CN106332953A - Preparation method of meat product non-phosphorus water retaining agent - Google Patents

Preparation method of meat product non-phosphorus water retaining agent Download PDF

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Publication number
CN106332953A
CN106332953A CN201610746875.5A CN201610746875A CN106332953A CN 106332953 A CN106332953 A CN 106332953A CN 201610746875 A CN201610746875 A CN 201610746875A CN 106332953 A CN106332953 A CN 106332953A
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water retaining
water
rhizoma amorphophalli
retaining agent
meat
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丁玉琴
张晶
陆娜
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23BPRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
    • A23B4/00General methods for preserving meat, sausages, fish or fish products
    • A23B4/14Preserving with chemicals not covered by groups A23B4/02 or A23B4/12
    • A23B4/18Preserving with chemicals not covered by groups A23B4/02 or A23B4/12 in the form of liquids or solids
    • A23B4/20Organic compounds; Microorganisms; Enzymes
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Microbiology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Meat, Egg Or Seafood Products (AREA)

Abstract

The invention discloses a preparation method of a meat product non-phosphorus water retaining agent and belongs to the technical field of water retaining agents. The method includes the steps that konjak is subjected to enzymolysis to obtain enzymolysis extract, the enzymolysis extract, sodium alginate and calcium salt are compounded to prepare a gel-like mixture, the gel-like mixture is blend-modified with plant fermentation liquor, and finally the water retaining agent is prepared. Konjak glucan substances rich in konjak zymolyte enter meat through the permeation to be combined with myogen, the stability of protein is enhanced, the protein structure is kept loose, water binding capacity is improved, the material is compounded with sodium alginate gel, the plant fermentation liquor rich in hydrophilic group is used for blending modification, the water retaining capacity is improved, the water retaining agent forms a macromolecular hydrophilic net structure in the meat, a better water retaining effect is achieved, and the water retaining agent can be suitable for meat water retaining.

Description

A kind of preparation method of meat productss phosphate-free water-retaining agent
Technical field
The invention discloses a kind of preparation method of meat productss phosphate-free water-retaining agent, belong to water-retaining agent technical field.
Background technology
Muscle water-retaining property also known as being waterpower or retention ability, refer to when muscle be subject to external force act on when, keep original moisture with Add the ability of moisture, percentage of water loss shows as the amount of liquid discharging under external force from muscle protein system or through certain The moisture that time is lost accounts for the percent of meat weight before dehydration.Muscle water-retaining property and percentage of water loss have certain dependency, and muscle is protected Aqueouss can be stronger, represents that percentage of water loss is lower, meat is soft, meat is better.The moisture of muscle is 70~75%, and major part is Free state.Another part moisture in muscle is motionless water, and the presence of this part water is to be subject to steric to affect and tie The attraction of Heshui, it is present in the structure of muscle but is not combined with neutral protein, and this part water is in the meat after firm government official Can not freely flow, when being dried nor take away, also be not easy frozen, but stablize water change with cyto-architectural and This part water of the decline of ph is eventually discharged.
Participate in the mainly free water of water-retaining property change.The holding of free water with protein space structure is relevant, electrostatic Lotus amount etc. has substantial connection.When the network-like structure for conveying of protein, more juicy can be contained;Amount of electrostatic charge has two aspects Impact, on the one hand, the presence of electrostatic charge attracts hydrone to assemble to it;On the other hand, it makes to produce electrostatic between protein molecule Repulsion, higher electrostatic charge produces larger repulsive force, leads to protein structure to relax, improves retention ability.Protein molecule drops Solution also results in the rising of retention ability, and original albumen is changed into small molecule, and aminoacid makes osmotic pressure raise, and strengthens retention ability.Tradition Water-retaining agent be the retention ability improving meat productss using the mix preparation of tripolyphosphate and a small amount of hexametaphosphate.In meals Phosphate content excessively can be combined into, in intestinal, the orthophosphate being insoluble in water for a long time with calcium, thus reducing the suction to calcium for the human body Receive.The inappropriate food of life-time service calcium-phosphorus ratio, can lead to discharge the insufficient section of calcium or phosphorus from skeleton.When continuing Between can cause hypoevolutism, skeleton deformity, bone and tooth poor quality for a long time, and then human body is caused with certain harm.
Content of the invention
Present invention mainly solves technical problem: be mostly tripolyphosphate and a small amount of for meat water-retaining agent traditional at present The mix preparation of hexametaphosphate, human body can be detrimental to health after being eaten for a long time absorption and lead to hypoevolutism, skeleton deformity Defect, the method obtains enzymatic hydrolyzed extract by digesting Rhizoma amorphophalli, itself and sodium alginate and calcium salt is compounded prepared gel and mixes Compound, then with plant fermented liquid to its blending and modifying, water-retaining agent is finally obtained.The present invention is using the evil spirit being rich in Rhizoma amorphophalli zymolyte Taro glucan material is entered inside meat by osmosiss, is combined with myogen, strengthens the stability of protein, makes albumen Matter structure keeps lax, improves retentiveness, then compounds with sodium alginate gel, with the plant fermented liquid rich in hydrophilic radical altogether Mixed modification, improves its water holding capacity, makes water-retaining agent form the hydrophilic network structure of macromole in meat, has splendid water conservation and makees With going for meat water conservation.
In order to solve above-mentioned technical problem, the technical solution adopted in the present invention is:
(1) weigh and be cut into the cubed pieces that the length of side is 2~4cm after 8~10kg Rhizoma amorphophalli is peeled and put it in stone mortar, use stone pestle Smash 40~50min to pieces and obtain Rhizoma amorphophalli mud, Rhizoma amorphophalli mud is placed on gauze, with 10~15l deionized water rinsing Rhizoma amorphophalli mud, collect from The milky filtrate flowing down in gauze, the filtrate obtaining is loaded in ceramic cylinder, staticly settles 3~4 days, extracts the supernatant out, Leave the konjak starch slurry that cylinder bottom is sticky;
(2) starched and loaded in enzymatic vessel with the ferrum spoon scraping above-mentioned konjak starch of 400~500g, then add 1~3g manna in tank Dextranase, 1~2g amylase, 2~3g glucanase and 1~3g cellulase and 100~200ml deionized water, will digest Tank filters after being placed on insulation enzymolysis 2~3h in 40~50 DEG C of calorstats and removes filtering residue, obtains filtrate, then filter vacuum is concentrated into The 1/3 of its original volume, obtains Rhizoma amorphophalli enzymolysis concentrated solution;
(3) above-mentioned Rhizoma amorphophalli enzymolysis concentrated solution is poured in beaker, then beaker is moved in water-bath, be heated to 40~50 DEG C, it is placed on and is stirred with 200~300r/min rotating speed on magnetic stirrer, add concentrated solution in the state of stirring total The sodium alginate of quality 10~12% and 0.5~0.8% calcium lactate, insulated and stirred 30~40min obtains gelatinous mixture, standby With;
(4) meter weighs 30~40 portions of Semen sojae atricolor, 40~50 portions of Fructus Citri Limoniaes and 10~12 portions of Radix Glycyrrhizaes and 40~50 parts of steamings by weight Distilled water loads in fermentation flask, and sealing tank mouth, in 25~35 DEG C of bottom fermentations 20~30 days, filters after fermentation ends and removes filtering residue, obtain Fermentation liquid;
(5) it is that 5:1 is equal by putting into dispersion and emulsion after standby gelatinous mixture and above-mentioned fermentation liquid mix homogeneously in mass ratio Proceed in vacuum concentration pot with after 6000~7000r/min rotating speed sterilization treatment 10~15min in matter machine, reduce pressure inside the tank extremely 900~1000pa, discharging after concentrating under reduced pressure 5~10min, obtain final product meat productss phosphate-free water-retaining agent after vacuum packaging.
The application process of the present invention is: after taking 200g fresh pork to be cleared up, adds 3.0~3.2g Sal, Rhizoma Zingiberis Recens 3.0 ~3.2g, Bulbus Allii 3.0~3.2g, cooking wine 4.0~4.5g, then use one after water-retaining agent 8.0~8.5g and water 30~35g is sufficiently mixed In Carnis Sus domestica after secondary property syringe injection process, and roll under the conditions of vacuum 0.06~0.08mpa, rotating speed 12~14r/min Rub 30~32min, then be placed in and pickle 12h at 0~4 DEG C, after vacuum packaging, after pickling, put into quick-freezing in refrigerator, -18~-17 Freezing under the conditions of DEG C, in 25 DEG C of naturally to thaws when edible, after testing, the water retention of Carnis Sus domestica is 70~85%.
The invention has the beneficial effects as follows:
(1) gained water-retaining agent of the present invention be used primarily in water-holding fresh-keeping in meat productss anti-corrosion, absorb moisture content, increase weight, after addition The stability of product can be improved, keep food product retentiveness;
(2) phosphate-free water-retaining agent of gained is suitable for cold preservation class meat productss, tenderization meat, can shorten digestion time, improve the shape of food State, local flavor, mouthfeel, color and luster, suitable large-scale production and application.
Specific embodiment
Weigh first and be cut into the cubed pieces that the length of side is 2~4cm after 8~10kg Rhizoma amorphophalli is peeled and put it in stone mortar, Smash 40~50min to pieces with stone pestle and obtain Rhizoma amorphophalli mud, Rhizoma amorphophalli mud is placed on gauze, with 10~15l deionized water rinsing Rhizoma amorphophalli mud, Collect the milky filtrate flowing down from gauze, the filtrate obtaining is loaded in ceramic cylinder, staticly settles 3~4 days, extract upper strata out Clear liquid, leaves the konjak starch slurry that cylinder bottom is sticky;Starched and loaded enzymatic vessel with the ferrum spoon scraping above-mentioned konjak starch of 400~500g In, then add in tank 1~3g mannonase 1~2g amylase, 2~3g glucanase and 1~3g cellulase and 100~200ml deionized water, enzymatic vessel is placed on after insulation enzymolysis 2~3h in 40~50 DEG C of calorstats and filters removal filtering residue, obtain To filtrate, then filter vacuum is concentrated into the 1/3 of its original volume, obtains Rhizoma amorphophalli enzymolysis concentrated solution;Above-mentioned Rhizoma amorphophalli is digested and concentrates Liquid is poured in beaker, then beaker is moved in water-bath, is heated to 40~50 DEG C, is placed on magnetic stirrer with 200 ~300r/min rotating speed is stirred, and adds the sodium alginate and 0.5 of concentrated solution gross mass 10~12% in the state of stirring ~0.8% calcium lactate, insulated and stirred 30~40min obtains gelatinous mixture, standby;Meter weighs 30~40 by weight Part Semen sojae atricolor, 40~50 portions of Fructus Citri Limoniaes and 10~12 portions of Radix Glycyrrhizaes and 40~50 parts of distilled water load in fermentation flasks, and sealing tank mouth is 25 ~35 DEG C of bottom fermentations 20~30 days, filter after fermentation ends and remove filtering residue, obtain fermentation liquid;In mass ratio will be standby for 5:1 Put into equal with 6000~7000r/min rotating speed in dispersion and emulsion homogenizer after gelatinous mixture and above-mentioned fermentation liquid mix homogeneously Matter proceeds in vacuum concentration pot after processing 10~15min, reduction pressure inside the tank to 900~1000pa, concentrating under reduced pressure 5~10min Discharging afterwards, obtains final product meat productss phosphate-free water-retaining agent after vacuum packaging.
Example 1
Weigh first and be cut into the cubed pieces that the length of side is 2cm after 8kg Rhizoma amorphophalli is peeled and put it in stone mortar, smashed to pieces with stone pestle 40min obtains Rhizoma amorphophalli mud, Rhizoma amorphophalli mud is placed on gauze, with 10l deionized water rinsing Rhizoma amorphophalli mud, collects and flows down from gauze Milky filtrate, the filtrate obtaining is loaded in ceramic cylinder, staticly settles 3 days, extracts the supernatant out, leaves the evil spirit that cylinder bottom is sticky Taro starch slurry;Starched and loaded in enzymatic vessel with the ferrum spoon scraping above-mentioned konjak starch of 400g, then add 1g mannonase in tank 1g amylase, 2g glucanase and 1g cellulase and 100ml deionized water, enzymatic vessel is placed on insulation in 40 DEG C of calorstats Filter after enzymolysis 2h and remove filtering residue, obtain filtrate, then filter vacuum is concentrated into the 1/3 of its original volume, obtain Rhizoma amorphophalli enzymolysis dense Contracting liquid;Above-mentioned Rhizoma amorphophalli enzymolysis concentrated solution is poured in beaker, then beaker is moved in water-bath, be heated to 40 DEG C, place Magnetic stirrer is stirred with 200r/min rotating speed, adds the sea of concentrated solution gross mass 10% in the state of stirring Sodium alginate and 0.5% calcium lactate, insulated and stirred 30min obtains gelatinous mixture, standby;Meter weighs 30 parts by weight Semen sojae atricolor, 40 portions of Fructus Citri Limoniaes and 10 portions of Radix Glycyrrhizaes and 40 parts of distilled water load in fermentation flasks, and sealing tank mouth, in 25 DEG C of bottom fermentations 20 days, is sent out Ferment filters after terminating and removes filtering residue, obtains fermentation liquid;It is 5:1 in mass ratio by standby gelatinous mixture and above-mentioned fermentation liquid Putting into after mix homogeneously in dispersion and emulsion homogenizer proceeds in vacuum concentration pot with after 6000r/min rotating speed sterilization treatment 10min, Reduce pressure inside the tank to 900pa, discharging after concentrating under reduced pressure 5min, after vacuum packaging, obtain final product meat productss phosphate-free water-retaining agent.
The application process of the present invention is: after taking 200g fresh pork to be cleared up, adds 3.0g Sal, Rhizoma Zingiberis Recens 3.0g, Bulbus Allii 3.0g, cooking wine 4.0g, then the Carnis Sus domestica after being processed with disposable syringe injection after water-retaining agent 8.0g and water 30g is sufficiently mixed In, and tumbling 30min under the conditions of vacuum 0.06mpa, rotating speed 12r/min, then be placed in and pickle 12h at 0 DEG C, through true after pickling Quick-freezing in refrigerator is put into after empty package, freezing under the conditions of -18 DEG C, in 25 DEG C of naturally to thaws when edible, after testing, The water retention of Carnis Sus domestica is 70%.
Example 2
Weigh first and be cut into the cubed pieces that the length of side is 3cm after 9kg Rhizoma amorphophalli is peeled and put it in stone mortar, smashed to pieces with stone pestle 45min obtains Rhizoma amorphophalli mud, Rhizoma amorphophalli mud is placed on gauze, with 13l deionized water rinsing Rhizoma amorphophalli mud, collects and flows down from gauze Milky filtrate, the filtrate obtaining is loaded in ceramic cylinder, staticly settles 3.5 days, extracts the supernatant out, stays cylinder bottom sticky Konjak starch is starched;Starched and loaded in enzymatic vessel with the ferrum spoon scraping above-mentioned konjak starch of 450g, then add 2g mannan in tank Enzyme, 1.5g amylase, 2.5g glucanase and 2g cellulase and 150ml deionized water, enzymatic vessel is placed on 45 DEG C of constant temperature Filter after insulation enzymolysis 2.5h in case and remove filtering residue, obtain filtrate, then filter vacuum is concentrated into the 1/3 of its original volume, obtain Rhizoma amorphophalli digests concentrated solution;Above-mentioned Rhizoma amorphophalli enzymolysis concentrated solution is poured in beaker, then beaker is moved in water-bath, be heated to 45 DEG C, it is placed on and is stirred with 250r/min rotating speed on magnetic stirrer, in the state of stirring, add the total matter of concentrated solution Measure 11% sodium alginate and 0.7% calcium lactate, insulated and stirred 35min obtains gelatinous mixture, standby;Count by weight Weigh 35 portions of Semen sojae atricolor, 45 portions of Fructus Citri Limoniaes and 11 portions of Radix Glycyrrhizaes and 45 parts of distilled water load in fermentation flask, sealing tank mouth issues at 30 DEG C Ferment 25 days, filters after fermentation ends and removes filtering residue, obtain fermentation liquid;Be in mass ratio 5:1 by standby gelatinous mixture and Put into true to proceed to after 6500r/min rotating speed sterilization treatment 13min in dispersion and emulsion homogenizer after above-mentioned fermentation liquid mix homogeneously In empty concentration tank, reduce pressure inside the tank to 950pa, discharging after concentrating under reduced pressure 7min, after vacuum packaging, obtain final product the without phosphorus guarantor of meat productss Water preparation.
The application process of the present invention is: after taking 200g fresh pork to be cleared up, adds 3.1g Sal, Rhizoma Zingiberis Recens 3.1g, Bulbus Allii 3.1g, cooking wine 4.3g, then the Carnis Sus domestica after being processed with disposable syringe injection after water-retaining agent 8.3g and water 33g is sufficiently mixed In, and tumbling 31min under the conditions of vacuum 0.07mpa, rotating speed 13r/min, then be placed in and pickle 12h at 2 DEG C, through true after pickling Quick-freezing in refrigerator is put into, freezing under the conditions of -17.5 DEG C, in 25 DEG C of naturally to thaws when edible, through inspection after empty package Survey, the water retention of Carnis Sus domestica is 78%.
Example 3
Weigh first and be cut into the cubed pieces that the length of side is 4cm after 10kg Rhizoma amorphophalli is peeled and put it in stone mortar, smashed to pieces with stone pestle 50min obtains Rhizoma amorphophalli mud, Rhizoma amorphophalli mud is placed on gauze, with 15l deionized water rinsing Rhizoma amorphophalli mud, collects and flows down from gauze Milky filtrate, the filtrate obtaining is loaded in ceramic cylinder, staticly settles 4 days, extracts the supernatant out, leaves the evil spirit that cylinder bottom is sticky Taro starch slurry;Starched and loaded in enzymatic vessel with the ferrum spoon scraping above-mentioned konjak starch of 500g, then add 3g mannonase in tank 2g amylase, 3g glucanase and 3g cellulase and 200ml deionized water, enzymatic vessel is placed on insulation in 50 DEG C of calorstats Filter after enzymolysis 3h and remove filtering residue, obtain filtrate, then filter vacuum is concentrated into the 1/3 of its original volume, obtain Rhizoma amorphophalli enzymolysis dense Contracting liquid;Above-mentioned Rhizoma amorphophalli enzymolysis concentrated solution is poured in beaker, then beaker is moved in water-bath, be heated to 50 DEG C, place Magnetic stirrer is stirred with 300r/min rotating speed, adds the sea of concentrated solution gross mass 12% in the state of stirring Sodium alginate and 0.8% calcium lactate, insulated and stirred 40min obtains gelatinous mixture, standby;Meter weighs 40 parts by weight Semen sojae atricolor, 50 portions of Fructus Citri Limoniaes and 12 portions of Radix Glycyrrhizaes and 50 parts of distilled water load in fermentation flasks, and sealing tank mouth, in 35 DEG C of bottom fermentations 30 days, is sent out Ferment filters after terminating and removes filtering residue, obtains fermentation liquid;It is 5:1 in mass ratio by standby gelatinous mixture and above-mentioned fermentation liquid Putting into after mix homogeneously in dispersion and emulsion homogenizer proceeds in vacuum concentration pot with after 7000r/min rotating speed sterilization treatment 15min, Reduce pressure inside the tank to 1000pa, discharging after concentrating under reduced pressure 10min, after vacuum packaging, obtain final product meat productss phosphate-free water-retaining agent.
The application process of the present invention is: after taking 200g fresh pork to be cleared up, adds 3.2g Sal, Rhizoma Zingiberis Recens 3.2g, Bulbus Allii 3.2g, cooking wine 4.5g, then the Carnis Sus domestica after being processed with disposable syringe injection after water-retaining agent 8.5g and water 35g is sufficiently mixed In, and tumbling 32min under the conditions of vacuum 0.08mpa, rotating speed 14r/min, then be placed in and pickle 12h at 4 DEG C, through true after pickling Quick-freezing in refrigerator is put into after empty package, freezing under the conditions of -17 DEG C, in 25 DEG C of naturally to thaws when edible, after testing, The water retention of Carnis Sus domestica is 85%.

Claims (1)

1. a kind of preparation method of meat productss phosphate-free water-retaining agent is it is characterised in that concrete preparation process is:
(1) weigh and be cut into the cubed pieces that the length of side is 2~4cm after 8~10kg Rhizoma amorphophalli is peeled and put it in stone mortar, use stone pestle Smash 40~50min to pieces and obtain Rhizoma amorphophalli mud, Rhizoma amorphophalli mud is placed on gauze, with 10~15l deionized water rinsing Rhizoma amorphophalli mud, collect The milky filtrate flowing down from gauze, the filtrate obtaining is loaded in ceramic cylinder, staticly settles 3~4 days, extracts upper strata out clear Liquid, leaves the konjak starch slurry that cylinder bottom is sticky;
(2) starched and loaded in enzymatic vessel with the ferrum spoon scraping above-mentioned konjak starch of 400~500g, then add 1~3g manna in tank Dextranase, 1~2g amylase, 2~3g glucanase and 1~3g cellulase and 100~200ml deionized water, will digest Tank filters after being placed on insulation enzymolysis 2~3h in 40~50 DEG C of calorstats and removes filtering residue, obtains filtrate, then filter vacuum is concentrated into The 1/3 of its original volume, obtains Rhizoma amorphophalli enzymolysis concentrated solution;
(3) above-mentioned Rhizoma amorphophalli enzymolysis concentrated solution is poured in beaker, then beaker is moved in water-bath, be heated to 40~50 DEG C, it is placed on and is stirred with 200~300r/min rotating speed on magnetic stirrer, add concentrated solution in the state of stirring total The sodium alginate of quality 10~12% and 0.5~0.8% calcium lactate, insulated and stirred 30~40min obtains gelatinous mixture, standby With;
(4) meter weighs 30~40 portions of Semen sojae atricolor, 40~50 portions of Fructus Citri Limoniaes and 10~12 portions of Radix Glycyrrhizaes and 40~50 parts of steamings by weight Distilled water loads in fermentation flask, and sealing tank mouth, in 25~35 DEG C of bottom fermentations 20~30 days, filters after fermentation ends and removes filtering residue, obtain Fermentation liquid;
(5) it is that 5:1 is equal by putting into dispersion and emulsion after standby gelatinous mixture and above-mentioned fermentation liquid mix homogeneously in mass ratio Proceed in vacuum concentration pot with after 6000~7000r/min rotating speed sterilization treatment 10~15min in matter machine, reduce pressure inside the tank extremely 900~1000pa, discharging after concentrating under reduced pressure 5~10min, obtain final product meat productss phosphate-free water-retaining agent after vacuum packaging.
CN201610746875.5A 2016-08-29 2016-08-29 Preparation method of meat product non-phosphorus water retaining agent Pending CN106332953A (en)

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CN109123461A (en) * 2018-09-13 2019-01-04 西华大学 A kind of less salt meat products and its processing method
CN109619166A (en) * 2019-01-30 2019-04-16 刘建飞 Green safe meat antistaling agent

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Publication number Priority date Publication date Assignee Title
CN108576695A (en) * 2018-04-26 2018-09-28 江苏省农业科学院 A kind of production method of freezing conditioning mandarin fish
CN109123461A (en) * 2018-09-13 2019-01-04 西华大学 A kind of less salt meat products and its processing method
CN109619166A (en) * 2019-01-30 2019-04-16 刘建飞 Green safe meat antistaling agent

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Application publication date: 20170118