CN106266078A - The control method of a kind of Fructus Gardeniae Technology for Heating Processing and device - Google Patents
The control method of a kind of Fructus Gardeniae Technology for Heating Processing and device Download PDFInfo
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- CN106266078A CN106266078A CN201610770296.4A CN201610770296A CN106266078A CN 106266078 A CN106266078 A CN 106266078A CN 201610770296 A CN201610770296 A CN 201610770296A CN 106266078 A CN106266078 A CN 106266078A
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- heat treatment
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/74—Rubiaceae (Madder family)
- A61K36/744—Gardenia
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/13—Preparation or pretreatment of starting material involving cleaning, e.g. washing or peeling
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- Natural Medicines & Medicinal Plants (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Alternative & Traditional Medicine (AREA)
- Biotechnology (AREA)
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- Medicinal Chemistry (AREA)
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- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Cleaning By Liquid Or Steam (AREA)
Abstract
The present invention provides control method and the device of a kind of Fructus Gardeniae Technology for Heating Processing, and it is capable of the stability contorting of Fructus Gardeniae heat treatment process technological parameter.The control method of a kind of Fructus Gardeniae Technology for Heating Processing, comprises the steps, A, temperature control: the steam intake of the chuck of regulation heat treatment tank controls temperature in tank, temperature in monitoring tank, when temperature is more than 95 DEG C in tank, adds acid for adjusting pH value in heat treated tank；B, pH control: the pH value in monitoring heat treatment tank, when in tank, pH value is close to setting value, and the addition speed of acid of slowing down, make pH value be less than setting value；C, foam control: the foam height in monitoring heat treatment tank, when foam height reaches setting height, reduce the steam intake of heat treatment tank chuck；Force value in detection heat treatment tank simultaneously, if force value non-normal pressure value, stops being passed through steam and emptying the steam of heat treatment tank chuck；Continue to be passed through steam after force value is normal pressure value and the removal of foam.
Description
Technical field
The present invention relates to field of traditional Chinese medicine pharmacy, be specifically related to control method and the device of a kind of Fructus Gardeniae Technology for Heating Processing.
Background technology
Reduning injection is the new drug of Kangyuan Pharmaceutical Co., Ltd., Jiangsu Prov's independent research, belongs to Chinese medicine compound injection
Agent, is mainly formed by Flos Lonicerae, Fructus Gardeniae and Herba Artemisiae Annuae three taste Chinese medicine extraction are refined.Fructus Gardeniae is as the main crude drug of Reduning injection
One of, Fructus Gardeniae heat treatment process is the important step in Reduning injection production process, to the safety of final products, effectively
Property, stability etc. play an important role.Traditional heat-treating methods be feed intake after, control work by manual adjustment valve
Skill parameter, but system is affected by vapour system complexity, manual operation proficiency, the phase close with quality such as pH value, temperature
The technological parameter closed can not get effectively controlling, and Fructus Gardeniae heat treatment process technological parameter is unstable, has a strong impact on intermediate and final
The quality of product.Secondly, Fructus Gardeniae heat treatment process is easily generated a large amount of foam, if process parameter control is unstable, then may
Cause acidic foam to overflow, cause material waste, equipment is caused corrosion.
Summary of the invention
For the problems referred to above, it is an object of the invention to provide control method and the device of a kind of Fructus Gardeniae Technology for Heating Processing, its
It is capable of the stability contorting of Fructus Gardeniae heat treatment process technological parameter.
For solving above-mentioned technical problem, the present invention adopts the following technical scheme that
The control method of a kind of Fructus Gardeniae Technology for Heating Processing, comprises the steps,
A, temperature control: the steam intake of the chuck of regulation heat treatment tank controls temperature in tank, and temperature in monitoring tank, when in tank
When temperature is more than 95 DEG C, in heat treated tank, add acid for adjusting pH value；
B, pH control: the pH value in monitoring heat treatment tank, when in tank, pH value is close to setting value, and the addition speed of acid of slowing down, make
PH value is less than setting value；
C, foam control: the foam height in monitoring heat treatment tank, when foam height reaches setting height, reduce heat treatment tank
The steam intake of chuck；Force value in detection heat treatment tank simultaneously, if force value non-normal pressure value, stops being passed through steam side by side
The steam of empty heat treatment tank chuck；Continue to be passed through steam after force value is normal pressure value and the removal of foam.
Preferably, in step A, by temperature in the temperature transmitter monitoring tank in heat treatment tank.
Preferably, in step A, regulate steam intake by the steam control valve in heat treatment tank.
Preferably, in step B, by pH value in the pH meter monitoring tank in heat treatment tank.
It is highly preferred that in step B, by the peristaltic pump acid adding in heat treatment tank.
Preferably, in step C, monitor the foam height in tank by the foam electrode in heat treatment tank.
It is highly preferred that in step C, detect pressure inside the tank value by the pressure transmitter in heat treatment tank.
Preferably, this control method also includes step D, and paraffin adds and controls: paraffin adds melting pot and stirs, Xiang Rong
Being passed through steam in changing tank chuck, temperature in detection melting pot, when temperature reaches paraffin melting point, by stone after the setting time
Wax adds in heat treatment tank.
Preferably, this control method also includes step E, cleaning control: after heat treatment process terminates, by heat treatment tank
Material is transferred to cold-storage jar, starts CIP on-line cleaning system and heat treatment tank and melting pot are carried out CIP on-line cleaning.
The control device of a kind of Fructus Gardeniae Technology for Heating Processing, including heat treatment tank, for acid adding in described heat treatment tank
Peristaltic pump, the heat treatment stirring motor being located in described heat treatment tank, melting pot, be located on described melting pot fusing stirring electricity
Machine, described control device also includes:
Controller, described controller is electrically connected mutually with described peristaltic pump, heat treatment stirring motor, fusing stirring motor respectively；And
The Temperature being electrically connected mutually with described controller, described Temperature is located in described heat treatment tank；
The steam control valve being electrically connected mutually with described controller, described steam control valve is located in described heat treatment tank；
The pH meter being electrically connected mutually with described controller, described pH meter is located in described heat treatment tank；
The foam electrode being electrically connected mutually with described controller, it is interior to monitor heat treatment tank that described foam electrode is located at described heat treatment tank
Foam height in 1；
The pressure transmitter being electrically connected mutually with described controller, described pressure transmitter is located in described heat treatment tank；
And/or, the thermometer being electrically connected mutually with described controller, described thermometer is arranged in described melting pot；
And/or, the paraffin being electrically connected mutually with described controller enters pot valve, and described paraffin enters pot valve and is arranged on described melting pot；
And/or, with described controller be electrically connected mutually for heat treatment tank and melting pot are carried out CIP on-line cleaning system clearly
System.
The present invention uses above scheme, has the advantage that and is capable of Fructus Gardeniae heat treatment process technique by the method
The stability contorting of parameter, it is achieved that the stable of technological parameter accurately controls, it is achieved froth breaking and foam control, maintain intermediate and
The quality of final products.
Accompanying drawing explanation
Fig. 1 is the control device of a kind of Fructus Gardeniae Technology for Heating Processing of the present invention;
Fig. 2 is the temperature variation curve of the control method of the present invention.
In above-mentioned accompanying drawing, 1-heat treatment tank, 2-temperature transmitter, 3-steam control valve, 4-pH counts, 5-peristaltic pump, and 6-steeps
Foam electrode, 7-pressure transmitter, 8-annealer stirring motor, the paraffin melting tank of 9-, 10-melting pot jacket steam enters valve, 11-
Melting tank stirring motor, 12-thermometer, 13-paraffin enters pot valve, 14-CIP on-line cleaning system, 15-controller.
Detailed description of the invention
Below presently preferred embodiments of the present invention is described in detail so that advantages and features of the invention can be easier to by
Those skilled in the art understands, thus protection scope of the present invention is made apparent clear and definite defining.Embodiment is adopted
Implementation condition can do further adjustment according to specific requirement, not marked implementation condition is usually the bar in normal experiment
Part.During it addition, do not have specified otherwise, detection epidemic disaster is without specific requirement and restriction.
Fig. 1 show the control device of a kind of Fructus Gardeniae Technology for Heating Processing.Shown in Fig. 1, this Fructus Gardeniae annealing device bag
Include heat treatment tank 1, temperature transmitter 2, steam control valve 3, pH meter 4, peristaltic pump 5, foam electrode 6, pressure transmitter 7, Re Chu
Reason stirring motor 8, melting tank 9, melting pot jacket steam enter valve 10, fusing stirring motor 11, thermometer 12, paraffin enter pot valve
13, CIP on-line cleaning system 14 and controller 15.Controller 15 and temperature transmitter 2, steam control valve 3, pH meter 4, peristaltic pump
5, foam electrode 6, pressure transmitter 7, heat treatment stirring motor 8, fusing stirring motor 11, thermometer 12, paraffin enter pot valve 13,
CIP on-line cleaning system 14 is the most mutually electrically connected to be controlled above-mentioned each element.
The control method of a kind of Fructus Gardeniae Technology for Heating Processing, comprises the steps: that A, temperature control；B, pH control；C, foam
Control；D, paraffin add and control；E, cleaning control.
A, temperature control
The steam intake of the chuck of regulation heat treatment tank 1 controls temperature in tank, and temperature in monitoring tank, when in tank, temperature is more than 95
Time DEG C (feed liquid is in fluidized state in tank), in heat treated tank 1, add acid for adjusting pH value.Specifically, by heat treatment tank 1
Temperature in tank monitored by temperature transmitter 2, regulates steam intake by the steam control valve 3 in heat treatment tank 1.Wherein, temperature
Transmitter 2 is electrically connected mutually with controller 15, and controller 15 obtains temperature that temperature transmitter 2 detects to control heat treated tank 1
Interior automatical dosing.Steam control valve 3 is electrically connected to be automatically adjusted steam control valve 3 mutually and changes quantity of steam with controller 15.
B, pH control
Start the peristaltic pump 5 of heat treatment tank 1, carry out adding hydrochloric acid operation；Heat treatment tank 1 is monitored by the pH meter 4 in heat treatment tank 1
Interior pH value, when pH value is close to setting value in tank, controls the flow velocity of peristaltic pump 5, and the addition speed of acid of slowing down makes pH value close
And less than setting value.Wherein, pH meter 4 is electrically connected mutually with controller 15 so that controller 15 obtains the pH value that pH meter 4 detects, compacted
Dynamic pump 5 is electrically connected mutually with controller 15, and the pH value of acquisition and pH setting value are compared the stream being automatically adjusted peristaltic pump 5 by controller 15
Speed.
C, foam control
The foam height in heat treatment tank 1 is monitored, when foam height reaches to set height by the foam electrode 6 in heat treatment tank 1
When spending, reduce the steam intake of heat treatment tank 1 chuck, reduce foam and produce；Simultaneously by the pressure inverting in heat treatment tank 1
Device 7 detects the force value in heat treatment tank 1, has detected whether that the situation that builds the pressure produces, if force value non-normal pressure value, stops being passed through steaming
Vapour also empties the steam of heat treatment tank 1 chuck；Continue to be passed through steam after force value is normal pressure value and the removal of foam.Wherein, bubble
Foam electrode 6 is electrically connected mutually with controller 15 so that controller 15 obtains the foam height that foam electrode 6 detects, pressure transmitter 7
Be electrically connected so that controller 15 obtains the force value that pressure transmitter 7 detects mutually with controller 15, controller 15 is according to acquisition
Foam height and force value also compare with foam setting height, normal pressure value respectively, regulate steam and are passed through controlling steam control valve 3
Amount.
Step D, paraffin adds and controls
Paraffin is added melting pot 9, opens melting pot jacket steam and enter valve 10, in melting pot 9 chuck, be passed through steam, start molten
Change tank stirring motor 11, thermometer 12 detect temperature in melting pot, controller 15 and thermometer 12 be electrically connected mutually with obtain detect
Temperature, when temperature reaches paraffin melting point, after one sets time (5 minutes), controller 15 is opened paraffin and is entered pot valve 13
Paraffin is added in heat treatment tank 1.
Step E, cleaning control
After heat treatment process terminates, the material in heat treatment tank 1 is transferred to cold-storage jar, starts CIP on-line cleaning system 14 right
Heat treatment tank 1 and melting pot carry out CIP on-line cleaning.Wherein, controller 15 is electrically connected with CIP on-line cleaning system 14 phase.
This control method also includes mixing control: in acid adding control, and controller 15 controls the start and stop of stirring motor, and
Monitor motor operating state, abnormal alarm in real time.
This control method also includes that motor status monitors: in heat treatment process, annealer stirring motor 8 and paraffin melting
The current signal Real-time Feedback of tank 9 stirring motor is to controller 15, and controller 15 judges motor operating state, fault alarm.
With a specific embodiment, the control method of the present invention is illustrated below.
A, liter temperature control
B, pH control
The hydrochloric acid using 20 ~ 70% regulates the pH value of extractum to 2.0 ~ 4.0
(1) traditional control method is: sampling, off-line measurement pH value, needed for continuing regulation pH value, regulation pH according to measurement result
Time is about 2 hours.
(2) present invention uses on-line checking, the method for On-line Control, and regulation pH required time is about 20min, significantly carries
High production efficiency.
C, preservation and controlling
Maintaining slight boiling condition 1 hour, keeping temperature is 90 ~ 100 DEG C
Record temperature controlled processes, draw temperature variation curve as in figure 2 it is shown, as can be seen from the figure temperature fluctuation less, this
Inventive method achieves temperature controlled stability, and temperature fluctuation is less than ± 2 DEG C
D, foam control
E, paraffin add and control
After paraffin has added, continue agitating heating 10 minutes, steam off valve, enter next step.
F, cleaning control
Above-described embodiment is only for illustrating technology design and the feature of the present invention, and its object is to person skilled in the art can
Understand present disclosure and implement according to this, protection scope of the present invention can not be limited with this.All spirit according to the present invention
Equivalent transformation that essence is made or modification, all should contain within protection scope of the present invention.
Claims (10)
1. the control method of a Fructus Gardeniae Technology for Heating Processing, it is characterised in that comprise the steps,
A, temperature control: the steam intake of the chuck of regulation heat treatment tank controls temperature in tank, and temperature in monitoring tank, when in tank
When temperature is more than 95 DEG C, in heat treated tank, add acid for adjusting pH value；
B, pH control: the pH value in monitoring heat treatment tank, when in tank, pH value is close to setting value, and the addition speed of acid of slowing down, make
PH value is less than setting value；
C, foam control: the foam height in monitoring heat treatment tank, when foam height reaches setting height, reduce heat treatment tank
The steam intake of chuck；Force value in detection heat treatment tank simultaneously, if force value non-normal pressure value, stops being passed through steam side by side
The steam of empty heat treatment tank chuck；Continue to be passed through steam after force value is normal pressure value and the removal of foam.
Control method the most according to claim 1, it is characterised in that: in step A, by the temperature pick-up in heat treatment tank
Temperature in device monitoring tank.
Control method the most according to claim 1, it is characterised in that: in step A, regulated by the steam in heat treatment tank
Valve regulation steam intake.
Control method the most according to claim 1, it is characterised in that: in step B, monitored by the pH meter in heat treatment tank
PH value in tank.
5. according to the control method described in claim 1 or 4, it is characterised in that: in step B, by the wriggling in heat treatment tank
Pump acid adding.
Control method the most according to claim 1, it is characterised in that: in step C, by the foam electrode in heat treatment tank
Foam height in monitoring tank.
7. according to the control method described in claim 1 or 6, it is characterised in that: in step C, by the pressure in heat treatment tank
Transmitters sense pressure inside the tank value.
Control method the most according to claim 1, it is characterised in that this control method also includes step D, paraffin adds control
System: paraffin adds melting pot and stirs, is passed through steam in melting pot chuck, and temperature in detection melting pot, when temperature reaches
During paraffin melting point, after the setting time, paraffin is added in heat treatment tank.
Control method the most according to claim 1, it is characterised in that this control method also includes step E, cleaning control:
After heat treatment process terminates, the material in heat treatment tank is transferred to cold-storage jar, starts CIP on-line cleaning system to heat treatment tank
CIP on-line cleaning is carried out with melting pot.
10. a control device for Fructus Gardeniae Technology for Heating Processing, including heat treatment tank, compacted for acid adding in described heat treatment tank
Dynamic pump, the heat treatment stirring motor being located in described heat treatment tank, melting pot, the fusing stirring electricity that is located on described melting pot
Machine, its feature exists, and described control device also includes:
Controller, described controller is electrically connected mutually with described peristaltic pump, heat treatment stirring motor, fusing stirring motor respectively；And
The Temperature being electrically connected mutually with described controller, described Temperature is located in described heat treatment tank；
The steam control valve being electrically connected mutually with described controller, described steam control valve is located in described heat treatment tank；
The pH meter being electrically connected mutually with described controller, described pH meter is located in described heat treatment tank；
The foam electrode being electrically connected mutually with described controller, it is interior to monitor heat treatment tank that described foam electrode is located at described heat treatment tank
Foam height in 1；
And/or, the pressure transmitter being electrically connected mutually with described controller, described pressure transmitter is located in described heat treatment tank；
And/or, the thermometer being electrically connected mutually with described controller, described thermometer is arranged in described melting pot；
And/or, the paraffin being electrically connected mutually with described controller enters pot valve, and described paraffin enters pot valve and is arranged on described melting pot；
And/or, with described controller be electrically connected mutually for the CIP on-line cleaning system that heat treatment tank and melting pot are carried out
System.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610770296.4A CN106266078B (en) | 2016-08-30 | 2016-08-30 | A kind of control method and device of cape jasmine heat treatment process |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610770296.4A CN106266078B (en) | 2016-08-30 | 2016-08-30 | A kind of control method and device of cape jasmine heat treatment process |
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| Publication Number | Publication Date |
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| CN106266078A true CN106266078A (en) | 2017-01-04 |
| CN106266078B CN106266078B (en) | 2019-08-16 |
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| CN201610770296.4A Active CN106266078B (en) | 2016-08-30 | 2016-08-30 | A kind of control method and device of cape jasmine heat treatment process |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107951941A (en) * | 2017-11-29 | 2018-04-24 | 江苏康缘药业股份有限公司 | A kind of cape jasmine medicinal extract cold storage procedure control method |
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| CN1876045A (en) * | 2003-01-08 | 2006-12-13 | 江苏康缘药业股份有限公司 | A Chinese medicinal composition, its preparation process and quality control method |
| CN103135530A (en) * | 2013-01-28 | 2013-06-05 | 浙江科美制药机械有限公司 | Automatic control system and method thereof for extracting jar |
| CN103893991A (en) * | 2014-04-22 | 2014-07-02 | 广东世信药业有限公司 | Heat cycle extraction concentration method for traditional Chinese medicine |
-
2016
- 2016-08-30 CN CN201610770296.4A patent/CN106266078B/en active Active
Patent Citations (3)
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| CN1876045A (en) * | 2003-01-08 | 2006-12-13 | 江苏康缘药业股份有限公司 | A Chinese medicinal composition, its preparation process and quality control method |
| CN103135530A (en) * | 2013-01-28 | 2013-06-05 | 浙江科美制药机械有限公司 | Automatic control system and method thereof for extracting jar |
| CN103893991A (en) * | 2014-04-22 | 2014-07-02 | 广东世信药业有限公司 | Heat cycle extraction concentration method for traditional Chinese medicine |
Non-Patent Citations (1)
| Title |
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| 简继华: "中药提取生产与自动化控制初探", 《机电信息》 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107951941A (en) * | 2017-11-29 | 2018-04-24 | 江苏康缘药业股份有限公司 | A kind of cape jasmine medicinal extract cold storage procedure control method |
| CN107951941B (en) * | 2017-11-29 | 2019-12-24 | 江苏康缘药业股份有限公司 | Method for controlling refrigeration process of gardenia extract |
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| CN106266078B (en) | 2019-08-16 |
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