermal-insulation coating

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103819989A (en) * 2014-02-24 2014-05-28 浙江大学 Aqueous anticorrosive heat-insulation paint and preparation method
CN105623400A (en) * 2014-11-04 2016-06-01 赵燕 Thermal-insulation coating
CN104845473A (en) * 2015-04-29 2015-08-19 广德嘉宝莉化工有限公司 High-strength, shock-resistant and abrasion-resistant mechanical paint
CN104877484A (en) * 2015-06-18 2015-09-02 常州益和节能科技有限公司 Water-borne energy-saving heat insulation and preservation coating for petrochemical engineering oil tank and preparation method thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106928782A (en) * 2017-03-14 2017-07-07 天津千岛汽车配件有限公司 A kind of bicycle electric light paint

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