CN106323507A - Constant temperature oil groove oil-mercury separation device, constant temperature oil groove mercury processing device, and method for oil-mercury separation and mercury processing - Google Patents
Constant temperature oil groove oil-mercury separation device, constant temperature oil groove mercury processing device, and method for oil-mercury separation and mercury processing Download PDFInfo
- Publication number
- CN106323507A CN106323507A CN201610683357.3A CN201610683357A CN106323507A CN 106323507 A CN106323507 A CN 106323507A CN 201610683357 A CN201610683357 A CN 201610683357A CN 106323507 A CN106323507 A CN 106323507A
- Authority
- CN
- China
- Prior art keywords
- oil
- hydrargyrum
- mercury
- control unit
- groove
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01K—MEASURING TEMPERATURE; MEASURING QUANTITY OF HEAT; THERMALLY-SENSITIVE ELEMENTS NOT OTHERWISE PROVIDED FOR
- G01K15/00—Testing or calibrating of thermometers
- G01K15/005—Calibration
-
- A—HUMAN NECESSITIES
- A62—LIFE-SAVING; FIRE-FIGHTING
- A62D—CHEMICAL MEANS FOR EXTINGUISHING FIRES OR FOR COMBATING OR PROTECTING AGAINST HARMFUL CHEMICAL AGENTS; CHEMICAL MATERIALS FOR USE IN BREATHING APPARATUS
- A62D3/00—Processes for making harmful chemical substances harmless or less harmful, by effecting a chemical change in the substances
- A62D3/30—Processes for making harmful chemical substances harmless or less harmful, by effecting a chemical change in the substances by reacting with chemical agents
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D17/00—Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
- B01D17/02—Separation of non-miscible liquids
- B01D17/0208—Separation of non-miscible liquids by sedimentation
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01K—MEASURING TEMPERATURE; MEASURING QUANTITY OF HEAT; THERMALLY-SENSITIVE ELEMENTS NOT OTHERWISE PROVIDED FOR
- G01K15/00—Testing or calibrating of thermometers
- G01K15/007—Testing
-
- A—HUMAN NECESSITIES
- A62—LIFE-SAVING; FIRE-FIGHTING
- A62D—CHEMICAL MEANS FOR EXTINGUISHING FIRES OR FOR COMBATING OR PROTECTING AGAINST HARMFUL CHEMICAL AGENTS; CHEMICAL MATERIALS FOR USE IN BREATHING APPARATUS
- A62D2101/00—Harmful chemical substances made harmless, or less harmful, by effecting chemical change
- A62D2101/40—Inorganic substances
- A62D2101/43—Inorganic substances containing heavy metals, in the bonded or free state
Abstract
The invention relates to the constant temperature oil groove oil-mercury separation device and a constant temperature oil groove mercury processing device. The constant temperature oil groove oil-mercury separation device comprises a constant temperature oil groove main body; the constant temperature oil groove main body is provided with a control unit, a touch-control displayer, an indication lamp, and a thermometer hanging rack for supporting the thermometer to perform detection, wherein the touch-control displayer and the indication lamp are connected to the control unit; the oil groove of the constant temperature oil groove main body has an arc bottom; the oil groove is provided with an oil outlet pipe I which is communicated with the oil groove and is flush with the lower end of an arc bottom; the oil outlet pipe I is provided with a control valve I; a mercury groove is arranged on the arc bottom of the oil groove; the bottom of the mercury groove is provided with an oil outlet; the oil outlet is positioned right under the thermometer rack; the two ends of the mercury groove are in inclined transition toward the oil outlet and the cross section of the mercury groove is arc; and the oil outlet is provided with a control device in order to let the mercury deposited in the mercury groove discharge along the oil. The constant temperature oil groove oil-mercury separation device, the constant temperature oil groove mercury processing device, and the method for oil-mercury separation and mercury processing can timely detect the mercury fallen into the oil groove, perform separation and subsequent processing on the mercury in the oil tank and effectively solve a problem that the prior art cannot timely clean the mercury in the oil groove.
Description
Technical field
The present invention relates to detection thermostatic oil bath technical field, be specifically related to a kind of thermostatic oil bath oil hydrargyrum and separate and hydrargyrum process
Device, method.
Background technology
Thermostatic oil bath is the necessary equipment of thermometer calibrating, and temperature range 100 DEG C～300 DEG C is usually used in mercurial thermometer
Deng calibrating and calibration.
In the verification process of mercurial thermometer, it is susceptible to thermometer and drops, the situation such as crush, cause mercurial thermometer
Interior hydrargyrum enters in thermostatic oil bath.All discharge generally by by the fluid (oil is contained within hydrargyrum) in oil groove under prior art
After, the mode utilizing sulfur to bring it about the chemical reaction nontoxic cinnabar of generation (Hg+S=HgS) reaches to remove the purpose of hydrargyrum,
But this mode wastes time and energy in operation, add the biggest burden to operator.
Summary of the invention
It is desirable to provide a kind of hydrargyrum that can efficiently separate in oil groove, and the perseverance that isolated hydrargyrum is processed
Temperature oil groove oil hydrargyrum separates and hydrargyrum processing means, method.
The present invention is achieved through the following technical solutions:
A kind of thermostatic oil bath oil hydrargyrum segregation apparatus, includes thermostatic oil bath body, and thermostatic oil bath body is provided with control unit, connection
Control unit also carries out, with control unit, the touch control display that information is mutual, connects control unit and carries out the instruction that state shows
Lamp, support temperature meter carries out the thermometer hanger examined and determine, and it is characterized in that and also includes oil hydrargyrum segregation apparatus, and oil hydrargyrum divides
It is on the oil groove have arcuate bottom, to be communicated with oil groove the flowline I concordant with arcuate bottom lower end, on flowline I from device
Being provided with control valve I, be additionally provided with a mercury tank, be provided with oil-out bottom mercury tank bottom the arcuate bottom of oil groove, oil-out is positioned at temperature
The underface of meter hanger, mercury tank to oil-out angled transition and is had arc-shaped cross-section by two ends, and at oil-out, connection has fuel-displaced
Pipe II, flowline II is provided with control valve II, and control valve II, control valve I electrically connect with control unit respectively, to realize by touching
Control display controls folding.
In the verification process of mercurial thermometer, when thermometer is dropped, broken caused the hydrargyrum in mercurial thermometer to enter perseverance
After in temperature oil groove, owing to the density of hydrargyrum is big, it can sink down into interior and along mercury tank the tilting bottom of mercury tank and assemble to oil-out, this
Time opened by the operation control valve II that controls at oil-out of touch control display, the hydrargyrum in mercury tank can be made to discharge with fluid.
Being additionally provided with the probe unit of mercury content in detecting oil groove, this probe unit is connected with control unit；Detection is single
Sending information to control unit after unit is mercurous in detecting oil groove, control unit automatically controls control valve II after receiving information
Open, make the hydrargyrum in mercury tank discharge with fluid.
As preferably, probe unit uses mercury ion fluorescence probe to detect.
It is additionally provided with the thermometer whether being broken for detecting thermometer and crushes detector unit, for being broken at thermometer
Time send the alarm unit of caution sound, thermometer crushes detector unit, alarm unit is connected with control unit.
As preferably, it is to be located at presence or absence based on temperature sensor on thermometer hanger that thermometer crushes detector unit
Pressure transducer, when thermometer is broken, pressure transducer sends the signal to control unit.
A kind of thermostatic oil bath hydrargyrum processing means, it is isolated that this hydrargyrum processing means is used for processing above-mentioned oil hydrargyrum segregation apparatus
Hydrargyrum, this hydrargyrum processing means includes removing device, storage device and delivery device；
Wherein, device is removed: accommodate the hydrargyrum discharged by flowline II；
Storage device: be used for storing Cosan；
Delivery device: the Cosan in storage device is put into and removes device so that it is to carry out chemical reaction nontoxic to generate with hydrargyrum
Compound, this delivery device electrically connects and accepts the control of control unit with control unit, and control unit controls oil hydrargyrum and separates dress
Put after isolating hydrargyrum, can continue to control delivery device action, by hydrargyrum processing means, the hydrargyrum discharged be processed.
More preferably, above-mentioned removing device is a container that can accommodate hydrargyrum；Storage device is a container storing Cosan；
Delivery device is an input control valve, and this input control valve is located on the Cosan transfer passage between storage device and removing device
And this input control valve also electrically connects with control unit.
A kind of utilize above-mentioned thermostatic oil bath oil hydrargyrum segregation apparatus and hydrargyrum processing means carry out oil hydrargyrum separate and hydrargyrum process side
Method, it is characterised in that comprise the steps:
Whether there is the existence of hydrargyrum in S1, probe unit detection oil groove, and result of detection is sent to control unit；
If S2 detects without hydrargyrum, then controlled to continue detection by control unit；If being detected with hydrargyrum, then control unit controls constant temperature
Oil groove quits work, and controls control valve II afterwards and opens, and makes the hydrargyrum sinking down in mercury tank be expelled to remove device with fluid；
S3, to be discharged complete after, control unit control control valve II close, control unit continue control delivery device open, make
Storage device throws in sulfur in removing device, makes sulfur and hydrargyrum carry out chemical reaction to generate non-toxic compound.
More preferably, in S1, while probe unit works, thermometer crushes detector unit and works and to control the most simultaneously
Unit sends testing result information, and control alarm unit is sent report after receiving the information that thermometer is broken by control unit
Alert, perform the action command identical with when detecting hydrargyrum simultaneously.
The beneficial effects of the present invention is: it can detect the hydrargyrum falling in oil groove in time, and the hydrargyrum in oil groove is carried out point
From rear and follow-up process, efficiently solve and under prior art, be not easy to remove in time a difficult problem for hydrargyrum in oil groove.
Accompanying drawing explanation
The present invention is further illustrated below in conjunction with the accompanying drawings.
Fig. 1 is the external structure schematic diagram of the present invention.
Fig. 2 is the side structure schematic diagram of oil hydrargyrum segregation apparatus.
Fig. 3 is the Facad structure schematic diagram of oil hydrargyrum segregation apparatus.
Fig. 4 is the structural representation of hydrargyrum processing means.
Fig. 5 is the functional frame composition of the present invention.
Fig. 6 is the control flow chart of the present invention.
In figure, 1 thermostatic oil bath body, 2 thermometer hangers, 3 thermometeies, 4 touch control displays, 5 display lamps, 6 oil grooves, 7 go out
Oil pipe I, 8 control valve I, 9 mercury tank, 11 flowline II, 12 control valve II, 13 oil-outs.
Detailed description of the invention
Accompanying drawing 1,2,3 is the embodiment of thermostatic oil bath oil hydrargyrum segregation apparatus in the present invention.This embodiment includes thermostatical oil
Groove body 1, thermostatic oil bath body be provided with control unit, connect control unit and with control unit carry out the mutual touch-control of information show
Show device 4, connect control unit and carry out switching on and shutting down, run, stop, display lamp 5 that fault, the state such as warning shows, support warm
Degree meter 3 carries out the thermometer hanger 2 examined and determine, and oil hydrargyrum segregation apparatus is to be communicated with oil groove also on the oil groove 6 have arcuate bottom
The flowline I 7 concordant with arcuate bottom lower end, flowline I is provided with control valve I 8, is additionally provided with a hydrargyrum bottom the arcuate bottom of oil groove
Groove 9, is provided with oil-out 13 bottom mercury tank, oil-out is positioned at the underface of thermometer hanger, and mercury tank is tilted to oil-out by two ends
Transition and have arc-shaped cross-section, connects at oil-out and has flowline II 11, flowline II is provided with control valve II 12, control
Valve II, control valve I electrically connect with control unit respectively, to realize being controlled folding by touch control display；It is additionally provided with employing mercury ion
Fluorescent probe carries out detecting the detector unit of mercury content in oil groove；Also it is located on thermometer hanger and exists based on temperature sensor
Whether pressure transducer (can determine whether whether thermometer is broken by this pressure transducer) and for being broken at thermometer
Time send the alarm unit of caution sound；Above-mentioned detector unit, pressure transducer, alarm unit are connected with control unit respectively.
Accompanying drawing 4 show the embodiment of thermostatic oil bath hydrargyrum processing means, and this embodiment includes the hydrargyrum that can accommodate discharge
Remove device (being a container that can accommodate hydrargyrum), store the storage device (being a container storing Cosan) of Cosan,
With hydrargyrum, the Cosan input removing device in storage device is carried out chemical reaction (set with the delivery device generating non-toxic compound
Input control valve on storage device and the Cosan transfer passage removed between device, this input control valve also with control unit
Electrical connection).
As shown in Figure 5,6, in the present invention, the method that thermostatic oil bath oil hydrargyrum separates and hydrargyrum processes comprises the steps:
Whether there is the existence of hydrargyrum in S1, probe unit detection oil groove, and result of detection is sent to control unit；
If S2 detects without hydrargyrum, then controlled to continue detection by control unit；If being detected with hydrargyrum, then control unit controls constant temperature
Oil groove quits work, and control valve II is opened afterwards, makes the hydrargyrum sinking down in mercury tank be expelled to remove device with fluid；
S3, to be discharged complete after, control unit control control valve II close, control unit continue control throw in control valve to removing
Throw in sulfur in device, make sulfur and hydrargyrum carry out chemical reaction to generate non-toxic compound.
Further, in S1, while probe unit works, thermometer crushes detector unit and works and to control the most simultaneously
Unit sends testing result information, and control alarm unit is sent report after receiving the information that thermometer is broken by control unit
Alert, perform the action command identical with when detecting hydrargyrum simultaneously.
Claims (9)
1. a thermostatic oil bath oil hydrargyrum segregation apparatus, includes thermostatic oil bath body (1), and described thermostatic oil bath body is provided with control
Unit, connection control unit also carry out the mutual touch control display of information (4) with control unit, connect control unit and also carry out shape
The display lamp (5) that state shows, support temperature meter (3) carries out the thermometer hanger (2) examined and determine, it is characterised in that: described oil hydrargyrum divides
It is on the oil groove (6) with arcuate bottom, be communicated with oil groove the flowline I (7) concordant with arcuate bottom lower end, institute from device
State flowline I and be provided with control valve I (8), be additionally provided with a mercury tank (9) bottom the arcuate bottom of described oil groove, be provided with bottom mercury tank
Oil-out (13), described oil-out is positioned at the underface of thermometer hanger, described mercury tank by two ends to oil-out angled transition and
Having arc-shaped cross-section, connecting at described oil-out has flowline II (11), and described flowline II is provided with control valve II
(12), described control valve II, control valve I electrically connect with control unit respectively, to realize being controlled folding by touch control display.
Thermostatic oil bath oil hydrargyrum segregation apparatus the most according to claim 1, it is characterised in that: it is additionally provided with hydrargyrum in detecting oil groove
Probe unit, described probe unit electrically connects with control unit, and described control unit is according to the result of detection control of probe unit
The folding of control valve II processed.
Thermostatic oil bath oil hydrargyrum segregation apparatus the most according to claim 2, it is characterised in that: described probe unit be use hydrargyrum from
Sub-fluorescent probe carries out detecting.
Thermostatic oil bath oil hydrargyrum segregation apparatus the most according to claim 1, it is characterised in that: it is additionally provided with for detecting thermometer and is
The no thermometer being broken crushes detector unit, for sending the alarm unit of caution sound when thermometer is broken, described temperature
The broken detector unit of degree meter, alarm unit are connected with control unit.
Thermostatic oil bath oil hydrargyrum segregation apparatus the most according to claim 4, it is characterised in that: described thermometer crushes detector unit
For being located on thermometer hanger the pressure transducer of presence or absence based on temperature sensor.
6. a thermostatic oil bath hydrargyrum processing means, described hydrargyrum processing means is used for locating oil hydrargyrum according to any one of reason power 1-5 and divides
From the isolated hydrargyrum of device, it is characterised in that: described hydrargyrum processing means includes removing device, storage device and delivery device；
Wherein, described removing device: accommodate the hydrargyrum discharged by flowline II；
Described storage device: be used for storing Cosan；
Described delivery device: the Cosan in storage device is put into and removes device so that it is carry out chemical reaction to generate with hydrargyrum
Non-toxic compound.
Thermostatic oil bath hydrargyrum processing means the most according to claim 6, it is characterised in that: described removing device is one can to accommodate hydrargyrum
Container；Described storage device is a container storing Cosan；Described delivery device is an input control valve, this input control
Valve processed is located on the Cosan transfer passage between storage device and removing device and this input control valve is also electrically connected with control unit
Connect.
8. thermostatic oil bath oil hydrargyrum segregation apparatus according to any one of exploitation right 1-5 and power 6 or 7 according to any one of thermostatical oil
Groove hydrargyrum processing means carries out the method that oil hydrargyrum separates and hydrargyrum processes, it is characterised in that comprise the steps:
Whether there is the existence of hydrargyrum in S1, probe unit detection oil groove, and result of detection is sent to control unit；
If S2 detects without hydrargyrum, then controlled to continue detection by control unit；If being detected with hydrargyrum, then control unit controls constant temperature
Oil groove quits work, and control valve II is opened afterwards, makes the hydrargyrum sinking down in mercury tank be expelled to remove device with fluid；
S3, to be discharged complete after, control unit control control valve II close, control unit continue control delivery device open, make
Storage device throws in sulfur in removing device, makes sulfur and hydrargyrum carry out chemical reaction to generate non-toxic compound.
The method that the most according to claim 8, oil hydrargyrum separates and hydrargyrum processes, it is characterised in that: in S1, work at probe unit
While, thermometer crushes detector unit and works the most simultaneously and send testing result information to control unit, and control unit receives
After the information that thermometer is broken, control alarm unit is sent warning, perform the action identical with when detecting hydrargyrum simultaneously and refer to
Order.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610683357.3A CN106323507B (en) | 2016-08-18 | 2016-08-18 | A kind of separation of thermostatic oil bath oil mercury and mercury processing unit, method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610683357.3A CN106323507B (en) | 2016-08-18 | 2016-08-18 | A kind of separation of thermostatic oil bath oil mercury and mercury processing unit, method |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN106323507A true CN106323507A (en) | 2017-01-11 |
| CN106323507B CN106323507B (en) | 2019-01-08 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201610683357.3A Expired - Fee Related CN106323507B (en) | 2016-08-18 | 2016-08-18 | A kind of separation of thermostatic oil bath oil mercury and mercury processing unit, method |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE19522596A1 (en) * | 1995-06-19 | 1997-01-02 | Hertz Inst Heinrich | Unit recovers and purifies special oil used e.g. in semiconductor mfr. |
| CN202777565U (en) * | 2012-07-10 | 2013-03-13 | 浙江大学 | Harmless negative-pressure mercury collector |
| CN204855030U (en) * | 2015-06-26 | 2015-12-09 | 江苏东方航天校准检测有限公司 | Thermometer is markd with constant temperature oil groove |
| CN105258816A (en) * | 2015-11-18 | 2016-01-20 | 高丽萍 | Device for processing mercury leakage |
| CN205341466U (en) * | 2016-01-25 | 2016-06-29 | 门述强 | Mercury collector |
-
2016
- 2016-08-18 CN CN201610683357.3A patent/CN106323507B/en not_active Expired - Fee Related
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE19522596A1 (en) * | 1995-06-19 | 1997-01-02 | Hertz Inst Heinrich | Unit recovers and purifies special oil used e.g. in semiconductor mfr. |
| CN202777565U (en) * | 2012-07-10 | 2013-03-13 | 浙江大学 | Harmless negative-pressure mercury collector |
| CN204855030U (en) * | 2015-06-26 | 2015-12-09 | 江苏东方航天校准检测有限公司 | Thermometer is markd with constant temperature oil groove |
| CN105258816A (en) * | 2015-11-18 | 2016-01-20 | 高丽萍 | Device for processing mercury leakage |
| CN205341466U (en) * | 2016-01-25 | 2016-06-29 | 门述强 | Mercury collector |
Non-Patent Citations (1)
| Title |
|---|
| 陈慧珠: "重力式液-液分离器的设计与调节", 《化工设备设计》 * |
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| CN106323507B (en) | 2019-01-08 |
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