CN106310701A - Equipment specially used for sublimating and purifying small organic molecules - Google Patents
Equipment specially used for sublimating and purifying small organic molecules Download PDFInfo
- Publication number
- CN106310701A CN106310701A CN201610891712.6A CN201610891712A CN106310701A CN 106310701 A CN106310701 A CN 106310701A CN 201610891712 A CN201610891712 A CN 201610891712A CN 106310701 A CN106310701 A CN 106310701A
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- China
- Prior art keywords
- fixed
- regulator cubicle
- vacuum
- heating system
- railroad
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D7/00—Sublimation
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The invention discloses equipment specially used for sublimating and purifying small organic molecules. The equipment comprises an electrical cabinet, wherein a sliding rail device is fixed at one end of the surface of the electrical cabinet, a vacuum system is fixed at the other end of the surface of the electrical cabinet, a heating system is fixed between the sliding rail device and the vacuum system, a test tube is arranged in the middle of the heating system, a special flange is fixed at one end, close to the sliding rail device, of the test tube, the special flange freely slides on the sliding rail device, a vacuum detection meter is fixed at one end, close to the sliding rail device, of the test tube, and cooling fans are uniformly distributed in the heating system. The equipment disclosed by the invention has the advantages that only horizontal movement function of the special flange is added; meanwhile, vacuum requirement is improved by arranging the vacuum detection meter, effective control on a small organic molecule material vacuum sublimating and purifying process is realized, the purity, the quality and the speed of the material are improved, and pollution and material waste are reduced.
Description
Technical field
The invention belongs to sublimation purification apparatus field, particularly relate to a kind of organic molecule sublimation purification special equipment.
Background technology
Organic small molecule material is purified by prior art frequently with vacuum sublimation technology.Currently used vacuum sublimation
Equipment for purifying uses three sections of temperature controls or the design of five sections of temperature controls, obtains fine vacuum by the combination of mechanical pump, molecular pump
Different warm areas are regulated and controled by atmosphere the most respectively, utilize the different sublimation temperatures of different component material to carry out separating-purifying and obtain
High-quality, highly purified organic small molecule material.Traditional vacuum sublimation equipment for purifying can not realize organic small molecule material
Effective control of vacuum sublimation purification process, causes purity and the inferior quality of material.
Summary of the invention
It is an object of the invention to the problem above overcoming prior art to exist, it is provided that a kind of organic molecule sublimation purification
Special equipment, it is possible to realize organic small molecule material vacuum sublimation purification process is control effectively, improve the purity of material
And quality.
For realizing above-mentioned technical purpose, reaching above-mentioned technique effect, the present invention is achieved through the following technical solutions:
A kind of organic molecule sublimation purification special equipment, including regulator cubicle, one end, described regulator cubicle surface is fixed with cunning
Rail device, the described regulator cubicle surface other end is fixed with vacuum system, is fixed with and adds between described railroad and vacuum system
Hot systems, is provided with test tube in the middle of described heating system, described test tube is fixed with special flange near railroad one end, described
On railroad slidably, described test tube is further fixed on vacuum detection meter near railroad one end to special flange, described
Heating system is evenly equipped with heat emission fan.
Further, described regulator cubicle is provided with touch control screen near vacuum system one end, it is simple to the intelligence to equipment
Control.
Further, described regulator cubicle side is provided with regulator cubicle instrument, is effectively utilized the structure space of regulator cubicle.
Further, uniform blissful horse wheel bottom described regulator cubicle, it is simple to the movement of regulator cubicle is with fixing.
Further, all it is inter-connected via a bolt joint bottom described railroad, heating system and between regulator cubicle, strengthens
Attachment structure intensity bottom railroad, heating system and between regulator cubicle.
The invention has the beneficial effects as follows:
The present invention not only increases the horizontally moving functions of special flange, and improves vacuum by the setting of vacuometer
Requirement, it is achieved that organic small molecule material vacuum sublimation purification process is control effectively, improve the purity of material, quality with
And speed, decrease the waste polluted with material.
Accompanying drawing explanation
Accompanying drawing described herein is used for providing a further understanding of the present invention, constitutes the part of the application, this
Bright schematic description and description is used for explaining the present invention, is not intended that inappropriate limitation of the present invention.In the accompanying drawings:
Fig. 1 is the structural representation of the present invention；
Label declaration in figure: 1-railroad, 2-special flange, 3-vacuum detection meter, 4-test tube, 5-heating system, 6-
Heat emission fan, 7-vacuum system, 8-touch control screen, 9-regulator cubicle.
Detailed description of the invention
Below with reference to the accompanying drawings and in conjunction with the embodiments, the present invention is described in detail.
A kind of organic molecule sublimation purification special equipment as shown in Figure 1, including regulator cubicle 9, one end, regulator cubicle 9 surface
Being fixed with railroad 1, the regulator cubicle 9 surface other end is fixed with vacuum system 7, and regulator cubicle 9 side is provided with regulator cubicle instrument,
Being effectively utilized the structure space of regulator cubicle 9, regulator cubicle 9 is provided with touch control screen 8 near vacuum system 7 one end, it is simple to right
The Based Intelligent Control of equipment, is fixed with between railroad 1 and vacuum system 7 in the middle of heating system 5, heating system 5 and is provided with examination
Pipe 4, test tube 4 is fixed with special flange 2 near railroad 1 one end, special flange 2 on railroad 1 slidably, test tube
4 are further fixed on vacuum detection meter 3 near railroad 1 one end, are evenly equipped with heat emission fan 6 in heating system 5, bottom regulator cubicle 9 all
The blissful horse of cloth is taken turns, it is simple to the movement of regulator cubicle 9, with fixing, is all passed through bottom railroad 1, heating system 5 and between regulator cubicle 9
Bolt is connected with each other, and strengthens the attachment structure intensity bottom railroad 1, heating system 5 and between regulator cubicle 9.
The present invention makes special flange 2 to move horizontally by railroad 1, and its effect has 2 points, and one is convenient
Picking and placeing material, two is thoroughly to clean the test tube after using, it is to avoid the existence of pollutant, is greatly improved purification quality；Pin
Vacuum detection meter 3 is arranged on feed end by property, invisible spectro vacuum environment made harsher detection mode, significantly carries
High purification quality；Place organic material by test tube 4, and make material completely cut off with atmospheric environment；Essence is provided by heating system 5
True warm field；Because needing fast cooling to improve output after organic material distillation, heat so inciting somebody to action after heating process terminates
System 5 is opened and passes through the operating raising heat dissipation capacity increase output of heat emission fan 6；Required vacuum ring is obtained by vacuum system 7
Border；Parameter is controlled by touch control screen 8 set device.
The present invention not only increases the horizontally moving functions of special flange, and improves vacuum by the setting of vacuometer
Requirement, it is achieved that organic small molecule material vacuum sublimation purification process is control effectively, improve the purity of material, quality with
And speed, decrease the waste polluted with material.
The ultimate principle of the present invention, principal character and advantages of the present invention have more than been shown and described.The technology of the industry
Personnel, it should be appreciated that the present invention is not restricted to the described embodiments, simply illustrating this described in above-described embodiment and description
The principle of invention, without departing from the spirit and scope of the present invention, the present invention also has various changes and modifications, and these become
Change and improvement both falls within scope of the claimed invention.
Claims (5)
1. an organic molecule sublimation purification special equipment, including regulator cubicle (9), it is characterised in that: described regulator cubicle (9) table
One end, face is fixed with railroad (1), and described regulator cubicle (9) the surface other end is fixed with vacuum system (7), described railroad
(1) and it is fixed with between vacuum system (7) in the middle of heating system (5), described heating system (5) and test tube (4), described examination are installed
Pipe (4) is fixed with special flange (2) near railroad (1) one end, and described special flange (2) is upper freely at railroad (1)
Sliding, described test tube (4) is further fixed on vacuum detection meter (3) near railroad (1) one end, in described heating system (5) all
It is furnished with heat emission fan (6).
A kind of organic molecule sublimation purification special equipment the most according to claim 1, it is characterised in that: described regulator cubicle
(9) it is provided with touch control screen (8) near vacuum system (7) one end.
A kind of organic molecule sublimation purification special equipment the most according to claim 1, it is characterised in that: described regulator cubicle
(9) side is provided with regulator cubicle instrument.
A kind of organic molecule sublimation purification special equipment the most according to claim 1, it is characterised in that: described regulator cubicle
(9) the uniform blissful horse in bottom wheel.
A kind of organic molecule sublimation purification special equipment the most according to claim 1, it is characterised in that: described slide rail fills
Put (1), be all inter-connected via a bolt joint between heating system (5) bottom and regulator cubicle (9).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610891712.6A CN106310701A (en) | 2016-10-12 | 2016-10-12 | Equipment specially used for sublimating and purifying small organic molecules |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610891712.6A CN106310701A (en) | 2016-10-12 | 2016-10-12 | Equipment specially used for sublimating and purifying small organic molecules |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106310701A true CN106310701A (en) | 2017-01-11 |
Family
ID=57821458
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610891712.6A Pending CN106310701A (en) | 2016-10-12 | 2016-10-12 | Equipment specially used for sublimating and purifying small organic molecules |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106310701A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107376394A (en) * | 2017-08-04 | 2017-11-24 | 贵州自然生物科技有限公司 | Sublimed method pyrogallic acid automatically adjusts speed of exhaust retracting device |
| CN109646987A (en) * | 2019-01-10 | 2019-04-19 | 合肥欧莱迪光电技术有限公司 | A kind of continuous feeding and discharging high vacuum small organic molecule purification special equipment |
| CN111233710A (en) * | 2018-11-28 | 2020-06-05 | 弗萨姆材料美国有限责任公司 | Low halide lanthanide precursors for vapor deposition |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20130104162A (en) * | 2012-03-13 | 2013-09-25 | 주식회사 피브이디 | Sublimation purifying apparatus of organic matter having independently heating part |
| CN203231642U (en) * | 2013-04-25 | 2013-10-09 | 安徽贝意克设备技术有限公司 | Slide rail type furnace fast in heating and cooling |
| CN204601666U (en) * | 2015-02-13 | 2015-09-02 | 安徽贝意克设备技术有限公司 | A kind of multiple combined purification high vacuum purification system |
| CN204630370U (en) * | 2015-05-07 | 2015-09-09 | 安徽贝意克设备技术有限公司 | A kind of tube furnace being furnished with vacuum driven rod |
-
2016
- 2016-10-12 CN CN201610891712.6A patent/CN106310701A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20130104162A (en) * | 2012-03-13 | 2013-09-25 | 주식회사 피브이디 | Sublimation purifying apparatus of organic matter having independently heating part |
| CN203231642U (en) * | 2013-04-25 | 2013-10-09 | 安徽贝意克设备技术有限公司 | Slide rail type furnace fast in heating and cooling |
| CN204601666U (en) * | 2015-02-13 | 2015-09-02 | 安徽贝意克设备技术有限公司 | A kind of multiple combined purification high vacuum purification system |
| CN204630370U (en) * | 2015-05-07 | 2015-09-09 | 安徽贝意克设备技术有限公司 | A kind of tube furnace being furnished with vacuum driven rod |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107376394A (en) * | 2017-08-04 | 2017-11-24 | 贵州自然生物科技有限公司 | Sublimed method pyrogallic acid automatically adjusts speed of exhaust retracting device |
| CN111233710A (en) * | 2018-11-28 | 2020-06-05 | 弗萨姆材料美国有限责任公司 | Low halide lanthanide precursors for vapor deposition |
| US20210363162A1 (en) * | 2018-11-28 | 2021-11-25 | Versum Materials Us, Llc | Low Halide Lanthanum Precursors For Vapor Deposition |
| US11753420B2 (en) * | 2018-11-28 | 2023-09-12 | Versum Materials Us, Llc | Low halide lanthanum precursors for vapor deposition |
| CN109646987A (en) * | 2019-01-10 | 2019-04-19 | 合肥欧莱迪光电技术有限公司 | A kind of continuous feeding and discharging high vacuum small organic molecule purification special equipment |
| CN109646987B (en) * | 2019-01-10 | 2024-03-26 | 合肥百思智能装备有限公司 | Continuous feeding and discharging high-vacuum organic micromolecule purifying special equipment |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20170111 |
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| RJ01 | Rejection of invention patent application after publication |