CN1062415A - Method and device for manufacturing segmented deposition ferrograph - Google Patents

Method and device for manufacturing segmented deposition ferrograph Download PDF

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Publication number
CN1062415A
CN1062415A CN 90109739 CN90109739A CN1062415A CN 1062415 A CN1062415 A CN 1062415A CN 90109739 CN90109739 CN 90109739 CN 90109739 A CN90109739 A CN 90109739A CN 1062415 A CN1062415 A CN 1062415A
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substrate
wedge shape
magnetic
yoke
ferrograph
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CN 90109739
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CN1022466C (en
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杨志伊
夏德胜
舒凤翔
王晓雷
杨广有
唐小行
李浩平
高贺凤
程坚
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China University of Mining and Technology CUMT
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China University of Mining and Technology CUMT
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Abstract

A method for preparing the segmental deposited ferrograph features that the flowing direction of liquid medium to be tested is parallel to the direction of magnetic field. The magnetic head of the device is arranged by a magnet and a filling block of nonmagnetic material with the same shape at intervals in parallel, a group of shoe-like pole shoes are attached to the upper surface of the magnetic head, yoke irons are installed at the lower end and two sides of the magnetic head, and non-magnetic-conductive materials are filled between the pole shoes and between the magnet and the yoke irons, so that spacing magnetic fields with different magnetic field strengths are formed above gaps between the pole shoes and between the yoke irons, and a current limiting plate made of non-wetting material with liquid medium is arranged on a substrate, so that the inclination of the magnetic head can be adjusted, and the device is simple in structure and excellent in spectrum making.

Description

A kind of making sublevel sedimentary iron spectrum and device thereof
The present invention relates to the iron that abrasive dust is used in a kind of analytic liquid body medium and compose the method for work and device thereof, be particularly related to a kind of ferromagnetic abrasive dust that is used in the separating liquid medium, make ferromagnetic abrasive particle by size regularly segmented deposition on iron spectrum substrate, the spectrum sheet is observed, thereby the iron that abrasive particle carries out qualitative and quantitative analysis is composed the method for work and device thereof.
When making the iron spectrum sheet that abrasive dust is used in the analytic liquid body medium with existing analyzing ferrogram machine, the flow direction of the fluid to be measured medium on it all is vertical at on-chip projecting direction with the magnetic line of force of field region, used ferrograph basic structure is with two block permanent magnets and pole shoe, yoke is formed a rectangular gap magnetic field, the magnetic line of force of its work field region is at the flow direction perpendicular quadrature of on-chip projecting direction and liquid medium (as oil sample), therefore, after oil sample was extracted on the substrate by peristaltic pump, the ferromagnetic particle in the oil sample was deposited on the substrate by size in magnetic field force effect lower edge magnetic line of force direction.Because the magnetic line of force of its work field region is at on-chip projecting direction and liquid medium flow direction perpendicular quadrature, the deposition that at first flows through the ferromagnetic particle in the liquid medium in work magnetic field certainly will play inhibition (as " dykes and dams ") to follow-up liquid, and the track of liquid stream is affected.Especially near the liquid medium inflow end in work magnetic field,, make the zone of the deposited particles formation " spindle shape " in whole work magnetic field because the ferromagnetic particle settled density is big.The packing phenomenon of inlet end sedimentary province field width and particle is more serious, thereby has a strong impact on the reliability of spectrum sheet qualitative and quantitative analysis.In addition, the angle of inclination of substrate can only be 1-2 ° because of the influence that is subjected to magnetic field intensity, because if the excessive inlet end in inclination angle is too far away from the magnetic field distance, magnetic field intensity there is too little, will influence deposition efficiency, and impel liquid medium little along the downslide component that substrate flows, liquid flow is slower, the contamination particle of some nonferromagnetics has time enough to deposit on substrate, many contamination particles is arranged simultaneously because of before " climbing only dykes and dams " be blocked in " strut rail " ferromagnetic field particle chain in liquid medium stream.Therefore this analyzing ferrogram machine dirt-removing power when making the spectrum sheet is very poor, and contamination particle is stayed on the substrate in a large number, even " flooded " the interested ferromagnetic particle of people, and cause qualitative iron spectrum to observe difficulty, quantitatively iron spectrum reading also causes extreme inaccurate because of the contamination particle shading.
For guaranteeing that liquid medium above the work magnetic field of all flowing through on the iron spectrum substrate, needs fixed current limliting groove on substrate, this just makes substrate make difficulty, cost height.
The liquid medium of existing rotary-ferrograph and magnetic line of force direction tangent (magnetic line of force for radially, liquid medium flows through work magnetic field along hand of helix) have certain angle therebetween.And this rotary-ferrograph because of must have whirligig and its rotating speed of control steadily and the electronic circuit of record rotating speed cause its complex structure, price is more expensive.
The objective of the invention is to propose a kind of liquid medium flow direction and magnetic line of force in work magnetic field of making and compose the sheet method for making at the iron that on-chip projecting direction is parallel to each other; The liquid medium that has a ferromagnetic particle is deposited on the ferromagnetic particle piecewise to form iron spectrum sheet on the substrate flowing through work field region that several are parallel to each other, are mutually independent, discontinuous on the substrate.For this reason, the present invention proposes segmented deposition formula ferrograph for a kind of simple in structure, cheap, the reliable operation that reaches that this purpose designs.When becoming spectrum with this ferrograph, iron spectrum substrate can with magnetic head with arbitrarily angled inclination to adapt to the needs of removing or keeping dissimilar non-ferromagnetic debris.The magnetic field intensity in the magnetic field that the perform region is parallel to each other can be mutually the same and different, and its arrangement can be linear or nonlinear, but to increase progressively or evenly distributed for good.The purpose of doing like this is: the chain sedimentary province and the liquid medium flow direction that form of the ferromagnetic particle of deposition is consistent earlier for (1) liquid medium flow direction parallel with the direction of the projection of the work field region magnetic line of force on the spectrum sheet (and with the magnetic line of force acute angle) each other, can not cause the accumulation of particle.(2) substrate and magnetic head are convenient to cleaning with arbitrarily angled inclination and are removed contamination particle when the inclination angle is 1 °-2 ° (but the interested non-ferromagnetic debris of retention analysis personnel) again.
The method for making of the iron spectrum of the segmented deposition of the present invention's proposition is for this reason:
1, on the substrate that tilts, forms the shape magnetic field, bar crack of longitudinal separation, the intensity in this each shape magnetic field, bar crack is linearity or nonlinearities change from the arrangement of inclination top from the below of substrate, to spare strong or to increase progressively to good, and the magnetic line of force of the field region in each shape magnetic field, bar crack is parallel with the substrate longitudinal direction at on-chip projecting direction.
2, instillation fluid to be measured medium, keeps flowing in the parallel direction of on-chip projecting direction with the magnetic line of force of each bar crack property field region, and crosses over each slit, magnetic field along the inclination substrate according to its gravity on described substrate.
3, take off substrate, preserve and be deposited on on-chip abrasive dust iron spectrum for analyzing usefulness.
This step also can be described as:
(1), on substrate, form longitudinal separation, magnetic field intensity be linear or nonlinear variation, with increase progressively or even be by force good, and the magnetic line of force of field region is in several crack property magnetic fields of on-chip projecting direction and substrate parallel longitudinal.
(2), according to test solution body medium pollution level substrate is tilted, arrange under the situation about increasing progressively in magnetic field intensity, make the most weak magnetic field of magnetic field intensity be positioned at eminence, annotate and drip the test solution body medium on substrate, make the gravity of test solution body medium by itself, maintenance is flowed in the parallel direction of on-chip projecting direction with the magnetic line of force of on-chip field region and is crossed over each magnetic field.
(3), take off together with substrate, because of bar crack shape the action of a magnetic field segmented deposition is composed at on-chip iron.
The device that the method that proposes with the present invention is made segmented deposition iron spectrum be segmented deposition formula ferrograph mainly by magnetic head, substrate, current limiting plate and fulcrum arrangement are formed.The magnet that described magnetic head has or the polylith parallel interval is placed, perhaps also can be the filling block parallel interval placement that one or more rectangle magnet nonmagnetic substance the same with described rectangle magnet geomery with one or more made, " class wedge shape " pole shoe that the one deck that respectively reclines above described rectangle magnet or rectangle magnet and filling block is made with high permeability material, should have the gap of filling between " class wedge shape " pole shoe with the non-magnetic material, the tabular yoke iron that below described rectangle magnet and filling block, reclines and settle a high magnetic conductive material to make, described tabular yoke iron two ends respectively recline and settle " class wedge shape " yoke of a high permeability material, should " class wedge shape " yoke respectively and have the gap of non-magnet material filling between above-mentioned " class wedge shape " pole shoe, thereby constitute magnetic circuit system.All fill nonmagnetic substance in the space between described pole shoe, yoke and rectangle magnet and filling block (if having filling block).Magnetic head is integrally placed shell.
Substrate is placed on the upper surface of magnetic head, recline with the upper surface of described " class wedge shape " pole shoe, " class wedge shape " yoke, therefore on substrate, the top that is positioned on the gap between " class boot-shaped " yoke and " class boot last " pole shoe forms at interval, separate magnetic field parallel to each other, and the magnetic line of force of this field region is at on-chip projecting direction and magnetic head parallel longitudinal.
Current limiting plate places on the substrate, current limiting plate is made by the nonwettable material of liquid medium, polytetrafluoroethylene for example, current limiting plate is tabular, its one side that contacts with substrate has the rib with some longitudinal extensions of its all-in-one-piece, and one be positioned at the lengthways of rod termination and this lengthways of rod joins and the horizontal rib of all-in-one-piece, the current limliting groove that constitutes between the lengthways of rod have a through hole near horizontal rib place so that the fluid to be measured medium injects and along mobile along substrate in the current limliting groove institute limit scope.
The shell that magnetic head an is housed end longitudinally is articulated on the fulcrum arrangement, the magnetic head other end is supported on and promotes magnetic head and make on its magnetic head inclination stationary installation that favours different degree of tilt, and magnetic head is together with substrate placed on it and current limiting plate can tilt in 0-85 ° of scope and fix.
Because it is that the magnetic line of force of field region on flow direction and the substrate of test solution body medium is parallel in on-chip projecting direction direction that the iron that the present invention proposes is composed as method.According to the geometric position in shape magnetic field, bar crack, the ferromagnetism abrasive dust is with segmented deposition, because the magnetic that big abrasive dust itself has is apart from big, in following magnetic field force induced big deposition earlier of identical external magnetic field effect; Deposit behind the in like manner less ferromagnetism abrasive dust.Therefore near the deposition earlier of big abrasive dust in the magnetic field of working together that splashes into a little, the work abrasive dust size that deposits in the magnetic field of bar crack shape a little far away is gradually little from splashing into, and the average-size that is to say the abrasive dust that deposits in the work magnetic field is from splashing into far away more more little of a distance.Therefore be highly advantageous to the qualitative and quantitative analysis of iron spectrum, and degree of tilt is adjustable, is applicable to that the liquid medium of different pollution levels is made the iron spectrum, dirt-removing power is also strong, and its structure is very simple in addition, and cost is very cheap.
That is to say that the iron that the present invention proposes a kind of segmented deposition composes the method for work, steps of the method are:
(1) on substrate, form longitudinal separation, be parallel to each other separately, magnetic field intensity is arranged and is linearity or nonlinearities change, and the magnetic line of force of field region is in several crack shapes of the projecting direction of substrate and substrate parallel longitudinal magnetic fields of working;
(2) according to test solution body medium pollution level, substrate and magnetic head are tilted together, arrange under the situation about increasing progressively in magnetic field intensity, make the most weak magnetic field of magnetic field intensity be positioned at eminence, annotate to drip the test solution body medium on substrate, make the test solution body medium rely on itself gravity in current limliting groove institute limit scope, to keep the magnetic line of force with on-chip field region in parallel each magnetic field of the mobile leap of direction of on-chip projecting direction;
(3) take off because of bar crack shape the action of a magnetic field segmented deposition together with substrate and compose at on-chip iron;
The described magnetic head that the ferrograph of the iron spectrum of described making segmented deposition has has one or more magnet (5), the filling block (1) that one or more nonferromugnetic material the same with described magnet (5) geomery is made, this magnet (5) is placed with filling block (1) parallel interval and is reclined respectively thereon and settles " class wedge shape " pole shoe (2), its below then reclines with utmost point shape yoke (10), arrangement one " class wedge shape " yoke (3) reclines respectively in the two ends of described tabular yoke iron (10), has gap (12) between described " class wedge " pole shoe (2) and between this pole shoe and " class wedge shape " yoke (3) with the filling of non-magnetic material, (13), (14), magnetic head integral body is inserted in the shell (9), vertical end of shell is articulated on the chassis (19), and other end is fixing with fulcrum arrangement (4) supporting of adjustable tilt degree longitudinally for it;
Described substrate (6) is the plain film that a non-magnet material is made, and places on the magnetic head, leans with baffle plate (18);
Described ferrograph also has a current limiting plate (17), this current limiting plate (17) downside has some the ribs 24 along its longitudinal extension that become one with current limiting plate (17), this rib 24 constitutes current limliting groove (20) and interval trough (23), also have with rib (24) at an end of rib (24) and to join and all-in-one-piece transverse rod strip (21), (22) communicate with current limliting groove (20) to locate to have through hole near this transverse rod strip (21), the end face of rib (24) and transverse rod strip (21) on a plane, and with substrate (16) near;
The inclined-plane of " class wedge shape " pole shoe (2) and described " class wedge shape " yoke (3) is the plane described in the described segmented deposition formula ferrograph, and this plane and its wire clamp angle, center are 5 °~85 °;
The inclined-plane with described " class wedge shape " yoke (3) of " class wedge shape " pole shoe is a curved surface described in the described segmented deposition formula ferrograph;
The width of between " class wedge shape " pole shoe (2) and the gap (12) between " class wedge shape " pole shoe (2) and " class wedge shape " yoke (3), (13), (14) described in the described segmented deposition formula ferrograph and be identical highly;
The height and the width in gap are different described in the described segmented deposition formula ferrograph, and height is between 0~5mm, and width is between 0.1~5mm;
Current limiting plate (17) is made by the non-wettable material of liquid medium described in the described segmented deposition formula ferrograph, polytetrafluoroethylene for example, and the rib on it (24) width is between 0.1~10mm.
Elaborate below in conjunction with the method for making and the device thereof of accompanying drawing to the segmented deposition iron spectrum of the present invention's proposition.
Fig. 1 is the diagrammatic cross-section of the segmented deposition formula ferrograph that proposes of the present invention;
Fig. 2 is the schematic top plan view of the segmented deposition formula ferrograph that proposes of the present invention shown in Figure 1;
Fig. 3 is the magnetic head cross-sectional schematic;
Fig. 4 is the schematic top plan view of magnetic head shown in Figure 3;
Fig. 5 is the current limiting plate diagrammatic cross-section;
Fig. 6 is that current limiting plate partial side shown in Figure 5 is cutd open synoptic diagram.
See Fig. 1 and Fig. 3 for details, magnetic head A is installed in the shell 9, an end longitudinally of shell 9 is articulated on the support 11 on the chassis 19 and can rotates around pivot is becoming 85 ° scope from the level to the surface level in, fixing on its other end by fulcrum arrangement 4 supportings, make magnetic head and shell 9 thereof be obliquity, rectangle magnet 5 and nonmagnetic substance are made, and geomery and described rectangular magnets and identical filling block 1 are parallel to each other and place at interval.In the described rectangular magnets 5 and the arrangement that reclines respectively above the described filling block, " class wedge shape " pole shoe 2 made from high permeability material that geomery is identical, has the gap 12 of filling between this bipolar shoe 2 with non-magnetic material, the tabular yoke iron 10 that reclines below described rectangle magnet 5 and the filling block 1 and settle a high permeability material to make, " class wedge shape " yoke 3 that high permeability material is made of arrangement respectively reclines at these yoke 10 two ends, should " class wedge shape " yoke 3 respectively and have gap 13 and 14 between above-mentioned " class wedge shape " pole shoe with the non-magnet material filling, at described pole shoe, equal filling non-magnetic material 15 in the space between the yoke.Substrate 16 reclines and is placed in the magnetic head upper surface, current limiting plate 17 recline be placed in above the substrate 16, substrate 16 and current limiting plate 17 all be fixed on baffle plate 18 on the shell 9 and stop and prevent its downslide.Current limiting plate 17 is tabular, rib 24(Fig. 5 and Fig. 6 of having six longitudinal extensions below it), this rib width is 0.1~10mm, constitute current limliting groove 20 and isolation channel 23 between this rib 24, one end of rib 24 has coupled transverse rod strip 21, have through hole 22 near transverse rod strip 21 places, communicate, inject current limliting groove 20 for the test solution body medium with this current limliting groove 20.The end face of rib 24 and transverse rod strip 21 is entirely in the same plane, and reclines with substrate 16.
Pollution level according to the test solution body medium, regulate supporting fixed device 4, make magnetic head favour certain angle, the test solution body medium injected from the hole 22 of current limiting plate 17 together with shell 9 and substrate 16 and current limiting plate 17, the test solution body medium along current limliting groove 20 on substrate along vertically flowing.Because between " class wedge shape " pole shoe 2, and this pole shoe 2 is parallel with the longitudinal direction of magnetic head A at on-chip projecting direction at the magnetic line of force of the field region of the respective surfaces formation of substrate 16 with the gap location 13,12,14 between " class wedge shape " yoke 3, therefore, this test solution body medium flow direction that vertically flows is also parallel at on-chip projecting direction with the magnetic line of force of field region.Gap width between " class wedge shape " pole shoe 2 and " class wedge shape " yoke 3 is 0.1~5mm.The thickness of gap location " class wedge shape " pole shoe 2 and " class wedge shape " yoke 3 (promptly the height in gap) therebetween is 0~5mm.The wedge shape inclined-plane of " class wedge shape " pole shoe and " class wedge shape " yoke and the angle of wedge shape center vertical line are 5 °~85 °.This wedge shape inclined-plane can be the plane and also can be curved surface.When only with a block length square magnet 5, gap 14 place's magnetic field intensitys away from this rectangle magnet 5 are the most weak, the magnetic field intensity at 12 places, gap between " class wedge shape " pole shoe 2 is strong and the strongest near the magnetic field at 13 places, gap at rectangle magnet 5 places, this just is suitable for the segmented deposition of the ferromagnetism abrasive dust of different size granularity, and the shape that can change clearance height, width and " class wedge shape " pole shoe 2 and " class wedge shape " yoke 3 inclined-planes magnetic field intensity that changes each gap location is with the segmented deposition of the ferromagnetism abrasive dust that is fit to the different size granularity.
Current limiting plate 17 is made with liquid medium non-infiltration material polytetrafluoroethylene, can prevent like this current limiting plate 17 and the slit that reclines between the substrate 16 of liquid medium on being placed on substrate 16, because capillary tension effect and to the other seepage of side, this has not only simplified substrate greatly must have the structure of fixed current limliting groove but also easy to use.

Claims (7)

1, a kind of iron of segmented deposition is composed the method for work, it is characterized in that, steps of the method are:
(1) on substrate, form longitudinal separation, be parallel to each other separately, magnetic field intensity is arranged and is linearity or nonlinearities change, and the magnetic line of force of field region is in several crack shapes of the projecting direction of substrate and substrate parallel longitudinal magnetic fields of working;
(2) according to test solution body medium pollution level, substrate and magnetic head are tilted together, arrange under the situation about increasing progressively in magnetic field intensity, make the most weak magnetic field of magnetic field intensity be positioned at eminence, annotate to drip the test solution body medium on substrate, make the test solution body medium rely on itself gravity in current limliting groove institute limit scope, to keep the magnetic line of force with on-chip field region in parallel each magnetic field of the mobile leap of direction of on-chip projecting direction;
(3) take off because of bar crack shape the action of a magnetic field segmented deposition together with substrate and compose at on-chip iron.
2, a kind of segmented deposition formula ferrograph, this ferrograph comprises: magnetic head, substrate, current limiting plate and fulcrum arrangement, it is characterized in that: the described magnetic head that described ferrograph has has one or more magnet (5), the filling block (1) that one or more nonferromugnetic material the same with described magnet (5) geomery is made, this magnet (5) is placed with filling block (1) parallel interval and is reclined respectively thereon and settles " class wedge shape " pole shoe (2), its below then reclines with utmost point shape yoke (10), arrangement one " class wedge shape " yoke (3) reclines respectively in the two ends of described tabular yoke iron (10), has gap (12) between described " class wedge " pole shoe (2) and between this pole shoe and " class wedge shape " yoke (3) with the filling of non-magnetic material, (13), (14), magnetic head integral body is inserted in the shell (9), vertical end of shell is articulated on the chassis (19), and other end is fixing with fulcrum arrangement (4) supporting of adjustable tilt degree longitudinally for it;
Described substrate (6) is the plain film that a non-magnet material is made, and places on the magnetic head, leans with baffle plate (18);
Described ferrograph also has a current limiting plate (17), this current limiting plate (17) downside has some the ribs 24 along its longitudinal extension that become one with current limiting plate (17), this rib 24 constitutes current limliting groove (20) and interval trough (23), also have with rib (24) at an end of rib (24) and to join and all-in-one-piece transverse rod strip (21), (22) communicate with current limliting groove (20) to locate to have through hole near this transverse rod strip (21), the end face of rib (24) and transverse rod strip (21) on a plane, and with substrate (16) near.
According to the described segmented deposition formula of claim 2 ferrograph, it is characterized in that 3, the inclined-plane of described " class wedge shape " pole shoe (2) and described " class wedge shape " yoke (3) is the plane, this plane and its wire clamp angle, center are 5 °~85 °.
According to the described segmented deposition formula of claim 2 ferrograph, it is characterized in that 4, the inclined-plane with described " class wedge shape " yoke (3) of described " class wedge shape " pole shoe is a curved surface.
5, according to claim 3 or 4 described segmented deposition formula ferrographs, it is characterized in that the width of between described " class wedge shape " pole shoe (2) and the gap (12) between " class wedge shape " pole shoe (2) and " class wedge shape " yoke (3), (13), (14) and be identical highly.
6, according to claim 3 or 4 described segmented deposition formula ferrographs, it is characterized in that: the height and the width in described gap are different, and height is between 0~5mm, and width is between 0.1~5mm.
7, segmented deposition formula ferrograph according to claim 6 is characterized in that, described current limiting plate (17) is made by the non-wettable material of liquid medium, polytetrafluoroethylene for example, and the rib on it (24) width is between 0.1~10mm.
CN 90109739 1990-12-12 1990-12-12 Sectional deposition type iron spectrum device Expired - Fee Related CN1022466C (en)

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Application Number Priority Date Filing Date Title
CN 90109739 CN1022466C (en) 1990-12-12 1990-12-12 Sectional deposition type iron spectrum device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 90109739 CN1022466C (en) 1990-12-12 1990-12-12 Sectional deposition type iron spectrum device

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CN1062415A true CN1062415A (en) 1992-07-01
CN1022466C CN1022466C (en) 1993-10-20

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102519753A (en) * 2011-11-18 2012-06-27 武汉理工大学 Magnetic iron spectral collecting device
CN103358322A (en) * 2012-04-02 2013-10-23 精工爱普生株式会社 Robot
CN110595963A (en) * 2019-10-14 2019-12-20 中国矿业大学 Online rotary ferrograph and online oil monitoring method of equipment
CN111282713A (en) * 2020-02-14 2020-06-16 山东大学 Electromagnetic device and method for ordered deposition of wear particles

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102519753A (en) * 2011-11-18 2012-06-27 武汉理工大学 Magnetic iron spectral collecting device
CN103358322A (en) * 2012-04-02 2013-10-23 精工爱普生株式会社 Robot
CN110595963A (en) * 2019-10-14 2019-12-20 中国矿业大学 Online rotary ferrograph and online oil monitoring method of equipment
CN110595963B (en) * 2019-10-14 2024-03-22 中国矿业大学 Online rotary ferrograph and equipment oil online monitoring method
CN111282713A (en) * 2020-02-14 2020-06-16 山东大学 Electromagnetic device and method for ordered deposition of wear particles
WO2021159908A1 (en) * 2020-02-14 2021-08-19 山东大学 Electromagnetic device for ordered deposition of wear particles and method
CN111282713B (en) * 2020-02-14 2021-11-12 山东大学 Electromagnetic device and method for ordered deposition of wear particles

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