CN106281693A - A kind of dual path quintessence oil preparation method - Google Patents
A kind of dual path quintessence oil preparation method Download PDFInfo
- Publication number
- CN106281693A CN106281693A CN201510269366.3A CN201510269366A CN106281693A CN 106281693 A CN106281693 A CN 106281693A CN 201510269366 A CN201510269366 A CN 201510269366A CN 106281693 A CN106281693 A CN 106281693A
- Authority
- CN
- China
- Prior art keywords
- quintessence oil
- dual path
- dried
- oil preparation
- raw material
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Fats And Perfumes (AREA)
Abstract
The present invention relates to extract application, particularly relate to a kind of dual path quintessence oil preparation method.Comprise the steps of: be dried, collect the mixture of dried steam and volatile component；Vapours is lowered the temperature by condenser, collects condensate, i.e. obtains volatile spirits and condensed water mixture；Separating mixture, i.e. available required quintessence oil；Beneficial effect: 1. utilize the mode drying evaporation, obtain the volatile ingredient in raw material, carry out the high efficiency separation of target component in raw material selectively, be effectively improved the quality of product.2. the energy of production process, solvent-oil ratio are greatly lowered, reduce production cost, improve the market competitiveness of product.The most effectively shorten process route, reduce discharge.4. use group technology, be effectively improved raw material availability.Raw material after 5 productions can directly store, it is simple to following process.
Description
Technical field
The present invention relates to extract application, particularly relate to a kind of dual path quintessence oil preparation method.
Background technology
Volatile oil is also known as quintessence oil, and English is essentialoils, the class being present in plant have aromatic odor, can with vapor distillation out and the general name of the volatility oily composition the most miscible with water.Volatile oil is a mixture, and its component is complex.Mainly produce quintessence oil by steam distillation, milling process, extraction perfume (or spice) method and solvent method.In volatile oil component common with ter penoids, it addition, still contain little molecular fat compounds of group and little molecule aromatic compound.
The method extracting quintessence oil has many kinds, and each of which needs special equipment.
Conventional processing methods processing predominantly steam distillation method obtains endophytic volatile ingredient quintessence oil, and major way has three kinds: water distillation, distilling above water and straight-through steam distillation.
The program is the most conventional process program, produces improvement through for many years, and technical maturity is stable.Its greatest drawback is that course of processing energy consumption is big, and yield is low, and Product processing cost is high, first carries out raw material through decocting in water, as being dried not in time, easily rots, have greater environmental impacts.
Meanwhile, if individually using a kind of pattern, a lot of quintessence oils can be deposited in material and can not extract out.
Summary of the invention
The purpose of invention: in order to provide a kind of effect more preferable dual path quintessence oil preparation method, specific purposes are shown in the multiple substantial technological effects being embodied as part.
In order to reach as above purpose, the present invention adopts the following technical scheme that:
A kind of dual path quintessence oil preparation method, it is characterised in that comprise the steps of:
1) feed product being inserted in container and be dried, make material be continuously heated, volatile ingredient therein spreads spilling successively, collects the mixture of dried steam and volatile component；
2) vapours is lowered the temperature by condenser, collects condensate, i.e. obtains volatile spirits and condensed water mixture；
3) separating mixture, i.e. available required quintessence oil；
4) simultaneously by the material of drying, packing stores, and can continue to use extraction or subcritical abstraction to take other compositions.
The further technical scheme of the present invention is, also comprises the steps of: 5 after described step 4)) extraction or the extract of subcritical abstraction, use the method for molecular distillation to continue to obtain remaining quintessence oil.
The further technical scheme of the present invention is, described being dried is dried for evacuation.
The further technical scheme of the present invention is, described dry employing continuous drying equipment.
The further technical scheme of the present invention is, described step 3) is the distillate stratification after cooling down, and obtains top quintessence oil.
The further technical scheme of the present invention is, also comprises the step mixed by the quintessence oil of step 3) and step 5).
Use the present invention of as above technical scheme, have the advantages that relative to prior art:
1. utilize the mode drying evaporation, obtain the volatile ingredient in raw material, carry out extraction and the separation of target component in raw material selectively, improve the quality of product further.
2. effectively reduce the energy of system, solvent-oil ratio, reduce production cost, improve the market competitiveness of product.
The most effectively shorten process route, reduce discharge.
4. use group technology, be effectively improved raw material availability.
5 reduce steam, the consumption of water, economize on resources further.
Accompanying drawing explanation
In order to further illustrate the present invention, it is further illustrated below in conjunction with the accompanying drawings:
Fig. 1 is invented technology flow chart；
Fig. 2 is apparatus sketch.
Detailed description of the invention
Illustrating embodiments of the invention below in conjunction with the accompanying drawings, embodiment is not construed as limiting the invention:
The purpose of the present invention is by realizing by the following technical solutions: a kind of method separating quintessence oil from plant material, and it is mainly characterized by comprising following steps:
(1) by raw material pulverizing, pan dryer is loaded continuously；
(2) open vacuum pump, cooling water, cool down distillating steam；
(3) material successively falls under agitator effect, controls mixing speed, it is ensured that when material is discharged from bottom, and water content reaches to store or following process requirement, and steam is imported cooler by top, and gold cooling flows into lower end mixed liquor catcher；
(4) when mixed liquor reaches a certain amount of in catcher, close vacuum, open bottom liquid valve, release bottom water and supernatant quintessence oil respectively.
(5) dried material slag is merged, utilize subcritical abstraction oils and fats therein；
(6) subcritical abstraction thing evaporates through molecular distillation, isolates quintessence oil and other liposoluble constituents.
The described method extracting, separating quintessence oil from raw material also comprises the following steps that
(7) being passed through steam bottom material disc in coil pipe, heated material dish, 5 × 10- 2Under the vacuum state of Pa, moisture in material and and volatile oil by thermal evaporation, overflow in material, separate；Condensation, recovery i.e. can get combination cooling liquid.
The described method separating quintessence oil from plant material, its mode of heating can be to use the forms such as electrical heating, steam heating, heat-conducting oil heating, far infrared and microwave heating.
The described method of extract and separate quintessence oil from plant material, its drying equipment includes fluid bed drying, cylinder tunnel drying, disc driers, tray drier etc..
The described method of extract and separate quintessence oil from dried material, its extracting method includes traditional extraction, subcritical abstraction and carbon dioxide supercritical fluid extraction, and molecular distillation separates.
Below in conjunction with accompanying drawing, most preferred embodiment is described in further detail:
Embodiment 1: oven drying method separation quintessence oil
The present embodiment comprises the following steps that fresh-rose is sent into drying machine with this by conveyer by (1), opens steam and cooling water.
(2) vacuum pump is started, it is ensured that inside unit, be in negative pressure state.
(3) steam volatilized is imported condenser, cooled inflow lower end mixed liquor catcher.
(4) when mixed liquor reaches a certain amount of in catcher, close vacuum, open bottom liquid valve, release bottom water and supernatant Flos Rosae Rugosae quintessence oil respectively.
(5) dried material slag is merged, utilize subcritical abstraction oils and fats therein；
(6) complete the material slag after extraction to get rid of outside still, may be used for extracting other compositions such as pigment；Merge and release extract.
(7) subcritical abstraction thing is heated to 40-55 DEG C, inputs molecular distillation afterwards, separate volatile essential oil therein further.
Obtain Flos Rosae Rugosae extractum simultaneously.It should be noted that multiple schemes that this patent provides comprise the basic scheme of itself, separate, the most mutually restrict, but it can also be mutually combined in the case of not conflicting, reach multiple effect and jointly realize.
Using this technique, with employing water distillation, distilling above water and the material of straight-through steam distilled PROCESS FOR TREATMENT same amount, feature contrast is as follows:
| The present invention | Water distillation | Distilling above water | Straight-through steam distillation | |
| Yield ‰ | 0.41 | 0.4 | 0.42 | 0.46 |
| Speed of production | Hurry up | Slowly | Slower | Comparatively fast |
| Environmental protection degree | Zero-emission | Seriously | Seriously | Relatively low |
| Processing cost | Low | High | Higher | Relatively low |
| Risk (such as whether needing to be dried in time) | Low | High | Higher | Relatively low |
The ultimate principle of the present invention, principal character and advantages of the present invention have more than been shown and described.Those skilled in the art is it should be recognized that the present invention is not restricted to the described embodiments; the principle that the present invention is simply described described in above-described embodiment and description; without departing from the spirit and scope of the present invention; the present invention also has various changes and modifications, and these changes and improvements both fall within claimed scope.
Claims (6)
1. a dual path quintessence oil preparation method, it is characterised in that comprise the steps of:
1) feed product being inserted in container and be dried, make material be continuously heated, volatile ingredient therein spreads spilling successively, collects the mixture of dried steam and volatile component；
2) vapours is lowered the temperature by condenser, collects condensate, i.e. obtains volatile spirits and condensed water mixture；
3) separating mixture, i.e. available required quintessence oil；
4) simultaneously by the material of drying, packing stores, and can continue to use extraction or subcritical abstraction to take other compositions.
2. dual path quintessence oil preparation method as claimed in claim 1 a kind of, it is characterised in that also comprise the steps of after described step 4): 5) extraction or the extract of subcritical abstraction, use the method for molecular distillation to continue to obtain remaining quintessence oil.
3. a kind of dual path quintessence oil preparation method as claimed in claim 1, it is characterised in that described being dried is dried for evacuation.
4. a kind of dual path quintessence oil preparation method as claimed in claim 1, it is characterised in that described dry employing continuous drying equipment.
5. a kind of dual path quintessence oil preparation method as claimed in claim 1, it is characterised in that described step 3) is the distillate stratification after cooling down, and obtains top quintessence oil.
6. a kind of dual path quintessence oil preparation method as claimed in claim 2, it is characterised in that also comprise the step mixed by the quintessence oil of step 3) and step 5).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510269366.3A CN106281693A (en) | 2015-05-25 | 2015-05-25 | A kind of dual path quintessence oil preparation method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510269366.3A CN106281693A (en) | 2015-05-25 | 2015-05-25 | A kind of dual path quintessence oil preparation method |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106281693A true CN106281693A (en) | 2017-01-04 |
Family
ID=57632803
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510269366.3A Pending CN106281693A (en) | 2015-05-25 | 2015-05-25 | A kind of dual path quintessence oil preparation method |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106281693A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108949351A (en) * | 2017-05-25 | 2018-12-07 | 无限极（中国）有限公司 | Fennel seeds extraction process of active component |
| RU2802439C1 (en) * | 2022-08-22 | 2023-08-28 | Владимир Викторович Михайлов | Device for processing essential oil raw materials |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101775337A (en) * | 2010-02-05 | 2010-07-14 | 四川日香桂农业科技开发有限公司 | Method for simultaneously preparing osmanthus essential oil, dry osmanthus product and osmanthus essential lotion |
| CN101851559A (en) * | 2010-06-11 | 2010-10-06 | 平阴县玫瑰研究所 | Method for extracting rose essential oil from rose dregs |
| CN103461556A (en) * | 2013-09-11 | 2013-12-25 | 济南惠农玫瑰花精油有限公司 | Production process for drying rosebuds at low temperature and recovering effective constituents and production equipment thereof |
| CN103766796A (en) * | 2014-01-02 | 2014-05-07 | 云南万兴隆生物科技集团有限公司 | Joint production process of dried ginger slices and fresh ginger bioactive water |
| CN104059779A (en) * | 2014-06-27 | 2014-09-24 | 融安县金宜林生物技术有限责任公司 | Sarcandra glabra vacuum-drying and volatile oil separating method |
-
2015
- 2015-05-25 CN CN201510269366.3A patent/CN106281693A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101775337A (en) * | 2010-02-05 | 2010-07-14 | 四川日香桂农业科技开发有限公司 | Method for simultaneously preparing osmanthus essential oil, dry osmanthus product and osmanthus essential lotion |
| CN101851559A (en) * | 2010-06-11 | 2010-10-06 | 平阴县玫瑰研究所 | Method for extracting rose essential oil from rose dregs |
| CN103461556A (en) * | 2013-09-11 | 2013-12-25 | 济南惠农玫瑰花精油有限公司 | Production process for drying rosebuds at low temperature and recovering effective constituents and production equipment thereof |
| CN103766796A (en) * | 2014-01-02 | 2014-05-07 | 云南万兴隆生物科技集团有限公司 | Joint production process of dried ginger slices and fresh ginger bioactive water |
| CN104059779A (en) * | 2014-06-27 | 2014-09-24 | 融安县金宜林生物技术有限责任公司 | Sarcandra glabra vacuum-drying and volatile oil separating method |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108949351A (en) * | 2017-05-25 | 2018-12-07 | 无限极（中国）有限公司 | Fennel seeds extraction process of active component |
| RU2802439C1 (en) * | 2022-08-22 | 2023-08-28 | Владимир Викторович Михайлов | Device for processing essential oil raw materials |
| RU2804951C1 (en) * | 2022-10-31 | 2023-10-09 | Владимир Викторович Михайлов | Method for distillation of plant raw materials |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US7857975B2 (en) | System for liquid extraction, and methods | |
| CN1524007A (en) | Method and device for extracting active substances and concentrating extracts from natural products | |
| CN104046514B (en) | A kind of Bulbus Allii quintessence oil extracting method | |
| CN105925377A (en) | Agilawood essential oil extraction process and agilawood essential oil extraction equipment | |
| CN105296163A (en) | Extraction equipment for fragrant plant essential oil and headspace volatile | |
| CN106350214B (en) | A kind of extracting method of cinnamon oil | |
| US8951593B2 (en) | Oilseed crushing heat recovery process | |
| CN104120036A (en) | Processing method of litsea cubeba oil | |
| KR101125132B1 (en) | Oil extraction device for leaves of the cypress | |
| CN106281693A (en) | A kind of dual path quintessence oil preparation method | |
| JP7068226B2 (en) | Extract manufacturing equipment | |
| WO2019113289A1 (en) | Extractor system that removes organic compounds from exhaust gas using feedstock being processed | |
| CN1356920A (en) | Solvent extraction process | |
| DE60013146T2 (en) | DEVICE AND METHOD FOR REMOVING SOLVENT RESIDUES | |
| Malekydozzadeh et al. | Application of multistage steam distillation column for extraction of essential oil of Rosemarinuse officinialis L | |
| US2377136A (en) | Extraction apparatus | |
| US20230242835A1 (en) | Oleaginous material extraction using alcohol solvent | |
| CN1384764A (en) | Apparatus and method for separating mixed liquids | |
| CN103394208A (en) | White spirit fragrance component separation method and device | |
| CN107903998A (en) | A kind of technique for processing extraction camphorated oil using yellow cinnamon leaf | |
| CA2562410A1 (en) | A method for extracting vegetable oils and a counterflow device for performing said method | |
| CN108383702A (en) | A method of extracting citronellal from fruit of a cubeb litsea tree hair oil | |
| US20130084375A1 (en) | Process for deodorizing edible oil | |
| JP6519895B1 (en) | Equipment for producing extract | |
| CN207734628U (en) | A kind of integral type distilling apparatus for obtaining different fractions |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20170104 |