CN106281604A - A kind of preparation method of Green Machining cooling lubricant - Google Patents
A kind of preparation method of Green Machining cooling lubricant Download PDFInfo
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- CN106281604A CN106281604A CN201610636468.9A CN201610636468A CN106281604A CN 106281604 A CN106281604 A CN 106281604A CN 201610636468 A CN201610636468 A CN 201610636468A CN 106281604 A CN106281604 A CN 106281604A
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- cooling lubricant
- white mice
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
- C10M169/04—Mixtures of base-materials and additives
- C10M169/045—Mixtures of base-materials and additives the additives being a mixture of compounds of unknown or incompletely defined constitution and non-macromolecular compounds
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/04—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions containing sulfur-to-oxygen bonds, i.e. sulfones, sulfoxides
- C10M2219/044—Sulfonic acids, Derivatives thereof, e.g. neutral salts
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/06—Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2040/00—Specified use or application for which the lubricating composition is intended
- C10N2040/20—Metal working
- C10N2040/22—Metal working with essential removal of material, e.g. cutting, grinding or drilling
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Lubricants (AREA)
Abstract
The invention discloses the preparation method of a kind of Green Machining cooling lubricant, belong to technical field of lubricant preparation.nullFirst the method takes white mice liver，It is ground into homogenate，Again will homogenate and second pond activated sludge mixed fermentation，Heated and hydrogen peroxide processes sterilization，Rotary-classify technology obtains the concentrated solution of rich in proteins and nucleic acid，Utilize nitrogen therein、Sulfur、The elements such as phosphorus，A stratification protecting film is formed at friction surface，Play a protective role，Again with Ilex latifolia tea-leaf as raw material，React with the stirring of Oleum Brassicae campestris constant temperature after mouldy，To improve Oleum Brassicae campestris oxidation resistance，After being performing centrifugal separation on，Green Machining cooling lubricant is obtained with Mouse Liver concentrated solution and surfactant sodium dodecyl base benzene sulfonic acid sodium salt ultrasonic vibration，The present invention is oil based on Oleum Brassicae campestris，White mice liver is EP agent，And other additives make Green Machining cooling lubricant，The use requirement of machining can be met，And to environment and human body without any harm，There is bigger market potential.
Description
Technical field
The invention discloses the preparation method of a kind of Green Machining cooling lubricant, belong to technical field of lubricant preparation.
Background technology
In metal cutting process, for improving stock-removing efficiency, improve the precision of workpiece and reduce workpiece surface roughness, extending cutter
Have service life, reach optimal economic effect, be necessary for reducing the friction between cutter and workpiece, cutter and chip, in time
The heat taking away cutting region endogenous cause of ill material deformation and produce.Reach these purposes, be on the one hand by the exploitation resistance to height of high rigidity
The cutter material of temperature and the geometry of improvement of cutter；On the other hand use the cutting lubricant of function admirable to improve cutting effect
Rate, reduces workpiece surface roughness, tool life, obtains good economic benefit.Metal cutting process selects
Good lubrication, cleaning and the effect such as antirust can be played with suitable metal cutting lubricant, thus it is resistance to improve cutter
Expenditure, it is ensured that crudy and machining accuracy, improves production efficiency.
Cooling for cut lubricant of good performance has good lubrication, cools down, cleans and rustless property, to improving cutting
Crudy and efficiency, minimizing tool wear etc. have remarkable result.Cooling for cut lubricant develops into today, in machining
Industry is widely used, usage amount very big, become huge number, industrial products covering extensive fields, achieve huge economic benefit.
But, along with being widely used of metal cutting cooling lubricant, it has been found that cooling for cut lubricant exists many
Harm, primarily to collect lubrication, cooling, the good characteristic such as anticorrosive, stable in one cooling for cut lubricant, causes greatly
Harmful additive of amount is frequently used, the material such as such as nitrite, formaldehyde, sulfur, chlorine, phosphorus, is good for the health of operator
Health and environment bring huge hidden danger.The safety of cooling for cut lubricant and the impact on environment have become cooling for cut lubrication
Agent develops the major issue that must take into.Therefore, exploitation environmental type product has become a kind of main trend.
Summary of the invention
The technical problem that present invention mainly solves: contain many virose additives for existing cooling for cut lubricant,
Human body and environment can be worked the mischief, and after use, cutting fluid is the most degradable, after discharge, easily environment be produced secondary pollution
Problem, it is provided that the preparation method of a kind of Green Machining cooling lubricant, first the method takes white mice liver, is ground into homogenate,
Again will homogenate and second pond activated sludge mixed fermentation, heated and hydrogen peroxide processes sterilization, rotary-classify technology obtain rich in
Protein and the concentrated solution of nucleic acid, utilize the elements such as nitrogen therein, sulfur, phosphorus, form a stratification protecting film at friction surface, rises
To protective effect, then with Ilex latifolia tea-leaf as raw material, mouldy rear and Oleum Brassicae campestris constant temperature stirring reaction, to improve Oleum Brassicae campestris antioxidation energy
Power, after being performing centrifugal separation on, obtains Green Machining with Mouse Liver concentrated solution and surfactant sodium dodecyl base benzene sulfonic acid sodium salt sonic oscillation
Cooling lubricant.The present invention is oil based on Oleum Brassicae campestris, and white mice liver concentrated solution is EP agent, and other additive systems
Become Green Machining cooling lubricant, the use requirement of various machining can be met, and to environment and human body non-hazardous, have
Bigger market potential.
In order to solve above-mentioned technical problem, the technical solution adopted in the present invention is:
(1) taking 2～4 births 3～the live body white mice of 5 months, artificial place after death takes liver and is washed with deionized 3～5 times,
Again white mice liver is proceeded in animal tissue's pulverizer, add 300～400mL normal saline, pulverize and obtain white mice liver homogenate；
(2) in sealing and fermenting tank, add 200～300mL above-mentioned gained white mice liver homogenate, add 10～20g second ponds and live
Property mud, after Glass rod stirring mixing 6～8min, stand sealing and fermenting 3～5 days, pour material in fermentation tank into burning subsequently
In Bei, then beaker is proceeded to digital display test the speed constant temperature blender with magnetic force, set speed of agitator to 360～420r/min, regulate water-bath
Temperature is to 75～80 DEG C, and under constant temperature stirring condition, adding 10～15mL mass concentrations is 10～12% hydrogen peroxide, continues constant temperature
Stirring reaction 15～20min；
(3) question response terminates, and material in beaker is proceeded to centrifuge, is centrifuged 20～30min with 3800～4000r/min rotating speeds,
Discarding lower sediment thing, obtain the supernatant, proceeded in Rotary Evaporators, at a temperature of 85～90 DEG C, concentrated by rotary evaporation is to former
The 1/3 of volume, obtains concentrated extracting solution, standby；
(4) weigh fresh Ilex latifolia tea-leaf 60～80g, put in plant tissue pulverizer and be ground into fragment, then by equal for Folium Camelliae sinensis fragment
Even be laid in Fructus Ananadis comosi sieve in, subsequently by Fructus Ananadis comosi sieve be placed in lucifuge ventilation, every 6～8h to Folium Camelliae sinensis surface sprinkling 6～8mL biogas
Liquid, stands 5～7 days so that it is the most mouldy；
(5) treat mouldy end, Folium Camelliae sinensis fragment is put in the beaker filling 30～40mL Oleum Brassicae campestriss, subsequently beaker is placed in digital display
Testing the speed in constant temperature blender with magnetic force, setting speed to 450～500r/min, regulation oil bath temperature is to 180～200 DEG C, and constant temperature stirs
Mix reaction 60～80min, treat that it naturally cools to room temperature, material in beaker is proceeded to centrifuge, turn with 2800～3200r/min
Speed centrifugal 10～15min, discards lower sediment thing, obtains mixed oil liquid；
(6) count by weight, beaker is sequentially added into 60～80 parts of standby concentrated extracting solutions of step (3), on 40～50 parts
State gained mixed oil liquid, 10～12 parts of dodecylbenzene sodium sulfonate, subsequently beaker proceeded in sonic oscillation instrument, with 25～
30kHz frequency ultrasound vibration 30～45min, obtains homogeneous latex emulsion, fill, obtains Green Machining cooling lubricant.
The application process of the present invention is: the Green Machining the cooling lubricant 100～300L present invention prepared with low-lift pump
Squeezing in pipeline, flow out from nozzle through valve, nozzle is arranged on close to cutting zone, and cooling for cut lubricant flows through cutting region
After then flow on the different parts of lathe, be then pooled in draw-off tray, then flow back to cutting fluid case from draw-off tray, circulation makes
With.After testing, use the Green Machining cooling lubricant for preparing of the present invention for machining 8～12 months, through field instrumentation
Tracing detection, does not measures harmful material, makes cutting tool service life than using original cooling profit simultaneously
Lubrication prescription improves 3～5 times, can meet every Cutting Process requirement, and the cooling for cut lubricant after use is through microbial treatments
Can be degradable in 3～5 weeks.
The invention has the beneficial effects as follows:
(1) present invention oil based on Oleum Brassicae campestris, white mice liver is EP agent, and other additives make green cooling
Lubricant, can meet the use requirement of machining, green, environmental protection, be safe from harm environment and human body；
(2) the green cooling lubricant of the present invention is applicable to the working condition requirement of various machining, lubricates superior with cooling performance,
Cutting force can be substantially reduced and take away heat in metal cutting, therefore can improve work efficiency and reduce cutter and the consumption of emery wheel；
(3) the green cooling lubricant low cost of the present invention, has higher cost performance, has bigger market potential.
Detailed description of the invention
First taking 2～4 births 3～the live body white mice of 5 months, artificial place after death takes liver and is washed with deionized 3
～5 times, then white mice liver is proceeded in animal tissue's pulverizer, add 300～400mL normal saline, pulverize and obtain white mice
Liver homogenate；In sealing and fermenting tank, add 200～300mL above-mentioned gained white mice liver homogenate subsequently, add 10～20g bis-and sink
Pond activated sludge, after Glass rod stirring mixing 6～8min, standing sealing and fermenting 3～5 days, subsequently material in fermentation tank is fallen
Enter in beaker, then beaker is proceeded to digital display test the speed constant temperature blender with magnetic force, set speed of agitator to 360～420r/min, regulation
Bath temperature is to 75～80 DEG C, and under constant temperature stirring condition, adding 10～15mL mass concentrations is 10～12% hydrogen peroxide, continues
Constant temperature stirring reaction 15～20min；Question response terminates, and material in beaker is proceeded to centrifuge, with 3800～4000r/min rotating speeds
Centrifugal 20～30min, discard lower sediment thing, obtain the supernatant, proceeded in Rotary Evaporators, in 85～90 DEG C of temperature
Under, the 1/3 of concentrated by rotary evaporation to original volume, obtain concentrated extracting solution, standby；Weigh fresh Ilex latifolia tea-leaf 60～80g again, put into plant
Tissue pulverizer is ground into fragment, then by evenly laid out for Folium Camelliae sinensis fragment in Fructus Ananadis comosi is sieved, subsequently Fructus Ananadis comosi sieve be placed in lucifuge and lead to
At wind, every 6～8h to Folium Camelliae sinensis surface sprinkling 6～8mL methane liquid, stand 5～7 days so that it is the most mouldy；Treat mouldy end,
Folium Camelliae sinensis fragment is put into and fills in the beaker of 30～40mL Oleum Brassicae campestriss, subsequently beaker is placed in digital display and tests the speed constant temperature blender with magnetic force
On, setting speed to 450～500r/min, regulation oil bath temperature is to 180～200 DEG C, and constant temperature stirring reacts 60～80min, treats
It naturally cools to room temperature, and material in beaker is proceeded to centrifuge, is centrifuged 10～15min with 2800～3200r/min rotating speeds, abandons
Sub-cloud precipitate, obtains mixed oil liquid；Finally count by weight, beaker is sequentially added into 60～80 parts of above-mentioned steps standby
Concentrated extracting solution, 40～50 parts of above-mentioned gained mixed oil liquids, 10～12 parts of dodecylbenzene sodium sulfonate, proceed to surpass by beaker subsequently
In sound oscillation instrument, with 25～30kHz frequency ultrasound vibrations 30～45min, obtain homogeneous latex emulsion, fill, obtain Green Machining cooling
Lubricant.
Example 1
First taking 2 births live body white mice of 3 months, artificial place after death takes liver and is washed with deionized 3 times, then by little Bai
Hepar Mus proceeds in animal tissue's pulverizer, adds 300mL normal saline, pulverizes and obtains white mice liver homogenate；Send out in sealing subsequently
Ferment tank adds 200mL above-mentioned gained white mice liver homogenate, adds 10g second pond activated sludge, with Glass rod stirring mixing
After 6min, stand sealing and fermenting 3 days, subsequently by during beaker poured into by material in fermentation tank, then beaker is proceeded to digital display test the speed constant temperature
Magnetic stirring apparatus, setting speed of agitator to 360r/min, regulation bath temperature is to 75 DEG C, under constant temperature stirring condition, adds
10mL mass concentration is 10% hydrogen peroxide, continues constant temperature stirring reaction 15min；Question response terminates, and proceeds to be centrifuged by material in beaker
Machine, is centrifuged 20min with 3800r/min rotating speed, discards lower sediment thing, obtains the supernatant, is proceeded in Rotary Evaporators, in
At a temperature of 85 DEG C, the 1/3 of concentrated by rotary evaporation to original volume, obtain concentrated extracting solution, standby；Weigh fresh Ilex latifolia tea-leaf 60g again, put into
Plant tissue pulverizer is ground into fragment, then by evenly laid out for Folium Camelliae sinensis fragment in Fructus Ananadis comosi is sieved, Fructus Ananadis comosi sieve be placed in keep away subsequently
Light ventilation, every 6h to Folium Camelliae sinensis surface sprinkling 6mL methane liquid, stands 5 days so that it is the most mouldy；Treat mouldy end, by Folium Camelliae sinensis
Fragment puts in the beaker filling 30mL Oleum Brassicae campestris, beaker is placed in digital display subsequently and tests the speed in constant temperature blender with magnetic force, sets and turns
Speed is to 450r/min, and regulation oil bath temperature is to 180 DEG C, and 60min is reacted in constant temperature stirring, treats that it naturally cools to room temperature, by beaker
Middle material proceeds to centrifuge, is centrifuged 10min with 2800r/min rotating speed, discards lower sediment thing, obtains mixed oil liquid；Finally by weight
Amount number meter, is sequentially added into 60 parts of standby concentrated extracting solutions of above-mentioned steps in beaker, 40 parts of above-mentioned gained mixed oil liquids, 10 parts
Dodecylbenzene sodium sulfonate, proceeds to beaker in sonic oscillation instrument subsequently, with 25kHz frequency ultrasound vibration 30min, obtains uniformly breast
Liquid, fill, obtain Green Machining cooling lubricant.
This example operation is easy, and the Green Machining cooling lubricant with low-lift pump, the 100L present invention prepared during use is squeezed into
In pipeline, flowing out from nozzle through valve, nozzle is arranged on close to cutting zone, and cooling for cut lubricant flows through behind cutting region again
Flow to, on the different parts of lathe, then be pooled in draw-off tray, then flow back to cutting fluid case from draw-off tray, recycle.Warp
Detection, use the Green Machining cooling lubricant for preparing of the present invention for machining 8 months, through field instrumentation tracing detection,
Do not measure harmful material, make cutting tool improve than the original cooling lubricant of use service life simultaneously
3 times, can meet every Cutting Process requirement, the cooling for cut lubricant after use can be the most complete through microbial treatments
Degraded.
Example 2
First taking 3 births live body white mice of 4 months, artificial place after death takes liver and is washed with deionized 4 times, then by little Bai
Hepar Mus proceeds in animal tissue's pulverizer, adds 350mL normal saline, pulverizes and obtains white mice liver homogenate；Send out in sealing subsequently
Ferment tank adds 250mL above-mentioned gained white mice liver homogenate, adds 15g second pond activated sludge, with Glass rod stirring mixing
After 7min, stand sealing and fermenting 4 days, subsequently by during beaker poured into by material in fermentation tank, then beaker is proceeded to digital display test the speed constant temperature
Magnetic stirring apparatus, setting speed of agitator to 390r/min, regulation bath temperature is to 78 DEG C, under constant temperature stirring condition, adds
13mL mass concentration is 11% hydrogen peroxide, continues constant temperature stirring reaction 18min；Question response terminates, and proceeds to be centrifuged by material in beaker
Machine, is centrifuged 25min with 3900r/min rotating speed, discards lower sediment thing, obtains the supernatant, is proceeded in Rotary Evaporators, in
At a temperature of 88 DEG C, the 1/3 of concentrated by rotary evaporation to original volume, obtain concentrated extracting solution, standby；Weigh fresh Ilex latifolia tea-leaf 70g again, put into
Plant tissue pulverizer is ground into fragment, then by evenly laid out for Folium Camelliae sinensis fragment in Fructus Ananadis comosi is sieved, Fructus Ananadis comosi sieve be placed in keep away subsequently
Light ventilation, every 7h to Folium Camelliae sinensis surface sprinkling 7mL methane liquid, stands 6 days so that it is the most mouldy；Treat mouldy end, by Folium Camelliae sinensis
Fragment puts in the beaker filling 35mL Oleum Brassicae campestris, beaker is placed in digital display subsequently and tests the speed in constant temperature blender with magnetic force, sets and turns
Speed is to 475r/min, and regulation oil bath temperature is to 190 DEG C, and 70min is reacted in constant temperature stirring, treats that it naturally cools to room temperature, by beaker
Middle material proceeds to centrifuge, is centrifuged 13min with 3000r/min rotating speed, discards lower sediment thing, obtains mixed oil liquid；Finally by weight
Amount number meter, is sequentially added into 70 parts of standby concentrated extracting solutions of above-mentioned steps in beaker, 45 parts of above-mentioned gained mixed oil liquids, 11 parts
Dodecylbenzene sodium sulfonate, proceeds to beaker in sonic oscillation instrument subsequently, with 28kHz frequency ultrasound vibration 38min, obtains uniformly breast
Liquid, fill, obtain Green Machining cooling lubricant.
This example operation is easy, and the Green Machining cooling lubricant with low-lift pump, the 200L present invention prepared during use is squeezed into
In pipeline, flowing out from nozzle through valve, nozzle is arranged on close to cutting zone, and cooling for cut lubricant flows through behind cutting region again
Flow to, on the different parts of lathe, then be pooled in draw-off tray, then flow back to cutting fluid case from draw-off tray, recycle.Warp
Detection, use the Green Machining cooling lubricant for preparing of the present invention for machining 10 months, through field instrumentation tracing detection,
Do not measure harmful material, make cutting tool improve than the original cooling lubricant of use service life simultaneously
4 times, can meet every Cutting Process requirement, the cooling for cut lubricant after use can be the most complete through microbial treatments
Degraded.
Example 3
First taking 4 births live body white mice of 5 months, artificial place after death takes liver and is washed with deionized 5 times, then by little Bai
Hepar Mus proceeds in animal tissue's pulverizer, adds 400mL normal saline, pulverizes and obtains white mice liver homogenate；Send out in sealing subsequently
Ferment tank adds 300mL above-mentioned gained white mice liver homogenate, adds 20g second pond activated sludge, with Glass rod stirring mixing
After 8min, stand sealing and fermenting 5 days, subsequently by during beaker poured into by material in fermentation tank, then beaker is proceeded to digital display test the speed constant temperature
Magnetic stirring apparatus, setting speed of agitator to 420r/min, regulation bath temperature is to 80 DEG C, under constant temperature stirring condition, adds
15mL mass concentration is 12% hydrogen peroxide, continues constant temperature stirring reaction 20min；Question response terminates, and proceeds to be centrifuged by material in beaker
Machine, is centrifuged 30min with 3800～4000r/min rotating speeds, discards lower sediment thing, obtain the supernatant, proceeded to rotary evaporation
In instrument, at a temperature of 90 DEG C, the 1/3 of concentrated by rotary evaporation to original volume, obtain concentrated extracting solution, standby；Weigh fresh Ilex latifolia tea-leaf again
80g, puts into and is ground into fragment in plant tissue pulverizer, then by evenly laid out for Folium Camelliae sinensis fragment in Fructus Ananadis comosi is sieved, subsequently by Fructus Ananadis comosi
Sieve is placed in lucifuge ventilation, every 8h to Folium Camelliae sinensis surface sprinkling 8mL methane liquid, stands 7 days so that it is the most mouldy；Treat mouldy knot
Bundle, puts into Folium Camelliae sinensis fragment and fills in the beaker of 40mL Oleum Brassicae campestris, beaker is placed in digital display subsequently and tests the speed constant temperature blender with magnetic force
On, setting speed to 500r/min, regulation oil bath temperature is to 200 DEG C, and 80min is reacted in constant temperature stirring, treats that it naturally cools to room
Temperature, proceeds to centrifuge by material in beaker, is centrifuged 15min with 3200r/min rotating speed, discards lower sediment thing, obtains mixed oil liquid；
Finally count by weight, beaker is sequentially added into 80 parts of standby concentrated extracting solutions of above-mentioned steps, 50 parts of above-mentioned gained mixing
Fluid, 12 parts of dodecylbenzene sodium sulfonate, subsequently beaker is proceeded in sonic oscillation instrument, vibrate with 30kHz frequency ultrasound
45min, obtains homogeneous latex emulsion, fill, obtains Green Machining cooling lubricant.
This example operation is easy, and the Green Machining cooling lubricant with low-lift pump, the 300L present invention prepared during use is squeezed into
In pipeline, flowing out from nozzle through valve, nozzle is arranged on close to cutting zone, and cooling for cut lubricant flows through behind cutting region again
Flow to, on the different parts of lathe, then be pooled in draw-off tray, then flow back to cutting fluid case from draw-off tray, recycle.Warp
Detection, use the Green Machining cooling lubricant for preparing of the present invention for machining 12 months, through field instrumentation tracing detection,
Do not measure harmful material, make cutting tool improve than the original cooling lubricant of use service life simultaneously
5 times, can meet every Cutting Process requirement, the cooling for cut lubricant after use can be the most complete through microbial treatments
Degraded.
Claims (1)
1. the preparation method of a Green Machining cooling lubricant, it is characterised in that concrete preparation process is:
(1) taking 2～4 births 3～the live body white mice of 5 months, artificial place after death takes liver and is washed with deionized 3～5 times,
Again white mice liver is proceeded in animal tissue's pulverizer, add 300～400mL normal saline, pulverize and obtain white mice liver homogenate；
(2) in sealing and fermenting tank, add 200～300mL above-mentioned gained white mice liver homogenate, add 10～20g second ponds and live
Property mud, after Glass rod stirring mixing 6～8min, stand sealing and fermenting 3～5 days, pour material in fermentation tank into burning subsequently
In Bei, then beaker is proceeded to digital display test the speed constant temperature blender with magnetic force, set speed of agitator to 360～420r/min, regulate water-bath
Temperature is to 75～80 DEG C, and under constant temperature stirring condition, adding 10～15mL mass concentrations is 10～12% hydrogen peroxide, continues constant temperature
Stirring reaction 15～20min；
(3) question response terminates, and material in beaker is proceeded to centrifuge, is centrifuged 20～30min with 3800～4000r/min rotating speeds,
Discarding lower sediment thing, obtain the supernatant, proceeded in Rotary Evaporators, at a temperature of 85～90 DEG C, concentrated by rotary evaporation is to former
The 1/3 of volume, obtains concentrated extracting solution, standby；
(4) weigh fresh Ilex latifolia tea-leaf 60～80g, put in plant tissue pulverizer and be ground into fragment, then by equal for Folium Camelliae sinensis fragment
Even be laid in Fructus Ananadis comosi sieve in, subsequently by Fructus Ananadis comosi sieve be placed in lucifuge ventilation, every 6～8h to Folium Camelliae sinensis surface sprinkling 6～8mL biogas
Liquid, stands 5～7 days so that it is the most mouldy；
(5) treat mouldy end, Folium Camelliae sinensis fragment is put in the beaker filling 30～40mL Oleum Brassicae campestriss, subsequently beaker is placed in digital display
Testing the speed in constant temperature blender with magnetic force, setting speed to 450～500r/min, regulation oil bath temperature is to 180～200 DEG C, and constant temperature stirs
Mix reaction 60～80min, treat that it naturally cools to room temperature, material in beaker is proceeded to centrifuge, turn with 2800～3200r/min
Speed centrifugal 10～15min, discards lower sediment thing, obtains mixed oil liquid；
(6) count by weight, beaker is sequentially added into 60～80 parts of standby concentrated extracting solutions of step (3), on 40～50 parts
State gained mixed oil liquid, 10～12 parts of dodecylbenzene sodium sulfonate, subsequently beaker proceeded in sonic oscillation instrument, with 25～
30kHz frequency ultrasound vibration 30～45min, obtains homogeneous latex emulsion, fill, obtains Green Machining cooling lubricant.
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Citations (4)
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| WO2008096875A1 (en) * | 2007-02-09 | 2008-08-14 | Fujifilm Corporation | Lubricant composition, and mechanical element |
| JP2010215898A (en) * | 2009-02-17 | 2010-09-30 | Nippon Synthetic Chem Ind Co Ltd:The | Synthetic lubricant |
| CN104804836A (en) * | 2015-04-29 | 2015-07-29 | 青岛千帆高新技术有限公司 | Lubricating type stainless steel cutting liquid |
| CN105296117A (en) * | 2015-11-26 | 2016-02-03 | 上海帕卡兴产化工有限公司 | Environment-friendly low-odor rolling oil and preparation method thereof |
-
2016
- 2016-08-05 CN CN201610636468.9A patent/CN106281604B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2008096875A1 (en) * | 2007-02-09 | 2008-08-14 | Fujifilm Corporation | Lubricant composition, and mechanical element |
| JP2010215898A (en) * | 2009-02-17 | 2010-09-30 | Nippon Synthetic Chem Ind Co Ltd:The | Synthetic lubricant |
| CN104804836A (en) * | 2015-04-29 | 2015-07-29 | 青岛千帆高新技术有限公司 | Lubricating type stainless steel cutting liquid |
| CN105296117A (en) * | 2015-11-26 | 2016-02-03 | 上海帕卡兴产化工有限公司 | Environment-friendly low-odor rolling oil and preparation method thereof |
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|---|---|
| CN106281604B (en) | 2019-02-12 |
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Effective date of registration: 20210416 Address after: 214000 plot B28, phase VI, Shuofang industrial concentration zone, Wuxi New District, Jiangsu Province Patentee after: Jiangsu Langsi Automobile Products Co.,Ltd. Address before: 212000 No.6, Shengdan Road, Dantu District, Zhenjiang City, Jiangsu Province Patentee before: Zhou Baiqin |
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