CN106268594A - Stirred autoclave with heat ray filter - Google Patents
Stirred autoclave with heat ray filter Download PDFInfo
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- CN106268594A CN106268594A CN201610884833.8A CN201610884833A CN106268594A CN 106268594 A CN106268594 A CN 106268594A CN 201610884833 A CN201610884833 A CN 201610884833A CN 106268594 A CN106268594 A CN 106268594A
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
- B01J19/20—Stationary reactors having moving elements inside in the form of helices, e.g. screw reactors
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0073—Sealings
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00054—Controlling or regulating the heat exchange system
- B01J2219/00056—Controlling or regulating the heat exchange system involving measured parameters
- B01J2219/00058—Temperature measurement
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00076—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements inside the reactor
- B01J2219/00085—Plates; Jackets; Cylinders
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/0015—Controlling the temperature by thermal insulation means
- B01J2219/00155—Controlling the temperature by thermal insulation means using insulating materials or refractories
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
nullThe present invention relates to stirred autoclave manufacturing technology field，A kind of simple in construction、Easy cleaning、Can be by the stirred autoclave of the heat within reactor kettle with the band heat ray filter of sealing device isolation，It is characterized in that being provided with the circulation cavity being set on shaft，Circulation fluid entrance and circulation fluid outlet is offered on circulation cavity，Direct fluid plate it is provided with in torus body，Circulation cavity bottom is additionally provided with the separate cavities being set on shaft，Separate cavities is the cavity of middle control，Separate cavities is provided with drain plug，Drain plug of the present invention is condensed fluid or the passage of other dirts eliminating，Vertebral body shape is taked in the upper end of passage，It is more convenient for the discharge of liquid，The present invention is compared with prior art，There is simple in construction、Easy cleaning、Can be by the significantly advantage such as the heat within reactor kettle and sealing device isolation.
Description
Technical field
The present invention relates to chemical mechanical equipment technical field, specifically a kind of simple in construction, easy cleaning, can be by
The stirred autoclave of the band heat ray filter that the heat within reactor kettle completely cuts off with sealing device.
Background technology
It is known that reaction temperature, reaction pressure, material concentration, catalyst etc. have different impacts to chemical reaction, certainly
Can fixed reaction be carried out, the size of reaction rate and the difference of product, to the endothermic reaction, when temperature raises, positive reaction speed
Rising, back reaction speed declines, and chemical equilibrium is moved to positive reaction direction, and chemical equilibrium constant raises；Otherwise, positive reaction speed
Declining, back reaction speed rises chemical equilibrium and moves to back reaction direction, and chemical equilibrium constant declines.Exothermic reaction is risen high temperature
Degree, reduces temperature with the endothermic reaction, and exothermic reaction is reduced temperature, rises high-temperature with the endothermic reaction, and it follows Le Chatelier's principle
Reason.
Temperature stabilization in the kettle of reactor is one of necessary factor maintaining chemical reaction, and on the kettle of reactor
Portion's flange will connect sealing device (including magnetic seal, mechanical seal), and the working environment of sealing device (sealing device
Temperature and pressure during operation) need maintain, not so can cause the inefficacy of sealing device, this be accomplished by sealing device per se with
The loop structures such as cooling maintain the working environment of sealing device.But the operating ambient temperature of sealing device and the reaction of reactor
Often there is temperature difference in temperature, the temperature at two so will necessarily be caused to carry out heating power exchange, reaches a balance of temperature,
Prominent is presented with: during A pyroreaction: the temperature in reactor has a declining tendency, need continuous additional heat；Seal dress
The temperature put has the trend of constantly rising, needs to strengthen the intensity of cooling circulation.During B low-temp reaction: the temperature in reactor has
The trend risen, needs constantly to reduce temperature；The temperature of sealing device can constantly reduce, and needing constantly heats up ensures
Sealing device properly functioning, maybe needs to select low temperature resistant circulating liquid, etc..Increase so can to the manufacturer of sealing device
Add design, manufacture difficulty, use unit to strengthen the consumption of the energy to equipment.
Reactor magnetic drive device is dependent on the magnetic of permanent magnet and penetrates the seal closure of nonmagnetic substance, and mutual
Attract reach transmission stirring power and accomplish a kind of device of positive confinement, typically by shaft, inner supporting body, sealing cover body,
Outer support, interior magnetic revolving body, outer magnetic revolving body and adpting flange, bearing composition.Outer magnetic revolving body passes through adpting flange, bearing
Being assembled on outer support, outer magnetic revolving body is made up of materials such as permanent magnets；It is to seal cover body, by non-within outer magnetic revolving body
Magnetic material forms, and sealing cover body can be tightened together with reactor kettle by bolt and gasket seal, accomplishes reactor
Positive confinement；Being interior magnetic revolving body within sealing cover body, interior magnetic revolving body is also made up of materials such as permanent magnets, itself and shaft
Tighten together, by bearing arrangement on inner supporting body.Outer magnetic revolving body, sealing cover body and interior magnetic revolving body keep coaxial,
During work, reductor drives outer magnetic revolving body to rotate, and then passes through revolving body in sealing cover body attracts and rotates, drives shaft to turn
Dynamic, thus realize stirring magnetic drives and the positive confinement of reactor of power.Rotated real by agitator in electric machine rotation to still
It is to complete electric energy to kinetic energy, kinetic energy to magnetic energy, the transition process of magnetic energy to kinetic energy on border.Energy loss is in this process
Inevitably, the most inside and outside magnetic is turned by sealing the mutual cutting magnetic line of cover body, and the energy loss caused, these damage
The energy lost mostly is changed into heat energy, bleeds around, and the duration of runs is the longest, rotating speed is the fastest, the heat energy of generation is the most, these heat
Amount needs cooled, because these heats enough reach the Curie temperature of magnetic steel ingot, makes magnetic steel ingot demagnetize, makes inside and outside magnetic turn
Ineffective.The mode of cooling coil is set up in the many employings of the existing type of cooling in rotating shaft, safeguards inconvenience during using,
And inhomogeneous cooling is even, weak effect.
Summary of the invention
The present invention is directed to the deficiency that prior art exists, it is provided that a kind of simple in construction, easy cleaning, can be by reactor
The stirred autoclave of the band heat ray filter that the heat within kettle completely cuts off with sealing device.
The technical solution adopted for the present invention to solve the technical problems is:
The stirred autoclave of a kind of band heat ray filter, is provided with reactor kettle, it is characterised in that be provided with heat-shield mechanism, described heat insulation
Mechanism includes the circulation cavity being set on shaft, and circulation cavity is offered circulation fluid entrance and circulation fluid outlet, torus
The internal direct fluid plate that is provided with, circulation cavity bottom is additionally provided with the separate cavities being set on shaft, and separate cavities is the chamber of middle control
Body, separate cavities is provided with drain plug；Being additionally provided with high temperature resistant magnetic coupling, described high temperature resistant magnetic coupling is provided with stirring
Axle, inner supporting body, sealing cover body, outer support, interior magnetic revolving body, outer magnetic revolving body and adpting flange, bearing and circulate cold
But mechanism, described cooling body is provided with cyclic water jacket, and cyclic water jacket is arranged between sealing cover body and outer support, described
Cyclic water jacket is provided with A chamber, B chamber, and A chamber does not connects with B chamber, and A chamber is positioned at B intracavity side, and outer magnetic revolving body is through adpting flange and bearing
Being arranged on outer support, outer magnetic revolving body, adpting flange and bearing are respectively positioned in A chamber, and A intracavity filling heat transfer liquids, on A chamber
Being provided with heat transfer liquids air vent, B chamber filling circulating cooling liquid, B chamber is provided with circulation of fluid entrance, circulation of fluid outlet；Also
Being provided with the heat-transfer fluid form for observing A intracavity heat-transfer fluid, heat-transfer fluid form is arranged on A chamber, simultaneously corresponding in B chamber
Position be provided with transparent window；Circulation of fluid entrance on B chamber is positioned at bottom, B chamber, and circulation of fluid outlet is positioned at top, B chamber,
Make the circulating cooling liquid of B intracavity constantly circulate by outer loop pump during using, reduce the temperature of A intracavity heat transfer liquids
Degree, to reach to cool down A chamber and the purpose of internal unit thereof；Dividing plate between A chamber and B chamber uses the sheet material system that heat conductivility is good
Becoming, be additionally provided with cooling controlling organization, described cooling controlling organization includes the circulating cooling liquid temperature that controller is connected with controller
The degree liquid level detection circuit that is connected with controller of testing circuit be connected with controller for controlling circulating cooling liquid stream
The circulating pump control circuit that the flow valve of amount is connected with controller, wherein flow valve is arranged on the pipeline being connected with B chamber
On, temperature sensing circuit is provided with temperature sensor, liquid level detection circuit is provided with liquid level sensor.
The present invention gathers the temperature of circulating cooling liquid during using by temperature sensor, when temperature exceedes threshold
Value, can in time ON cycle pump accelerate circulating cooling liquid circulation, raising cooling effect；And liquid level detection circuit can be real-time
The liquid level data of monitoring circulating cooling liquid, prevents circulating cooling liquid not enough；Cooling controlling organization be additionally provided with respectively with controller phase
Display, input button and the acousto-optic hint circuit connected, it is also possible to be provided with the radio communication circuit being connected with controller,
Radio communication circuit uses GPRS module or gsm module, and the real time remote completing to monitor data sends.
Drain plug of the present invention is condensed fluid or the passage of other dirts eliminating, takes vertebral body in the upper end of passage
Shape, the discharge of liquid of being more convenient for, guide plate is positioned at circulation inside cavity, and circulating liquid is imported and exported and is fixed on heat ray filter
On housing, with circulation cavity UNICOM, form a passage capable of circulation, liquid can be made by the regular fortune of guide plate
OK, use isolated tube connect with on the housing of heat ray filter, with the lower end surface of circulation cavity collectively constitute downside gaseous state every
From chamber, to slow down the exchange of the temperature at reactor kettle upper flange, this can be reduced in isolated tube and the direct gap of torus
The circulation of the gaseous material at place's gaseous material and upper flange, the described circulation upper end of cavity, shaft and heat insulation dress
On the upside of the housing composition put, the separate cavities of gaseous state, slows down the temperature exchange of sealing device, and described drain plug is fixed on heat insulation
On device, it is condensed fluid or the passage of other dirts eliminating, and takes vertebral body shape in the upper end of passage, liquid of being more convenient for
Discharge.
The present invention is further also provided with the oils and fats for preventing from reacting outer material and enters the oils and fats leakage preventing mechanism of reactor, institute
State oils and fats leakage preventing mechanism and be arranged on reactor kettle inner tip, including on the shaft being socketed in reactor connect oil cylinder, connect
Oil cylinder upper end is connected through connecting plate and fixing screw and reactor casing ledge are fixing, is provided with oil retaining umbrella, oil retaining umbrella in connecing oily cylinder
Being fixed by socket on shaft through little round nut, stop washer, briquetting, connect and be provided with oil extraction adapter bottom oil cylinder, oil extraction adapter can
Being got rid of by oils and fats, this device can be used in high-viscosity material reaction, can prevent from polluting because of shaft sealing system leakage oils and fats
Reaction mass, and size adjusting, manufacture can be carried out according to the diameter of axle of shaft.
The present invention compared with prior art, have simple in construction, easy cleaning, can be by the heat within reactor kettle
With the significantly advantage such as sealing device isolation, add cyclic water jacket sealing to cool down between cover body and outer support to strive outside space, make
Cooling space and cyclic water jacket form circulation spacer, solve the drawback of former cooling structure, have the advantages that (1) is followed
Ring cooling medium is spatially separating with internal cooling, decreases owing to the possibility of impurity is brought in circulatory mediator flowing into, particularly has
Magnetizable iron impurities, can be adsorbed by outer magnetic revolving body, jointly operate with it, stays latent to sealing cover body (primary load-carrying members)
In danger；(2) medium that internal cooling space uses makes all running gears be in the lubrication working environment of liquid, it is to avoid
Integral device is made to shut down for adding lubricant to outer magnetic revolving body running gear；(3) avoid owing to circulatory mediator is former simultaneously
Running orbit in structure is uneven, say, that the position cooling down outer magnetic revolving body is uneven, is single Jie inside the present invention
Matter makes outer magnetic revolving body entirety ooze to spread out of in external agency into, even heat, be conducive to the temperature one of outer magnetic revolving body entirety
Causing, cooling is convenient.(4) adnexaes such as the flow-control that can set up thermometric, liquid level, circulatory mediator thereon, make magnetic drives fill
Put one parts being excused from a college course of composition to become a reality.
Accompanying drawing explanation
Accompanying drawing 1 is the structural representation of heat ray filter in the present invention.
Accompanying drawing 2 is heat ray filter and the assembling schematic diagram of reactor kettle in the present invention.
Accompanying drawing 3 is the structural representation of high temperature resistant magnetic coupling in the present invention.
Accompanying drawing 4 is the structural representation of oils and fats leakage preventing mechanism in the present invention.
Reference: the housing 1 of heat ray filter, circulating liquid outlet 2, guide plate 3, circulation cavity 4, drain plug 5, every
From chamber 6, circulating liquid entrance 7, shaft 8, sealing device 9, reactor kettle 10, heat transfer liquids 11, cyclic water jacket 12, outer magnetic
Revolving body 13, outer support 14, sealing cover body 15, circulation spacer adnexa 16, circulation of fluid entrance 17, bearing 18, circulation of fluid
Outlet 19, heat-transfer fluid air vent 20, heat-transfer fluid form 21, anti-connecting plate 22, top board 23, connect oil cylinder cylinder 24, connect oil cylinder
Inner barrel 25, base plate 26, T-shaped jacking block 27, reactor casing ledge 28, holding screw 29, oil extraction adapter 30, oil retaining umbrella 31, little
Round nut 32, stop washer 33, briquetting 34.
Detailed description of the invention
The invention will be further described below in conjunction with the accompanying drawings:
As shown in drawings, the present invention proposes the stirred autoclave of a kind of band heat ray filter, is provided with reactor kettle 10, its feature
Being to be provided with heat-shield mechanism, described heat-shield mechanism includes the circulation cavity 4 being set on shaft, circulation cavity 4 is offered and follows
Ring liquid entrance 7 and circulation fluid outlet 2, be provided with direct fluid plate 3 in circulation cavity 4, circulation cavity 4 bottom is additionally provided with to be set in be stirred
Mixing the separate cavities 6 on axle, separate cavities 6 is the cavity of hollow, and separate cavities 6 is provided with drain plug 5；Also set on reactor kettle 10
High temperature resistant magnetic coupling, described high temperature resistant magnetic coupling is had to include shaft 8, inner supporting body, sealing cover body, outer support
14, interior magnetic revolving body, outer magnetic revolving body 13 and adpting flange, bearing 18 and cooling body, described cooling body
Being provided with cyclic water jacket, cyclic water jacket is arranged between sealing cover body and outer support, and described cyclic water jacket is provided with A chamber, B chamber, A chamber
Not connecting with B chamber, A chamber is positioned at B intracavity side, and outer magnetic revolving body is arranged on outer support through adpting flange and bearing, and outer magnetic returns
Turn, adpting flange and bearing are respectively positioned in A chamber, and A intracavity filling heat transfer liquids 11, A chamber is provided with heat transfer liquids air vent, B
Chamber filling circulating cooling liquid, B chamber is provided with circulation of fluid entrance, circulation of fluid outlet；It is additionally provided with for observing the heat transfer of A intracavity
The heat-transfer fluid form of fluid, heat-transfer fluid form is arranged on A chamber, is provided with transparent window on the position that B chamber is corresponding simultaneously；
Circulation of fluid entrance on B chamber is positioned at bottom, B chamber, and circulation of fluid outlet is positioned at top, B chamber, by outside during using
Circulating pump makes the circulating cooling liquid of B intracavity constantly circulate, and reduces the temperature of A intracavity heat transfer liquids, to reach to cool down A chamber and interior
The purpose of portion's equipment；Dividing plate between A chamber and B chamber uses the sheet material that heat conductivility is good to make, and is additionally provided with cooling controlling organization,
Described cooling controlling organization includes circulating cooling liquid temperature sensing circuit and the controller phase that controller is connected with controller
Flow valve and the controller phase for controlling circulating cooling flow quantity that the liquid level detection circuit connected is connected with controller
The circulating pump control circuit connected, wherein flow valve is arranged on the pipeline being connected with B chamber, is provided with temperature in temperature sensing circuit
Degree sensor, liquid level detection circuit is provided with liquid level sensor.
The present invention gathers the temperature of circulating cooling liquid during using by temperature sensor, when temperature exceedes threshold
Value, can in time ON cycle pump accelerate circulating cooling liquid circulation, raising cooling effect；And liquid level detection circuit can be real-time
The liquid level data of monitoring circulating cooling liquid, prevents circulating cooling liquid not enough；Cooling controlling organization be additionally provided with respectively with controller phase
Display, input button and the acousto-optic hint circuit connected, it is also possible to be provided with the radio communication circuit being connected with controller,
Radio communication circuit uses GPRS module or gsm module, and the real time remote completing to monitor data sends.
Drain plug of the present invention is condensed fluid or the passage of other dirts eliminating, takes vertebral body in the upper end of passage
Shape, the discharge of liquid of being more convenient for, guide plate is positioned at circulation inside cavity, and circulating liquid is imported and exported and is fixed on heat ray filter
On housing, with circulation cavity UNICOM, form a passage capable of circulation, liquid can be made by the regular fortune of guide plate
OK, on the upside of the housing composition of the described circulation upper end of cavity, shaft and heat ray filter, the separate cavities of gaseous state, slows down close
The temperature exchange of seal apparatus, described drain plug is fixed on heat ray filter, is condensed fluid or the passage of other dirts eliminating,
And take vertebral body shape in the upper end of passage, the discharge of liquid of being more convenient for.
The present invention is further also provided with the oils and fats for preventing from reacting outer material and enters the oils and fats leakage preventing mechanism of reactor, institute
State oils and fats leakage preventing mechanism and be arranged on reactor kettle inner tip, including on the shaft being socketed in reactor connect oil cylinder, connect
Oil cylinder upper end is connected through connecting plate and fixing screw are fixing with reactor casing ledge 28, is provided with oil retaining umbrella 31, keeps off in connecing oily cylinder
Oil umbrella 31 is fixed by socket on shaft 8 through little round nut, stop washer 33, briquetting 34, connects and is provided with oil extraction adapter bottom oil cylinder,
Oils and fats can be got rid of by oil extraction adapter, and this device can be used for, in high-viscosity material reaction, can preventing because shaft sealing system leaks
Oils and fats and pollute reaction mass, and size adjusting, manufacture can be carried out according to the diameter of axle of shaft.
The present invention compared with prior art, have simple in construction, easy cleaning, can be by the heat within reactor kettle
With the significantly advantage such as sealing device isolation, add cyclic water jacket sealing to cool down between cover body and outer support to strive outside space, make
Cooling space and cyclic water jacket form circulation spacer, solve the drawback of former cooling structure, have the advantages that (1) is followed
Ring cooling medium is spatially separating with internal cooling, decreases owing to the possibility of impurity is brought in circulatory mediator flowing into, particularly has
Magnetizable iron impurities, can be adsorbed by outer magnetic revolving body, jointly operate with it, stays latent to sealing cover body (primary load-carrying members)
In danger；(2) medium that internal cooling space uses makes all running gears be in the lubrication working environment of liquid, it is to avoid
Integral device is made to shut down for adding lubricant to outer magnetic revolving body running gear；(3) avoid owing to circulatory mediator is former simultaneously
Running orbit in structure is uneven, say, that the position cooling down outer magnetic revolving body is uneven, is single Jie inside the present invention
Matter makes outer magnetic revolving body entirety ooze to spread out of in external agency into, even heat, be conducive to the temperature one of outer magnetic revolving body entirety
Causing, cooling is convenient.(4) adnexaes such as the flow-control that can set up thermometric, liquid level, circulatory mediator thereon, make magnetic drives fill
Put one parts being excused from a college course of composition to become a reality.
Claims (4)
1. a stirred autoclave for band heat ray filter, is provided with reactor kettle, it is characterised in that be provided with heat-shield mechanism, described every
Heat engine structure includes the circulation cavity being set on shaft, and circulation cavity is offered circulation fluid entrance and circulation fluid outlet, circulation
Being provided with direct fluid plate in cavity, circulation cavity bottom is additionally provided with the separate cavities being set on shaft, and separate cavities is middle control
Cavity, separate cavities is provided with drain plug；Being additionally provided with high temperature resistant magnetic coupling, described high temperature resistant magnetic coupling is provided with stirring
Axle, inner supporting body, sealing cover body, outer support, interior magnetic revolving body, outer magnetic revolving body and adpting flange, bearing and circulate cold
But mechanism, described cooling body is provided with cyclic water jacket, and cyclic water jacket is arranged between sealing cover body and outer support, described
Cyclic water jacket is provided with A chamber, B chamber, and A chamber does not connects with B chamber, and A chamber is positioned at B intracavity side, and outer magnetic revolving body is through adpting flange and bearing
Being arranged on outer support, outer magnetic revolving body, adpting flange and bearing are respectively positioned in A chamber, and A intracavity filling heat transfer liquids, on A chamber
Being provided with heat transfer liquids air vent, B chamber filling circulating cooling liquid, B chamber is provided with circulation of fluid entrance, circulation of fluid outlet；Also
Being provided with the heat-transfer fluid form for observing A intracavity heat-transfer fluid, heat-transfer fluid form is arranged on A chamber, simultaneously corresponding in B chamber
Position be provided with transparent window；Circulation of fluid entrance on B chamber is positioned at bottom, B chamber, and circulation of fluid outlet is positioned at top, B chamber,
Make the circulating cooling liquid of B intracavity constantly circulate by outer loop pump during using, reduce the temperature of A intracavity heat transfer liquids
Degree, to reach to cool down A chamber and the purpose of internal unit thereof；Dividing plate between A chamber and B chamber uses the sheet material system that heat conductivility is good
Becoming, be additionally provided with cooling controlling organization, described cooling controlling organization includes the circulating cooling liquid temperature that controller is connected with controller
The degree liquid level detection circuit that is connected with controller of testing circuit be connected with controller for controlling circulating cooling liquid stream
The circulating pump control circuit that the flow valve of amount is connected with controller, wherein flow valve is arranged on the pipeline being connected with B chamber
On, temperature sensing circuit is provided with temperature sensor, liquid level detection circuit is provided with liquid level sensor.
The stirred autoclave of a kind of band heat ray filter the most according to claim 1, it is characterised in that cooling controlling organization is also
It is provided with display, input button and the acousto-optic hint circuit being connected with controller respectively, is additionally provided with and is connected with controller
Radio communication circuit, radio communication circuit uses GPRS module or gsm module, and the real time remote completing to monitor data sends.
The stirred autoclave of a kind of band heat ray filter the most according to claim 1, it is characterised in that described drain plug is
The passage that condensed fluid or other dirts are got rid of, takes vertebral body shape in the upper end of passage, the discharge of liquid of being more convenient for, guide plate
Being positioned at circulation inside cavity, circulating liquid is imported and exported and is fixed on the housing of heat ray filter, and with circulation cavity UNICOM, described follows
On the upside of the housing composition of the upper end of ring cavity body, shaft and heat ray filter, the separate cavities of gaseous state, slows down the temperature of sealing device
Degree exchange, described drain plug is fixed on heat ray filter, is condensed fluid or the passage of other dirts eliminating, and at passage
Vertebral body shape is taked in upper end, the discharge of liquid of being more convenient for.
The stirred autoclave of a kind of band heat ray filter the most according to claim 1, it is characterised in that be additionally provided with for preventing
The oils and fats reacting outer material enters the oils and fats leakage preventing mechanism of reactor, and described oils and fats leakage preventing mechanism is arranged on inside reactor kettle
Top, including connecing oil cylinder on the shaft being socketed in reactor, connects oil cylinder upper end through connecting plate and fixing screw and reactor
Casing ledge is fixing to be connected, and is provided with oil retaining umbrella in connecing oil cylinder, and oil retaining umbrella is fixed by socket through little round nut, stop washer, briquetting
On shaft, connect and bottom oil cylinder, be provided with oil extraction adapter.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610884833.8A CN106268594A (en) | 2016-10-11 | 2016-10-11 | Stirred autoclave with heat ray filter |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610884833.8A CN106268594A (en) | 2016-10-11 | 2016-10-11 | Stirred autoclave with heat ray filter |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106268594A true CN106268594A (en) | 2017-01-04 |
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ID=57717346
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610884833.8A Pending CN106268594A (en) | 2016-10-11 | 2016-10-11 | Stirred autoclave with heat ray filter |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111365460A (en) * | 2020-03-16 | 2020-07-03 | 威海化工机械有限公司 | Magnetic coupling transmission sealing device with efficient heat exchange system |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN200954441Y (en) * | 2006-09-28 | 2007-10-03 | 威海化工机械有限公司 | Magnetic driving device for high-temperature reaction pot |
| CN202860539U (en) * | 2012-11-09 | 2013-04-10 | 北京世纪森朗实验仪器有限公司 | Soft-driving magnetic coupling-stirring high-temperature high-pressure reaction kettle |
| CN202893299U (en) * | 2012-08-20 | 2013-04-24 | 青岛联康油脂制品有限公司 | Mechanical sealing device for reaction kettle tank |
| CN103055768A (en) * | 2012-12-18 | 2013-04-24 | 烟台华阳环保锅炉有限公司 | Self-priming stirrer |
| CN204359104U (en) * | 2014-12-19 | 2015-05-27 | 中山凯旋真空技术工程有限公司 | The mounting structure of vacuum dryer and wherein magnetic fan |
-
2016
- 2016-10-11 CN CN201610884833.8A patent/CN106268594A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN200954441Y (en) * | 2006-09-28 | 2007-10-03 | 威海化工机械有限公司 | Magnetic driving device for high-temperature reaction pot |
| CN202893299U (en) * | 2012-08-20 | 2013-04-24 | 青岛联康油脂制品有限公司 | Mechanical sealing device for reaction kettle tank |
| CN202860539U (en) * | 2012-11-09 | 2013-04-10 | 北京世纪森朗实验仪器有限公司 | Soft-driving magnetic coupling-stirring high-temperature high-pressure reaction kettle |
| CN103055768A (en) * | 2012-12-18 | 2013-04-24 | 烟台华阳环保锅炉有限公司 | Self-priming stirrer |
| CN204359104U (en) * | 2014-12-19 | 2015-05-27 | 中山凯旋真空技术工程有限公司 | The mounting structure of vacuum dryer and wherein magnetic fan |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111365460A (en) * | 2020-03-16 | 2020-07-03 | 威海化工机械有限公司 | Magnetic coupling transmission sealing device with efficient heat exchange system |
| CN111365460B (en) * | 2020-03-16 | 2022-02-08 | 威海化工机械有限公司 | Magnetic coupling transmission sealing device with efficient heat exchange system |
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Application publication date: 20170104 |