CN106280790A - A kind of low-poison and combustion-resisting type room temperature solvent gage mark coating and preparation method thereof - Google Patents
A kind of low-poison and combustion-resisting type room temperature solvent gage mark coating and preparation method thereof Download PDFInfo
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- CN106280790A CN106280790A CN201610645816.9A CN201610645816A CN106280790A CN 106280790 A CN106280790 A CN 106280790A CN 201610645816 A CN201610645816 A CN 201610645816A CN 106280790 A CN106280790 A CN 106280790A
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- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
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- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
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- C08K3/26—Carbonates; Bicarbonates
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- C08K5/00—Use of organic ingredients
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- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
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- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
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- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
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Abstract
The open a kind of low-poison and combustion-resisting type room temperature solvent gage mark coating of the present invention, the primary raw material weight portion preparing described gage mark coating consists of: hard resin 190 275 parts, pigment 25 150 parts, filler 225 500 parts and auxiliary agent 27.5 39 parts, and dimethyl carbonate and/or 210 425 parts of aromatic hydrocarbon, 10 20 parts of acetone and butyl acetate 10 20 parts;Chlorohydrocarbon 100 250 parts and rudimentary saturated monohydroxy alcohol 16 27 parts.The low-poison and combustion-resisting type room temperature solvent gage mark coating that the present invention provides, this formulation for coating material is scientific and reasonable, and each component works in coordination with compatibility, and while improving product excellent properties, solvent selects toxicity to be substantially reduced than prior art, gage mark coating more safety and environmental protection;The characteristic of existing coating detonation is improved as flammable by the gage mark coating of the present invention, has good flame retardant effect;This production technology solves the danger that room temperature solvent gage mark coating is inflammable, explosive, decreases the harm of toxic solvent, can effectively protect production, transport, workmen and contact the life security of this product related personnel.
Description
Technical field
The invention belongs to technical field of coatings, particularly relate to a kind of low-poison and combustion-resisting type room temperature solvent gage mark coating and preparation thereof
Method.
Background technology
Road mark paint is applied on road, for indicating the coating of roadmarking.Road mark paint is a kind of
Safety label, is the one " language " in highway communication.Roadmarking is the important component part of means of transportation.Distinct complete
Roadmarking can give drivers and pedestrians with good trained reflex, can effectively minimizing accident and improve driving efficiency.
The road mark paint that China uses has heat molten type, two-component type, aqueous and room temperature solvent-borne type four class.Normal temperature type road
Mark coating is the traditional product of China's marking paint, the advantage few with its easy construction, one-time investment and by the green grass or young crops of user
Look at.But existing room temperature solvent-borne type gage mark coating produces the solvent used and is inflammable and explosive hazardous chemical, is producing
Following great risk is there is during journey, transportation and use;
Production process: needing to open sand mill in process of production and be ground, abrasive media rotates with material high-speed
Forming bigger collision, friction with mechanical bucket wall, feeding engine slightly fault will produce a large amount of gas when causing cut-off material simultaneously,
When not having material to block air, abrasive media collision bucket wall is easy for producing spark, will occur quick-fried as long as producing spark material
Combustion, even if delivery pump does not has fault, it is also possible to there is other fault, such as: transmission line of electricity short circuit, loose contact also can cause fire
Flower, when spark runs into certain density solvent flashing will detonation, operator's life security is constituted great threat;
Transportation: room temperature coatings volatile organic compounds belongs to inflammable and explosive hazardous chemical, needs specialty HAZMAT vehicle transport, fortune
Defeated cost is high, and not in time, small lot user cannot connect goods on time in transport;
Use process: road construction environment is more complicated, the construction of limit, a lot of building site is just open to traffic, the Vehicular exhaust of normal transport
Pipe does not has flash hider, and the spark that once coatings volatile organic compounds gushes out with offgas duct contacts and detonation will occur, the machinery of normal construction
Fault, the error of operator all can cause fire, serious threat workmen and the life security of periphery personnel.
In order to make up the deficiency of existing prescription, inventor has carried out substantial amounts of experimentation, finally determines the present invention.
Summary of the invention
For above-mentioned problems of the prior art and defect, it is an object of the invention to provide a kind of low-poison and combustion-resisting type normal
Temperature solvent gage mark coating.
It is a further object of the present invention to provide the preparation method of above-mentioned low-poison and combustion-resisting type room temperature solvent gage mark coating.
The present invention provides a kind of low-poison and combustion-resisting type room temperature solvent gage mark coating, prepares the primary raw material weight of described gage mark coating
Amount part consists of: hard resin 190-275 part, pigment 25-150 part, filler 225-500 part and auxiliary agent 27.5-39 part, and
Including A, the solvent of B two-component, wherein,
Component A formula by weight is: dimethyl carbonate and/or aromatic hydrocarbon 210-425 part, acetone 10-20 part and second
Acid butyl ester 10-20 part;
B component formula by weight is: chlorohydrocarbon 100-250 part and rudimentary saturated monohydroxy alcohol 16-27 part.
Preferably, described hard resin is solid propenoic acid resin, solids modified acrylic's resin or Solid Modified poly-ammonia
One or more mixture of ester resin.
Preferably, described aromatic hydrocarbon is dimethylbenzene and/or ethylbenzene, and described chlorohydrocarbon is dichloromethane, 1,1,1-tri-chloroethene
One or more mixture of alkane or tetrachloroethylene.
Preferably, described rudimentary saturated monohydroxy alcohol is one or more mixed of the tert-butyl alcohol, n-butyl alcohol or isopropanol
Compound.
Preferably, described filler includes the raw material of following weight portion: Paris white 100-175 part, barium sulfate 100-175
Part, Pulvis Talci 25-150 part.
Preferably, described auxiliary agent includes the raw material of following weight portion: DOP and/or DBP plasticizer 25-30 part, levelling moistening
Dispersant 2-6 part, defoamer 0.5-3 part.
Preferably, described pigment is titanium dioxide, organic yellow, chrome yellow, chrome vermillion, permanent bordeaux, white carbon black, iron oxide red, phthalocyanine blue or phthalein
One or more mixture of dark green premetallized dye.
Further, the present invention provides the preparation method of a kind of low-poison and combustion-resisting type room temperature solvent gage mark coating, described method
Comprise the steps:
1) by weight the solvent of B component is squeezed into reactor, after stirring 15 minutes, by weight by the solvent of component A
Squeeze into reactor, add above-mentioned parts by weight solids resin, make reactor rotating speed be 300-800 rev/min, make hard resin the most molten
Solve;
2) in step 1) in the slurry prepared, under the temperature conditions less than 45 DEG C, under the rotating speed of 600-2000 rev/min
Add the pigment of above-mentioned parts by weight, filler and auxiliary agent to stir 30-40 minute so that it is be uniformly dispersed;
3) in step 2) by material dispersion uniformly after by the way of delivery pump or Scattered Kettle pressurization average rate material is inputted
Grinder, in process of lapping, grinder chuck remains that cooling system opens the state of cooling, controls temperature for being less than
35 DEG C, treat that material is ground to less than 15 microns and starts finished product packing after filtering.
Further, the present invention provides a kind of low-poison and combustion-resisting type room temperature solvent gage mark coating, by described solid propenoic acid tree
Fat, acrylic resin modified or modified polyurethane resin replace with liquid acrylic, acrylic resin modified or modified poly-
Urethane resin, described liquid acrylic, acrylic resin modified or modified polyurethane resin are 316-458 part, and it contains admittedly
Amount is 30%-75%, and described solvent is reduced to 194-513 part.
Preferably, described liquid acrylic, acrylic resin modified or modified polyurethane resin solid content are
60%.
The weight of composition described above raw material is using weight portion as proportioning, can proportionally increase when producing or reduce, as
Large-scale production can by kilogram in units of, or in units of ton, small-scale production can also by gram or milligram in units of, weight
Can increase or reduce, but the constant rate of the weight proportion between each composition.And the ratio of above weight proportion be through
Science screening obtains, and can adjust the proportioning of the amount of composition accordingly, be increased or decreased less than 100%, and effect is constant.
Beneficial effect: the low-poison and combustion-resisting type room temperature solvent gage mark coating that the present invention provides, this formulation for coating material is scientific and reasonable, respectively
Component works in coordination with compatibility, and effect is as follows:
1) the wear-resisting antiskid when gage mark coating of the present invention makes to use by the synergism between component, good springiness, phase
Capacitive is obviously improved, and presents excellent advection, and the plasticising performance of coating is more stable, and the gage mark coating of the present invention is attached
Putting forth effort strong, impact resistance excellence, the coating of the present invention and road surface adhesion are higher by more than 60% than conventional hot melt coating, not only may be used
Erosion with natural weathers such as opposing sleet hardships, hails, it is also possible to the physics of opposing rubble, greasy dirt etc. and chemical depletion;
2) material choice of the gage mark coating of the present invention is while improving product excellent properties, and solvent selects toxicity ratio existing
Technology is had to be substantially reduced, gage mark coating more safety and environmental protection;
3) characteristic of existing coating detonation is improved as flammable by the gage mark coating of the present invention, has good fire-retardant effect
Really,
Production process: have changed into nonflammable solvent, i.e. during the mixing of flame-retardant normal-temperature solvent gage mark coating production solvent
Just directly contacting with naked light, solvent also will not occur detonation, and the spark that in production process, mechanical accident causes more will not ignition substance
Material;
Transportation: flame-retardant normal-temperature solvent gage mark coating need not specialty hazardous materials transportation vehicle, reduces cost of transportation
While the most safe and convenient, fast can arrive construction site;
Work progress: flame-retardant normal-temperature solvent gage mark coating contacts fragmentary spark will not occur detonation, even if cigarette end is lost
Enter paint can and detonation also will not occur.
This production technology solves the danger that room temperature solvent gage mark coating is inflammable, explosive, it is to avoid produces, transport, construct
During detonation hidden danger, decrease the harm of toxic solvent, can effectively protect production, transport, workmen and contact this product
The life security of product related personnel, reduces the pollution to environment.
Detailed description of the invention
Below in conjunction with specific embodiment further describe the present invention, advantages of the present invention and feature will be with describe and
Apparent.It should be understood that described embodiment is only exemplary, the scope of the present invention is not constituted any restriction.This area
Skilled artisans appreciated that, lower without departing from the spirit and scope of the present invention can to the details of technical solution of the present invention and
Form is modified or replaces, but these amendments or replacement each fall within protection scope of the present invention.
It is a further object of the present invention to provide the preparation method of above-mentioned low-poison and combustion-resisting type room temperature solvent gage mark coating.
The present invention provides a kind of low-poison and combustion-resisting type room temperature solvent gage mark coating, prepares the primary raw material weight of described gage mark coating
Amount part consists of: hard resin 190-275 part, pigment 25-150 part, filler 225-500 part and auxiliary agent 27.5-39 part, and
Including A, the solvent of B two-component, wherein,
Component A formula by weight is: dimethyl carbonate and/or aromatic hydrocarbon 210-425 part, acetone 10-20 part and second
Acid butyl ester 10-20 part;
B component formula by weight is: chlorohydrocarbon 100-250 part and rudimentary saturated monohydroxy alcohol 16-27 part.
Preferably, described hard resin is solid propenoic acid resin, solids modified acrylic's resin or Solid Modified poly-ammonia
One or more mixture of ester resin.
Preferably, described aromatic hydrocarbon is dimethylbenzene and/or ethylbenzene, and described chlorohydrocarbon is dichloromethane, 1,1,1-tri-chloroethene
One or more mixture of alkane or tetrachloroethylene.Dimethyl carbonate and/or aromatic hydrocarbon 210-425 part, described fragrance
Hydrocarbon is dimethylbenzene and/or ethylbenzene, i.e. refer to can be any one weight portion of dimethyl carbonate, dimethylbenzene or ethylbenzene be 210-
425 parts, it is also possible to be any two weight portion be 210-425 part, it is also possible to three kinds of total weight portions are 210-425 part.
Preferably, described rudimentary saturated monohydroxy alcohol is one or more mixed of the tert-butyl alcohol, n-butyl alcohol or isopropanol
Compound.It refers to that the weight portion of rudimentary saturated monohydroxy alcohol, in the range of 16-27 part, can be the tert-butyl alcohol, n-butyl alcohol or isopropanol
Any one weight portion be 16-27 part, it is also possible to be any two weight portion be 16-27 part, it is also possible to three kinds of total weight portions
For 16-27 part.
Concrete, existing solvent toxicity data:
Dimethylbenzene (low toxicity) workshop safe level 100mg/m3;
Dimethyl carbonate (micro-poison) workshop safe level is without mg/m3;
Ethylbenzene: (low toxicity) workshop safe level 868mg/m3;
Butyl acetate (low toxicity) workshop safe level 300mg/m3;
Acetone (low toxicity) low toxicity workshop safe level 360mg/;
Dichloromethane (low toxicity) workshop safe level 1740mg/m3;
1.1.1 trichloroethane (low toxicity) workshop safe level 1100-1900mg/m3;
Tetrachloroethylene (low toxicity) workshop safe level 335-670mg/m3;
N-butyl alcohol (low toxicity) workshop safe level 200mg/m3;
The tert-butyl alcohol (low toxicity) workshop safe level 300mg/m3;
Isopropanol (low toxicity) low toxicity workshop safe level 1020mg/m3。
The present inventor is through lot of experiments, it is ensured that the material choice of gage mark coating is improving product excellent properties
Meanwhile, solvent selects toxicity to be substantially reduced than prior art, gage mark coating more safety and environmental protection;
Preferably, described filler includes the raw material of following weight portion: Paris white 100-175 part, barium sulfate 100-175
Part, Pulvis Talci 25-150 part.
Preferably, described auxiliary agent includes the raw material of following weight portion: DOP and/or DBP plasticizer 25-30 part, levelling moistening
Dispersant 2-6 part, defoamer 0.5-3 part.
Preferably, described pigment is titanium dioxide, organic yellow, chrome yellow, chrome vermillion, permanent bordeaux, white carbon black, iron oxide red, phthalocyanine blue or phthalein
One or more mixture of dark green premetallized dye.
Further, the present invention provides the preparation method of a kind of low-poison and combustion-resisting type room temperature solvent gage mark coating, described method
Comprise the steps:
1) by weight the solvent of B component is squeezed into reactor, after stirring 15 minutes, by weight by the solvent of component A
Squeeze into reactor, add above-mentioned parts by weight solids resin, make reactor rotating speed be 300-800 rev/min, make hard resin the most molten
Solve;
2) in step 1) in the slurry prepared, under the temperature conditions less than 45 DEG C, under the rotating speed of 600-2000 rev/min
Add the pigment of above-mentioned parts by weight, filler and auxiliary agent to stir 30-40 minute so that it is be uniformly dispersed;
3) in step 2) by material dispersion uniformly after by the way of delivery pump or Scattered Kettle pressurization average rate material is inputted
Grinder, in process of lapping, grinder chuck remains that cooling system opens the state of cooling, controls temperature for being less than
35 DEG C, treat that material is ground to less than 15 microns and starts finished product packing after filtering.
Further, the present invention provides a kind of low-poison and combustion-resisting type room temperature solvent gage mark coating, by described solid propenoic acid tree
Fat, acrylic resin modified or modified polyurethane resin replace with liquid acrylic, acrylic resin modified or modified poly-
Urethane resin, described liquid acrylic, acrylic resin modified or modified polyurethane resin are 316-458 part, and it contains admittedly
Amount is 30%-75%, and described solvent is reduced to 194-513 part.
Preferably, described liquid acrylic, acrylic resin modified or modified polyurethane resin solid content are
60%.
Below in conjunction with embodiment, the present invention is described in further details.
Embodiment 1
The low-poison and combustion-resisting type room temperature solvent gage mark coating of the present embodiment, in terms of parts by weight, primary raw material consists of: preparation
The primary raw material weight portion of described gage mark coating consists of: solid propenoic acid resin 190 parts, pigment 25 parts, Paris white 100
Part, 100 parts of barium sulfate, Pulvis Talci 25 parts, DOP and/or DBP plasticizer 25 parts, levelling wetting dispersing agent 2 parts, defoamer 0.5
Part, and
Including A, the solvent of B two-component, wherein,
Component A formula by weight is: dimethyl carbonate 210 parts, 10 parts of acetone and butyl acetate 10 parts;
B component formula by weight is: dichloromethane 100 parts and the tert-butyl alcohol 16 parts.
It should be noted that described pigment is titanium dioxide, organic yellow, chrome yellow, chrome vermillion, permanent bordeaux, white carbon black, iron oxide red, phthalein green grass or young crops
Indigo plant or one or more mixture of phthalein viridescent premetallized dye.
The present embodiment provides the preparation method of a kind of low-poison and combustion-resisting type room temperature solvent gage mark coating, and described method includes as follows
Step:
1) by weight the solvent of B component is squeezed into reactor, after stirring 15 minutes, by weight by the solvent of component A
Squeeze into reactor, add above-mentioned parts by weight solids resin, make reactor rotating speed be 300-800 rev/min, make hard resin the most molten
Solve;
2) in step 1) in the slurry prepared, under the temperature conditions less than 45 DEG C, under the rotating speed of 600-2000 rev/min
Add the pigment of above-mentioned parts by weight, filler and auxiliary agent to stir 30-40 minute so that it is be uniformly dispersed;
3) in step 2) by material dispersion uniformly after by the way of delivery pump or Scattered Kettle pressurization average rate material is inputted
Grinder, in process of lapping, grinder chuck remains that cooling system opens the state of cooling, controls temperature for being less than
35 DEG C, pack after starting finished product packing mix homogeneously after material is ground to below 15 microns.
Embodiment 2
The low-poison and combustion-resisting type room temperature solvent gage mark coating of the present embodiment, in terms of parts by weight, primary raw material consists of: preparation
The primary raw material weight portion of described gage mark coating consists of: solid propenoic acid resin 275 parts, pigment 150 parts, Paris white 175
Part, 175 parts of barium sulfate, Pulvis Talci 150 parts, DOP and/or DBP plasticizer 30 parts, levelling wetting dispersing agent 6 parts, defoamer 3 parts,
And
Including A, the solvent of B two-component, wherein,
Component A formula by weight is: dimethyl carbonate 425 parts, 20 parts of acetone and butyl acetate 20 parts;
B component formula by weight is: dichloromethane 250 parts and the tert-butyl alcohol 27 parts.
It should be noted that described pigment is titanium dioxide, organic yellow, chrome yellow, chrome vermillion, permanent bordeaux, white carbon black, iron oxide red, phthalein green grass or young crops
Indigo plant or one or more mixture of phthalein viridescent premetallized dye.
The preparation method of the present embodiment low-poison and combustion-resisting type room temperature solvent gage mark coating is same as in Example 1.
Embodiment 3
The low-poison and combustion-resisting type room temperature solvent gage mark coating of the present embodiment, in terms of parts by weight, primary raw material consists of: preparation
The primary raw material weight portion of described gage mark coating consists of: solid propenoic acid resin 220 parts, pigment 100 parts, Paris white 130
Part, 130 parts of barium sulfate, Pulvis Talci 70 parts, DOP and/or DBP plasticizer 27 parts, levelling wetting dispersing agent 4 parts, defoamer 2 parts,
And
Including A, the solvent of B two-component, wherein,
Component A formula by weight is: dimethyl carbonate 310 parts, 15 parts of acetone and butyl acetate 15 parts;
B component formula by weight is: dichloromethane 200 parts and the tert-butyl alcohol 20 parts.
It should be noted that described pigment is titanium dioxide, organic yellow, chrome yellow, chrome vermillion, permanent bordeaux, white carbon black, iron oxide red, phthalein green grass or young crops
Indigo plant or one or more mixture of phthalein viridescent premetallized dye.
The preparation method of the present embodiment low-poison and combustion-resisting type room temperature solvent gage mark coating is same as in Example 1.
Embodiment 4
The low-poison and combustion-resisting type room temperature solvent gage mark coating of the present embodiment, in terms of parts by weight, primary raw material consists of: preparation
The primary raw material weight portion of described gage mark coating consists of: solid propenoic acid resin 190 parts, pigment 25 parts, Paris white 100
Part, 100 parts of barium sulfate, Pulvis Talci 25 parts, DOP and/or DBP plasticizer 25 parts, levelling wetting dispersing agent 2 parts, defoamer 0.5
Part, and
Including A, the solvent of B two-component, wherein,
Component A formula by weight is: dimethylbenzene 210 parts, 10 parts of acetone and butyl acetate 10 parts;
B component formula by weight is: 1,1,1-trichloroethane 100 parts and isopropanol 16 parts.
It should be noted that described pigment is titanium dioxide, organic yellow, chrome yellow, chrome vermillion, permanent bordeaux, white carbon black, iron oxide red, phthalein green grass or young crops
Indigo plant or one or more mixture of phthalein viridescent premetallized dye.
The preparation method of the present embodiment low-poison and combustion-resisting type room temperature solvent gage mark coating is same as in Example 1.
Embodiment 5
The low-poison and combustion-resisting type room temperature solvent gage mark coating of the present embodiment, in terms of parts by weight, primary raw material consists of: preparation
The primary raw material weight portion of described gage mark coating consists of: solids modified acrylic's resin 275 parts, pigment 150 parts, Paris white
175 parts, 175 parts of barium sulfate, Pulvis Talci 150 parts, DOP and/or DBP plasticizer 30 parts, levelling wetting dispersing agent 6 parts, defoamer 3
Part, and
Including A, the solvent of B two-component, wherein,
Component A formula by weight is: dimethylbenzene 425 parts, 20 parts of acetone and butyl acetate 20 parts;
B component formula by weight is: 1,1,1-trichloroethane 250 parts and isopropanol 27 parts.
It should be noted that described pigment is titanium dioxide, organic yellow, chrome yellow, chrome vermillion, permanent bordeaux, white carbon black, iron oxide red, phthalein green grass or young crops
Indigo plant or one or more mixture of phthalein viridescent premetallized dye.
The preparation method of the present embodiment low-poison and combustion-resisting type room temperature solvent gage mark coating is same as in Example 1.
Embodiment 6
The low-poison and combustion-resisting type room temperature solvent gage mark coating of the present embodiment, in terms of parts by weight, primary raw material consists of: preparation
The primary raw material weight portion of described gage mark coating consists of: solids modified acrylic's resin 235 parts, pigment 90 parts, Paris white
130 parts, 130 parts of barium sulfate, Pulvis Talci 90 parts, DOP and/or DBP plasticizer 28 parts, levelling wetting dispersing agent 3 parts, defoamer 2
Part, and
Including A, the solvent of B two-component, wherein,
Component A formula by weight is: dimethylbenzene 305 parts, 18 parts of acetone and butyl acetate 16 parts;
B component formula by weight is: 1,1,1-trichloroethane 190 parts and isopropanol 24 parts.
It should be noted that described pigment is titanium dioxide, organic yellow, chrome yellow, chrome vermillion, permanent bordeaux, white carbon black, iron oxide red, phthalein green grass or young crops
Indigo plant or one or more mixture of phthalein viridescent premetallized dye.
The preparation method of the present embodiment low-poison and combustion-resisting type room temperature solvent gage mark coating is same as in Example 1.
Embodiment 7
The low-poison and combustion-resisting type room temperature solvent gage mark coating of the present embodiment, in terms of parts by weight, primary raw material consists of: preparation
The primary raw material weight portion of described gage mark coating consists of: Solid Modified polyurethane resin 190 parts, pigment 25 parts, Paris white
100 parts, 100 parts of barium sulfate, Pulvis Talci 25 parts, DOP and/or DBP plasticizer 25 parts, levelling wetting dispersing agent 2 parts, defoamer
0.5 part, and
Including A, the solvent of B two-component, wherein,
Component A formula by weight is: dimethyl carbonate 110 parts, dimethylbenzene 110 parts, 10 parts of acetone and butyl acetate
10 parts;
B component formula by weight is: dichloromethane 50 parts, 1,1,1-trichloroethane 50 parts and isopropanol 16 parts.
It should be noted that described pigment is titanium dioxide, organic yellow, chrome yellow, chrome vermillion, permanent bordeaux, white carbon black, iron oxide red, phthalein green grass or young crops
Indigo plant or one or more mixture of phthalein viridescent premetallized dye.
The preparation method of the present embodiment low-poison and combustion-resisting type room temperature solvent gage mark coating is same as in Example 1.
Embodiment 8
The low-poison and combustion-resisting type room temperature solvent gage mark coating of the present embodiment, in terms of parts by weight, primary raw material consists of: preparation
The primary raw material weight portion of described gage mark coating consists of: solids modified acrylic's resin 275 parts, pigment 150 parts, Paris white
175 parts, 175 parts of barium sulfate, Pulvis Talci 150 parts, DOP and/or DBP plasticizer 30 parts, levelling wetting dispersing agent 6 parts, defoamer 3
Part, and
Including A, the solvent of B two-component, wherein,
Component A formula by weight is: dimethyl carbonate 210 parts, dimethylbenzene 215 parts, 20 parts of acetone and butyl acetate
20 parts;
B component formula by weight is: dichloromethane 100 parts, 1,1,1-trichloroethane 150 parts and isopropanol 27 parts.
It should be noted that described pigment is titanium dioxide, organic yellow, chrome yellow, chrome vermillion, permanent bordeaux, white carbon black, iron oxide red, phthalein green grass or young crops
Indigo plant or one or more mixture of phthalein viridescent premetallized dye.
The preparation method of the present embodiment low-poison and combustion-resisting type room temperature solvent gage mark coating is same as in Example 1.
Embodiment 9
The low-poison and combustion-resisting type room temperature solvent gage mark coating of the present embodiment, in terms of parts by weight, primary raw material consists of: preparation
The primary raw material weight portion of described gage mark coating consists of: solids modified acrylic's resin 240 parts, pigment 95 parts, Paris white
130 parts, 135 parts of barium sulfate, Pulvis Talci 90 parts, DOP and/or DBP plasticizer 27 parts, levelling wetting dispersing agent 5 parts, defoamer 2
Part, and
Including A, the solvent of B two-component, wherein,
Component A formula by weight is: dimethyl carbonate 235 parts, dimethylbenzene 115 parts, 15 parts of acetone and butyl acetate
15 parts;
B component formula by weight is: dichloromethane 100 parts, 1,1,1-trichloroethane 90 parts and isopropanol 20 parts.
It should be noted that described pigment is titanium dioxide, organic yellow, chrome yellow, chrome vermillion, permanent bordeaux, white carbon black, iron oxide red, phthalein green grass or young crops
Indigo plant or one or more mixture of phthalein viridescent premetallized dye.
The preparation method of the present embodiment low-poison and combustion-resisting type room temperature solvent gage mark coating is same as in Example 1.
Embodiment 10
The low-poison and combustion-resisting type room temperature solvent gage mark coating of the present embodiment, in terms of parts by weight, primary raw material consists of: preparation
The primary raw material weight portion of described gage mark coating consists of: solid propenoic acid resin 90 parts, solids modified acrylic's resin 100
Part, pigment 25 parts, Paris white 100 parts, 100 parts of barium sulfate, Pulvis Talci 25 parts, DOP and/or DBP plasticizer 25 parts, levelling profit
Hygroscopic water powder 2 parts, defoamer 0.5 part, and
Including A, the solvent of B two-component, wherein,
Component A formula by weight is: 110 parts of ethylbenzene, dimethylbenzene 110 parts, 10 parts of acetone and butyl acetate 10 parts;
B component formula by weight is: tetrachloroethylene 50 parts, 1,1,1-trichloroethane 50 parts, the tert-butyl alcohol 6 parts and isopropyl
Alcohol 10 parts.
It should be noted that described pigment is titanium dioxide, organic yellow, chrome yellow, chrome vermillion, permanent bordeaux, white carbon black, iron oxide red, phthalein green grass or young crops
Indigo plant or one or more mixture of phthalein viridescent premetallized dye.
The preparation method of the present embodiment low-poison and combustion-resisting type room temperature solvent gage mark coating is same as in Example 1.
Embodiment 11
The low-poison and combustion-resisting type room temperature solvent gage mark coating of the present embodiment, in terms of parts by weight, primary raw material consists of: preparation
The primary raw material weight portion of described gage mark coating consists of: solid propenoic acid resin 150 parts, solids modified acrylic's resin 125
Part, pigment 150 parts, Paris white 175 parts, 175 parts of barium sulfate, Pulvis Talci 150 parts, DOP and/or DBP plasticizer 30 parts, levelling
Wetting dispersing agent 6 parts, defoamer 3 parts, and
Including A, the solvent of B two-component, wherein,
Component A formula by weight is: 215 parts of ethylbenzene, dimethylbenzene 210 parts, 20 parts of acetone and butyl acetate 20 parts;
B component formula by weight is: tetrachloroethylene 100 parts, 1,1,1-trichloroethane 150 parts, the tert-butyl alcohol 17 parts and
Isopropanol 10 parts.
It should be noted that described pigment is titanium dioxide, organic yellow, chrome yellow, chrome vermillion, permanent bordeaux, white carbon black, iron oxide red, phthalein green grass or young crops
Indigo plant or one or more mixture of phthalein viridescent premetallized dye.
The preparation method of the present embodiment low-poison and combustion-resisting type room temperature solvent gage mark coating is same as in Example 1.
Embodiment 12
The low-poison and combustion-resisting type room temperature solvent gage mark coating of the present embodiment, in terms of parts by weight, primary raw material consists of: preparation
The primary raw material weight portion of described gage mark coating consists of: solid propenoic acid resin 120 parts, solids modified acrylic's resin 125
Part, pigment 85 parts, Paris white 135 parts, 135 parts of barium sulfate, Pulvis Talci 120 parts, DOP and/or DBP plasticizer 28 parts, levelling
Wetting dispersing agent 5 parts, defoamer 2 parts, and
Including A, the solvent of B two-component, wherein,
Component A formula by weight is: 135 parts of ethylbenzene, dimethylbenzene 215 parts, 14 parts of acetone and butyl acetate 14 parts;
B component formula by weight is: tetrachloroethylene 100 parts, 1,1,1-trichloroethane 120 parts, the tert-butyl alcohol 4 parts and different
Propanol 9 parts.
It should be noted that described pigment is titanium dioxide, organic yellow, chrome yellow, chrome vermillion, permanent bordeaux, white carbon black, iron oxide red, phthalein green grass or young crops
Indigo plant or one or more mixture of phthalein viridescent premetallized dye.
The preparation method of the present embodiment low-poison and combustion-resisting type room temperature solvent gage mark coating is same as in Example 1.
Embodiment 13
The low-poison and combustion-resisting type room temperature solvent gage mark coating of the present embodiment, in terms of parts by weight, primary raw material consists of: preparation
The primary raw material weight portion of described gage mark coating consists of: solid propenoic acid resin 80 parts, solids modified acrylic's resin 60 parts,
Solid Modified polyurethane resin 50 parts, pigment 25 parts, Paris white 100 parts, 100 parts of barium sulfate, Pulvis Talci 25 parts, DOP and/or
DBP plasticizer 25 parts, levelling wetting dispersing agent 2 parts, defoamer 0.5 part, and
Including A, the solvent of B two-component, wherein,
Component A formula by weight is: dimethyl carbonate 60 parts, 70 parts of ethylbenzene, dimethylbenzene 80 parts, 10 parts of acetone and second
Acid butyl ester 10 parts;
B component formula by weight is: dichloromethane 35, tetrachloroethylene 35 parts, 1,1,1-trichloroethane 30 parts, positive fourth
Alcohol 6, the tert-butyl alcohol 4 parts and isopropanol 6 parts.
It should be noted that described pigment is titanium dioxide, organic yellow, chrome yellow, chrome vermillion, permanent bordeaux, white carbon black, iron oxide red, phthalein green grass or young crops
Indigo plant or one or more mixture of phthalein viridescent premetallized dye.
The preparation method of the present embodiment low-poison and combustion-resisting type room temperature solvent gage mark coating is same as in Example 1.
Embodiment 14
The low-poison and combustion-resisting type room temperature solvent gage mark coating of the present embodiment, in terms of parts by weight, primary raw material consists of: preparation
The primary raw material weight portion of described gage mark coating consists of: solid propenoic acid resin 70 parts, solids modified acrylic's resin 125
Part, Solid Modified polyurethane resin 80 parts, pigment 150 parts, Paris white 175 parts, 175 parts of barium sulfate, Pulvis Talci 150 parts, DOP
And/or DBP plasticizer 30 parts, levelling wetting dispersing agent 6 parts, defoamer 3 parts, and
Including A, the solvent of B two-component, wherein,
Component A formula by weight is: dimethyl carbonate 160 parts, 170 parts of ethylbenzene, dimethylbenzene 95 parts, 20 parts of acetone and
Butyl acetate 20 parts;
B component formula by weight is: dichloromethane 75, tetrachloroethylene 95 parts, 1,1,1-trichloroethane 80 parts, positive fourth
Alcohol 9, the tert-butyl alcohol 5 parts and isopropanol 13 parts.
It should be noted that described pigment is titanium dioxide, organic yellow, chrome yellow, chrome vermillion, permanent bordeaux, white carbon black, iron oxide red, phthalein green grass or young crops
Indigo plant or one or more mixture of phthalein viridescent premetallized dye.
The preparation method of the present embodiment low-poison and combustion-resisting type room temperature solvent gage mark coating is same as in Example 1.
Embodiment 15
The low-poison and combustion-resisting type room temperature solvent gage mark coating of the present embodiment, in terms of parts by weight, primary raw material consists of: preparation
The primary raw material weight portion of described gage mark coating consists of: solid propenoic acid resin 80 parts, solids modified acrylic's resin 80 parts,
Solid Modified polyurethane resin 80 parts, pigment 90 parts, Paris white 115 parts, 115 parts of barium sulfate, Pulvis Talci 85 parts, DOP and/or
DBP plasticizer 28 parts, levelling wetting dispersing agent 4 parts, defoamer 1 part, and
Including A, the solvent of B two-component, wherein,
Component A formula by weight is: dimethyl carbonate 110 parts, 120 parts of ethylbenzene, dimethylbenzene 105 parts, 17 parts of acetone
With butyl acetate 17 parts;
B component formula by weight is: dichloromethane 65, tetrachloroethylene 55 parts, 1,1,1-trichloroethane 60 parts, positive fourth
Alcohol 7, the tert-butyl alcohol 4 parts and isopropanol 9 parts.
It should be noted that described pigment is titanium dioxide, organic yellow, chrome yellow, chrome vermillion, permanent bordeaux, white carbon black, iron oxide red, phthalein green grass or young crops
Indigo plant or one or more mixture of phthalein viridescent premetallized dye.
The preparation method of the present embodiment low-poison and combustion-resisting type room temperature solvent gage mark coating is same as in Example 1.
Embodiment 16
The low-poison and combustion-resisting type room temperature solvent gage mark coating of the present embodiment, in terms of parts by weight, primary raw material consists of: preparation
The primary raw material weight portion of described gage mark coating consists of: liquid acrylic or acrylic resin modified 316 parts, pigment 25
Part, Paris white 100 parts, 100 parts of barium sulfate, Pulvis Talci 25 parts, DOP and/or DBP plasticizer 25 parts, levelling wetting dispersing agent 2
Part, defoamer 0.5 part, and
Including A, the solvent of B two-component, wherein,
Component A formula by weight is: dimethyl carbonate 40 parts, 40 parts of ethylbenzene, dimethylbenzene 30 parts, 7 parts of acetone and second
Acid butyl ester 5 parts;
B component formula by weight is: dichloromethane 15, tetrachloroethylene 25 parts, 1,1,1-trichloroethane 20 parts, positive fourth
Alcohol 3, the tert-butyl alcohol 4 parts and isopropanol 5 parts.
It should be noted that described pigment is titanium dioxide, organic yellow, chrome yellow, chrome vermillion, permanent bordeaux, white carbon black, iron oxide red, phthalein green grass or young crops
Indigo plant or one or more mixture of phthalein viridescent premetallized dye.
The preparation method of the present embodiment low-poison and combustion-resisting type room temperature solvent gage mark coating is same as in Example 1.
Embodiment 17
The low-poison and combustion-resisting type room temperature solvent gage mark coating of the present embodiment, in terms of parts by weight, primary raw material consists of: preparation
The primary raw material weight portion of described gage mark coating consists of: liquid acrylic or acrylic resin modified 458 parts, pigment
150 parts, Paris white 175 parts, 175 parts of barium sulfate, Pulvis Talci 150 parts, DOP and/or DBP plasticizer 30 parts, levelling moistening divide
Powder 6 parts, defoamer 3 parts, and
Including A, the solvent of B two-component, wherein,
Component A formula by weight is: dimethyl carbonate 90 parts, 90 parts of ethylbenzene, dimethylbenzene 130 parts, 17 parts of acetone and
Butyl acetate 15 parts;
B component formula by weight is: dichloromethane 25, tetrachloroethylene 35 parts, 1,1,1-trichloroethane 50 parts, positive fourth
Alcohol 13, the tert-butyl alcohol 14 parts and isopropanol 15 parts.
It should be noted that described pigment is titanium dioxide, organic yellow, chrome yellow, chrome vermillion, permanent bordeaux, white carbon black, iron oxide red, phthalein green grass or young crops
Indigo plant or one or more mixture of phthalein viridescent premetallized dye.
The preparation method of the present embodiment low-poison and combustion-resisting type room temperature solvent gage mark coating is same as in Example 1.
Embodiment 18
The low-poison and combustion-resisting type room temperature solvent gage mark coating of the present embodiment, in terms of parts by weight, primary raw material consists of: preparation
The primary raw material weight portion of described gage mark coating consists of: liquid acrylic or acrylic resin modified 400 parts, pigment
120 parts, Paris white 135 parts, 135 parts of barium sulfate, Pulvis Talci 110 parts, DOP and/or DBP plasticizer 26 parts, levelling moistening divide
Powder 5 parts, defoamer 2 parts, and
Including A, the solvent of B two-component, wherein,
Component A formula by weight is: dimethyl carbonate 60 parts, 70 parts of ethylbenzene, dimethylbenzene 90 parts, 12 parts of acetone and second
Acid butyl ester 11 parts;
B component formula by weight is: dichloromethane 15, tetrachloroethylene 25 parts, 1,1,1-trichloroethane 30 parts, positive fourth
Alcohol 19, the tert-butyl alcohol 11 parts and isopropanol 11 parts.
It should be noted that described pigment is titanium dioxide, organic yellow, chrome yellow, chrome vermillion, permanent bordeaux, white carbon black, iron oxide red, phthalein green grass or young crops
Indigo plant or one or more mixture of phthalein viridescent premetallized dye.
The preparation method of the present embodiment low-poison and combustion-resisting type room temperature solvent gage mark coating is same as in Example 1.
It is obvious to a person skilled in the art that the invention is not restricted to the details of above-mentioned one exemplary embodiment, Er Qie
In the case of the spirit or essential attributes of the present invention, it is possible to realize the present invention in other specific forms.Therefore, no matter
From the point of view of which point, all should regard embodiment as exemplary, and be nonrestrictive, the scope of the present invention is by appended power
Profit requires rather than described above limits, it is intended that all by fall in the implication of equivalency and scope of claim
Change is included in the present invention.
Although moreover, it will be appreciated that this specification is been described by according to embodiment, but the most each embodiment only wraps
Containing an independent technical scheme, this narrating mode of description is only that for clarity sake those skilled in the art should
Description can also be formed those skilled in the art through appropriately combined as an entirety, the technical scheme in each embodiment
May be appreciated other embodiments.
Claims (10)
1. a low-poison and combustion-resisting type room temperature solvent gage mark coating, it is characterised in that prepare the primary raw material weight of described gage mark coating
Amount part consists of: hard resin 190-275 part, pigment 25-150 part, filler 225-500 part and auxiliary agent 27.5-39 part, and
Including A, the solvent of B two-component, wherein,
Component A formula by weight is: dimethyl carbonate and/or aromatic hydrocarbon 210-425 part, acetone 10-20 part and acetic acid fourth
Ester 10-20 part;
B component formula by weight is: chlorohydrocarbon 100-250 part and rudimentary saturated monohydroxy alcohol 16-27 part.
Low-poison and combustion-resisting type room temperature solvent gage mark coating the most according to claim 1, it is characterised in that described hard resin is
One or more mixing of solid propenoic acid resin, solids modified acrylic's resin or Solid Modified polyurethane resin
Thing.
Low-poison and combustion-resisting type room temperature solvent gage mark coating the most according to claim 1, it is characterised in that described aromatic hydrocarbon is two
Toluene and/or ethylbenzene, described chlorohydrocarbon is one or more of dichloromethane, 1,1,1-trichloroethane or tetrachloroethylene
Mixture.
Low-poison and combustion-resisting type room temperature solvent gage mark coating the most according to claim 1, it is characterised in that described rudimentary saturated one
Unit's alcohol is one or more mixture of the tert-butyl alcohol, n-butyl alcohol or isopropanol.
Low-poison and combustion-resisting type room temperature solvent gage mark coating the most according to claim 1, it is characterised in that described filler include as
The raw material of lower weight portion: Paris white 100-175 part, barium sulfate 100-175 part, Pulvis Talci 25-150 part.
Low-poison and combustion-resisting type room temperature solvent gage mark coating the most according to claim 1, it is characterised in that described auxiliary agent include as
The raw material of lower weight portion: DOP and/or DBP plasticizer 25-30 part, levelling wetting dispersing agent 2-6 part, defoamer 0.5-3 part.
Low-poison and combustion-resisting type room temperature solvent gage mark coating the most according to claim 1, it is characterised in that described pigment is titanium white
Powder, organic yellow, chrome yellow, chrome vermillion, permanent bordeaux, white carbon black, iron oxide red, phthalocyanine blue or phthalein viridescent premetallized dye one or both with
On mixture.
8. a preparation method for the low-poison and combustion-resisting type room temperature solvent gage mark coating as described in claim 1 to 7, its feature exists
In, described method comprises the steps:
1) by weight the solvent of B component is squeezed into reactor, after stirring 15 minutes, by weight the solvent of component A is squeezed into
Reactor, adds above-mentioned parts by weight solids resin, makes reactor rotating speed be 300-800 rev/min, makes hard resin be completely dissolved;
2) in step 1) in the slurry prepared, under the temperature conditions less than 45 DEG C, add under the rotating speed of 600-2000 rev/min
The pigment of above-mentioned parts by weight, filler and auxiliary agent stir 30-40 minute so that it is be uniformly dispersed;
3) in step 2) by material dispersion uniformly after by the way of delivery pump or Scattered Kettle pressurization average rate material input is ground
Machine, in process of lapping, grinder chuck remains that cooling system opens the state of cooling, and controlling temperature is less than 35 DEG C,
Treat that material is ground to less than 15 microns and starts finished product packing after filtering.
9. a low-poison and combustion-resisting type room temperature solvent gage mark coating as claimed in claim 1, it is characterised in that by described solid third
Olefin(e) acid resin, acrylic resin modified or modified polyurethane resin replace with liquid acrylic, acrylic resin modified or
Modified polyurethane resin, described liquid acrylic, acrylic resin modified or modified polyurethane resin are 316-458 part,
Its solid content is 30%-75%, and described solvent is reduced to 194-513 part.
Low-poison and combustion-resisting type room temperature solvent gage mark coating the most according to claim 9, it is characterised in that described liquid propene
Acid resin, acrylic resin modified or modified polyurethane resin solid content are 60%.
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