CN106323966A - Detection paper for disinfector residue and preparation method thereof - Google Patents

Detection paper for disinfector residue and preparation method thereof Download PDF

Info

Publication number
CN106323966A
CN106323966A CN201610926836.3A CN201610926836A CN106323966A CN 106323966 A CN106323966 A CN 106323966A CN 201610926836 A CN201610926836 A CN 201610926836A CN 106323966 A CN106323966 A CN 106323966A
Authority
CN
China
Prior art keywords
parts
slurry
detection paper
paper
fiber
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610926836.3A
Other languages
Chinese (zh)
Inventor
周朱晨
朱倩倩
张根义
胡彬
张进
吴念绮
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
100 Olson Jiangsu Food Safety Technology Co Ltd
Original Assignee
100 Olson Jiangsu Food Safety Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 100 Olson Jiangsu Food Safety Technology Co Ltd filed Critical 100 Olson Jiangsu Food Safety Technology Co Ltd
Priority to CN201610926836.3A priority Critical patent/CN106323966A/en
Publication of CN106323966A publication Critical patent/CN106323966A/en
Pending legal-status Critical Current

Links

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/75Systems in which material is subjected to a chemical reaction, the progress or the result of the reaction being investigated
    • G01N21/77Systems in which material is subjected to a chemical reaction, the progress or the result of the reaction being investigated by observing the effect on a chemical indicator
    • G01N21/78Systems in which material is subjected to a chemical reaction, the progress or the result of the reaction being investigated by observing the effect on a chemical indicator producing a change of colour

Landscapes

  • Physics & Mathematics (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Plasma & Fusion (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Apparatus For Disinfection Or Sterilisation (AREA)
  • Paper (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention discloses detection paper for disinfector residue. The detection paper comprises the following raw materials in parts by weight: 35-40 parts of wood pulp cellulose, 2-5 parts of bast fiber, 4-8 parts of glass fiber, 6-10 parts of polyester fiber, 5-8 parts of regenerated cellulose fiber, 2-5 parts of polynosic, 3-6 parts of starch, 4-5 parts of binder, 1-2 parts of polyvinyl alcohol, 0.3-0.6 part of sodium carbonate, 3-4 parts of potassium iodide, 2-3 parts of tetramethyl benzidine, 100-150 parts of ethyl alcohol, 5-10 parts of weak acid modifier, 3-5 parts of anhydrous monopotassium phosphate and 0.5-1.0 part of mercuric chloride. The invention also discloses a preparation method for the detection paper for disinfector residue. The detection paper for disinfector residue, prepared according to the method, is high in sensitivity. A simple, accurate and low-cost detection method for the disinfector residue is supplied for sterilizing in food industries, hospitals and public health places.

Description

A kind of disinfectant residues detection paper and preparation method thereof
Technical field
The present invention relates to disinfectant detection technique field, specifically a kind of disinfectant residues detection paper and preparation side thereof Method.
Background technology
Disinfectant is used for killing pathogenic microorganism on communication media so that it is reaches innoxious requirement, is disappeared by pathogenic microorganism Go out outside human body, cut off the route of transmission of infectious disease, reach to control the purpose of infectious disease.Along with the development in epoch, Ren Menyue More paying attention to environmental health, therefore the application of disinfectant is more and more extensive.As a example by swimming pool, swimming pool is accomplished by periodically entering Row is disinfected, to ensure water quality.After using disinfectant that water is carried out disinfection, water typically can remain disinfectant, if in water The residual quantity of disinfectant is too high, will affect health, and therefore, the detection of disinfectant residual quantity is significant.
Tradition, for the detection of disinfectant residual quantity, mainly uses Ortho-tolidine method and iodimetric titration, these methods Complex operation, analytical cycle is long, but also needs professional and technical personnel, it is impossible to meet the requirement being used for quickly detecting water quality, Being unsuitable for field assay, being additionally, since o-tolidine reagent has carcinogenecity, is the most gradually eliminated.The most also go out Having showed some disinfectant residual quantity quick detection test paper, these quick detection test paper generally need deployed various solution, then Filter paper being soaked and dries, just can be normally carried out detection, this quick detection test paper often Detection results is inconspicuous, and step is numerous Trivial, and detection sensitivity is the highest.
Summary of the invention
It is an object of the invention to provide a kind of disinfectant residues detection paper and preparation method thereof, to solve above-mentioned background The problem proposed in technology.
For achieving the above object, the present invention provides following technical scheme:
A kind of disinfectant residues detection paper, is made up of according to the raw material of weight portion following: wood pulp cellulose 35-40 part, bast fibre Dimension 2-5 part, glass fibre 4-8 part, polyester fiber 6-10 part, regenerated celulose fibre 5-8 part, polynosic 2-5 part, starch 3- 6 parts, binding agent 4-5 part, polyvinyl alcohol 1-2 part, sodium carbonate 0.3-0.6 part, potassium iodide 3-4 part, tetramethyl benzidine 2-3 part, Ethanol 100-150 part, weak acid regulator 5-10 part, anhydrous potassium dihydrogenphosphate 3-5 part, mercuric chloride 0.5-1.0 part.
As the further scheme of the present invention: be made up of according to the raw material of weight portion following: wood pulp cellulose 36-39 part, tough Hide fiber 3-4 part, glass fibre 5-7 part, polyester fiber 7-9 part, regenerated celulose fibre 6-7 part, polynosic 3-4 part, shallow lake Powder 4-5 part, binding agent 4.2-4.7 part, polyvinyl alcohol 1.1-1.8 part, sodium carbonate 0.4-0.5 part, potassium iodide 3.3-3.8 part, four Methyl biphenyl amine 2.2-2.9 part, ethanol 110-140 part, weak acid regulator 6-9 part, anhydrous potassium dihydrogenphosphate 3.4-4.7 part, chlorine Change hydrargyrum 0.6-0.9 part.
As the present invention further scheme: be made up of according to the raw material of weight portion following: wood pulp cellulose 37.5 parts, tough Hide fiber 3.5 parts, glass fibre 6 parts, 8 parts of polyester fiber, regenerated celulose fibre 6.4 parts, polynosic 3.7 parts, starch 4.3 Part, binding agent 4.5 parts, polyvinyl alcohol 1.6 parts, sodium carbonate 0.4 part, potassium iodide 3.5 parts, tetramethyl benzidine 2.7 parts, ethanol 120 parts, weak acid regulator 7 parts, anhydrous potassium dihydrogenphosphate 3.8 parts, 0.7 part of mercuric chloride.
As the present invention further scheme: described glass fibre is short glass fiber.
As the present invention further scheme: described binding agent be polyacrylate and epoxy resin according to weight ratio 1: 1.5 mix.
As the present invention further scheme: described weak acid regulator is that acetic acid and citric acid mix according to weight ratio 2:1 Conjunction forms.
The preparation method of described disinfectant residues detection paper, step is as follows:
1) weighing wood pulp cellulose and ethanol, put into beater by the ethanol of wood pulp cellulose and total amount 60-80%, making beating processes 30-40min, it is thus achieved that the first slurry;
2) weigh phloem fiber, glass fibre and regenerated celulose fibre, add to the first slurry, continue making beating and process 20- 30min, it is thus achieved that the second slurry;
3) weigh starch, polyvinyl alcohol, tetramethyl benzidine and mercuric chloride, add to the second slurry, be warming up to 50-60 DEG C, And the process 40-50min that pulls an oar, then it is cooled to 20-25 DEG C, it is thus achieved that the 3rd slurry;
4) weigh binding agent, polyester fiber and polynosic, add to the 3rd slurry, continue making beating and process 10-20min, obtain Obtain the 4th slurry;
5) it is warming up to 40-45 DEG C through the 4th slurry, weighs and add sodium carbonate, potassium iodide, anhydrous potassium dihydrogenphosphate and residue Ethanol, continue making beating and process 10-20min, be subsequently adding weak acid regulator, continue making beating and process 1-2h, it is thus achieved that the 5th slurry;
6) the 5th slurry is put into molding in net paper machine, it is thus achieved that the filter paper of molding;
7) filter paper of molding is put into baking oven, at 100-105 DEG C, carry out drying and processing, after drying, obtain disinfectant residual Amount detection paper.
Compared with prior art, the invention has the beneficial effects as follows:
1, the disinfectant residues detection paper that prepared by the present invention, in preparation process, in the medicament needed for detection is modulated at, with Traditional detection paper soaked that relies on is compared, and Detection results is good;
2, the disinfectant residues detection paper that prepared by the present invention, service life is long, good stability, and detection paper is difficult at storing process Middle variable color;
3, the disinfectant residues detection paper that prepared by the present invention, highly sensitive, for food service industry, hospital and sanitarian sterilization Sterilizing provides simplicity, accurate, the disinfectant residue detection mode of low cost.
Detailed description of the invention
Below in conjunction with detailed description of the invention, technical scheme is described in more detail.
Embodiment 1
A kind of disinfectant residues detection paper, is made up of according to the raw material of weight portion following: wood pulp cellulose 35 parts, phloem fiber 2 Part, glass fibre 4 parts, 6 parts of polyester fiber, regenerated celulose fibre 5 parts, polynosic 2 parts, starch 3 parts, binding agent 4 parts, poly- Vinyl alcohol 1 part, sodium carbonate 0.3 part, potassium iodide 3 parts, tetramethyl benzidine 2 parts, ethanol 100 parts, weak acid regulator 5 parts, anhydrous Potassium dihydrogen phosphate 3 parts, 0.5 part of mercuric chloride;Wherein, described glass fibre is short glass fiber, and described binding agent is polypropylene Acid esters and epoxy resin mix according to weight ratio 1:1.5, and described weak acid regulator is that acetic acid and citric acid are according to weight ratio 2:1 mixes.
In the present embodiment, the preparation method of described disinfectant residues detection paper, step is as follows:
1) weighing wood pulp cellulose and ethanol, put into beater by the ethanol of wood pulp cellulose and total amount 60%, making beating processes 30min, it is thus achieved that the first slurry;
2) weigh phloem fiber, glass fibre and regenerated celulose fibre, add to the first slurry, continue making beating and process 20min, it is thus achieved that the second slurry;
3) weigh starch, polyvinyl alcohol, tetramethyl benzidine and mercuric chloride, add to the second slurry, be warming up to 50 DEG C, and beat Slurry processes 40min, then is cooled to 20 DEG C, it is thus achieved that the 3rd slurry;
4) weigh binding agent, polyester fiber and polynosic, add to the 3rd slurry, continue making beating and process 10min, it is thus achieved that the Four slurries;
5) it is warming up to 40 DEG C through the 4th slurry, weighs and add sodium carbonate, potassium iodide, anhydrous potassium dihydrogenphosphate and remaining second Alcohol, continues making beating and processes 10min, be subsequently adding weak acid regulator, continues making beating and processes 1h, it is thus achieved that the 5th slurry;
6) the 5th slurry is put into molding in net paper machine, it is thus achieved that the filter paper of molding;
7) filter paper of molding is put into baking oven, at 100 DEG C, carry out drying and processing, after drying, obtain the inspection of disinfectant residual quantity Survey paper.
Embodiment 2
A kind of disinfectant residues detection paper, is made up of according to the raw material of weight portion following: wood pulp cellulose 36 parts, phloem fiber 3 Part, glass fibre 4.5 parts, 7 parts of polyester fiber, regenerated celulose fibre 7 parts, polynosic 5 parts, starch 4 parts, binding agent 4.3 Part, polyvinyl alcohol 1.4 parts, sodium carbonate 0.5 part, potassium iodide 3 parts, tetramethyl benzidine 2.6 parts, ethanol 108 parts, weak acid regulator 7 parts, anhydrous potassium dihydrogenphosphate 4 parts, 0.7 part of mercuric chloride;Wherein, described glass fibre is short glass fiber, described binding agent Mix according to weight ratio 1:1.5 for polyacrylate and epoxy resin, described weak acid regulator be acetic acid and citric acid by Mix according to weight ratio 2:1.
In the present embodiment, the preparation method of described disinfectant residues detection paper, step is as follows:
1) weighing wood pulp cellulose and ethanol, put into beater by the ethanol of wood pulp cellulose and total amount 65%, making beating processes 32min, it is thus achieved that the first slurry;
2) weigh phloem fiber, glass fibre and regenerated celulose fibre, add to the first slurry, continue making beating and process 25min, it is thus achieved that the second slurry;
3) weigh starch, polyvinyl alcohol, tetramethyl benzidine and mercuric chloride, add to the second slurry, be warming up to 53 DEG C, and beat Slurry processes 45min, then is cooled to 22 DEG C, it is thus achieved that the 3rd slurry;
4) weigh binding agent, polyester fiber and polynosic, add to the 3rd slurry, continue making beating and process 13min, it is thus achieved that the Four slurries;
5) it is warming up to 41 DEG C through the 4th slurry, weighs and add sodium carbonate, potassium iodide, anhydrous potassium dihydrogenphosphate and remaining second Alcohol, continues making beating and processes 16min, be subsequently adding weak acid regulator, continues making beating and processes 1.5h, it is thus achieved that the 5th slurry;
6) the 5th slurry is put into molding in net paper machine, it is thus achieved that the filter paper of molding;
7) filter paper of molding is put into baking oven, at 101 DEG C, carry out drying and processing, after drying, obtain the inspection of disinfectant residual quantity Survey paper.
Embodiment 3
A kind of disinfectant residues detection paper, is made up of according to the raw material of weight portion following: wood pulp cellulose 37.5 parts, phloem fiber 3.5 parts, glass fibre 6 parts, 8 parts of polyester fiber, regenerated celulose fibre 6.4 parts, polynosic 3.7 parts, starch 4.3 parts, viscous Knot agent 4.5 parts, polyvinyl alcohol 1.6 parts, sodium carbonate 0.4 part, potassium iodide 3.5 parts, tetramethyl benzidine 2.7 parts, ethanol 120 parts, Weak acid regulator 7 parts, anhydrous potassium dihydrogenphosphate 3.8 parts, 0.7 part of mercuric chloride;Wherein, described glass fibre is that staple glass is fine Dimension, described binding agent is polyacrylate and epoxy resin mixes according to weight ratio 1:1.5, and described weak acid regulator is vinegar Acid and citric acid mix according to weight ratio 2:1.
In the present embodiment, the preparation method of described disinfectant residues detection paper, step is as follows:
1) weighing wood pulp cellulose and ethanol, put into beater by the ethanol of wood pulp cellulose and total amount 70%, making beating processes 35min, it is thus achieved that the first slurry;
2) weigh phloem fiber, glass fibre and regenerated celulose fibre, add to the first slurry, continue making beating and process 25min, it is thus achieved that the second slurry;
3) weigh starch, polyvinyl alcohol, tetramethyl benzidine and mercuric chloride, add to the second slurry, be warming up to 55 DEG C, and beat Slurry processes 45min, then is cooled to 23 DEG C, it is thus achieved that the 3rd slurry;
4) weigh binding agent, polyester fiber and polynosic, add to the 3rd slurry, continue making beating and process 15min, it is thus achieved that the Four slurries;
5) it is warming up to 43 DEG C through the 4th slurry, weighs and add sodium carbonate, potassium iodide, anhydrous potassium dihydrogenphosphate and remaining second Alcohol, continues making beating and processes 15min, be subsequently adding weak acid regulator, continues making beating and processes 1.5h, it is thus achieved that the 5th slurry;
6) the 5th slurry is put into molding in net paper machine, it is thus achieved that the filter paper of molding;
7) filter paper of molding is put into baking oven, at 103 DEG C, carry out drying and processing, after drying, obtain the inspection of disinfectant residual quantity Survey paper.
Embodiment 4
A kind of disinfectant residues detection paper, is made up of according to the raw material of weight portion following: wood pulp cellulose 38 parts, phloem fiber 4 Part, glass fibre 5 parts, 6 parts of polyester fiber, regenerated celulose fibre 7.5 parts, polynosic 4.8 parts, starch 3 parts, binding agent 4.7 parts, polyvinyl alcohol 1.4 parts, sodium carbonate 0.6 part, potassium iodide 4 parts, tetramethyl benzidine 2.3 parts, ethanol 130 parts, weak acid adjust Joint agent 8 parts, anhydrous potassium dihydrogenphosphate 4.5 parts, 0.7 part of mercuric chloride;Wherein, described glass fibre is short glass fiber, described Binding agent is polyacrylate and epoxy resin mixes according to weight ratio 1:1.5, and described weak acid regulator is acetic acid and lemon Lemon acid mixes according to weight ratio 2:1.
In the present embodiment, the preparation method of described disinfectant residues detection paper, step is as follows:
1) weighing wood pulp cellulose and ethanol, put into beater by the ethanol of wood pulp cellulose and total amount 75%, making beating processes 37min, it is thus achieved that the first slurry;
2) weigh phloem fiber, glass fibre and regenerated celulose fibre, add to the first slurry, continue making beating and process 26min, it is thus achieved that the second slurry;
3) weigh starch, polyvinyl alcohol, tetramethyl benzidine and mercuric chloride, add to the second slurry, be warming up to 55 DEG C, and beat Slurry processes 47min, then is cooled to 21 DEG C, it is thus achieved that the 3rd slurry;
4) weigh binding agent, polyester fiber and polynosic, add to the 3rd slurry, continue making beating and process 18min, it is thus achieved that the Four slurries;
5) it is warming up to 44 DEG C through the 4th slurry, weighs and add sodium carbonate, potassium iodide, anhydrous potassium dihydrogenphosphate and remaining second Alcohol, continues making beating and processes 20min, be subsequently adding weak acid regulator, continues making beating and processes 2h, it is thus achieved that the 5th slurry;
6) the 5th slurry is put into molding in net paper machine, it is thus achieved that the filter paper of molding;
7) filter paper of molding is put into baking oven, at 104 DEG C, carry out drying and processing, after drying, obtain the inspection of disinfectant residual quantity Survey paper.
Embodiment 5
A kind of disinfectant residues detection paper, is made up of according to the raw material of weight portion following: wood pulp cellulose 40 parts, phloem fiber 5 Part, glass fibre 8 parts, 10 parts of polyester fiber, regenerated celulose fibre 8 parts, polynosic 5 parts, starch 6 parts, binding agent 5 parts, Polyvinyl alcohol 2 parts, sodium carbonate 0.6 part, potassium iodide 4 parts, tetramethyl benzidine 3 parts, ethanol 150 parts, weak acid regulator 10 parts, nothing Water potassium dihydrogen phosphate 5 parts, 1.0 parts of mercuric chloride;Wherein, described glass fibre is short glass fiber, and described binding agent is poly-third Olefin(e) acid ester and epoxy resin mix according to weight ratio 1:1.5, and described weak acid regulator is that acetic acid and citric acid are according to weight Mix than 2:1.
In the present embodiment, the preparation method of described disinfectant residues detection paper, step is as follows:
1) weighing wood pulp cellulose and ethanol, put into beater by the ethanol of wood pulp cellulose and total amount 80%, making beating processes 40min, it is thus achieved that the first slurry;
2) weigh phloem fiber, glass fibre and regenerated celulose fibre, add to the first slurry, continue making beating and process 30min, it is thus achieved that the second slurry;
3) weigh starch, polyvinyl alcohol, tetramethyl benzidine and mercuric chloride, add to the second slurry, be warming up to 60 DEG C, and beat Slurry processes 50min, then is cooled to 25 DEG C, it is thus achieved that the 3rd slurry;
4) weigh binding agent, polyester fiber and polynosic, add to the 3rd slurry, continue making beating and process 20min, it is thus achieved that the Four slurries;
5) it is warming up to 45 DEG C through the 4th slurry, weighs and add sodium carbonate, potassium iodide, anhydrous potassium dihydrogenphosphate and remaining second Alcohol, continues making beating and processes 20min, be subsequently adding weak acid regulator, continues making beating and processes 2h, it is thus achieved that the 5th slurry;
6) the 5th slurry is put into molding in net paper machine, it is thus achieved that the filter paper of molding;
7) filter paper of molding is put into baking oven, at 105 DEG C, carry out drying and processing, after drying, obtain the inspection of disinfectant residual quantity Survey paper.
Disinfectant residues detection paper prepared by the present invention, in preparation process, in the medicament needed for detection is modulated at, Compared with traditional detection paper relying on immersion, Detection results is good;Disinfectant residues detection paper prepared by the present invention, uses the longevity Life is long, good stability, and detection paper is difficult to variable color in storing process;Disinfectant residues detection paper prepared by the present invention is sensitive Degree height, provides simplicity, accurate, the disinfectant residual inspection of low cost for food service industry, hospital and sanitarian sterilization Survey mode.
Above the better embodiment of the present invention is explained in detail, but the present invention is not limited to above-mentioned embodiment party Formula, in the ken that one skilled in the relevant art is possessed, it is also possible on the premise of without departing from present inventive concept Various changes can be made.

Claims (7)

1. a disinfectant residues detection paper, it is characterised in that be made up of according to the raw material of weight portion following: wood pulp cellulose 35-40 part, phloem fiber 2-5 part, glass fibre 4-8 part, polyester fiber 6-10 part, regenerated celulose fibre 5-8 part, rich and powerful fibre Dimension 2-5 part, starch 3-6 part, binding agent 4-5 part, polyvinyl alcohol 1-2 part, sodium carbonate 0.3-0.6 part, potassium iodide 3-4 part, tetramethyl Base benzidine 2-3 part, ethanol 100-150 part, weak acid regulator 5-10 part, anhydrous potassium dihydrogenphosphate 3-5 part, mercuric chloride 0.5- 1.0 part.
Disinfectant residues detection paper the most according to claim 1, it is characterised in that by the following raw material according to weight portion Composition: wood pulp cellulose 36-39 part, phloem fiber 3-4 part, glass fibre 5-7 part, polyester fiber 7-9 part, regenerated celulose fibre 6-7 part, polynosic 3-4 part, starch 4-5 part, binding agent 4.2-4.7 part, polyvinyl alcohol 1.1-1.8 part, sodium carbonate 0.4-0.5 Part, potassium iodide 3.3-3.8 part, tetramethyl benzidine 2.2-2.9 part, ethanol 110-140 part, weak acid regulator 6-9 part, anhydrous phosphorus Acid dihydride potassium 3.4-4.7 part, mercuric chloride 0.6-0.9 part.
Disinfectant residues detection paper the most according to claim 2, it is characterised in that by the following raw material according to weight portion Composition: wood pulp cellulose 37.5 parts, phloem fiber 3.5 parts, glass fibre 6 parts, 8 parts of polyester fiber, regenerated celulose fibre 6.4 Part, polynosic 3.7 parts, starch 4.3 parts, binding agent 4.5 parts, polyvinyl alcohol 1.6 parts, sodium carbonate 0.4 part, potassium iodide 3.5 parts, Tetramethyl benzidine 2.7 parts, ethanol 120 parts, weak acid regulator 7 parts, anhydrous potassium dihydrogenphosphate 3.8 parts, 0.7 part of mercuric chloride.
Disinfectant residues detection paper the most according to claim 3, it is characterised in that described glass fibre is staple glass Fiber.
Disinfectant residues detection paper the most according to claim 4, it is characterised in that described binding agent is polyacrylate Mix according to weight ratio 1:1.5 with epoxy resin.
Disinfectant residues detection paper the most according to claim 5, it is characterised in that described weak acid regulator be acetic acid and Citric acid mixes according to weight ratio 2:1.
7. the preparation method of the disinfectant residues detection paper as described in claim 1-6 is arbitrary, it is characterised in that step As follows:
1) weighing wood pulp cellulose and ethanol, put into beater by the ethanol of wood pulp cellulose and total amount 60-80%, making beating processes 30-40min, it is thus achieved that the first slurry;
2) weigh phloem fiber, glass fibre and regenerated celulose fibre, add to the first slurry, continue making beating and process 20- 30min, it is thus achieved that the second slurry;
3) weigh starch, polyvinyl alcohol, tetramethyl benzidine and mercuric chloride, add to the second slurry, be warming up to 50-60 DEG C, And the process 40-50min that pulls an oar, then it is cooled to 20-25 DEG C, it is thus achieved that the 3rd slurry;
4) weigh binding agent, polyester fiber and polynosic, add to the 3rd slurry, continue making beating and process 10-20min, obtain Obtain the 4th slurry;
5) it is warming up to 40-45 DEG C through the 4th slurry, weighs and add sodium carbonate, potassium iodide, anhydrous potassium dihydrogenphosphate and residue Ethanol, continue making beating and process 10-20min, be subsequently adding weak acid regulator, continue making beating and process 1-2h, it is thus achieved that the 5th slurry;
6) the 5th slurry is put into molding in net paper machine, it is thus achieved that the filter paper of molding;
7) filter paper of molding is put into baking oven, at 100-105 DEG C, carry out drying and processing, after drying, obtain disinfectant residual Amount detection paper.
CN201610926836.3A 2016-10-31 2016-10-31 Detection paper for disinfector residue and preparation method thereof Pending CN106323966A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610926836.3A CN106323966A (en) 2016-10-31 2016-10-31 Detection paper for disinfector residue and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610926836.3A CN106323966A (en) 2016-10-31 2016-10-31 Detection paper for disinfector residue and preparation method thereof

Publications (1)

Publication Number Publication Date
CN106323966A true CN106323966A (en) 2017-01-11

Family

ID=57819281

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610926836.3A Pending CN106323966A (en) 2016-10-31 2016-10-31 Detection paper for disinfector residue and preparation method thereof

Country Status (1)

Country Link
CN (1) CN106323966A (en)

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2104445U (en) * 1991-05-10 1992-05-13 浏阳县卫生防疫站 Disinfectant density test-paper
CN1796985A (en) * 2004-12-21 2006-07-05 上海三爱思试剂有限公司 Test paper for detecting disinfector of chlorine dioxide, and preparation method
CN101592612A (en) * 2008-05-26 2009-12-02 刘侠 Test paper for rapidly checking residual content of sterilizing agent
CN102331423A (en) * 2011-09-19 2012-01-25 苏州浩欧博生物医药有限公司 Feces occult blood test paper and preparation method thereof
CN105548166A (en) * 2015-12-30 2016-05-04 广州市医德生物科技有限责任公司 OPA (o-phthalaldehyde) disinfector concentration range detection test paper
CN105755901A (en) * 2016-02-18 2016-07-13 浙江华川实业集团有限公司 Rapid detection paper for disinfection residue content and preparation method thereof

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2104445U (en) * 1991-05-10 1992-05-13 浏阳县卫生防疫站 Disinfectant density test-paper
CN1796985A (en) * 2004-12-21 2006-07-05 上海三爱思试剂有限公司 Test paper for detecting disinfector of chlorine dioxide, and preparation method
CN101592612A (en) * 2008-05-26 2009-12-02 刘侠 Test paper for rapidly checking residual content of sterilizing agent
CN102331423A (en) * 2011-09-19 2012-01-25 苏州浩欧博生物医药有限公司 Feces occult blood test paper and preparation method thereof
CN105548166A (en) * 2015-12-30 2016-05-04 广州市医德生物科技有限责任公司 OPA (o-phthalaldehyde) disinfector concentration range detection test paper
CN105755901A (en) * 2016-02-18 2016-07-13 浙江华川实业集团有限公司 Rapid detection paper for disinfection residue content and preparation method thereof

Similar Documents

Publication Publication Date Title
MXPA04000684A (en) Highly carboxylated cellulose fibers and process of making the same.
GB1559766A (en) Low ph preparation of cationic starches and flours
AU692667B2 (en) Peracid compositions
CN106323966A (en) Detection paper for disinfector residue and preparation method thereof
CN108049230A (en) A kind of iron catalyzing hydrogen peroxide oxidation prepares nano-cellulose method
CN105548166A (en) OPA (o-phthalaldehyde) disinfector concentration range detection test paper
US8183051B2 (en) Method and system for determining residual chlorine or chloramine concentration in solution by colorimetry
CN104611771A (en) Mulberry silk fiber oil removing and adhesive preserving process
CN105755901A (en) Rapid detection paper for disinfection residue content and preparation method thereof
CN107287061A (en) A kind of cleaning and disinfecting liquid of aroma type 84 containing natural soap base and preparation method thereof
CN101545896B (en) Application of pH test paper in testing effective chloride content of disinfectant containing chloride
CN111378328A (en) Indicator and indicator card for low-temperature ethylene oxide sterilization
JPS6411668B2 (en)
CN109444121A (en) The detection kit and detection method of calper calcium peroxide in a kind of flour
CN102087257A (en) Test paper for measuring content of available chlorine
CN109678733A (en) A kind of quaternary ammonium salt abietyl cationic surfactant and the preparation method and application thereof
CN1103124A (en) Bamboo material fibre fluff pulp and making method
CN114594093A (en) Preparation method of iodophor disinfectant content detection test paper
ES2102008T3 (en) BLEACHING OF CHEMICAL PAPER PASTE.
KR20110029724A (en) Composition for dissociating an absorption goods
WO2020245071A1 (en) Eucalyptus globulus bark pulp for tissue products
CN106061891B (en) Hydrogen peroxide composition and application thereof for plant material delignification
CN106525831A (en) Test paper for detecting hydrogen peroxide in food
CN1177222C (en) Method for producing chlorine residue test paper
CN1426450A (en) Yarn strength enhancing agents and composition and methods employing same

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication
RJ01 Rejection of invention patent application after publication

Application publication date: 20170111