CN106268580A - Reactor - Google Patents
Reactor Download PDFInfo
- Publication number
- CN106268580A CN106268580A CN201610662110.3A CN201610662110A CN106268580A CN 106268580 A CN106268580 A CN 106268580A CN 201610662110 A CN201610662110 A CN 201610662110A CN 106268580 A CN106268580 A CN 106268580A
- Authority
- CN
- China
- Prior art keywords
- reactor
- ring
- annular rotor
- kettle
- guide rail
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 230000002349 favourable effect Effects 0.000 claims abstract description 19
- 230000001869 rapid Effects 0.000 claims abstract description 14
- 238000006243 chemical reaction Methods 0.000 abstract description 11
- 238000003756 stirring Methods 0.000 abstract description 7
- 239000000126 substance Substances 0.000 abstract description 6
- 239000000463 material Substances 0.000 abstract description 4
- 230000002262 irrigation Effects 0.000 abstract 1
- 238000003973 irrigation Methods 0.000 abstract 1
- 239000012530 fluid Substances 0.000 description 4
- 239000000376 reactant Substances 0.000 description 4
- 239000013078 crystal Substances 0.000 description 3
- 238000000034 method Methods 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 238000005275 alloying Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000003670 easy-to-clean Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 229960000980 entecavir Drugs 0.000 description 1
- YXPVEXCTPGULBZ-WQYNNSOESA-N entecavir hydrate Chemical compound O.C1=NC=2C(=O)NC(N)=NC=2N1[C@H]1C[C@H](O)[C@@H](CO)C1=C YXPVEXCTPGULBZ-WQYNNSOESA-N 0.000 description 1
- 239000000686 essence Substances 0.000 description 1
- 238000005194 fractionation Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 239000011259 mixed solution Substances 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Mixers Of The Rotary Stirring Type (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Accessories For Mixers (AREA)
Abstract
The invention discloses reactor, the reacting substance solving reactor edge and bottom can not the problem of full and uniform reaction, its drip irrigation device is reactor, the motor rotated including kettle, rotating shaft and drive shaft, also including making a connection in edge, described edge favourable turn includes ring-shaped guide rail, annular rotor and driving means；Annular rotor is concentric with ring-shaped guide rail to be rotationally connected, ring-shaped guide rail fixes kettle medial wall, annular rotor is provided with rapids and disturbs portion, driving means drives annular rotor to rotate, the advantage of this reactor is: the edge favourable turn within reactor can sufficiently stir the material failing fully to react of reactor inward flange, can make to fail the more full and uniform of reacting substance reaction in reactor, be easy to after reaction clean.
Description
Technical field
The present invention relates to a kind of reactor, particularly to a kind of reactor of chemical field.
Background technology
The broad understanding of reactor i.e. has the container physically or chemically reacted, by joining the design of the structure of container with parameter
Put, it is achieved the heating of technological requirement, evaporate, cool down and the mixture function of low high speed, be provided with in it for stirring, accelerate reaction
The stirring paddle carried out.Reaction solution and solid reactant, under the effect of stirring slurry, mix in reactor, react.Generally, meeting
In the kettle of reactor, it is vertically arranged a rotating shaft, rotating shaft is provided with the blade of stirring and carrys out reaction stirred and make it anti-
Should.
But, owing to the position of blade is in the center of kettle, it is difficult to the fluid of kettle sidewall is stirred；And
And, in kettle, fluid vortex direction is single, and the efficiency for mixing can decrease.
In the preparation process of Entecavir, owing to mixed solution is in saturated and semi-saturation state, its internal crystal
Have precipitation process, it is therefore desirable to constantly stirring prevents crystal from separating out, and owing to the edge of reactor lacks liquid flowing, pole
It is easily generated crystal separate out and be attached on medial wall.
Summary of the invention
The goal of the invention of the present invention is can not full and uniform to react to solve the reacting substance at reactor edge and bottom
Problem, it is provided that the reactor of a kind of reacting substance homogeneous reaction that can allow reactor edge and bottom.
In order to realize foregoing invention purpose, present invention employs techniques below scheme:
A kind of reactor, the motor rotated including kettle, rotating shaft and drive shaft, it is characterised in that: also include that edge turns
Machine, edge favourable turn is arranged at kettle medial wall, and edge favourable turn includes ring-shaped guide rail, annular rotor and driving means；Annular turns
Moving part is concentric with ring-shaped guide rail to be rotationally connected, and ring-shaped guide rail fixes kettle medial wall, and annular rotor is provided with rapids and disturbs portion, drives dress
Put driving annular rotor to rotate.
As preferably, described driving means includes motor and for the driver element driving annular rotor to rotate, and drives
Device is fixed on kettle medial wall, and driver element can use friction belt to move annular rotor and rotate, it would however also be possible to employ belt, chain
The various ways annular rotor such as bar, gear rotates.
As preferably, described driver element is gear, and annular rotor is provided with the ring gear engaged with gear.
As preferably, described kettle wall outwardly convex forms the accommodating cavity placed for motor, and motor is fixed on accommodating
In cavity, and motor is waterproof.
As preferably, the described rapids portion of disturbing is lamellar, and it is 0-that rapids disturbs the angle of portion and annular rotor inwall junction
90°。
As preferably, described ring-shaped guide rail is provided with guide groove, and annular rotor includes lead ring, channel configuration in " recessed " shape,
In the form of a ring, lead ring embeds in guide groove lead ring.
As preferably, make a connection at autoclave body bottom in described edge.
Compared with prior art, the invention has the beneficial effects as follows:
One, the edge favourable turn within reactor can be carried out the material failing fully to react of reactor inward flange fully
Stirring, can make to fail the more full and uniform of reacting substance reaction in reactor.
Two, by controlling the rotation direction of edge favourable turn, control rapids and disturb the rotation direction in portion, when rapids disturbs portion and middle part rotating shaft
On blade rotation direction identical time, can quickly make fluid in kettle produce eddy current；When rapids is disturbed in portion and middle part rotating shaft
Blade rotation direction contrary time, blade can be coordinated to upset fluid vortex, form substantial amounts of turbulent flow, accelerate the mixing of material.
Accompanying drawing explanation
The structural representation of Fig. 1: the present invention；
The internal structure diagram of Fig. 2: the present invention；
Fig. 3: favourable turn structural representation in edge in the present invention；
Fig. 4: the fractionation structural representation of edge favourable turn in the present invention；
Fig. 5: the structural representation of edge favourable turn in the present invention；
The top view of the edge favourable turn of Fig. 6: the present invention；
Fig. 7: for A-A sectional view in Fig. 6.
Reference: 1, kettle；2, rotating shaft；3, motor；4, edge favourable turn；5, ring-shaped guide rail；6, annular rotor；7, drive
Dynamic device；8, rapids disturbs portion；9, driver element；10, ring gear；11, guide groove；12, lead ring.
Detailed description of the invention
Below in conjunction with the accompanying drawings the present invention is described further.
A kind of reactor as shown in figures 1 to 6, the motor 3 rotated including kettle 1, rotating shaft 2 and drive shaft, also include limit
Edge favourable turn 4, edge favourable turn 4 is arranged at kettle medial wall, and edge favourable turn 4 includes ring-shaped guide rail 5, annular rotor 6 and drives dress
Put 7；Annular rotor 6 is concentric with ring-shaped guide rail 5 to be rotationally connected, and ring-shaped guide rail 5 fixes kettle 1 medial wall, and annular rotor 4 sets
Having rapids to disturb portion 8, driving means 7 drives annular rotor 6 to rotate.
Ring-shaped guide rail 5 is fixed on kettle 1 inwall preferably uses screw, and annular rotor 6 rotates with rotating shaft 2, the most simultaneously
To on the contrary, reactant so can be made fully to react uniform.
As it is shown on figure 3, driving means 7 includes motor 3 and for the driver element 9 driving annular rotor 4 to rotate, drive
Device 7 is fixed on kettle 1 medial wall, and driving means 7 is connected with screw preferably fixes with screw.
As shown in Figure 4, driver element 9 is preferably gear, and annular rotor 6 is provided with the ring gear 10 engaged with gear, drives
Unit 9 can rotate with the drive annular rotor 6 of steady and continuous.
As it is shown on figure 3, kettle 1 inwall has accommodating cavity, motor 3 to be fixed in the accommodating cavity of projection, so can keep away
Exempt to take reaction compartment or the removing from reaction space inconvenience reactant residual, and motor 3 is waterproof or has additional anti-outside motor 3
The device of water, it is to avoid in reactant, moisture entrance motor 3 causes motor 3 to cause damage.
As shown in Fig. 3 or 5, it is lamellar cube, preferably cuboid alloying metal sheet that described rapids disturbs portion 8, rotates with annular
Part 6 inwall is that angle is 0-90 ° and connects fixing, and preferably 85 °, quantity is multiple, preferably 8, and rapids is disturbed portion 8 and rotated with annular
Part 6 inwall has angle to be to increase rotation whirlpool, so that reaction is more abundant.
As shown in Fig. 4 or 7, ring-shaped guide rail 5 has guide groove 11, annular rotor 6 to include lead ring 12, guide groove 11 shape in
" recessed " shape, lead ring 12 shape ringwise, lead ring 12 embeds in guide groove 11, and mounting means preferably uses screw from annular rotor 6 inwall
It is connected fixing with lead ring 12, the most easy for installation, and be easy to clean.
Edge favourable turn 4 is bottom kettle 1, owing to fixing precipitate is deposited on bottom, and when reactor does not fills, and can
So that material unreacted bottom kettle 1 is stirred.
The foregoing is only presently preferred embodiments of the present invention, not in order to limit the present invention, all essences in the present invention
Any amendment, equivalent and the improvement etc. made within god and principle, should be included within the scope of the present invention.
Claims (7)
1. reactor, the motor (3) rotated including kettle (1), rotating shaft (2) and drive shaft, it is characterised in that: also include edge
Favourable turn (4), edge favourable turn (4) is arranged at kettle medial wall, and edge favourable turn (4) includes ring-shaped guide rail (5), annular rotor (6)
With driving means (7)；Annular rotor (6) is concentric with ring-shaped guide rail (5) to be rotationally connected, in the fixing kettle (1) of ring-shaped guide rail (5)
Sidewall, annular rotor (4) is provided with rapids and disturbs portion (8), and driving means (7) drives annular rotor (6) to rotate.
Reactor the most according to claim 1, it is characterised in that: driving means (7) includes motor (3) and is used for driving ring
The driver element (9) that shape tumbler (6) rotates, driving means (7) is fixed on kettle (1) medial wall.
Reactor the most according to claim 2, it is characterised in that: driver element (9) is gear, and annular rotor (6) sets
There is the ring gear (10) engaged with gear.
Reactor the most according to claim 2, it is characterised in that: kettle (1) wall outwardly convex is formed places for motor
Accommodating cavity, motor (3) is fixed in accommodating cavity, and motor (3) is waterproof.
Reactor the most according to claim 1, it is characterised in that: it is lamellar that described rapids disturbs portion (8), and rapids disturbs portion (8) and ring
The angle of shape tumbler (6) inwall junction is 0-90 °.
Reactor the most according to claim 1, it is characterised in that: ring-shaped guide rail (5) is provided with guide groove (11), annular rotor
(6) including lead ring (12), guide groove (11) shape is in " recessed " shape, and in the form of a ring, lead ring (12) embeds in guide groove (11) lead ring (12).
Reactor the most according to claim 1, it is characterised in that: edge favourable turn (4) is in kettle (1) bottom.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610662110.3A CN106268580B (en) | 2016-08-12 | 2016-08-12 | Reaction kettle |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610662110.3A CN106268580B (en) | 2016-08-12 | 2016-08-12 | Reaction kettle |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN106268580A true CN106268580A (en) | 2017-01-04 |
| CN106268580B CN106268580B (en) | 2018-06-08 |
Family
ID=57668994
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610662110.3A Active CN106268580B (en) | 2016-08-12 | 2016-08-12 | Reaction kettle |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106268580B (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110898783A (en) * | 2019-11-15 | 2020-03-24 | 江苏隆昌化工有限公司 | Preparation method of inorganic layered supramolecular material |
| CN115228412A (en) * | 2022-06-23 | 2022-10-25 | 彭秀明 | Reation kettle with separation work ability |
| CN115501787A (en) * | 2022-11-04 | 2022-12-23 | 烟台科达化工有限公司 | A high-efficient cauldron that mixes in advance for pesticide preparation processing |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN202638377U (en) * | 2012-07-06 | 2013-01-02 | 浙江长江搅拌设备有限公司 | Folding agitator |
| CN103721800A (en) * | 2014-01-10 | 2014-04-16 | 中信重工机械股份有限公司 | Spiral stirrer of vertical type spiral stirring grind |
| CN104307401A (en) * | 2014-11-12 | 2015-01-28 | 重庆市腾瀚工贸有限公司 | Mechanical turbulent mixer |
| CN205925696U (en) * | 2016-08-12 | 2017-02-08 | 胡海潮 | Reaction kettle |
-
2016
- 2016-08-12 CN CN201610662110.3A patent/CN106268580B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN202638377U (en) * | 2012-07-06 | 2013-01-02 | 浙江长江搅拌设备有限公司 | Folding agitator |
| CN103721800A (en) * | 2014-01-10 | 2014-04-16 | 中信重工机械股份有限公司 | Spiral stirrer of vertical type spiral stirring grind |
| CN104307401A (en) * | 2014-11-12 | 2015-01-28 | 重庆市腾瀚工贸有限公司 | Mechanical turbulent mixer |
| CN205925696U (en) * | 2016-08-12 | 2017-02-08 | 胡海潮 | Reaction kettle |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110898783A (en) * | 2019-11-15 | 2020-03-24 | 江苏隆昌化工有限公司 | Preparation method of inorganic layered supramolecular material |
| CN115228412A (en) * | 2022-06-23 | 2022-10-25 | 彭秀明 | Reation kettle with separation work ability |
| CN115501787A (en) * | 2022-11-04 | 2022-12-23 | 烟台科达化工有限公司 | A high-efficient cauldron that mixes in advance for pesticide preparation processing |
| CN115501787B (en) * | 2022-11-04 | 2023-10-24 | 烟台科达化工有限公司 | A high-efficient cauldron that mixes in advance for pesticide preparation processing |
Also Published As
| Publication number | Publication date |
|---|---|
| CN106268580B (en) | 2018-06-08 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| TA01 | Transfer of patent application right | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20180504 Address after: 201500 2-7, 366 Hai Jin Road, Jinshan Town, Jinshan District, Shanghai Applicant after: SHANGHAI XINXIN CHEMICAL Co.,Ltd. Address before: 325300 Zhoucun three hundred Lane 17, Dazhen Town, Wencheng County, Wenzhou, Zhejiang Applicant before: Hu Haichao |
|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Reaction kettle Effective date of registration: 20231020 Granted publication date: 20180608 Pledgee: Shanghai Rural Commercial Bank Co.,Ltd. Jinshan sub branch Pledgor: SHANGHAI XINXIN CHEMICAL Co.,Ltd. Registration number: Y2023310000664 |