CN106323805A - Quick qualitative detection method for heptafluoropropane fire extinguishing agent and implementation device of method - Google Patents

Quick qualitative detection method for heptafluoropropane fire extinguishing agent and implementation device of method Download PDF

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Publication number
CN106323805A
CN106323805A CN201610750907.9A CN201610750907A CN106323805A CN 106323805 A CN106323805 A CN 106323805A CN 201610750907 A CN201610750907 A CN 201610750907A CN 106323805 A CN106323805 A CN 106323805A
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CN
China
Prior art keywords
bottle
standard sample
heptafluoro
propane
sample bottle
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610750907.9A
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Chinese (zh)
Inventor
江月军
金星屹
刘兹壮
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
CHONGQING RISING GAS Co Ltd
Original Assignee
CHONGQING RISING GAS Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by CHONGQING RISING GAS Co Ltd filed Critical CHONGQING RISING GAS Co Ltd
Priority to CN201610750907.9A priority Critical patent/CN106323805A/en
Publication of CN106323805A publication Critical patent/CN106323805A/en
Pending legal-status Critical Current

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Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N7/00Analysing materials by measuring the pressure or volume of a gas or vapour
    • G01N7/14Analysing materials by measuring the pressure or volume of a gas or vapour by allowing the material to emit a gas or vapour, e.g. water vapour, and measuring a pressure or volume difference
    • G01N7/16Analysing materials by measuring the pressure or volume of a gas or vapour by allowing the material to emit a gas or vapour, e.g. water vapour, and measuring a pressure or volume difference by heating the material

Abstract

The invention discloses a quick qualitative detection method for a heptafluoropropane fire extinguishing agent and an implementation device of the method, and relates to the field of gaseous fire extinguishing agents. The method mainly comprises the steps that the medium pressure in a heptafluoropropane standard sample bottle and the medium pressure in a sampling bottle at the same temperature are measured according to the principle that at the same temperature, heptafluoropropane and other fire extinguishing agents have the different saturated vapor pressures; if the medium pressure in the standard sample bottle and the medium pressure in the sampling bottle are same, a sample to be detected is heptafluoropropane; if the medium pressure in the standard sample bottle and the medium pressure in the sampling bottle are different, the sample to be detected is not heptafluoropropane. Therefore, the function of quickly and conveniently detecting the heptafluoropropane fire extinguishing agent is achieved.

Description

The Quick qualitative detection method of heptafluoro-propane extinguishing chemical and enforcement device thereof
Technical field
The present invention relates to the Quick qualitative detection method of a kind of heptafluoro-propane extinguishing chemical and implement device, relating generally to gas Extinguishing chemical field.
Background technology
Heptafluoro-propane extinguishing chemical is widely used in telecommunications room, radio and television equipment, Generators, subway and light rail, electricity Gas equipment room, transformator, oil-break, book and file shop, scientific research and testing building, valuable instrument and equipment, large ship, oil product Factory Building In place.
Owing to heptafluoro-propane extinguishing chemical is with pressure being stored in gas cylinder, specify by " gas cylinder safely technology Supervision Code ", gas Bottle the detection cycle be 3 years once.First to discharge heptafluoro-propane in bottle during detection, detect qualified after, can be by original qualified seven Fluoro-propane is reinstalled gas cylinder.Heptafluoro-propane unit price is higher, presently, there are the part heptafluoro-propane built-in extinguishing chemical of extinguishing chemical bottle also Non-heptafluoro-propane problem, has a strong impact on extinguishing effect.Just should detect every when therefore dismantling heptafluoro-propane gas cylinder at user simultaneously Extinguishing me whether heptafluoro-propane in individual firefighting bottle bottle.
At present, gas chromatograph or spectrogrph is generally used to be analyzed detecting, but gas chromatograph or spectrogrph conduct Precision instrument, price is higher, operation complexity, mostly uses at laboratory.Therefore firefighting bottle to be detected can only be transported back detection After unit, it is sampled by bottle, with medium in gas chromatograph or spectrometer analysis detection bottle.This detection method, during detection Between longer, and be not to detect face to face at user, be easily generated objection.
Summary of the invention
For above the deficiencies in the prior art, the present invention proposes the fast qualitative detection of a kind of new heptafluoro-propane extinguishing chemical Method and enforcement device.
For reaching above-mentioned purpose, the technical scheme is that
The Quick qualitative detection method of heptafluoro-propane extinguishing chemical:
The first step, prepares heptafluoro-propane standard sample bottle, fills pure heptafluoro-propane, as standard sample bottle in bottle;
Second step, is filled with testing sample in sampling bottle;
3rd step, puts in water-bath bucket by standard sample bottle and sampling bottle, measurement standard sample bottle and sampling bottle temperature, treats standard Sample bottle is consistent with sampling bottle temperature;
4th step, respectively bioassay standard sample bottle and pressure medium in sampling bottle;
5th step, it is determined that: standard sample bottle is identical with pressure medium in sampling bottle, and testing sample is heptafluoro-propane, and pressure is different, Testing sample is non-heptafluoro-propane.
The know-why of the present invention and having the beneficial effect that: heptafluoro-propane and other extinguishing chemical at the same temperature full Different with vapour pressure.The present invention utilizes various extinguishing chemical saturated vapor pressure at the same temperature different, by with heptafluoro-propane mark The saturated vapor pressure of quasi-sample compares, and determines in firefighting bottle extinguishing chemical whether heptafluoro-propane, quick and precisely, simple and convenient, no Detecting in needing detection sample is delivered to laboratory, detection process detects in front of the user, improves the degree of belief of testing result.
The device of the Quick qualitative detection method of heptafluoro-propane extinguishing chemical, including device for detecting temperature, pressure measxurement external member With standard sample bottle, pressure measxurement external member includes precision pressure gauge, and the entrance point of precision pressure gauge is provided with snap joint, in precision It is provided with inlet valve between Pressure gauge and snap joint, precision pressure gauge is also associated with drain valve.
The know-why of the present invention and having the beneficial effect that: testing cost is cheap, and pressure measxurement external member structure is simple;Adopt With precision pressure gauge, detected value is accurate;Portable, pressure measxurement external member can load in small-sized aluminium alloy box, laboratory or scene All can carry out qualitative detection, easy to use, use snap joint, be conveniently connected with standard sample bottle, sampling bottle.
Accompanying drawing explanation
In order to be illustrated more clearly that the embodiment of the present invention or technical scheme of the prior art, embodiment will be described below The accompanying drawing used required in is briefly described, it should be apparent that, for those of ordinary skill in the art, do not paying On the premise of creative work, it is also possible to obtain other accompanying drawing according to these accompanying drawings.
Fig. 1 is the structural representation of the embodiment of the present invention.
Wherein, 1-precision pressure gauge, 2-inlet valve, 3-snap joint, 4-drain valve, 5-thermometer, 6-detects bottle.
Detailed description of the invention
Below in conjunction with accompanying drawing, the technical scheme in the present invention is clearly and completely described, it is clear that described Embodiment is only presently preferred embodiments of the present invention rather than whole embodiments.Based on the embodiment in the present invention, this area The every other embodiment that those of ordinary skill is obtained under not making creative work premise, broadly falls into present invention protection Scope.
Embodiment
As it is shown in figure 1, embodiments of the invention are as follows:
Including precision pressure gauge 1, this precision pressure meter connector 3, it is simple to quick and standard sample bottle, these detection bottles 6 of sampling bottle Connect.
Between snap joint 3 and precision pressure gauge 1, it is provided with inlet valve 2, precision instrument table 1 is additionally provided with drain valve 4.
Step one, preparation heptafluoro-propane standard sample bottle, fill pure heptafluoro-propane, as standard sample bottle in bottle;
Step 2, in sampling bottle, it is filled with testing sample as sampling bottle;
Step 3, standard sample bottle and sampling bottle are put in water-bath bucket, use thermometer 5 measurement standard sample bottle and sampling bottle Temperature, treats that standard sample bottle is consistent with sampling bottle temperature;
Step 4, respectively use snap joint 3 are connected with standard sample bottle, sampling bottle, open inlet valve 2, close drain valve 4, logical Cross precision pressure gauge 1 bioassay standard sample bottle and pressure medium in sampling bottle;
Step 5, judgement: standard sample bottle is identical with pressure medium in sampling bottle, testing sample is heptafluoro-propane;Pressure is different, Testing sample is non-heptafluoro-propane.
The foregoing is only presently preferred embodiments of the present invention, not in order to limit the present invention, all essences in the present invention Within god and principle, any modification, equivalent substitution and improvement etc. made, should be included within the scope of the present invention.

Claims (2)

1. heptafluoro-propane extinguishing chemical Quick qualitative detection method and implement device, it is characterised in that:
The first step, prepares heptafluoro-propane standard sample bottle, fills pure heptafluoro-propane, as standard sample bottle in bottle;
Second step, is filled with testing sample in sampling bottle;
3rd step, puts in water-bath bucket by standard sample bottle and sampling bottle, measurement standard sample bottle and sampling bottle temperature, treats standard Sample bottle is consistent with sampling bottle temperature;
4th step, respectively bioassay standard sample bottle and pressure medium in sampling bottle;
5th step, it is determined that: standard sample bottle is identical with pressure medium in sampling bottle, and testing sample is heptafluoro-propane, and pressure is different, Testing sample is non-heptafluoro-propane.
2. heptafluoro-propane extinguishing chemical Quick qualitative detection method and implement device, it is characterised in that include device for detecting temperature, Pressure measxurement external member and standard sample bottle, described pressure measxurement external member includes precision pressure gauge, the import of described precision pressure gauge End is provided with snap joint, is provided with inlet valve, the row of being also associated with on precision pressure gauge between precision pressure gauge and snap joint Put valve.
CN201610750907.9A 2016-08-30 2016-08-30 Quick qualitative detection method for heptafluoropropane fire extinguishing agent and implementation device of method Pending CN106323805A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610750907.9A CN106323805A (en) 2016-08-30 2016-08-30 Quick qualitative detection method for heptafluoropropane fire extinguishing agent and implementation device of method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610750907.9A CN106323805A (en) 2016-08-30 2016-08-30 Quick qualitative detection method for heptafluoropropane fire extinguishing agent and implementation device of method

Publications (1)

Publication Number Publication Date
CN106323805A true CN106323805A (en) 2017-01-11

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CN (1) CN106323805A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108918320A (en) * 2018-07-11 2018-11-30 九江中船化学科技有限公司 A kind of qualitative detection device of portable gas extinguishing chemical
CN113687012A (en) * 2020-05-19 2021-11-23 陈春来 Dry powder identification method and device

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN201867324U (en) * 2010-11-17 2011-06-15 郑州光力科技股份有限公司 Sulfur hexafluoride (SF6) gas sampling detection device
CN104020158A (en) * 2014-06-27 2014-09-03 宜特科技(昆山)电子有限公司 Method for detecting qualification of to-be-detected product
CN104458649A (en) * 2014-12-23 2015-03-25 深圳因特安全技术有限公司 Recognition and detection method of heptafluoropropane fire-extinguishing agent

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN201867324U (en) * 2010-11-17 2011-06-15 郑州光力科技股份有限公司 Sulfur hexafluoride (SF6) gas sampling detection device
CN104020158A (en) * 2014-06-27 2014-09-03 宜特科技(昆山)电子有限公司 Method for detecting qualification of to-be-detected product
CN104458649A (en) * 2014-12-23 2015-03-25 深圳因特安全技术有限公司 Recognition and detection method of heptafluoropropane fire-extinguishing agent

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108918320A (en) * 2018-07-11 2018-11-30 九江中船化学科技有限公司 A kind of qualitative detection device of portable gas extinguishing chemical
CN113687012A (en) * 2020-05-19 2021-11-23 陈春来 Dry powder identification method and device

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Application publication date: 20170111