CN106268571A - Stabilizer is with many stirring mode reation kettle - Google Patents
Stabilizer is with many stirring mode reation kettle Download PDFInfo
- Publication number
- CN106268571A CN106268571A CN201610713345.0A CN201610713345A CN106268571A CN 106268571 A CN106268571 A CN 106268571A CN 201610713345 A CN201610713345 A CN 201610713345A CN 106268571 A CN106268571 A CN 106268571A
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- reactor
- shaft
- stirring
- stabilizer
- stirring device
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- 238000003756 stirring Methods 0.000 title claims abstract description 37
- 239000003381 stabilizer Substances 0.000 title claims abstract description 14
- 238000006243 chemical reaction Methods 0.000 claims abstract description 24
- 239000000463 material Substances 0.000 claims abstract description 23
- 238000010907 mechanical stirring Methods 0.000 claims abstract description 17
- 238000007599 discharging Methods 0.000 claims abstract description 4
- 229910001220 stainless steel Inorganic materials 0.000 claims description 4
- 239000010935 stainless steel Substances 0.000 claims description 4
- 229910010293 ceramic material Inorganic materials 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 3
- 239000000178 monomer Substances 0.000 abstract description 6
- 229920000642 polymer Polymers 0.000 abstract description 6
- 238000013016 damping Methods 0.000 abstract description 4
- 239000000203 mixture Substances 0.000 abstract description 4
- 238000005204 segregation Methods 0.000 abstract description 3
- 238000010521 absorption reaction Methods 0.000 abstract 1
- 239000003638 chemical reducing agent Substances 0.000 abstract 1
- 230000035939 shock Effects 0.000 abstract 1
- 239000000376 reactant Substances 0.000 description 5
- 239000002994 raw material Substances 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical class [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 239000003513 alkali Substances 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 238000003486 chemical etching Methods 0.000 description 2
- 230000003628 erosive effect Effects 0.000 description 2
- 229920002521 macromolecule Polymers 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 238000001311 chemical methods and process Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000004070 electrodeposition Methods 0.000 description 1
- 230000001804 emulsifying effect Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 238000002372 labelling Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
- B01J19/10—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing sonic or ultrasonic vibrations
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F31/00—Mixers with shaking, oscillating, or vibrating mechanisms
- B01F31/80—Mixing by means of high-frequency vibrations above one kHz, e.g. ultrasonic vibrations
- B01F31/83—Mixing by means of high-frequency vibrations above one kHz, e.g. ultrasonic vibrations comprising a supplementary stirring element
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0066—Stirrers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/02—Apparatus characterised by being constructed of material selected for its chemically-resistant properties
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/02—Apparatus characterised by their chemically-resistant properties
- B01J2219/025—Apparatus characterised by their chemically-resistant properties characterised by the construction materials of the reactor vessel proper
- B01J2219/0263—Ceramic
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/02—Apparatus characterised by their chemically-resistant properties
- B01J2219/025—Apparatus characterised by their chemically-resistant properties characterised by the construction materials of the reactor vessel proper
- B01J2219/0277—Metal based
- B01J2219/0286—Steel
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/02—Apparatus characterised by their chemically-resistant properties
- B01J2219/025—Apparatus characterised by their chemically-resistant properties characterised by the construction materials of the reactor vessel proper
- B01J2219/0295—Synthetic organic materials
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The invention discloses a multi-stirring-mode reaction kettle for a stabilizer, which comprises a reaction kettle body, a stirring device and a motor, wherein a feeding hole is formed in the top end of the reaction kettle body, and a discharging hole is formed in the bottom end of the reaction kettle body; the stirring device comprises a mechanical stirring device, an ultrasonic wave generating device and a vibration stirring device; spring columns are arranged on the periphery of the lower side of the reaction kettle main body, supporting legs are arranged at the bottom ends of the spring columns, and shock absorption pads are arranged on the lower sides of the supporting legs; the stirring shaft is connected with the reaction kettle body through a speed reducer. This reation kettle is equipped with mechanical stirring device, ultrasonic wave generating device and vibration agitating unit, can realize the conversion and the synergism of multiple stirring mode, makes the material reach abundant mixture. For the multi-monomer reaction of some polymers, monomer segregation can be avoided by combining a plurality of stirring modes, and the product quality is improved. The damping device that reation kettle main part downside set up can weaken vibrations, noise reduction when carrying out machinery, vibrations stirring.
Description
Technical field
The present invention relates to a kind of chemical industry reactor, be specifically related to a kind of stabilizer many stir modes reactor.
Background technology
Reactor is through commonly used plant equipment in Chemical Manufacture, is production equipment important in chemical process, is used for
Material is reacted.As the preparation of the reaction of polymer, plastic formulation, additive etc. is required for using reactor, thus
Material in reactor is disperseed, emulsifying, mix or dissolve, the process such as stirring.Existing reactor, in reactor
Conventional single mechanical agitator, can only make the Flow of Goods and Materials of a reactor part, material when there is material undercompounding, work
Stirring uneven, chemical reaction is it would appear that react uneven, and unreacted material mixes with reactant and coexists, and have impact on reaction
The using effect of still.And reactor is mostly cylindrical, bottom is semicircle, bottom traditional agitating device and reactor
Gap-ratio is relatively big, and result causes the material of bottom to be not easy to be stirred to, and a part of electrodeposition substance can be made in bottom, cause material
Can not sufficiently disperse or react.Meanwhile, in existing reactor course of reaction, vibrations are big, it is impossible to meet the need of modern production
Ask.
Summary of the invention
The technical problem to be solved is that the existing agitating device of reactor can not fully make in material mixing, course of reaction
Vibrations are big, it is therefore intended that provide a kind of stabilizer many stir modes reactor, material reaction process in reactor can be made abundant
Carry out.
The present invention is achieved through the following technical solutions:
A kind of stabilizer many stir modes reactor, including reactor body, agitating device, motor, described reactor body
Top is provided with charging aperture, and reactor body bottom is provided with discharging opening, it is characterised in that:
Described agitating device includes mechanical stirring device, ultrasonic generator and vibrations agitating device;
Ultrasonic generator is located at reactor bodies top;
Described vibration stirring device is located at reactor body side;
On the downside of described reactor main body, surrounding is designed with spring stack, and each spring stack bottom is designed with a spike, each spike
Downside is designed with cushion;
Described mechanical stirring device includes shaft and the paddle being connected on shaft;
One end of described shaft is stretched out reactor bodies top and is connected with motor;
Described paddle comprises 4 semicircular arc puddlers being connected in turn on shaft, the two-end-point of puddler circular arc with
Shaft is connected, in 180 ° of angles between two adjacent puddlers;
Described paddle also includes a cross bar, and cross bar is positioned at below puddler, is connected with shaft end;
Described cross bar is circular arc, and the midpoint of circular arc cross bar is connected with shaft, and the two-end-point of circular arc is upward;
Described shaft is connected with reactor body by reductor.
This reactor is provided with mechanical stirring device, it is possible to realize the stirring of whole reactor, can not only be sufficiently stirred for bottom
Material, with arrange vibration stirring device synergism, vibrations stirring operationally produce vibrations, shaking force makes between material
Scattered more uniform;The reaction of monomer-polymers many for some macromolecule, re-uses ultrasonic generator, uses simultaneously
Three kinds of alr modes, the most dispersed polymer monomer, it is possible to avoid certain monomer that segregation occurs in course of reaction, carry
The quality of high product.Meanwhile, the damping device arranged on the downside of reactor main body can weaken when carrying out machinery, vibrations stirring
Vibrations, the structure of firm reactor, reduces noise.
Described agitating device and reactor body are stainless steel, ceramic material, the one of PP material.Stainless steel
It is capable of withstanding the chemical etching dielectric corrosions such as the weak corrosive medium such as air, steam, water and acid, alkali, salt, it is adaptable to raw material has corruption
The reaction of erosion medium.Pottery and the reaction being then applicable to without raw materials such as soda acids of PP material, and material is light.
Described reactor body is hemispherical for cylindric and bottom.Cylindrical shape can realize bigger reactant accumulated amount simultaneously
Floor space is less;And the hemispherical discharge being conducive to reactant in bottom.
Described reductor is connected with reactor body by bolt.So it is capable of the dismounting of reductor and bolt.
Described mechanical stirring device can arrange multiple.Can be real in multiple mechanical stirring devices are separately positioned on reactor
Existing larger range of stirring.
The present invention compared with prior art, has such advantages as and beneficial effect:
1, one stabilizer many stir modes reactor of the present invention, is provided with mechanical stirring device, ultrasonic generator and shakes
Dynamic agitating device, it is possible to realize conversion and the synergism of multiple alr mode, make material reach sufficiently and mix;
2, one stabilizer many stir modes reactor of the present invention, the damping device of setting can carry out machinery, shake and stir
When mixing, weaken vibrations, reduce noise.
Accompanying drawing explanation
Accompanying drawing described herein is used for providing being further appreciated by the embodiment of the present invention, constitutes of the application
Point, it is not intended that the restriction to the embodiment of the present invention.In the accompanying drawings:
Fig. 1 is present configuration schematic diagram.
The parts title of labelling and correspondence in accompanying drawing:
1-reactor body, 2-mechanical stirring device, 3-motor, 4-ultrasonic generator, 5-shakes agitating device, 6-spring
Post, 7-props up spike, 8-cushion, 9-reductor.
Detailed description of the invention
For making the object, technical solutions and advantages of the present invention clearer, below in conjunction with embodiment and accompanying drawing, to this
Invention is described in further detail, and the exemplary embodiment of the present invention and explanation thereof are only used for explaining the present invention, do not make
For limitation of the invention.
Embodiment 1
As it can be seen, one stabilizer many stir modes reactor of the present invention, including reactor body 1, agitating device, motor
3, described reactor body top is provided with charging aperture, and reactor body bottom is provided with discharging opening;
Described agitating device includes mechanical stirring device 2, ultrasonic generator 4 and vibrations agitating device 5;
Ultrasonic generator is located at reactor bodies top;
Described vibration stirring device is located at reactor body side;
On the downside of described reactor main body, surrounding is designed with spring stack 6, and each spring stack bottom is designed with a spike 7, each support
Side, underfooting is designed with cushion 8;
Described mechanical stirring device includes shaft and the paddle being connected on shaft;
One end of described shaft is stretched out reactor bodies top and is connected with motor;
Described paddle comprises 4 semicircular arc puddlers being connected in turn on shaft, the two-end-point of puddler circular arc with
Shaft is connected, in 180 ° of angles between two adjacent puddlers;
Described paddle also includes a cross bar, and cross bar is positioned at below puddler, is connected with shaft end;
Described cross bar is circular arc, and the midpoint of circular arc cross bar is connected with shaft, and the two-end-point of circular arc is upward;
Described shaft is connected with reactor body by reductor 9.
This reactor is provided with mechanical stirring device, it is possible to realize the stirring of whole reactor, can not only be sufficiently stirred for bottom
Material, with arrange vibration stirring device synergism, vibrations stirring operationally produce vibrations, shaking force makes between material
Scattered more uniform;The reaction of monomer-polymers many for some macromolecule, re-uses ultrasonic generator, uses simultaneously
Three kinds of alr modes, the most dispersed polymer monomer, it is possible to avoid certain monomer that segregation occurs in course of reaction, carry
The quality of high product.Meanwhile, the damping device arranged on the downside of reactor main body can weaken when carrying out machinery, vibrations stirring
Vibrations, the structure of firm reactor, reduces noise.
Embodiment 2
On the basis of above-described embodiment, described agitating device 2 is stainless steel, ceramic material, PP with reactor body 1
The one of material.It is rotten that rustless steel matter is capable of withstanding the chemical etching media such as the weak corrosive medium such as air, steam, water and acid, alkali, salt
Erosion, it is adaptable to have the reaction of corrosive medium in raw material.Pottery and the reaction being then applicable to without raw materials such as soda acids of PP material,
And material is light.
Embodiment 3
On the basis of above-described embodiment, described reactor body 1 is hemispherical for cylindric and bottom.Cylindrical shape can realize relatively
Big reactant accumulated amount floor space simultaneously is less;And the hemispherical discharge being conducive to reactant in bottom.
Embodiment 4
On the basis of above-described embodiment, described reductor 8 is connected with reactor body 1 by bolt.So it is capable of
Reductor and the dismounting of bolt.
Embodiment 5
On the basis of above-described embodiment, described mechanical stirring device 2 can arrange multiple.By multiple mechanical stirring devices respectively
Larger range of stirring can be realized in being arranged on reactor.
Above-described detailed description of the invention, has been carried out the purpose of the present invention, technical scheme and beneficial effect further
Describe in detail, be it should be understood that the detailed description of the invention that the foregoing is only the present invention, be not intended to limit the present invention
Protection domain, all within the spirit and principles in the present invention, any modification, equivalent substitution and improvement etc. done, all should comprise
Within protection scope of the present invention.
Claims (5)
1. stabilizer many stir modes reactor, including reactor body (1), agitating device, motor (3), described instead
Answering still body (1) top to be provided with charging aperture, reactor body bottom is provided with discharging opening, it is characterised in that:
Described agitating device includes mechanical stirring device (2), ultrasonic generator (4) and vibrations agitating device (5);
Ultrasonic generator (4) is located at reactor body (1) top;
Described vibration stirring device (5) is located at reactor body (1) sidepiece;
On the downside of described reactor main body, surrounding is designed with spring stack (6), and each spring stack bottom is designed with a spike (7), each
Support side, underfooting and be designed with cushion (8);
Described mechanical stirring device includes shaft and the paddle being connected on shaft;
One end of described shaft is stretched out reactor body (1) top and is connected with motor (3);
Described paddle comprises 4 semicircular arc puddlers being connected in turn on shaft, the two-end-point of puddler circular arc with
Shaft is connected, in 180 ° of angles between two adjacent puddlers;
Described paddle also includes a cross bar, and cross bar is positioned at below puddler, is connected with shaft end;
Described cross bar is circular arc, and the midpoint of circular arc cross bar is connected with shaft, and the two-end-point of circular arc is upward;
Described shaft is connected with reactor body (1) by reductor (9).
A kind of stabilizer many stir modes reactor the most according to claim 1, it is characterised in that: described machinery stirs
Mixing device (2) with reactor body (1) is stainless steel, ceramic material, the one of PP material.
A kind of stabilizer many stir modes reactor the most according to claim 1 and 2, it is characterised in that: described reaction
Still body (1) is hemispherical for cylindric and bottom.
A kind of stabilizer many stir modes reactor the most according to claim 3, it is characterised in that: described reductor
(9) it is connected with reactor body (1) by bolt.
5. according to the arbitrary described a kind of stabilizer many stir modes reactor of claim 1,2 or 4, it is characterised in that: institute
State mechanical stirring device (2) and can arrange multiple.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201610713345.0A CN106268571A (en) | 2016-08-24 | 2016-08-24 | Stabilizer is with many stirring mode reation kettle |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
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CN201610713345.0A CN106268571A (en) | 2016-08-24 | 2016-08-24 | Stabilizer is with many stirring mode reation kettle |
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CN106268571A true CN106268571A (en) | 2017-01-04 |
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CN201610713345.0A Pending CN106268571A (en) | 2016-08-24 | 2016-08-24 | Stabilizer is with many stirring mode reation kettle |
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107159035A (en) * | 2017-07-07 | 2017-09-15 | 刘艳芹 | A kind of clinical laboratory is mixed and shakes device automatically with Multifunction blood |
CN108034553A (en) * | 2018-02-09 | 2018-05-15 | 福建福清兴龙酒业有限公司 | A kind of wine brewing steaming plant |
CN108413827A (en) * | 2018-03-14 | 2018-08-17 | 安徽理工大学 | A kind of the destruction retracting device and method of waste emulsified explosive |
CN113477147A (en) * | 2021-05-31 | 2021-10-08 | 南京航空航天大学 | Ultrasonic mixer for tungsten-based nano composite powder |
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US5674956A (en) * | 1989-02-03 | 1997-10-07 | Hitachi, Ltd. | Method for producing high viscosity materials |
CN204933363U (en) * | 2015-07-09 | 2016-01-06 | 芜湖市恒峰科技有限公司 | A kind of new and effective agitating device |
CN205216836U (en) * | 2015-11-27 | 2016-05-11 | 战立启 | High -efficient simplification worker reation kettle |
CN206027690U (en) * | 2016-08-24 | 2017-03-22 | 成都米特瑞新材料科技有限公司 | Damping reaction kettle capable of realizing conversion of multiple stirring modes |
-
2016
- 2016-08-24 CN CN201610713345.0A patent/CN106268571A/en active Pending
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5674956A (en) * | 1989-02-03 | 1997-10-07 | Hitachi, Ltd. | Method for producing high viscosity materials |
CN204933363U (en) * | 2015-07-09 | 2016-01-06 | 芜湖市恒峰科技有限公司 | A kind of new and effective agitating device |
CN205216836U (en) * | 2015-11-27 | 2016-05-11 | 战立启 | High -efficient simplification worker reation kettle |
CN206027690U (en) * | 2016-08-24 | 2017-03-22 | 成都米特瑞新材料科技有限公司 | Damping reaction kettle capable of realizing conversion of multiple stirring modes |
Non-Patent Citations (1)
Title |
---|
李青山等: "《药学基本实验技术》", 31 August 2006 * |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107159035A (en) * | 2017-07-07 | 2017-09-15 | 刘艳芹 | A kind of clinical laboratory is mixed and shakes device automatically with Multifunction blood |
CN108034553A (en) * | 2018-02-09 | 2018-05-15 | 福建福清兴龙酒业有限公司 | A kind of wine brewing steaming plant |
CN108413827A (en) * | 2018-03-14 | 2018-08-17 | 安徽理工大学 | A kind of the destruction retracting device and method of waste emulsified explosive |
CN113477147A (en) * | 2021-05-31 | 2021-10-08 | 南京航空航天大学 | Ultrasonic mixer for tungsten-based nano composite powder |
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