CN106244929A - A kind of novel energy-conserving powder metallurgy - Google Patents
A kind of novel energy-conserving powder metallurgy Download PDFInfo
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- CN106244929A CN106244929A CN201610601756.0A CN201610601756A CN106244929A CN 106244929 A CN106244929 A CN 106244929A CN 201610601756 A CN201610601756 A CN 201610601756A CN 106244929 A CN106244929 A CN 106244929A
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- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/08—Ferrous alloys, e.g. steel alloys containing nickel
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
- B22F1/10—Metallic powder containing lubricating or binding agents; Metallic powder containing organic material
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
- B22F1/10—Metallic powder containing lubricating or binding agents; Metallic powder containing organic material
- B22F1/103—Metallic powder containing lubricating or binding agents; Metallic powder containing organic material containing an organic binding agent comprising a mixture of, or obtained by reaction of, two or more components other than a solvent or a lubricating agent
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- C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
- C10M169/04—Mixtures of base-materials and additives
- C10M169/048—Mixtures of base-materials and additives the additives being a mixture of compounds of unknown or incompletely defined constitution, non-macromolecular and macromolecular compounds
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- C22C33/02—Making ferrous alloys by powder metallurgy
- C22C33/0257—Making ferrous alloys by powder metallurgy characterised by the range of the alloying elements
- C22C33/0264—Making ferrous alloys by powder metallurgy characterised by the range of the alloying elements the maximum content of each alloying element not exceeding 5%
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- C22C38/60—Ferrous alloys, e.g. steel alloys containing lead, selenium, tellurium, or antimony, or more than 0.04% by weight of sulfur
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- C10M2207/10—Carboxylix acids; Neutral salts thereof
- C10M2207/12—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
- C10M2207/125—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids
- C10M2207/126—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids monocarboxylic
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- C10M2207/12—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
- C10M2207/125—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids
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- C10M2207/10—Carboxylix acids; Neutral salts thereof
- C10M2207/14—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to carbon atoms of six-membered aromatic rings
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- C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
- C10M2209/02—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- C10M2209/04—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds containing monomers having an unsaturated radical bound to an alcohol or ester thereof; bound to an aldehyde, ketonic, ether, ketal or acetal radical
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- C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
- C10M2209/10—Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
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- C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
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Abstract
The invention discloses a kind of novel energy-conserving powder metallurgy, in units of weight, it is made up of following raw material: water-atomized iron powder 132 195 parts, nikel powder 46 parts, 23 parts of Hydrocerussitum (Ceruse), magnesium oxide 12 parts, sulfuration sub-1.2 1.8 parts of manganese, aluminium oxide 0.9 1.4 parts, cathode copper 0.8 1.5 parts, graphite powder 0.6 1 parts, fatty acid 35 parts, cutting agent 0.4 0.6 parts, lubricant 0.3 0.6 parts, hardening agent 0.1 0.2 parts, binding agent 0.6 0.8 parts, viscosifier 0.1 0.2 parts, antiwear additive 0.5 0.8 parts, processing aid 0.2 0.3 parts, regulator 0.1 0.2 parts.The product that the preparation method of the present invention prepares improves hot strength and the hardness of product, meanwhile, by optimizing processing step, improves production efficiency, decreases the waste of the energy.
Description
[technical field]
The invention belongs to metallurgical technology field, be specifically related to a kind of novel energy-conserving powder metallurgy.
[background technology]
Powder metallurgical technique mainly comprises three steps, first, mainly comprises material and is broken down into various tiny
The powder of granule composition;Then, powder is loaded mold cavity, imposes certain pressure, formed have required part shape and
The pressed compact of size;Finally, pressed compact is sintered.
Owing to the main material of powder metallurgy is metal dust, and raw material is broken down into powder and needs pulverizer to former material
Material is constantly pulverized, and causes huge power consumption and sound pollution, during powder loads mold cavity, single
Amount of powder required for mold cavity is identical, but often occurs the amount of powder injecting Die different in the batch production of blank
Often, amount of powder is wasted and the exception of press too much as usual, and very little, pressed compact is the finest and close for amount of powder, even containing jagged, causes report
Useless.During sintering, the metallic crystal in view of blank is formed, and generally requires and repeatedly heats, and energy resource consumption is big.It addition, it is existing
Powder metallurgy prescription and technique still have limitation, production efficiency low, simultaneously product there is also hot strength and
The problem that hardness is relatively low.
[summary of the invention]
The present invention provides a kind of novel energy-conserving powder metallurgy, there is hot strength and hardness solving existing powder metallurgy
Relatively low, production efficiency is low, the problems such as energy resource consumption is big.The product that the preparation method of the present invention prepares improves product
Hot strength and hardness, meanwhile, by optimizing processing step, improve production efficiency, decrease the waste of the energy.
For solve above technical problem, the present invention by the following technical solutions:
A kind of novel energy-conserving powder metallurgy, in units of weight, is made up of following raw material: water-atomized iron powder 132-195 part,
Nikel powder 4-6 part, Hydrocerussitum (Ceruse) 2-3 part, magnesium oxide 1-2 part, sulfuration sub-manganese 1.2-1.8 part, aluminium oxide 0.9-1.4 part, cathode copper 0.8-
1.5 parts, graphite powder 0.6-1 part, fatty acid 3-5 part, cutting agent 0.4-0.6 part, lubricant 0.3-0.6 part, hardening agent 0.1-0.2
Part, binding agent 0.6-0.8 part, viscosifier 0.1-0.2 part, antiwear additive 0.5-0.8 part, processing aid 0.2-0.3 part, regulator
0.1-0.2 part;
Described water-atomized iron powder, nikel powder, Hydrocerussitum (Ceruse), magnesium oxide, sulfuration Asia manganese, aluminium oxide, cathode copper, graphite powder granularity equal
For 0.1-100 μm;
Described cutting agent, in units of weight, is made up of following raw material: cutting oil 14-16 part, tricresyl phosphate propyl ester 10-12
Part, dinonylnaphthalene sulfonic acid calcium 4-6 part, 2,6 ditertiary butyl p cresol 6-10 part, dodecenylsuccinic acid 5-7 part, triethanolamine
Borate 8-12 part, polyacrylamide 6-12 part, dodecylbenzene sodium sulfonate 8-10 part, benzoic acid 6-9 part, oleamide 3-8
Part, tetrasodium ethylenediamine tetraacetate 2-6 part, amino carboxylic acid quasi-chelate compound 1-2 part, Polyethylene Glycol 8-14 part;
Described lubricant, in units of weight, is made up of following raw material: polyvinyl isobutyl ether 20-40 part, chlorinated paraffin
8-14 part, magnesium oxide particle 4-8 part, fatty acid zinc 6-12 part, carboxylic acid amide 8-14 part, acetate butyl 12-15 part, boric acid 6-10
Part, N-Methyl pyrrolidone 7-12 part, dimethylformamide 6-10 part;
The preparation method of described novel energy-conserving powder metallurgy, comprises the following steps:
S1: the iron powder that makes water fogging, nikel powder, Hydrocerussitum (Ceruse), magnesium oxide, sulfuration Asia manganese, aluminium oxide, cathode copper, graphite powder, fat
Acid, cutting agent, lubricant, hardening agent, binding agent, viscosifier, antiwear additive, processing aid, regulator import in spice cylinder together
Being stirred forming mixed powder, filtered by drainage screen after stirring, in mixed powder, raw meal particle size is coarser than 140-
The particulate matter of 160 mesh carries out pulverizing screening after being isolated collection again, is subsequently poured in each standard dose bucket standby;
The preparation method of described cutting agent, comprises the following steps:
Step 1, will cutting oil, tricresyl phosphate propyl ester, dinonylnaphthalene sulfonic acid calcium, 2,6 ditertiary butyl p cresol, laurylene base
Succinic acid, triethanolamine borate, polyacrylamide, dodecylbenzene sodium sulfonate, benzoic acid mix homogeneously, then by mixture
It is heated to 52-58 DEG C;
Step 2, adds remaining ingredient in step 1 gained mixture, continues to be heated to 76-92 DEG C, and be incubated 2.5-
3.5h, prepares cutting agent;
Described lubricant is prepared by following preparation method:
The raw material components of lubricant is joined in reactor and react 11-19h in 420-480 DEG C, then use after solidification
Particle is had the cone mill of clipping power as mechanical dispersion equipment, be ground dispersion, prepare lubricant;
S2: the mixed powder in the standard dose bucket prepare step S1 is directly poured in pressed compact mould, at forcing press
Pressure is to suppress under 520-580MPa, makes the shape of part blank;
S3: blank step S2 prepared is sent in heating furnace and is sintered, and heating-up temperature is 720-840 DEG C, after cooling
Form fine and close semi-finished product;
S4: surface of semi-finished step S3 prepared is placed on shelf after being coated with antirust oil and carries out 2-6 days Ageing Treatment;
S5: the semi-finished product that the Ageing Treatment that step S4 prepares is crossed are carried out shaping and surface polishing, forms standardized product.
Further, described hardening agent is 701 powder hardening agents.
Further, described binding agent is mixed by fatty acid zinc and machine oil 2-5:1-2 in mass ratio.
Further, described viscosifier are glycidoxy-propyltrimethoxy silane.
Further, described antiwear additive is silicon dioxide.
Further, described processing aid is Manganese monosulfide..
Further, described regulator is esters of acrylic acid regulator.
The method have the advantages that
(1) preparation method of the present invention improves hot strength and the hardness of product, meanwhile, by optimizing processing step,
Improve production efficiency, decrease the waste of the energy;
(2) present invention uses standard dose bucket to pressed compact mould feeding, and precision is high, and part blank compactness is good, qualified
Rate is high, and have employed seasoning especially and process, crystal formation after internal stress little, good energy saving property.
[detailed description of the invention]
For ease of being more fully understood that the present invention, being illustrated by following example, these embodiments belong to the present invention's
Protection domain, but it is not intended to protection scope of the present invention.
In an embodiment, described novel energy-conserving powder metallurgy, in units of weight, it is made up of following raw material: water atomization ferrum
Powder 132-195 part, nikel powder 4-6 part, Hydrocerussitum (Ceruse) 2-3 part, magnesium oxide 1-2 part, sulfuration sub-manganese 1.2-1.8 part, aluminium oxide 0.9-1.4
Part, cathode copper 0.8-1.5 part, graphite powder 0.6-1 part, fatty acid 3-5 part, cutting agent 0.4-0.6 part, lubricant 0.3-0.6 part,
Hardening agent 0.1-0.2 part, binding agent 0.6-0.8 part, viscosifier 0.1-0.2 part, antiwear additive 0.5-0.8 part, processing aid 0.2-
0.3 part, regulator 0.1-0.2 part;
Described water-atomized iron powder, nikel powder, Hydrocerussitum (Ceruse), magnesium oxide, sulfuration Asia manganese, aluminium oxide, cathode copper, graphite powder granularity equal
For 0.1-100 μm;
Described cutting agent, in units of weight, is made up of following raw material: cutting oil 14-16 part, tricresyl phosphate propyl ester 10-12
Part, dinonylnaphthalene sulfonic acid calcium 4-6 part, 2,6 ditertiary butyl p cresol 6-10 part, dodecenylsuccinic acid 5-7 part, triethanolamine
Borate 8-12 part, polyacrylamide 6-12 part, dodecylbenzene sodium sulfonate 8-10 part, benzoic acid 6-9 part, oleamide 3-8
Part, tetrasodium ethylenediamine tetraacetate 2-6 part, amino carboxylic acid quasi-chelate compound 1-2 part, Polyethylene Glycol 8-14 part;
Described lubricant, in units of weight, is made up of following raw material: polyvinyl isobutyl ether 20-40 part, chlorinated paraffin
8-14 part, magnesium oxide particle 4-8 part, fatty acid zinc 6-12 part, carboxylic acid amide 8-14 part, acetate butyl 12-15 part, boric acid 6-10
Part, N-Methyl pyrrolidone 7-12 part, dimethylformamide 6-10 part;
Described hardening agent is 701 powder hardening agents;
Described binding agent is mixed by fatty acid zinc and machine oil 2-5:1-2 in mass ratio;
Described viscosifier are glycidoxy-propyltrimethoxy silane;
Described antiwear additive is silicon dioxide;
Described processing aid is Manganese monosulfide.;
Described regulator is esters of acrylic acid regulator;
The preparation method of described novel energy-conserving powder metallurgy, comprises the following steps:
S1: the iron powder that makes water fogging, nikel powder, Hydrocerussitum (Ceruse), magnesium oxide, sulfuration Asia manganese, aluminium oxide, cathode copper, graphite powder, fat
Acid, cutting agent, lubricant, hardening agent, binding agent, viscosifier, antiwear additive, processing aid, regulator import in spice cylinder together
Being stirred forming mixed powder, filtered by drainage screen after stirring, in mixed powder, raw meal particle size is coarser than 140-
The particulate matter of 160 mesh carries out pulverizing screening after being isolated collection again, is subsequently poured in each standard dose bucket standby;
The preparation method of described cutting agent, comprises the following steps:
Step 1, will cutting oil, tricresyl phosphate propyl ester, dinonylnaphthalene sulfonic acid calcium, 2,6 ditertiary butyl p cresol, laurylene base
Succinic acid, triethanolamine borate, polyacrylamide, dodecylbenzene sodium sulfonate, benzoic acid mix homogeneously, then by mixture
It is heated to 52-58 DEG C;
Step 2, adds remaining ingredient in step 1 gained mixture, continues to be heated to 76-92 DEG C, and be incubated 2.5-
3.5h, prepares cutting agent;
Described lubricant is prepared by following preparation method:
The raw material components of lubricant is joined in reactor and react 11-19h in 420-480 DEG C, then use after solidification
Particle is had the cone mill of clipping power as mechanical dispersion equipment, be ground dispersion, prepare lubricant;
S2: the mixed powder in the standard dose bucket prepare step S1 is directly poured in pressed compact mould, at forcing press
Pressure is to suppress under 520-580MPa, makes the shape of part blank;
S3: blank step S2 prepared is sent in heating furnace and is sintered, and heating-up temperature is 720-840 DEG C, after cooling
Form fine and close semi-finished product;
S4: surface of semi-finished step S3 prepared is placed on shelf after being coated with antirust oil and carries out 2-6 days Ageing Treatment;
S5: the semi-finished product that the Ageing Treatment that step S4 prepares is crossed are carried out shaping and surface polishing, forms standardized product.
Embodiment 1
A kind of novel energy-conserving powder metallurgy, in units of weight, is made up of following raw material: water-atomized iron powder 160 parts, nikel powder
5 parts, 2.5 parts of Hydrocerussitum (Ceruse), magnesium oxide 1.5 parts, sub-1.5 parts of the manganese of sulfuration, aluminium oxide 1.2 parts, cathode copper 1.2 parts, graphite powder 0.9 part,
Fatty acid 4 parts, cutting agent 0.5 part, lubricant 0.5 part, hardening agent 0.1 part, binding agent 0.7 part, viscosifier 0.1 part, antiwear additive
0.7 part, processing aid 0.2 part, regulator 0.1 part;
Described water-atomized iron powder, nikel powder, Hydrocerussitum (Ceruse), magnesium oxide, sulfuration Asia manganese, aluminium oxide, cathode copper, graphite powder granularity equal
For 0.1-100 μm;
Described cutting agent, in units of weight, is made up of following raw material: cutting oil 15 parts, tricresyl phosphate propyl ester 11 parts, two nonyls
Base LOMAR PWA EINECS 246-676-2 calcium 5 parts, 2,6 ditertiary butyl p cresol 8 parts, dodecenylsuccinic acid 6 parts, triethanolamine borate 10 parts, poly-third
Acrylamide 9 parts, dodecylbenzene sodium sulfonate 9 parts, 8 parts of benzoic acid, oleamide 6 parts, tetrasodium ethylenediamine tetraacetate 4 parts, amino
Carboxylic acids chelating agen 1 part, Polyethylene Glycol 12 parts;
Described lubricant, in units of weight, is made up of following raw material: 30 parts of polyvinyl isobutyl ether, chlorinated paraffin 12
Part, magnesium oxide particle 6 parts, fatty acid zinc 9 parts, carboxylic acid amide 12 parts, acetate butyl 13 parts, boric acid 8 parts, N-Methyl pyrrolidone
10 parts, dimethylformamide 8 parts;
Described hardening agent is 701 powder hardening agents;
Described binding agent is mixed by fatty acid zinc and machine oil 4:2 in mass ratio;
Described viscosifier are glycidoxy-propyltrimethoxy silane;
Described antiwear additive is silicon dioxide;
Described processing aid is Manganese monosulfide.;
Described regulator is esters of acrylic acid regulator;
The preparation method of described novel energy-conserving powder metallurgy, comprises the following steps:
S1: the iron powder that makes water fogging, nikel powder, Hydrocerussitum (Ceruse), magnesium oxide, sulfuration Asia manganese, aluminium oxide, cathode copper, graphite powder, fat
Acid, cutting agent, lubricant, hardening agent, binding agent, viscosifier, antiwear additive, processing aid, regulator import in spice cylinder together
Being stirred forming mixed powder, filtered by drainage screen after stirring, in mixed powder, raw meal particle size is coarser than 150 mesh
Particulate matter be isolated collection after carry out pulverizing screening again, be subsequently poured in each standard dose bucket standby;
The preparation method of described cutting agent, comprises the following steps:
Step 1, will cutting oil, tricresyl phosphate propyl ester, dinonylnaphthalene sulfonic acid calcium, 2,6 ditertiary butyl p cresol, laurylene base
Succinic acid, triethanolamine borate, polyacrylamide, dodecylbenzene sodium sulfonate, benzoic acid mix homogeneously, then by mixture
It is heated to 55 DEG C;
Step 2, adds remaining ingredient in step 1 gained mixture, continues to be heated to 85 DEG C, and be incubated 3h, prepare and cut
Cut agent;
Described lubricant is prepared by following preparation method:
The raw material components of lubricant is joined in reactor and react 10h in 450 DEG C, then use after solidification and particle is had
There is the cone mill of clipping power as mechanical dispersion equipment, be ground dispersion, prepare lubricant;
S2: the mixed powder in the standard dose bucket prepare step S1 is directly poured in pressed compact mould, at forcing press
Pressure is to suppress under 550MPa, makes the shape of part blank;
S3: blank step S2 prepared is sent in heating furnace and is sintered, and heating-up temperature is 780 DEG C, is formed after cooling
Fine and close semi-finished product;
S4: surface of semi-finished step S3 prepared is placed on shelf after being coated with antirust oil and carries out 4 days Ageing Treatment;
S5: the semi-finished product that the Ageing Treatment that step S4 prepares is crossed are carried out shaping and surface polishing, forms standardized product.
Embodiment 2
A kind of novel energy-conserving powder metallurgy, in units of weight, is made up of following raw material: water-atomized iron powder 132 parts, nikel powder
4 parts, 2 parts of Hydrocerussitum (Ceruse), magnesium oxide 1 part, sub-1.2 parts of the manganese of sulfuration, aluminium oxide 0.9 part, cathode copper 0.8 part, graphite powder 0.6 part, fat
Acid 3 parts, cutting agent 0.4 part, lubricant 0.3 part, hardening agent 0.1 part, binding agent 0.6 part, viscosifier 0.1 part, antiwear additive 0.5
Part, processing aid 0.2 part, regulator 0.1 part;
Described water-atomized iron powder, nikel powder, Hydrocerussitum (Ceruse), magnesium oxide, sulfuration Asia manganese, aluminium oxide, cathode copper, graphite powder granularity equal
For 0.1-100 μm;
Described cutting agent, in units of weight, is made up of following raw material: cutting oil 14 parts, tricresyl phosphate propyl ester 10 parts, two nonyls
Base LOMAR PWA EINECS 246-676-2 calcium 4 parts, 2,6 ditertiary butyl p cresol 6 parts, dodecenylsuccinic acid 5 parts, triethanolamine borate 8 parts, poly-third
Acrylamide 6 parts, dodecylbenzene sodium sulfonate 8 parts, 6 parts of benzoic acid, oleamide 3 parts, tetrasodium ethylenediamine tetraacetate 2 parts, amino
Carboxylic acids chelating agen 1 part, Polyethylene Glycol 8 parts;
Described lubricant, in units of weight, is made up of following raw material: 20 parts of polyvinyl isobutyl ether, chlorinated paraffin 8
Part, magnesium oxide particle 4 parts, fatty acid zinc 6 parts, carboxylic acid amide 8 parts, acetate butyl 12 parts, boric acid 6 parts, N-Methyl pyrrolidone 7
Part, dimethylformamide 6 parts;
Described hardening agent is 701 powder hardening agents;
Described binding agent is mixed by fatty acid zinc and machine oil 2:1 in mass ratio;
Described viscosifier are glycidoxy-propyltrimethoxy silane;
Described antiwear additive is silicon dioxide;
Described processing aid is Manganese monosulfide.;
Described regulator is esters of acrylic acid regulator;
The preparation method of described novel energy-conserving powder metallurgy, comprises the following steps:
S1: the iron powder that makes water fogging, nikel powder, Hydrocerussitum (Ceruse), magnesium oxide, sulfuration Asia manganese, aluminium oxide, cathode copper, graphite powder, fat
Acid, cutting agent, lubricant, hardening agent, binding agent, viscosifier, antiwear additive, processing aid, regulator import in spice cylinder together
Being stirred forming mixed powder, filtered by drainage screen after stirring, in mixed powder, raw meal particle size is coarser than 140 mesh
Particulate matter be isolated collection after carry out pulverizing screening again, be subsequently poured in each standard dose bucket standby;
The preparation method of described cutting agent, comprises the following steps:
Step 1, will cutting oil, tricresyl phosphate propyl ester, dinonylnaphthalene sulfonic acid calcium, 2,6 ditertiary butyl p cresol, laurylene base
Succinic acid, triethanolamine borate, polyacrylamide, dodecylbenzene sodium sulfonate, benzoic acid mix homogeneously, then by mixture
It is heated to 52 DEG C;
Step 2, adds remaining ingredient in step 1 gained mixture, continues to be heated to 76 DEG C, and be incubated 3.5h, prepare
Cutting agent;
Described lubricant is prepared by following preparation method:
The raw material components of lubricant is joined in reactor and react 19h in 420 DEG C, then use after solidification and particle is had
There is the cone mill of clipping power as mechanical dispersion equipment, be ground dispersion, prepare lubricant;
S2: the mixed powder in the standard dose bucket prepare step S1 is directly poured in pressed compact mould, at forcing press
Pressure is to suppress under 520MPa, makes the shape of part blank;
S3: blank step S2 prepared is sent in heating furnace and is sintered, and heating-up temperature is 720 DEG C, is formed after cooling
Fine and close semi-finished product;
S4: surface of semi-finished step S3 prepared is placed on shelf after being coated with antirust oil and carries out 2 days Ageing Treatment;
S5: the semi-finished product that the Ageing Treatment that step S4 prepares is crossed are carried out shaping and surface polishing, forms standardized product.
Embodiment 3
A kind of novel energy-conserving powder metallurgy, in units of weight, is made up of following raw material: water-atomized iron powder 195 parts, nikel powder
6 parts, 3 parts of Hydrocerussitum (Ceruse), magnesium oxide 2 parts, sulfuration sub-1.8 parts of manganese, aluminium oxide 1.4 parts, cathode copper 1.5 parts, graphite powder 1 part, fatty acid 5
Part, cutting 0.4-0.6 part, lubricant 0.6 part, hardening agent 0.2 part, binding agent 0.8 part, viscosifier 0.2 part, antiwear additive 0.8 part,
Processing aid 0.3 part, regulator 0.2 part;
Described water-atomized iron powder, nikel powder, Hydrocerussitum (Ceruse), magnesium oxide, sulfuration Asia manganese, aluminium oxide, cathode copper, graphite powder granularity equal
For 0.1-100 μm;
Described cutting agent, in units of weight, is made up of following raw material: cutting oil 16 parts, tricresyl phosphate propyl ester 12 parts, two nonyls
Base LOMAR PWA EINECS 246-676-2 calcium 6 parts, 2,6 ditertiary butyl p cresol 10 parts, dodecenylsuccinic acid 7 parts, triethanolamine borate 12 parts, poly-
Acrylamide 12 parts, dodecylbenzene sodium sulfonate 10 parts, 9 parts of benzoic acid, oleamide 8 parts, tetrasodium ethylenediamine tetraacetate 6 parts,
Amino carboxylic acid quasi-chelate compound 2 parts, Polyethylene Glycol 14 parts;
Described lubricant, in units of weight, is made up of following raw material: 40 parts of polyvinyl isobutyl ether, chlorinated paraffin 14
Part, magnesium oxide particle 8 parts, fatty acid zinc 12 parts, carboxylic acid amide 14 parts, acetate butyl 15 parts, boric acid 10 parts, N-crassitude
Ketone 12 parts, dimethylformamide 10 parts;
Described hardening agent is 701 powder hardening agents;
Described binding agent is mixed by fatty acid zinc and machine oil 2-5:1-2 in mass ratio;
Described viscosifier are glycidoxy-propyltrimethoxy silane;
Described antiwear additive is silicon dioxide;
Described processing aid is Manganese monosulfide.;
Described regulator is esters of acrylic acid regulator;
The preparation method of described novel energy-conserving powder metallurgy, comprises the following steps:
S1: the iron powder that makes water fogging, nikel powder, Hydrocerussitum (Ceruse), magnesium oxide, sulfuration Asia manganese, aluminium oxide, cathode copper, graphite powder, fat
Acid, cutting agent, lubricant, hardening agent, binding agent, viscosifier, antiwear additive, processing aid, regulator import in spice cylinder together
Being stirred forming mixed powder, filtered by drainage screen after stirring, in mixed powder, raw meal particle size is coarser than 160 mesh
Particulate matter be isolated collection after carry out pulverizing screening again, be subsequently poured in each standard dose bucket standby;
The preparation method of described cutting agent, comprises the following steps:
Step 1, will cutting oil, tricresyl phosphate propyl ester, dinonylnaphthalene sulfonic acid calcium, 2,6 ditertiary butyl p cresol, laurylene base
Succinic acid, triethanolamine borate, polyacrylamide, dodecylbenzene sodium sulfonate, benzoic acid mix homogeneously, then by mixture
It is heated to 58 DEG C;
Step 2, adds remaining ingredient in step 1 gained mixture, continues to be heated to 76-92 DEG C, and be incubated 2.5-
3.5h, prepares cutting agent;
Described lubricant is prepared by following preparation method:
The raw material components of lubricant is joined in reactor and react 11h in 480 DEG C, then use after solidification and particle is had
There is the cone mill of clipping power as mechanical dispersion equipment, be ground dispersion, prepare lubricant;
S2: the mixed powder in the standard dose bucket prepare step S1 is directly poured in pressed compact mould, at forcing press
Pressure is to suppress under 580MPa, makes the shape of part blank;
S3: blank step S2 prepared is sent in heating furnace and is sintered, and heating-up temperature is 840 DEG C, is formed after cooling
Fine and close semi-finished product;
S4: surface of semi-finished step S3 prepared is placed on shelf after being coated with antirust oil and carries out 6 days Ageing Treatment;
S5: the semi-finished product that the Ageing Treatment that step S4 prepares is crossed are carried out shaping and surface polishing, forms standardized product.
Following table lists embodiment of the present invention 1-3 novel energy-conserving powder metallurgy prescription, conventional powder metallurgy prescription and pure iron
Powder prepares product contrast in hot strength and hardness, and result is as shown in the table.
By in table it can be seen that use after novel energy-conserving powder metallurgy prescription of the present invention, the hot strength of product and hardness
All obtain significant raising.
Above content it cannot be assumed that the present invention be embodied as be confined to these explanation, technology belonging to the present invention is led
For the those of ordinary skill in territory, without departing from the inventive concept of the premise, it is also possible to make some simple deduction or replace,
All should be considered as belonging to the scope of patent protection that the present invention is determined by the claims submitted to.
Claims (7)
1. a novel energy-conserving powder metallurgy, it is characterised in that in units of weight, is made up of following raw material: water-atomized iron powder
132-195 part, nikel powder 4-6 part, Hydrocerussitum (Ceruse) 2-3 part, magnesium oxide 1-2 part, the sub-manganese 1.2-1.8 part of sulfuration, aluminium oxide 0.9-1.4 part,
Cathode copper 0.8-1.5 part, graphite powder 0.6-1 part, fatty acid 3-5 part, cutting agent 0.4-0.6 part, lubricant 0.3-0.6 part, strong
Agent 0.1-0.2 part, binding agent 0.6-0.8 part, viscosifier 0.1-0.2 part, antiwear additive 0.5-0.8 part, processing aid 0.2-0.3
Part, regulator 0.1-0.2 part;
Described water-atomized iron powder, nikel powder, Hydrocerussitum (Ceruse), magnesium oxide, sulfuration Asia manganese, aluminium oxide, cathode copper, the granularity of graphite powder are
0.1-100μm;
Described cutting agent, in units of weight, is made up of following raw material: cutting oil 14-16 part, tricresyl phosphate propyl ester 10-12 part, two
Nonyl LOMAR PWA EINECS 246-676-2 calcium 4-6 part, 2,6 ditertiary butyl p cresol 6-10 part, dodecenylsuccinic acid 5-7 part, triethanolamine borate
8-12 part, polyacrylamide 6-12 part, dodecylbenzene sodium sulfonate 8-10 part, benzoic acid 6-9 part, oleamide 3-8 part, second two
Amine tetraacethyl four sodium 2-6 part, amino carboxylic acid quasi-chelate compound 1-2 part, Polyethylene Glycol 8-14 part;
Described lubricant, in units of weight, is made up of following raw material: polyvinyl isobutyl ether 20-40 part, chlorinated paraffin 8-14
Part, magnesium oxide particle 4-8 part, fatty acid zinc 6-12 part, carboxylic acid amide 8-14 part, acetate butyl 12-15 part, boric acid 6-10 part,
N-Methyl pyrrolidone 7-12 part, dimethylformamide 6-10 part;
The preparation method of described novel energy-conserving powder metallurgy, comprises the following steps:
S1: the iron powder that makes water fogging, nikel powder, Hydrocerussitum (Ceruse), magnesium oxide, sulfuration Asia manganese, aluminium oxide, cathode copper, graphite powder, fatty acid, cut
Cut agent, lubricant, hardening agent, binding agent, viscosifier, antiwear additive, processing aid, regulator to import together in spice cylinder and stir
Mixing formation mixed powder, filtered by drainage screen after stirring, in mixed powder, raw meal particle size is coarser than 140-160 purpose
Particulate matter carries out pulverizing screening after being isolated collection again, is subsequently poured in each standard dose bucket standby;
The preparation method of described cutting agent, comprises the following steps:
Step 1, will cutting oil, tricresyl phosphate propyl ester, dinonylnaphthalene sulfonic acid calcium, 2,6 ditertiary butyl p cresol, laurylene base fourth two
Acid, triethanolamine borate, polyacrylamide, dodecylbenzene sodium sulfonate, benzoic acid mix homogeneously, then heat mixture
To 52-58 DEG C;
Step 2, adds remaining ingredient in step 1 gained mixture, continues to be heated to 76-92 DEG C, and be incubated 2.5-3.5h, system
Obtain cutting agent;
Described lubricant is prepared by following preparation method:
The raw material components of lubricant is joined in reactor and react 11-19h in 420-480 DEG C, then use grain after solidification
Son has the cone mill of clipping power as mechanical dispersion equipment, is ground dispersion, prepares lubricant;
S2: the mixed powder in the standard dose bucket prepare step S1 is directly poured in pressed compact mould, at the pressure of forcing press
For suppressing under 520-580MPa, make the shape of part blank;
S3: blank step S2 prepared is sent in heating furnace and is sintered, and heating-up temperature is 720-840 DEG C, is formed after cooling
Fine and close semi-finished product;
S4: surface of semi-finished step S3 prepared is placed on shelf after being coated with antirust oil and carries out 2-6 days Ageing Treatment;
S5: the semi-finished product that the Ageing Treatment that step S4 prepares is crossed are carried out shaping and surface polishing, forms standardized product.
Novel energy-conserving powder metallurgy the most according to claim 1, it is characterised in that described hardening agent is 701 powder hardening agents.
Novel energy-conserving powder metallurgy the most according to claim 1, it is characterised in that described binding agent is by fatty acid zinc and machine
Oil 2-5:1-2 in mass ratio mixes.
Novel energy-conserving powder metallurgy the most according to claim 1, it is characterised in that described viscosifier are epoxypropoxy
Trimethoxy silane.
Novel energy-conserving powder metallurgy the most according to claim 1, it is characterised in that described antiwear additive is silicon dioxide.
Novel energy-conserving powder metallurgy the most according to claim 1, it is characterised in that described processing aid is Manganese monosulfide..
Novel energy-conserving powder metallurgy the most according to claim 1, it is characterised in that described regulator is that esters of acrylic acid is adjusted
Joint agent.
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CN108559930A (en) * | 2018-04-02 | 2018-09-21 | 张庆 | A kind of iron-base powder metallurgy material and preparation method thereof |
CN110834093A (en) * | 2019-11-06 | 2020-02-25 | 南通冠达粉末冶金有限公司 | Energy-saving powder metallurgy process |
CN115678649A (en) * | 2022-09-30 | 2023-02-03 | 四川省星船城水泥股份有限公司 | Method for manufacturing gate valve of wind-heat air duct of rotary cement kiln |
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CN102921945A (en) * | 2012-11-21 | 2013-02-13 | 王恒傲 | Powder metallurgy formula and powder metallurgy method thereof |
CN103865617A (en) * | 2014-03-10 | 2014-06-18 | 苏州捷德瑞精密机械有限公司 | Lubrication cutting agent and preparation method thereof |
CN104096835A (en) * | 2014-07-18 | 2014-10-15 | 常熟市迅达粉末冶金有限公司 | Energy-saving powder metallurgy process |
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CN102921945A (en) * | 2012-11-21 | 2013-02-13 | 王恒傲 | Powder metallurgy formula and powder metallurgy method thereof |
CN103865617A (en) * | 2014-03-10 | 2014-06-18 | 苏州捷德瑞精密机械有限公司 | Lubrication cutting agent and preparation method thereof |
CN104096835A (en) * | 2014-07-18 | 2014-10-15 | 常熟市迅达粉末冶金有限公司 | Energy-saving powder metallurgy process |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
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CN108559930A (en) * | 2018-04-02 | 2018-09-21 | 张庆 | A kind of iron-base powder metallurgy material and preparation method thereof |
CN110834093A (en) * | 2019-11-06 | 2020-02-25 | 南通冠达粉末冶金有限公司 | Energy-saving powder metallurgy process |
CN115678649A (en) * | 2022-09-30 | 2023-02-03 | 四川省星船城水泥股份有限公司 | Method for manufacturing gate valve of wind-heat air duct of rotary cement kiln |
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