CN106277058B - A kind of processing technology of nanometer of wolframic acid caesium powder - Google Patents
A kind of processing technology of nanometer of wolframic acid caesium powder Download PDFInfo
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- CN106277058B CN106277058B CN201610675935.9A CN201610675935A CN106277058B CN 106277058 B CN106277058 B CN 106277058B CN 201610675935 A CN201610675935 A CN 201610675935A CN 106277058 B CN106277058 B CN 106277058B
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- 239000000843 powder Substances 0.000 title claims abstract description 51
- TVFDJXOCXUVLDH-UHFFFAOYSA-N caesium atom Chemical compound [Cs] TVFDJXOCXUVLDH-UHFFFAOYSA-N 0.000 title claims abstract description 43
- 229910052792 caesium Inorganic materials 0.000 title claims abstract description 42
- 239000002253 acid Substances 0.000 title claims abstract description 29
- 238000005516 engineering process Methods 0.000 title claims abstract description 24
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 claims abstract description 15
- 229910052721 tungsten Inorganic materials 0.000 claims abstract description 15
- 239000010937 tungsten Substances 0.000 claims abstract description 15
- 239000011812 mixed powder Substances 0.000 claims abstract description 13
- BEFDCLMNVWHSGT-UHFFFAOYSA-N ethenylcyclopentane Chemical compound C=CC1CCCC1 BEFDCLMNVWHSGT-UHFFFAOYSA-N 0.000 claims abstract description 9
- 229940075582 sorbic acid Drugs 0.000 claims abstract description 9
- 235000010199 sorbic acid Nutrition 0.000 claims abstract description 9
- 239000004334 sorbic acid Substances 0.000 claims abstract description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 9
- NLSCHDZTHVNDCP-UHFFFAOYSA-N caesium nitrate Chemical compound [Cs+].[O-][N+]([O-])=O NLSCHDZTHVNDCP-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000008367 deionised water Substances 0.000 claims abstract description 8
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 8
- 238000001035 drying Methods 0.000 claims abstract description 8
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims abstract description 4
- 239000007795 chemical reaction product Substances 0.000 claims abstract description 4
- 238000002156 mixing Methods 0.000 claims description 68
- 230000007246 mechanism Effects 0.000 claims description 48
- 239000002994 raw material Substances 0.000 claims description 41
- 239000000463 material Substances 0.000 claims description 35
- 238000003756 stirring Methods 0.000 claims description 24
- 238000003860 storage Methods 0.000 claims description 18
- 239000007788 liquid Substances 0.000 claims description 17
- 210000000078 claw Anatomy 0.000 claims description 16
- 238000006073 displacement reaction Methods 0.000 claims description 16
- 239000007921 spray Substances 0.000 claims description 15
- 230000003028 elevating effect Effects 0.000 claims description 14
- 238000001514 detection method Methods 0.000 claims description 13
- 238000012856 packing Methods 0.000 claims description 8
- 230000008520 organization Effects 0.000 claims description 6
- 230000035939 shock Effects 0.000 claims description 6
- 238000006243 chemical reaction Methods 0.000 claims description 4
- 230000006698 induction Effects 0.000 claims description 4
- 238000009527 percussion Methods 0.000 claims description 4
- 230000008450 motivation Effects 0.000 claims description 2
- 239000000047 product Substances 0.000 claims description 2
- 238000002360 preparation method Methods 0.000 abstract description 4
- 230000008901 benefit Effects 0.000 abstract description 3
- 230000000694 effects Effects 0.000 description 8
- 238000000034 method Methods 0.000 description 6
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 4
- 239000003795 chemical substances by application Substances 0.000 description 4
- 244000144985 peep Species 0.000 description 4
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
- 238000000151 deposition Methods 0.000 description 3
- 238000010586 diagram Methods 0.000 description 3
- 230000005611 electricity Effects 0.000 description 3
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 2
- 230000009471 action Effects 0.000 description 2
- 239000003513 alkali Substances 0.000 description 2
- 229910052786 argon Inorganic materials 0.000 description 2
- 239000004202 carbamide Substances 0.000 description 2
- 230000007423 decrease Effects 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 238000011068 loading method Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000002244 precipitate Substances 0.000 description 2
- 238000003466 welding Methods 0.000 description 2
- 230000007059 acute toxicity Effects 0.000 description 1
- 231100000403 acute toxicity Toxicity 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 230000001476 alcoholic effect Effects 0.000 description 1
- 239000012752 auxiliary agent Substances 0.000 description 1
- 230000006870 function Effects 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 239000003595 mist Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 238000011112 process operation Methods 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- 150000003657 tungsten Chemical class 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G41/00—Compounds of tungsten
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C19/00—Other disintegrating devices or methods
- B02C19/06—Jet mills
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Inorganic Chemistry (AREA)
- Accessories For Mixers (AREA)
Abstract
The invention provides the processing technology of a kind of nanometer of wolframic acid caesium powder.It is excessively complicated that it solves the step of existing preparation method, and needs manual operation, the technical problem such as complex operation.The processing technology of this nanometer of wolframic acid caesium powder, comprises the following steps：A, the ammonium metatungstate of reacting dose and cesium nitrate are dissolved in deionized water, above-mentioned solution is dried to obtain powder, then obtained powder is further crushed, so as to obtain tungsten, caesium mixed-powder；B, tungsten, caesium mixed-powder are added in reactor, and add sorbic acid thereto, the quality of sorbic acid is tungsten, 24 times of caesium mixed-powder quality；C, it will separate through the reaction product in step b, and washed using deionized water, dried afterwards by common baking oven, crushed after drying using airslide disintegrating mill, obtain a nanometer wolframic acid caesium powder.The present invention has the advantages of simple to operate.
Description
Technical field
The present invention relates to a kind of processing technology, the processing technology of particularly a kind of nanometer wolframic acid caesium powder.
Background technology
Wolframic acid caesium is a kind of chemical substance, and has acute toxicity, can be dissolved in water, the meeting under conditions of acid or alkali
React, should avoid meeting place with moisture, acid, alkali when storing under normal temperature, if touching skin, eyes of human body etc. accidentally,
Timely medical treatment is needed to handle.
Through retrieval, as Chinese patent literature discloses a kind of nanometer wolframic acid caesium powder and preparation method and application【Application
Number：201510323309.9；Publication number：CN 104925867A】.This nanometer wolframic acid caesium raw powder's production technology, its feature exist
In, including step：A, according to n (Cs)/n (W)=0.33：1, cesium salt and tungsten salt are dissolved in citric acid solution and alcoholic solvent,
After stirring, 2-3 hours are reacted under the conditions of 180-200 DEG C, obtain tungsten, caesium mixed liquor；B, added in tungsten, caesium mixed liquor
Appropriate urea, the pH value of reaction solution is adjusted to 3-5, stirs to urea and is completely dissolved；C, by the mixed liquor after being completely dissolved in step B
Washed with argon gas, and chemical reaction 2-6h is carried out through Ultrasonic Radiation under 70-90 DEG C and argon gas protection, obtain gelatinous precipitate
Thing；D, gelatinous precipitate is subjected to ageing 4-24h, filtered, washed afterwards, wash after be dried, finally calcined,
Obtain a nanometer wolframic acid caesium powder.
Although the preparation method disclosed in the patent has preferable cost advantage, the step of the preparation method excessively
Complexity, and need manual operation, complex operation, therefore, the processing technology for designing a kind of nanometer of wolframic acid caesium powder are that have very much must
Want.
The content of the invention
The purpose of the present invention is above mentioned problem be present for existing technology, it is proposed that a kind of nanometer of wolframic acid caesium powder plus
Work technique, the processing technology have the characteristics of simple to operate.
The purpose of the present invention can be realized by following technical proposal：A kind of processing technology of nanometer of wolframic acid caesium powder, its
It is characterised by, comprises the following steps：
A, the ammonium metatungstate of reacting dose and cesium nitrate are dissolved in deionized water, above-mentioned solution are dried to obtain powder,
Obtained powder is further crushed again, so as to obtain tungsten, caesium mixed-powder；
B, tungsten, caesium mixed-powder are added in reactor, and add sorbic acid thereto, in 240-460 DEG C, stirring is anti-
Answer 4-6h, the quality of sorbic acid is tungsten, 2-4 times of caesium mixed-powder quality；
C, it will separate through the reaction product in step b, and washed using deionized water, afterwards by common
Baking oven is dried, drying time 20-30min, is crushed after drying using airslide disintegrating mill, obtains a nanometer wolframic acid caesium powder
End.
Using process above, its procedure of processing can be greatly simplified, reduces the time of processing, it is simple to operate.
Airslide disintegrating mill in the step c includes frame, and feeding device, mixing dress are disposed with the frame
Put, reducing mechanism and packing apparatus, the feeding device include feeding tube, storage tank and the positioning branch for positioning raw material bag
Frame, locating support and storage tank are arranged in frame, and storage tank lower end has the first delivery outlet, is provided with the first delivery outlet
First magnetic valve, storage tank upper end have first charging aperture, and first charging aperture is connected with feeding tube one end, the feeding tube other end
Above locating support, and the end has guide portion, and a moving machine that guide portion can be driven to move up and down is provided with frame
Structure, the first delivery pump is additionally provided with feeding tube；The travel mechanism includes cylinder and mounting ring, and the cylinder body of cylinder is fixed on machine
On frame, straight down, the piston rod end of cylinder is connected the piston rod of cylinder by connecting rod with mounting ring, and guide portion is fixed on
The controlling organization that cylinder can be controlled to act is additionally provided with mounting ring, in frame；The mixing arrangement includes blending bin, fog-spray nozzle
And liquid reserve tank, blending bin and liquid reserve tank are each attached in frame, mixing upper box part has powder input port, and powder input port passes through
First connecting tube is connected with the first delivery outlet, and mixing lower box part has powder delivery outlet, and second is provided with powder delivery outlet
Magnetic valve, fog-spray nozzle are arranged in blending bin, and down, the inlet of fog-spray nozzle passes through delivery pipe and liquid storage to the liquid outlet of fog-spray nozzle
Case is connected, and the second delivery pump is provided with delivery pipe, and mixing upper box part is additionally provided with agitating shaft, agitating shaft upper end and stirring electricity
Machine is connected, and agitating shaft lower end is penetrated in blending bin to be connected with stirring vane, and material in blending bin can be drawn by being provided with frame
Draw frame machine, draw frame machine include suction pipe, the second push-rod electric machine, asepwirator pump, mounting blocks and case, and the second push-rod electric machine leads to
Crossing one can drive its moving structure moved horizontally to be arranged in blending bin, the push rod of the second push-rod electric machine straight down, second
The push rod end of push-rod electric machine is mutually fixed with mounting blocks, and the feed end of suction pipe is fixed on mounting blocks, and the feed end is down,
The discharge end of suction pipe passes blending bin and is located in case, and asepwirator pump is arranged in suction pipe；The packing apparatus includes depositing
Batch can, material stock tank are fixed in frame, and material stock tank top has the second input port, and the second input port passes through the second connecting tube and powder
Body delivery outlet is connected, and material stock tank bottom has the second delivery outlet, is provided with the 3rd magnetic valve in the second delivery outlet, is set in frame
The detent mechanism that finished bag edge can be positioned is equipped with, shock structure is additionally provided with frame, shock structure includes the second shake
Dynamic plate, the second vibration motor and the second installing plate, the second installing plate can drive the first elevating mechanism that it moves up and down by one
It is arranged in frame, the second jolting plate is arranged on the second installing plate, and the second jolting plate is in immediately below the second delivery outlet, the
There is the 3rd spring between two jolting plates and the second installing plate, the 3rd spring one end and the second jolting plate lower surface are connected, and the 3rd
The spring other end and the second installing plate upper surface are connected, and the second vibration motor is fixed on the second jolting plate lower surface.
The operation principle of airslide disintegrating mill is as follows：Locating support will be positioned at for depositing the raw material bag of raw material, opened
First delivery pump, the first delivery pump by feeding tube by the feedstock transportation in raw material bag into storage tank, with raw material bag
Raw material gradually decreases, and controls the piston rod of cylinder to drive mounting ring to move down, mounting ring drives guide portion to move down, and makes to lead
Material portion contacts with the raw material in raw material bag all the time；Raw material in storage tank is transported in blending bin by the first communicating pipe, control
The output shaft of stirring motor drives agitating shaft to rotate, and agitating shaft drives stirring vane to rotate, meanwhile, the second delivery pump is opened, the
Modifying agent in liquid reserve tank is transported in fog-spray nozzle by two delivery pumps by delivery pipe, modifying agent and raw material is uniformly mixed；It is mixed
Raw material in mould assembling is transported in material stock tank after crushing by the second communicating pipe, by detent mechanism by the edge of finished bag
It is fixed on the second delivery outlet, the 3rd magnetic valve of control makes the second equipped at outlet port in open mode；Pass through the first elevating mechanism band
Dynamic second installing plate moves up and down, and the second installing plate drives the second jolting plate to move up and down, and makes the second jolting plate and finished bag
Bottom is contacted, and drives the second jolting plate to shake by the second vibration motor, and the second jolting plate, which drives finished bag to produce vibrations, to be made into
Product are packed full, process operation so as to complete it, production efficiency is high.
The controlling organization includes displacement transducer, mounting rod and controller, and mounting rod one end is connected with mounting ring, peace
The dress bar other end is connected with displacement transducer, and the induction part of displacement transducer is fixed on machine towards locating support, controller
On frame, cylinder and displacement transducer are connected with the controller.
Using above structure, the distance of raw material in guide portion and material bag is detected by displacement transducer, signal is transmitted
To controller, the piston rod of controller control cylinder moves down, and control is accurate.
The locating support upper end has the locating dowel that can position raw material bag, and locating support lower end has that raw material bag can be entered
The percussion mechanism of row vibrations, the percussion mechanism include the first jolting plate and the first vibration motor, and the first jolting plate is arranged on fixed
On the bottom plate of position support, there is the first spring between the first jolting plate and the bottom plate of locating support, one end of the first spring and the
One jolting plate is mutually fixed, and the other end of the first spring is mutually fixed with the bottom plate of locating support, and the first vibration motor is fixed on first
Jolting plate lower surface.
When needing to shake raw material bag, the edge of raw material bag is penetrated in locating dowel, passes through the first vibration motor
The first jolting plate is set to produce vibrations, the first jolting plate drives raw material bag vibrations, moves down the material in raw material bag, vibrations side
Just.
Be additionally provided with anti-slipping mechanism on the locating support, anti-slipping mechanism includes claw and second spring, claw lower end and
Locating support is hinged, and one end of second spring is connected with claw middle part, and the other end of second spring is connected with locating support
Connect, claw upper end can be resisted against on locating support.
Using above structure, claw and locating support is set to lean by second spring, so as to avoid raw material bag from calmly
Slid out in the post of position, good antiskid effect.
The locating dowel upper end has introduction part.
Using above structure, it can be facilitated by introduction part and penetrate at raw material bag edge in locating dowel, guide effect is good.
The locating dowel lower end is arranged with rubber ring.
Using above structure, its frictional force can be increased by rubber ring, it is rational in infrastructure.
Some rollers are additionally provided with the locating support, roller and one can drive the second elevating mechanism of its oscilaltion
It is connected.
Using above structure, roller can be packed up or put down by the second elevating mechanism, it is practical.
Second elevating mechanism includes the first installing plate, the first push-rod electric machine, the first guide rail and the first sliding block, and first leads
Rail is fixed on locating support vertically, and the first sliding block is arranged in the first guide rail, and the first push-rod electric machine is fixed on locating support
On bottom plate, straight down, the push rod end of the first push-rod electric machine is connected the push rod of the first push-rod electric machine with the first sliding block, and first
Installing plate upper surface is connected with the first sliding block, and the first installing plate lower surface is connected with roller.
When needing that roller is packed up or put down, the push rod of the first push-rod electric machine of control drives the first sliding block to move up and down,
First sliding block drives the first installing plate to move up and down, and the first installing plate drives roller to move up and down, so as to roller is packed up or
Put down.
The delivery device that the material of blending bin side-walls can be pushed at agitating shaft is additionally provided with the frame, is pushed
Mechanism includes some push pipes and air compressor machine, and some push pipes are located in blending bin side wall vertically, and push pipe lower end is blind end,
It is inlet end to push pipe upper end, and push pipe is connected by communicating pipe with air compressor machine, and push tube side part offers some ventholes,
Venthole is towards agitating shaft.
Using above structure, delivered air to by air compressor machine in push pipe, air exports from venthole, in air-flow
In the presence of, the material of blending bin side-walls is pushed at agitating shaft, can significantly less stirring time, push effect it is good.
The moving structure includes drive cylinder, movable plate, the second sliding block and the second guide rail, and the second guide rail is horizontally fixed on
In blending bin, the second sliding block is arranged in the second guide rail, and the cylinder body of drive cylinder is fixed in blending bin, the piston of drive cylinder
Boom end and the second sliding block are connected, and movable plate is fixed on the second sliding block, and the second push-rod electric machine is fixed on movable plate.
When needing to move back and forth the second push-rod electric machine, the piston rod of drive cylinder is controlled to drive the second sliding block along the
Two guide rails move back and forth, and the second sliding block drives movable plate to move back and forth, and movable plate drives the second push-rod electric machine to move back and forth, so as to
Can move back and forth the second push-rod electric machine.
Flow control valve is additionally provided with the delivery pipe.
Using above structure, the uninterrupted of liquid in delivery pipe is can adjust by flow control valve, it is easy to adjust.
Peep hole is provided with the blending bin, transparent access panel is provided with peep hole.
Using above structure, working condition that can be in rapid examination to blending bin by access panel, observation is directly perceived, conveniently.
Passage is additionally provided with the suction pipe, passage upper end is connected with the feed end of suction pipe, under passage
End can be resisted against blending bin bottom.
Using above structure, conveniently it can be transported material to by passage in suction pipe, guide effect is good.
First elevating mechanism includes the 3rd push-rod electric machine, the 3rd sliding block and the 3rd guide rail, and the 3rd guide rail is fixed vertically
In frame, the 3rd sliding block is arranged in the 3rd guide rail, and the 3rd push-rod electric machine is fixed in frame, the push rod of the 3rd push-rod electric machine
Straight up, the push rod end of the 3rd push-rod electric machine is connected with the 3rd sliding block, and the second installing plate is fixed on the 3rd sliding block.
When needing to move up and down the second installing plate, the push rod of the 3rd push-rod electric machine of control drives the 3rd sliding block along the
Three guide rails move up and down, and the 3rd sliding block drives the second installing plate to move up and down, so as to move up and down the second installing plate.
The detent mechanism includes locating ring, locating piece and positioning cylinder, and locating ring is arranged and is fixed on the second delivery outlet
On, positioning cylinder is fixed in frame by support, piston rod the second delivery outlet of direction of positioning cylinder, the piston of positioning cylinder
Boom end is mutually fixed with locating piece, and the locating slot to match with locating ring is offered on locating piece.
When needing the edge by finished bag to be fixed on the second delivery outlet, the edge of finished bag is enclosed on locating ring,
The piston rod of positioning cylinder is controlled to drive locating piece movement, locating piece and locating ring lean, so as to by the edge of finished bag
It is fixed on the second delivery outlet, positioning is quick.
Rubber strip is provided with the locating slot, the protuberance on rubber strip with some protrusions.
Using above structure, its frictional force can be increased by rubber strip, avoid the occurrence of the phenomenon of slip, job stability
It is good.
Prompting mechanism is additionally provided with the frame, prompting mechanism, which includes travel switch, detection bar, alarm bell and PLC, to be compiled
Range controller, alarm bell are fixed in frame, and travel switch is fixed on the second installing plate lower surface, and detection bar is fixed in frame,
Detection bar can be in contact with travel switch, and travel switch and alarm bell are connected with the PLC.
After material is filled in finished bag, the push rod of the 3rd push-rod electric machine drives the second installing plate to move down, the second peace
Loading board drives travel switch to move down, and signal is passed to PLC programmable controls by travel switch and detection bar contact, travel switch
Device processed, PLC make alarm bell send alarm sound, prompt intuitively, conveniently.
3rd magnetic valve is connected with above-mentioned PLC.
Using above structure, the 3rd magnetic valve can control to obtain electric or dead electricity by PLC.
Some limited posts are fixed with second jolting plate, a high position for limited post is 30-50mm.
Using above structure, bottom progress that can be to finished bag by limited post is spacing, avoids finished bag from the second vibrations
Depart from plate, position-limiting action is good.
Compared with prior art, the processing technology of this nanometer of wolframic acid caesium powder has advantages below：
1st, its procedure of processing can be greatly simplified in the present invention, reduces the time of processing, it is simple to operate.
2nd, the first jolting plate is made to produce vibrations by the first vibration motor, the first jolting plate drives raw material bag vibrations, makes original
Material in pocket moves down, and vibrations are convenient.
3rd, claw and locating support is leant by second spring, raw material bag can be avoided to be slid out from locating dowel,
Good antiskid effect.
4th, by above and below suction pipe and will move horizontally, asepwirator pump is defeated by the mixture in blending bin everywhere by suction pipe
Go out into case, it is achievable comprehensive to being sampled in blending bin, check precisely.
5th, delivered air to by air compressor machine in push pipe, air exports from venthole, by blending bin side-walls
Material is pushed at agitating shaft, can significantly less stirring time, push effect it is good.
Brief description of the drawings
Fig. 1 is the planar structure schematic diagram of feeding device.
Fig. 2 is the close-up schematic view at A in Fig. 1.
Fig. 3 is the close-up schematic view at B in Fig. 1.
Fig. 4 is the sectional view of mixing arrangement.
Fig. 5 is the close-up schematic view at C in Fig. 4.
Fig. 6 is the sectional view of delivery device in mixing arrangement.
Fig. 7 is the planar structure schematic diagram of packing apparatus.
Fig. 8 is the close-up schematic view at D in Fig. 7.
Fig. 9 is the dimensional structure diagram that packing apparatus removes part.
In figure, 1, frame；2nd, the first magnetic valve；3rd, storage tank；3a, the first delivery outlet；3b, first charging aperture；4th, first
Delivery pump；5th, feeding tube；5a, guide portion；6th, link；7th, locating support；7a, bottom plate；8th, connecting rod；9th, mounting ring；10th, displacement
Sensor；10a, induction part；11st, mounting rod；12nd, cylinder；13rd, locating dowel；13a, introduction part；14th, claw；15th, second spring；
16th, the first installing plate；17th, the first vibration motor；18th, the first jolting plate；19th, the first spring；20th, the first push-rod electric machine；21st,
One guide rail；22nd, the first sliding block；23rd, roller；24th, controller；25th, blending bin；25a, powder delivery outlet；25b, peep hole；25c、
Powder input port；26th, stirring vane；27th, second solenoid valve；28th, case；29th, suction pipe；30th, asepwirator pump；31st, access panel；
32nd, agitating shaft；33rd, stirring motor；34th, the second guide rail；35th, fog-spray nozzle；36th, delivery pipe；37th, flow control valve；38th, second is defeated
Send pump；39th, liquid reserve tank；40th, drive cylinder；41st, the second sliding block；42nd, movable plate；43rd, the second push-rod electric machine；44th, mounting blocks；
45th, passage；46th, communicating pipe；47th, air compressor machine；48th, push pipe；48a, venthole；49th, PLC；50th, it is alert
Bell；51st, support；52nd, positioning cylinder；53rd, locating piece；53a, locating slot；54th, locating ring；55th, the 3rd magnetic valve；56th, material stock
Tank；56a, the second delivery outlet；56b, the second input port；57th, detection bar；58th, the 3rd push-rod electric machine；59th, the 3rd guide rail；60th,
Three sliding blocks；61st, limited post；62nd, the second jolting plate；63rd, the second vibration motor；64th, the second installing plate；65th, the 3rd spring；66、
Travel switch；67th, rubber strip.
Embodiment
It is the specific embodiment of the present invention and with reference to accompanying drawing below, technical scheme is further described,
But the present invention is not limited to these embodiments.
The processing technology of this nanometer of wolframic acid caesium powder, comprises the following steps：
A, the ammonium metatungstate of reacting dose and cesium nitrate are dissolved in deionized water, above-mentioned solution are dried to obtain powder,
Obtained powder is further crushed again, so as to obtain tungsten, caesium mixed-powder；
B, tungsten, caesium mixed-powder are added in reactor, and add sorbic acid thereto, in 240-460 DEG C, stirring is anti-
Answer 4-6h, the quality of sorbic acid is tungsten, 2-4 times of caesium mixed-powder quality, in the present embodiment, and in 300 DEG C, stirring reaction
5h, the quality of sorbic acid is tungsten, 3 times of caesium mixed-powder quality；
C, it will separate through the reaction product in step b, and washed using deionized water, afterwards by common
Baking oven is dried, drying time 20-30min, is crushed after drying using airslide disintegrating mill, obtains a nanometer wolframic acid caesium powder
End；In the present embodiment, drying time 25min.
Using the technique, its procedure of processing can be greatly simplified, reduces the time of processing, it is simple to operate.
As shown in Figure 1, Figure 2, shown in Fig. 4, Fig. 5, Fig. 7, Fig. 8, the airslide disintegrating mill in step c includes frame 1, in frame 1 according to
Secondary to be provided with feeding device, mixing arrangement, reducing mechanism and packing apparatus, reducing mechanism is using air-flow of the prior art
Grinding mode；Feeding device includes feeding tube 5, storage tank 3 and the locating support 7 for positioning raw material bag, locating support 7 and storage
Batch can 3 is arranged at 1 in frame, and the lower end of storage tank 3, which has in the first delivery outlet 3a, the first delivery outlet 3a, is provided with the first electromagnetism
There is first charging aperture 3b, first charging aperture 3b to be connected with the one end of feeding tube 5 for valve 2, the upper end of storage tank 3, the other end of feeding tube 5
Above locating support 7, and the end has guide portion 5a, and one is provided with frame 1 can drive what guide portion 5a was moved up and down
Travel mechanism, the first delivery pump 4 is additionally provided with feeding tube 5；Travel mechanism includes cylinder 12 and mounting ring 9, the cylinder of cylinder 12
Body is fixed in frame 1, and the cylinder body of cylinder 12 is fixed in frame 1 by link 6；The piston rod of cylinder 12 straight down,
The piston rod end of cylinder 12 is connected by connecting rod 8 with mounting ring 9, and guide portion 5a is fixed in mounting ring 9, and guide portion 5a leads to
Bolted mode is crossed to be fixed in mounting ring 9；The controlling organization that cylinder 12 can be controlled to act is additionally provided with frame 1；It is mixed
Attach together to put and be each attached to including blending bin 25, fog-spray nozzle 35 and liquid reserve tank 39, blending bin 25 and liquid reserve tank 39 in frame 1, mixed
Case 25 and liquid reserve tank 39 are fixed on by way of welding in frame 1；The top of blending bin 25 has powder input port 25c, powder
Body input port 25c is connected by the first connecting tube with the first delivery outlet 3a, and the bottom of blending bin 25 has powder delivery outlet 25a,
Second solenoid valve 27 is provided with powder delivery outlet 25a, fog-spray nozzle 35 is arranged in blending bin 25, the liquid outlet court of fog-spray nozzle 35
Under, the inlet of fog-spray nozzle 35 is connected by delivery pipe 36 with liquid reserve tank 39, and the second delivery pump 38 is provided with delivery pipe 36,
The top of blending bin 25 is additionally provided with agitating shaft 32, and the upper end of agitating shaft 32 is connected with stirring motor 33, and the upper end of agitating shaft 32 passes through
The mode of key connection is connected with the output shaft of stirring motor 33, and stirring motor 33 is fixed in blending bin 25；The lower end of agitating shaft 32
Penetrate in blending bin 25 and be connected with stirring vane 26, the lower end of agitating shaft 32 is by way of key connection and the phase of stirring vane 26
Even；The draw frame machine of material in blending bin 25 can be drawn by being provided with frame 1, and draw frame machine includes suction pipe 29, the second push rod
Motor 43, asepwirator pump 30, mounting blocks 44 and case 28, the second push-rod electric machine 43 can drive the movement that it moves horizontally by one
Structure setting in blending bin 25, the push rod of the second push-rod electric machine 43 straight down, the push rod end of the second push-rod electric machine 43 and
The phase of mounting blocks 44 is fixed, and the push rod end of the second push-rod electric machine 43 is mutually fixed with mounting blocks 44 by bolted connection；Inhale
The feed end of pipe 29 is taken to be fixed on mounting blocks 44, and the feed end is down, the discharge end of suction pipe 29 passes blending bin 25
In in case 28, asepwirator pump 30 is arranged in suction pipe 29；Packing apparatus includes material stock tank 56, and material stock tank 56 is fixed on frame
On 1, material stock tank 56 is fixed on by way of welding in frame 1；The top of material stock tank 56 has the second input port 56b, and second is defeated
Entrance 56b is connected by the second connecting tube with powder delivery outlet 25a, and the bottom of material stock tank 56 has the second delivery outlet 56a, and second
The 3rd magnetic valve 55 is provided with delivery outlet 56a, the detent mechanism that finished bag edge can be positioned, machine are provided with frame 1
Shock structure is additionally provided with frame 1, shock structure includes the second jolting plate 62, the second vibration motor 63 and the second installing plate 64,
Second installing plate 64 can drive its first elevating mechanism moved up and down to be arranged in frame 1 by one, and the second jolting plate 62 is set
Put on the second installing plate 64, and the second jolting plate 62 is in immediately below the second delivery outlet 56a, the second jolting plate 62 and the second peace
There is the 3rd spring 65, in the present embodiment, the quantity of the 3rd spring 65 is four between loading board 64；The one end of 3rd spring 65 and
The lower surface of second jolting plate 62 is connected, and the other end of the 3rd spring 65 and the upper surface of the second installing plate 64 are connected, the second vibration motor
63 are fixed on the lower surface of the second jolting plate 62, and the second vibration motor 63 is fixed on the second jolting plate 62 by bolted connection
Lower surface.
As shown in Figure 1 and Figure 2, controlling organization includes displacement transducer 10, mounting rod 11 and controller 24, mounting rod 11 1
End is connected with mounting ring 9, and one end of mounting rod 11 is connected with mounting ring 9 by bolted connection；Mounting rod 11 is another
One end is connected with displacement transducer 10, and the other end of mounting rod 11 is connected with displacement transducer 10 by bolted connection
Connect；And the induction part 10a of displacement transducer 10 is fixed in frame 1 towards locating support 7, controller 24, controller 24 passes through
The mode of bolted mode is fixed in frame 1, the single-chip microcomputer that controller 24 can be bought using in the market, single-chip microcomputer control
The program of cylinder and sensor processed is existing, and its program need not update；Cylinder 12 and displacement transducer 10 and the control
Device 24 processed is connected.
As shown in Figure 1, Figure 2, Figure 3 shows, the upper end of locating support 7 has the locating dowel 13 that can position raw material bag, in the present embodiment
In, the quantity of locating dowel 13 is four；The upper end of locating dowel 13 has introduction part 13a, can by introduction part 13a using the structure
Convenient to penetrate at raw material bag edge in locating dowel 13, guide effect is good；The lower end of locating dowel 13 is arranged with rubber ring, using the knot
Structure, its frictional force can be increased by rubber ring；The lower end of locating support 7 has the percussion mechanism that can be shaken to raw material bag, shake
Motivation structure includes the first jolting plate 18 and the first vibration motor 17, and the first jolting plate 18 is arranged on the bottom plate 7a of locating support 7,
There are the first spring 19, one end of the first spring 19 and the first vibrations between first jolting plate 18 and the bottom plate 7a of locating support 7
The phase of plate 18 is fixed, and the other end of the first spring 19 is fixed with the bottom plate 7a phases of locating support 7, and the first vibration motor 17 is fixed on
The lower surface of one jolting plate 18, the first vibration motor 17 are fixed on the lower surface of the first jolting plate 18 by bolted connection.
As shown in Figure 1 and Figure 2, anti-slipping mechanism is additionally provided with locating support 7, anti-slipping mechanism includes the bullet of claw 14 and second
Spring 15, the lower end of claw 14 and locating support 7 are hinged, and one end of second spring 15 is connected with the middle part of claw 14, second spring
15 other end is connected with locating support 7, and the upper end of claw 14 can be resisted against on locating support 7.
As shown in Figure 1, Figure 3, some rollers 23, in the present embodiment, the quantity of roller 23 are additionally provided with locating support 7
For four；Roller 23 can drive the second elevating mechanism of its oscilaltion to be connected with one, using the structure, pass through the second lift
Roller 23 can be packed up or put down by structure.
As shown in Figure 1, Figure 3, the second elevating mechanism includes the first installing plate 16, the first push-rod electric machine 20, the first guide rail 21
With the first sliding block 22, the first guide rail 21 is fixed on locating support 7 vertically, and the first guide rail 21 is fixed by bolted connection
On locating support 7；First sliding block 22 is arranged in the first guide rail 21, and the first sliding block 22 can move down along on the first guide rail 21
It is dynamic；First push-rod electric machine 20 is fixed on the bottom plate 7a of locating support 7, the push rod of the first push-rod electric machine 20 straight down, first
The push rod end of push-rod electric machine 20 is connected with the first sliding block 22, and the upper surface of the first installing plate 16 is connected with the first sliding block 22,
The lower surface of first installing plate 16 is connected with roller 23.
As shown in fig. 6, pushing away at agitating shaft 32 can be pushed to by the material of the side-walls of blending bin 25 by being additionally provided with frame 1
Mechanism is sent, delivery device includes some push pipes 48 and air compressor machine 47, and in the present embodiment, the quantity of push pipe 48 is 12
Root；Some push pipes 48 are located in the side wall of blending bin 25 vertically, and push pipe 48 lower end is blind end, and push pipe 48 upper end is air inlet
End, push pipe 48 are connected by communicating pipe 46 with air compressor machine 47, and air compressor machine 47 is fixed in frame 1；The push sidepiece of pipe 48 is opened
Provided with some venthole 48a, in the present embodiment, venthole 48a quantity is six；Venthole 48a is towards agitating shaft 32.
As shown in Figure 4, Figure 5, moving structure includes drive cylinder 40, movable plate 42, the second sliding block 41 and the second guide rail 34,
Second guide rail 34 is horizontally fixed in blending bin 25, and the second guide rail 34 is fixed in blending bin 25 by bolted connection；
Second sliding block 41 is arranged in the second guide rail 34, and the second sliding block 41 can move back and forth along the second guide rail 34；Drive cylinder 40
Cylinder body is fixed in blending bin 25, and the cylinder body of drive cylinder 40 is fixed in blending bin 25 by bolted connection；Driving
The piston rod end of cylinder 40 is connected with the second sliding block 41, the piston rod end of drive cylinder 40 by bolted connection and
Second sliding block 41 is connected；Movable plate 42 is fixed on the second sliding block 41, and movable plate 42 is fixed on by bolted connection
On two sliding blocks 41；Second push-rod electric machine 43 is fixed on movable plate 42, and the second push-rod electric machine 43 is solid by bolted connection
It is scheduled on movable plate 42.
As shown in figure 4, flow control valve 37 is additionally provided with delivery pipe 36；Peep hole 25b is provided with blending bin 25, is seen
Examine and transparent access panel 31 is provided with the 25b of hole, access panel 31 is organic plates.
As shown in Figure 4, Figure 5, passage 45, the charging of the upper end of passage 45 and suction pipe 29 are additionally provided with suction pipe 29
End is connected, and the lower end of passage 45 can be resisted against the bottom of blending bin 25, using the structure, can be facilitated material by passage 45
It is transported in suction pipe 29, guide effect is good.
As shown in Figure 7, Figure 8, the first elevating mechanism includes the 3rd push-rod electric machine 58, the 3rd sliding block 60 and the 3rd guide rail 59,
3rd guide rail 59 is fixed in frame 1 vertically, and the 3rd guide rail 59 is fixed in frame 1 by bolted connection；3rd slides
Block 60 is arranged in the 3rd guide rail 59, and the 3rd sliding block 60 can move up and down along the 3rd guide rail 59；3rd push-rod electric machine 58 is fixed
In frame 1, the 3rd push-rod electric machine 58 is fixed in frame 1 by bolted connection；The push rod of 3rd push-rod electric machine 58
Straight up, the push rod end of the 3rd push-rod electric machine 58 is connected with the 3rd sliding block 60, and the push rod end of the 3rd push-rod electric machine 58 leads to
Bolted mode is crossed with the 3rd sliding block 60 to be connected；Second installing plate 64 is fixed on the 3rd sliding block 60, the second installing plate 64
It is fixed on by bolted connection on the 3rd sliding block 60.
As shown in Fig. 7, Fig. 9, detent mechanism includes locating ring 54, locating piece 53 and positioning cylinder 52, and locating ring 54 is arranged
And be fixed on the second delivery outlet 56a, positioning cylinder 52 is fixed in frame 1 by support 51, the piston rod of positioning cylinder 52
Towards the second delivery outlet 56a, the piston rod end of positioning cylinder 52 is mutually fixed with locating piece 53, the tailpiece of the piston rod of positioning cylinder 52
Portion is mutually fixed with locating piece 53 by bolted connection；The locating slot to match with locating ring 54 is offered on locating piece 53
53a；In the present embodiment, the quantity of locating piece 53 and positioning cylinder 52 is two.
As shown in figure 9, being provided with rubber strip 67 in locating slot 53a, using the structure, it can be increased by rubber strip 67 and rubbed
Power is wiped, avoids the occurrence of the phenomenon of slip；There is the protuberance of some protrusions, in the present embodiment, protuberance on rubber strip 67
Quantity is 30.
As shown in Figure 7, Figure 8, prompting mechanism is additionally provided with frame 1, prompting mechanism includes travel switch 66, detection bar
57th, alarm bell 50 and PLC 49, alarm bell 50 are fixed in frame 1, and alarm bell 50 is fixed by bolted connection
In frame 1；Travel switch 66 is fixed on the lower surface of the second installing plate 64, and travel switch 66 is fixed by bolted connection
In the lower surface of the second installing plate 64；Detection bar 57 is fixed in frame 1, and detection bar 57 is fixed on by bolted connection
In frame 1；Detection bar 57 can and travel switch 66 be in contact, travel switch 66 and alarm bell 50 with the PLC
49 are connected, in the present embodiment, the controller that PLC 49 can be bought using in the market, controller control row
Cheng Kaiguan, alarm bell and the 3rd magnetic valve program are existing, and its program need not update；3rd magnetic valve 55 and PLC can
Programmable controller 49 is connected, and using the structure, can control the 3rd magnetic valve 55 to obtain electric or lose by PLC 49
Electricity.
As shown in Figure 7, Figure 8, be fixed with some limited posts 61 on the second jolting plate 62, the high position of limited post 61 for 30-
50mm, in the present embodiment, the height of limited post 61 is 40mm, can be to the bottom of finished bag by limited post 61 using the structure
Portion's progress is spacing, avoids finished bag from departing from from the second jolting plate 62, position-limiting action is good.
The operation principle of airslide disintegrating mill is as follows：It will penetrate in locating dowel 13, lead to for the raw material bag edge for depositing raw material
Crossing second spring 15 makes claw 14 and locating support 7 lean, and opens the first delivery pump 4, and the first delivery pump 4 passes through feeding tube 5
By the feedstock transportation in raw material bag into storage tank 3, as the raw material in raw material bag gradually decreases, examined by displacement transducer 10
The distance of raw material in guide portion 5a and material bag is surveyed, signal is passed into controller 24, controller 24 controls the piston of cylinder 12
Bar drive mounting ring 9 move down, mounting ring 9 drive guide portion 5a move down, make guide portion 5a all the time with raw material bag
Raw material contacts；Raw material in storage tank 3 is transported in blending bin 25 by the first communicating pipe, controls the output shaft of stirring motor 33
Agitating shaft 32 is driven to rotate, agitating shaft 32 drives stirring vane 26 to rotate, and push pipe 48 is delivered air to by air compressor machine 47
In, air is exported from venthole 48a, and in the presence of air-flow, the material of the side-walls of blending bin 25 is pushed into agitating shaft 32
Place；Meanwhile the second delivery pump 38 is opened, the modifying agent in liquid reserve tank 39 is transported to spray by the second delivery pump 38 by delivery pipe 36
In mist first 35, modifying agent and raw material is uniformly mixed, when needing to be sampled it, control the piston rod band of drive cylinder 40
Dynamic second sliding block 41 moves back and forth, and the second sliding block 41 drives movable plate 42 to move back and forth, and movable plate 42 drives the second push-rod electric machine
43 move back and forth；The push rod of the second push-rod electric machine 43 is controlled to drive mounting blocks 44 to move down, mounting blocks 44 drive suction pipe 29
Move down, the mixture in blending bin 25 everywhere can be output in case 28 by asepwirator pump 30 by suction pipe 29, can be real
It is existing comprehensive to being sampled in blending bin 25；Raw material in blending bin 25 is transported to material stock tank after crushing by the second communicating pipe
In 56, the edge of finished bag is enclosed on locating ring 54, the piston rod of control positioning cylinder 52 drives locating piece 53 to move, and positions
Block 53 and locating ring 54 are leant, and the edge of finished bag is fixed on the second delivery outlet 56a, passes through PLC
49 the 3rd magnetic valves 55 of control make the second delivery outlet 56a be in open mode；The push rod of the 3rd push-rod electric machine 58 is controlled to drive the
Three sliding blocks 60 move up, and the 3rd sliding block 60 drives the second installing plate 64 to move up, and the second installing plate 64 drives the second vibrations
Plate 62 is moved up, and contacts the bottom of the second jolting plate 62 and finished bag, and the second vibrations are driven by the second vibration motor 63
Plate 62 shakes, and the second jolting plate 62 drives finished bag to produce vibrations, as material gradually increases in finished bag, controls the 3rd push rod
The push rod of motor 58 drives the 3rd sliding block 60 to move gradually downward, and the 3rd sliding block 60 drives the second installing plate 64 to move gradually downward
Dynamic, after material is filled in finished bag, travel switch 66 and detection bar 57 contact, and signal is passed to PLC by travel switch 66 can
Programmable controller 49, PLC 49 make alarm bell 50 send alarm sound；The mixing of raw material and other auxiliary agents can be according to reality
Border needs to select the function.
Specific embodiment described herein is only to spirit explanation for example.Technical field that the present invention belongs to
Technical staff can be made various modifications or supplement to described specific embodiment or be substituted using similar mode, but
Without departing from the spiritual of invention or surmount scope defined in appended claims.
Claims (9)
1. the processing technology of a kind of nanometer of wolframic acid caesium powder, it is characterised in that comprise the following steps：
A, the ammonium metatungstate of reacting dose and cesium nitrate are dissolved in deionized water, above-mentioned solution is dried to obtain powder, then will
Obtained powder is further crushed, so as to obtain tungsten, caesium mixed-powder；
B, tungsten, caesium mixed-powder are added in reactor, and add sorbic acid thereto, in 240-460 DEG C, stirring reaction 4-
6h, the quality of sorbic acid is tungsten, 2-4 times of caesium mixed-powder quality；
C, it will separate through the reaction product in step b, and washed using deionized water, pass through common baking oven afterwards
Dried, drying time 20-30min, crushed after drying using airslide disintegrating mill, obtain a nanometer wolframic acid caesium powder；
Airslide disintegrating mill in the step c includes frame, and feeding device, mixing arrangement are disposed with the frame, crushes dress
Put and packing apparatus, the feeding device include feeding tube, storage tank and the locating support for positioning raw material bag, locating support
It is arranged at storage tank in frame, storage tank lower end has the first delivery outlet, and the first magnetic valve is provided with the first delivery outlet,
Storage tank upper end has first charging aperture, and first charging aperture is connected with feeding tube one end, and the feeding tube other end is positioned at positioning branch
Above frame, and the end has guide portion, is provided with a travel mechanism that guide portion can be driven to move up and down in frame, in feeding tube
It is additionally provided with the first delivery pump；The travel mechanism includes cylinder and mounting ring, and the cylinder body of cylinder is fixed in frame, cylinder
Straight down, the piston rod end of cylinder is connected piston rod by connecting rod with mounting ring, and guide portion is fixed in mounting ring, machine
The controlling organization that cylinder can be controlled to act is additionally provided with frame；The mixing arrangement includes blending bin, fog-spray nozzle and liquid reserve tank, mixes
Mould assembling and liquid reserve tank are each attached in frame, and mixing upper box part has powder input port, and powder input port passes through the first connecting tube
It is connected with the first delivery outlet, mixing lower box part has powder delivery outlet, and second solenoid valve is provided with powder delivery outlet, sprays
Head is arranged in blending bin, and down, the inlet of fog-spray nozzle is connected the liquid outlet of fog-spray nozzle by delivery pipe with liquid reserve tank, defeated
Send and the second delivery pump is provided with pipe, mixing upper box part is additionally provided with agitating shaft, and agitating shaft upper end is connected with stirring motor, stirring
Axle lower end is penetrated in blending bin to be connected with stirring vane, and the draw frame machine that can draw material in blending bin is provided with frame, is inhaled
Mechanism is taken to include suction pipe, the second push-rod electric machine, asepwirator pump, mounting blocks and case, the second push-rod electric machine can drive by one
Its moving structure moved horizontally is arranged in blending bin, the push rod of the second push-rod electric machine straight down, the second push-rod electric machine
Push rod end is mutually fixed with mounting blocks, and the feed end of suction pipe is fixed on mounting blocks, and the feed end is down, and suction pipe goes out
Material end passes blending bin and is located in case, and asepwirator pump is arranged in suction pipe；The packing apparatus includes material stock tank, material stock tank
It is fixed in frame, material stock tank top has the second input port, and the second input port passes through the second connecting tube and powder delivery outlet phase
Connection, material stock tank bottom has the second delivery outlet, the 3rd magnetic valve is provided with the second delivery outlet, and energy is provided with frame will be into
The detent mechanism that product bag edge positions, shock structure is additionally provided with frame, and shock structure includes the second jolting plate, the second shake
Dynamic motor and the second installing plate, the second installing plate can drive its first elevating mechanism moved up and down to be arranged on frame by one
On, the second jolting plate is arranged on the second installing plate, and the second jolting plate is in immediately below the second delivery outlet, the second jolting plate and
There is the 3rd spring, the 3rd spring one end and the second jolting plate lower surface are connected, the 3rd spring other end between second installing plate
It is connected with the second installing plate upper surface, the second vibration motor is fixed on the second jolting plate lower surface.
2. the processing technology of according to claim 1 nanometer of wolframic acid caesium powder, it is characterised in that the controlling organization includes
Displacement transducer, mounting rod and controller, mounting rod one end are connected with mounting ring, the mounting rod other end and displacement transducer phase
Connection, and the induction part of displacement transducer is fixed in frame towards locating support, controller, cylinder and displacement transducer are with being somebody's turn to do
Controller is connected.
3. the processing technology of according to claim 2 nanometer of wolframic acid caesium powder, it is characterised in that the locating support upper end
With the locating dowel that can position raw material bag, locating support lower end has the percussion mechanism that can be shaken to raw material bag, the shake
Motivation structure includes the first jolting plate and the first vibration motor, and the first jolting plate is arranged on the bottom plate of locating support, the first vibrations
There is the first spring, one end of the first spring is mutually fixed with the first jolting plate, the first spring between plate and the bottom plate of locating support
The other end mutually fixed with the bottom plate of locating support, the first vibration motor is fixed on the first jolting plate lower surface.
4. the processing technology of according to claim 3 nanometer of wolframic acid caesium powder, it is characterised in that on the locating support also
Anti-slipping mechanism is provided with, anti-slipping mechanism includes claw and second spring, and claw lower end and locating support are hinged, second spring
One end is connected with claw middle part, and the other end of second spring is connected with locating support, and claw upper end can be resisted against positioning branch
On frame.
5. the processing technology of according to claim 4 nanometer of wolframic acid caesium powder, it is characterised in that on the locating support also
Some rollers are provided with, roller can drive the second elevating mechanism of its oscilaltion to be connected with one；The second elevating mechanism bag
The first installing plate, the first push-rod electric machine, the first guide rail and the first sliding block are included, the first guide rail is fixed on locating support vertically, the
One sliding block is arranged in the first guide rail, and the first push-rod electric machine is fixed on the bottom plate of locating support, the push rod of the first push-rod electric machine
Straight down, the push rod end of the first push-rod electric machine is connected with the first sliding block, the first installing plate upper surface and the first sliding block phase
Connection, the first installing plate lower surface is connected with roller.
6. the processing technology of according to claim 1 nanometer of wolframic acid caesium powder, it is characterised in that also set up in the frame
There is the delivery device that the material of blending bin side-walls can be pushed at agitating shaft, delivery device includes some push pipes and pneumatics
Machine, some push pipes are located in blending bin side wall vertically, and push pipe lower end is blind end, and push pipe upper end is inlet end, push
Pipe is connected by communicating pipe with air compressor machine, pushes tube side part and offers some ventholes, and venthole is towards agitating shaft.
7. the processing technology of according to claim 6 nanometer of wolframic acid caesium powder, it is characterised in that the moving structure includes
Drive cylinder, movable plate, the second sliding block and the second guide rail, the second guide rail are horizontally fixed in blending bin, and the second sliding block is arranged on
In second guide rail, the cylinder body of drive cylinder is fixed in blending bin, and the piston rod end of drive cylinder is connected with the second sliding block, is moved
Dynamic plate is fixed on the second sliding block, and the second push-rod electric machine is fixed on movable plate.
8. the processing technology of according to claim 1 nanometer of wolframic acid caesium powder, it is characterised in that first elevating mechanism
Including the 3rd push-rod electric machine, the 3rd sliding block and the 3rd guide rail, the 3rd guide rail is fixed in frame vertically, and the 3rd sliding block is arranged on
In three guide rails, the 3rd push-rod electric machine is fixed in frame, and straight up, the 3rd push-rod electric machine pushes away the push rod of the 3rd push-rod electric machine
Boom end and the 3rd sliding block are connected, and the second installing plate is fixed on the 3rd sliding block；The detent mechanism includes locating ring, locating piece
And positioning cylinder, locating ring are arranged and be fixed on the second delivery outlet, positioning cylinder is fixed in frame by support, positions gas
The piston rod of cylinder is mutually fixed towards the second delivery outlet, the piston rod end of positioning cylinder with locating piece, offered on locating piece with
The locating slot that locating ring matches.
9. the processing technology of according to claim 8 nanometer of wolframic acid caesium powder, it is characterised in that also set up in the frame
There is prompting mechanism, prompting mechanism includes travel switch, detection bar, alarm bell and PLC, and alarm bell is fixed on frame
On, travel switch is fixed on the second installing plate lower surface, and detection bar is fixed in frame, and detection bar can connect with travel switch
Touch, travel switch and alarm bell are connected with the PLC；3rd magnetic valve and above-mentioned PLC PLC technologies
Device is connected.
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| CN201710442266.5A CN107032403B (en) | 2016-08-16 | 2016-08-16 | The processing technology of improved nanometer wolframic acid caesium powder |
| CN201610675935.9A CN106277058B (en) | 2016-08-16 | 2016-08-16 | A kind of processing technology of nanometer of wolframic acid caesium powder |
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| CN105668633A (en) * | 2016-01-11 | 2016-06-15 | 大连工业大学 | Sea urchin-shaped tungsten bronze particle prepared with template agent and preparation method thereof |
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| CN107032403B (en) | 2018-06-29 |
| CN106277058A (en) | 2017-01-04 |
| CN107032403A (en) | 2017-08-11 |
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