CN106268571A - Stabilizer is with many stirring mode reation kettle - Google Patents

Stabilizer is with many stirring mode reation kettle Download PDF

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Publication number
CN106268571A
CN106268571A CN201610713345.0A CN201610713345A CN106268571A CN 106268571 A CN106268571 A CN 106268571A CN 201610713345 A CN201610713345 A CN 201610713345A CN 106268571 A CN106268571 A CN 106268571A
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CN
China
Prior art keywords
reactor
shaft
stirring
stabilizer
stirring device
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610713345.0A
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Chinese (zh)
Inventor
倪玉英
包黎霞
倪念英
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Chengdu Miterui New Material Technology Co ltd
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Chengdu Miterui New Material Technology Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chengdu Miterui New Material Technology Co ltd filed Critical Chengdu Miterui New Material Technology Co ltd
Priority to CN201610713345.0A priority Critical patent/CN106268571A/en
Publication of CN106268571A publication Critical patent/CN106268571A/en
Pending legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/08Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J19/10Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing sonic or ultrasonic vibrations
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F31/00Mixers with shaking, oscillating, or vibrating mechanisms
    • B01F31/80Mixing by means of high-frequency vibrations above one kHz, e.g. ultrasonic vibrations
    • B01F31/83Mixing by means of high-frequency vibrations above one kHz, e.g. ultrasonic vibrations comprising a supplementary stirring element
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/0066Stirrers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/02Apparatus characterised by being constructed of material selected for its chemically-resistant properties
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/02Apparatus characterised by their chemically-resistant properties
    • B01J2219/025Apparatus characterised by their chemically-resistant properties characterised by the construction materials of the reactor vessel proper
    • B01J2219/0263Ceramic
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/02Apparatus characterised by their chemically-resistant properties
    • B01J2219/025Apparatus characterised by their chemically-resistant properties characterised by the construction materials of the reactor vessel proper
    • B01J2219/0277Metal based
    • B01J2219/0286Steel
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/02Apparatus characterised by their chemically-resistant properties
    • B01J2219/025Apparatus characterised by their chemically-resistant properties characterised by the construction materials of the reactor vessel proper
    • B01J2219/0295Synthetic organic materials

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

The invention discloses a multi-stirring-mode reaction kettle for a stabilizer, which comprises a reaction kettle body, a stirring device and a motor, wherein a feeding hole is formed in the top end of the reaction kettle body, and a discharging hole is formed in the bottom end of the reaction kettle body; the stirring device comprises a mechanical stirring device, an ultrasonic wave generating device and a vibration stirring device; spring columns are arranged on the periphery of the lower side of the reaction kettle main body, supporting legs are arranged at the bottom ends of the spring columns, and shock absorption pads are arranged on the lower sides of the supporting legs; the stirring shaft is connected with the reaction kettle body through a speed reducer. This reation kettle is equipped with mechanical stirring device, ultrasonic wave generating device and vibration agitating unit, can realize the conversion and the synergism of multiple stirring mode, makes the material reach abundant mixture. For the multi-monomer reaction of some polymers, monomer segregation can be avoided by combining a plurality of stirring modes, and the product quality is improved. The damping device that reation kettle main part downside set up can weaken vibrations, noise reduction when carrying out machinery, vibrations stirring.

Description

A kind of stabilizer many stir modes reactor
Technical field
The present invention relates to a kind of chemical industry reactor, be specifically related to a kind of stabilizer many stir modes reactor.
Background technology
Reactor is through commonly used plant equipment in Chemical Manufacture, is production equipment important in chemical process, is used for Material is reacted.As the preparation of the reaction of polymer, plastic formulation, additive etc. is required for using reactor, thus Material in reactor is disperseed, emulsifying, mix or dissolve, the process such as stirring.Existing reactor, in reactor Conventional single mechanical agitator, can only make the Flow of Goods and Materials of a reactor part, material when there is material undercompounding, work Stirring uneven, chemical reaction is it would appear that react uneven, and unreacted material mixes with reactant and coexists, and have impact on reaction The using effect of still.And reactor is mostly cylindrical, bottom is semicircle, bottom traditional agitating device and reactor Gap-ratio is relatively big, and result causes the material of bottom to be not easy to be stirred to, and a part of electrodeposition substance can be made in bottom, cause material Can not sufficiently disperse or react.Meanwhile, in existing reactor course of reaction, vibrations are big, it is impossible to meet the need of modern production Ask.
Summary of the invention
The technical problem to be solved is that the existing agitating device of reactor can not fully make in material mixing, course of reaction Vibrations are big, it is therefore intended that provide a kind of stabilizer many stir modes reactor, material reaction process in reactor can be made abundant Carry out.
The present invention is achieved through the following technical solutions:
A kind of stabilizer many stir modes reactor, including reactor body, agitating device, motor, described reactor body Top is provided with charging aperture, and reactor body bottom is provided with discharging opening, it is characterised in that:
Described agitating device includes mechanical stirring device, ultrasonic generator and vibrations agitating device;
Ultrasonic generator is located at reactor bodies top;
Described vibration stirring device is located at reactor body side;
On the downside of described reactor main body, surrounding is designed with spring stack, and each spring stack bottom is designed with a spike, each spike Downside is designed with cushion;
Described mechanical stirring device includes shaft and the paddle being connected on shaft;
One end of described shaft is stretched out reactor bodies top and is connected with motor;
Described paddle comprises 4 semicircular arc puddlers being connected in turn on shaft, the two-end-point of puddler circular arc with Shaft is connected, in 180 ° of angles between two adjacent puddlers;
Described paddle also includes a cross bar, and cross bar is positioned at below puddler, is connected with shaft end;
Described cross bar is circular arc, and the midpoint of circular arc cross bar is connected with shaft, and the two-end-point of circular arc is upward;
Described shaft is connected with reactor body by reductor.
This reactor is provided with mechanical stirring device, it is possible to realize the stirring of whole reactor, can not only be sufficiently stirred for bottom Material, with arrange vibration stirring device synergism, vibrations stirring operationally produce vibrations, shaking force makes between material Scattered more uniform;The reaction of monomer-polymers many for some macromolecule, re-uses ultrasonic generator, uses simultaneously Three kinds of alr modes, the most dispersed polymer monomer, it is possible to avoid certain monomer that segregation occurs in course of reaction, carry The quality of high product.Meanwhile, the damping device arranged on the downside of reactor main body can weaken when carrying out machinery, vibrations stirring Vibrations, the structure of firm reactor, reduces noise.
Described agitating device and reactor body are stainless steel, ceramic material, the one of PP material.Stainless steel It is capable of withstanding the chemical etching dielectric corrosions such as the weak corrosive medium such as air, steam, water and acid, alkali, salt, it is adaptable to raw material has corruption The reaction of erosion medium.Pottery and the reaction being then applicable to without raw materials such as soda acids of PP material, and material is light.
Described reactor body is hemispherical for cylindric and bottom.Cylindrical shape can realize bigger reactant accumulated amount simultaneously Floor space is less;And the hemispherical discharge being conducive to reactant in bottom.
Described reductor is connected with reactor body by bolt.So it is capable of the dismounting of reductor and bolt.
Described mechanical stirring device can arrange multiple.Can be real in multiple mechanical stirring devices are separately positioned on reactor Existing larger range of stirring.
The present invention compared with prior art, has such advantages as and beneficial effect:
1, one stabilizer many stir modes reactor of the present invention, is provided with mechanical stirring device, ultrasonic generator and shakes Dynamic agitating device, it is possible to realize conversion and the synergism of multiple alr mode, make material reach sufficiently and mix;
2, one stabilizer many stir modes reactor of the present invention, the damping device of setting can carry out machinery, shake and stir When mixing, weaken vibrations, reduce noise.
Accompanying drawing explanation
Accompanying drawing described herein is used for providing being further appreciated by the embodiment of the present invention, constitutes of the application Point, it is not intended that the restriction to the embodiment of the present invention.In the accompanying drawings:
Fig. 1 is present configuration schematic diagram.
The parts title of labelling and correspondence in accompanying drawing:
1-reactor body, 2-mechanical stirring device, 3-motor, 4-ultrasonic generator, 5-shakes agitating device, 6-spring Post, 7-props up spike, 8-cushion, 9-reductor.
Detailed description of the invention
For making the object, technical solutions and advantages of the present invention clearer, below in conjunction with embodiment and accompanying drawing, to this Invention is described in further detail, and the exemplary embodiment of the present invention and explanation thereof are only used for explaining the present invention, do not make For limitation of the invention.
Embodiment 1
As it can be seen, one stabilizer many stir modes reactor of the present invention, including reactor body 1, agitating device, motor 3, described reactor body top is provided with charging aperture, and reactor body bottom is provided with discharging opening;
Described agitating device includes mechanical stirring device 2, ultrasonic generator 4 and vibrations agitating device 5;
Ultrasonic generator is located at reactor bodies top;
Described vibration stirring device is located at reactor body side;
On the downside of described reactor main body, surrounding is designed with spring stack 6, and each spring stack bottom is designed with a spike 7, each support Side, underfooting is designed with cushion 8;
Described mechanical stirring device includes shaft and the paddle being connected on shaft;
One end of described shaft is stretched out reactor bodies top and is connected with motor;
Described paddle comprises 4 semicircular arc puddlers being connected in turn on shaft, the two-end-point of puddler circular arc with Shaft is connected, in 180 ° of angles between two adjacent puddlers;
Described paddle also includes a cross bar, and cross bar is positioned at below puddler, is connected with shaft end;
Described cross bar is circular arc, and the midpoint of circular arc cross bar is connected with shaft, and the two-end-point of circular arc is upward;
Described shaft is connected with reactor body by reductor 9.
This reactor is provided with mechanical stirring device, it is possible to realize the stirring of whole reactor, can not only be sufficiently stirred for bottom Material, with arrange vibration stirring device synergism, vibrations stirring operationally produce vibrations, shaking force makes between material Scattered more uniform;The reaction of monomer-polymers many for some macromolecule, re-uses ultrasonic generator, uses simultaneously Three kinds of alr modes, the most dispersed polymer monomer, it is possible to avoid certain monomer that segregation occurs in course of reaction, carry The quality of high product.Meanwhile, the damping device arranged on the downside of reactor main body can weaken when carrying out machinery, vibrations stirring Vibrations, the structure of firm reactor, reduces noise.
Embodiment 2
On the basis of above-described embodiment, described agitating device 2 is stainless steel, ceramic material, PP with reactor body 1 The one of material.It is rotten that rustless steel matter is capable of withstanding the chemical etching media such as the weak corrosive medium such as air, steam, water and acid, alkali, salt Erosion, it is adaptable to have the reaction of corrosive medium in raw material.Pottery and the reaction being then applicable to without raw materials such as soda acids of PP material, And material is light.
Embodiment 3
On the basis of above-described embodiment, described reactor body 1 is hemispherical for cylindric and bottom.Cylindrical shape can realize relatively Big reactant accumulated amount floor space simultaneously is less;And the hemispherical discharge being conducive to reactant in bottom.
Embodiment 4
On the basis of above-described embodiment, described reductor 8 is connected with reactor body 1 by bolt.So it is capable of Reductor and the dismounting of bolt.
Embodiment 5
On the basis of above-described embodiment, described mechanical stirring device 2 can arrange multiple.By multiple mechanical stirring devices respectively Larger range of stirring can be realized in being arranged on reactor.
Above-described detailed description of the invention, has been carried out the purpose of the present invention, technical scheme and beneficial effect further Describe in detail, be it should be understood that the detailed description of the invention that the foregoing is only the present invention, be not intended to limit the present invention Protection domain, all within the spirit and principles in the present invention, any modification, equivalent substitution and improvement etc. done, all should comprise Within protection scope of the present invention.

Claims (5)

1. stabilizer many stir modes reactor, including reactor body (1), agitating device, motor (3), described instead Answering still body (1) top to be provided with charging aperture, reactor body bottom is provided with discharging opening, it is characterised in that:
Described agitating device includes mechanical stirring device (2), ultrasonic generator (4) and vibrations agitating device (5);
Ultrasonic generator (4) is located at reactor body (1) top;
Described vibration stirring device (5) is located at reactor body (1) sidepiece;
On the downside of described reactor main body, surrounding is designed with spring stack (6), and each spring stack bottom is designed with a spike (7), each Support side, underfooting and be designed with cushion (8);
Described mechanical stirring device includes shaft and the paddle being connected on shaft;
One end of described shaft is stretched out reactor body (1) top and is connected with motor (3);
Described paddle comprises 4 semicircular arc puddlers being connected in turn on shaft, the two-end-point of puddler circular arc with Shaft is connected, in 180 ° of angles between two adjacent puddlers;
Described paddle also includes a cross bar, and cross bar is positioned at below puddler, is connected with shaft end;
Described cross bar is circular arc, and the midpoint of circular arc cross bar is connected with shaft, and the two-end-point of circular arc is upward;
Described shaft is connected with reactor body (1) by reductor (9).
A kind of stabilizer many stir modes reactor the most according to claim 1, it is characterised in that: described machinery stirs Mixing device (2) with reactor body (1) is stainless steel, ceramic material, the one of PP material.
A kind of stabilizer many stir modes reactor the most according to claim 1 and 2, it is characterised in that: described reaction Still body (1) is hemispherical for cylindric and bottom.
A kind of stabilizer many stir modes reactor the most according to claim 3, it is characterised in that: described reductor (9) it is connected with reactor body (1) by bolt.
5. according to the arbitrary described a kind of stabilizer many stir modes reactor of claim 1,2 or 4, it is characterised in that: institute State mechanical stirring device (2) and can arrange multiple.
CN201610713345.0A 2016-08-24 2016-08-24 Stabilizer is with many stirring mode reation kettle Pending CN106268571A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107159035A (en) * 2017-07-07 2017-09-15 刘艳芹 A kind of clinical laboratory is mixed and shakes device automatically with Multifunction blood
CN108034553A (en) * 2018-02-09 2018-05-15 福建福清兴龙酒业有限公司 A kind of wine brewing steaming plant
CN108413827A (en) * 2018-03-14 2018-08-17 安徽理工大学 A kind of the destruction retracting device and method of waste emulsified explosive
CN113477147A (en) * 2021-05-31 2021-10-08 南京航空航天大学 Ultrasonic mixer for tungsten-based nano composite powder

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5674956A (en) * 1989-02-03 1997-10-07 Hitachi, Ltd. Method for producing high viscosity materials
CN204933363U (en) * 2015-07-09 2016-01-06 芜湖市恒峰科技有限公司 A kind of new and effective agitating device
CN205216836U (en) * 2015-11-27 2016-05-11 战立启 High -efficient simplification worker reation kettle
CN206027690U (en) * 2016-08-24 2017-03-22 成都米特瑞新材料科技有限公司 Damping reaction kettle capable of realizing conversion of multiple stirring modes

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5674956A (en) * 1989-02-03 1997-10-07 Hitachi, Ltd. Method for producing high viscosity materials
CN204933363U (en) * 2015-07-09 2016-01-06 芜湖市恒峰科技有限公司 A kind of new and effective agitating device
CN205216836U (en) * 2015-11-27 2016-05-11 战立启 High -efficient simplification worker reation kettle
CN206027690U (en) * 2016-08-24 2017-03-22 成都米特瑞新材料科技有限公司 Damping reaction kettle capable of realizing conversion of multiple stirring modes

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
李青山等: "《药学基本实验技术》", 31 August 2006 *

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107159035A (en) * 2017-07-07 2017-09-15 刘艳芹 A kind of clinical laboratory is mixed and shakes device automatically with Multifunction blood
CN108034553A (en) * 2018-02-09 2018-05-15 福建福清兴龙酒业有限公司 A kind of wine brewing steaming plant
CN108413827A (en) * 2018-03-14 2018-08-17 安徽理工大学 A kind of the destruction retracting device and method of waste emulsified explosive
CN113477147A (en) * 2021-05-31 2021-10-08 南京航空航天大学 Ultrasonic mixer for tungsten-based nano composite powder

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