CN106226198A - Slow-release solid solubility property Lab-evaluation device - Google Patents
Slow-release solid solubility property Lab-evaluation device Download PDFInfo
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- CN106226198A CN106226198A CN201610700271.7A CN201610700271A CN106226198A CN 106226198 A CN106226198 A CN 106226198A CN 201610700271 A CN201610700271 A CN 201610700271A CN 106226198 A CN106226198 A CN 106226198A
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- Prior art keywords
- slow
- lab
- release solid
- evaluation device
- solubility property
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N13/00—Investigating surface or boundary effects, e.g. wetting power; Investigating diffusion effects; Analysing materials by determining surface, boundary, or diffusion effects
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
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- Sampling And Sample Adjustment (AREA)
Abstract
The invention discloses a kind of slow-release solid solubility property Lab-evaluation device, including pass sequentially through connect pipeline and be attached liquid pump, effusion meter, heater, pit shaft simulator, analytical sampling mouth;Liquid pump can regulate injected media speed, and flowmeter survey medium flows through the speed of pit shaft simulator, and heater is the firing equipment of temperature-adjustable.The present invention can the impact on solid rate of release with simulation wellbore hole temperature and water velocity, solid course of dissolution in the wellbore can be observed again, can more efficiently evaluate slow-release solid state in the wellbore.
Description
Technical field
The present invention relates to mechanical design field, especially a kind of slow-release solid solubility property Lab-evaluation device.
Background technology
Along with the development of oil & gas industry, the slow-release solid class material with slow solubility property is constantly researched and developed and throws
Enter to use, the products such as such as spacetabs type anti-scale rod, slow-release solid are sour.At present, to the Essential Performance Requirements of slow-release solid it is
There is under media flow state good slow-release capability, course of dissolution will not produce solid impurity affect equipment run or
Blocking stratum.
But indoor do not have a kind of experimental evaluation device evaluated its release performance and observe its dissolved state at present.
Summary of the invention
The technical problem to be solved is to provide a kind of release performance that can simulate slow-release solid, again can
Observe the slow-release solid solubility property Lab-evaluation device of its dissolved state.
In order to solve above-mentioned technical problem, the technical solution used in the present invention is: a kind of slow-release solid solubility property room
Inner evaluation device, including pass sequentially through connect pipeline be attached liquid pump, effusion meter, heater, pit shaft simulator, point
Analysis sample tap;Liquid pump can regulate injected media speed, and flowmeter survey medium flows through the speed of pit shaft simulator, heater
Firing equipment for temperature-adjustable.
Described liquid pump is the one in plunger displacement pump, screw pump, centrifugal pump.
The heating efficiency of described heater is 0 DEG C-100 DEG C.
Described pit shaft simulator is made up of one or several in rustless steel, plastics, fiberglass, PVA.
The material of described pit shaft simulator is opaque material, leaves on pit shaft simulator surface and is easy to observe spacetabs type admittedly
The observation window of body dissolved state in pit shaft simulator.
Described connection pipeline is made up of rustless steel, PVA or plastic material, and pipeline inside diameter ranges is 6mm-50mm.
Described connection pipeline exterior heat-insulation layer wraps up, and reduces medium as far as possible and flows through the heat damage caused in pipeline process
Lose.
The invention has the beneficial effects as follows: can the impact on solid rate of release with simulation wellbore hole temperature and water velocity, again
Solid course of dissolution in the wellbore can be observed, can more efficiently evaluate slow-release solid state in the wellbore.
Accompanying drawing explanation
Fig. 1 is the structural representation of the slow-release solid solubility property Lab-evaluation device of the present invention.
Detailed description of the invention
With detailed description of the invention, the present invention is described in further detail below in conjunction with the accompanying drawings:
As it is shown in figure 1, the slow-release solid solubility property Lab-evaluation device of the present invention, including passing sequentially through connection pipeline
The liquid pump 1 that is attached, effusion meter 2, heater 3, pit shaft simulator 4, analytical sampling mouth 6;Liquid pump 1 can regulate injection
Medium velocity, flowmeter survey medium flows through the speed of pit shaft simulator 4, and heater 3 is the firing equipment of temperature-adjustable.
Described liquid pump 1 is the one in plunger displacement pump, screw pump, centrifugal pump.The effect of liquid pump is to inject in pipeline
Fluid, this fluid is probably oily substance and is also likely to be water.
Heater is by the firing equipment of a kind of temperature-adjustable, it is ensured that medium can be heated to design temperature,
Simulation slow-release solid course of dissolution under temperature in wellbore, the heating efficiency of heater is 0 DEG C-100 DEG C.
Described pit shaft simulator 4 is made up of one or several in rustless steel, plastics, fiberglass, PVA.
The material of described pit shaft simulator is opaque material, leaves on pit shaft simulator surface and is easy to observe spacetabs type admittedly
The observation window 5 of body dissolved state in pit shaft simulator.
Described connection pipeline is made up of rustless steel, PVA or plastic material, and pipeline inside diameter ranges is 6mm-50mm.
Described connection pipeline exterior heat-insulation layer wraps up, and reduces medium as far as possible and flows through the heat damage caused in pipeline process
Lose.
There is sample tap in pipeline outlet position, the liquid taken out can be carried out active substance detection in sample tap.
The present invention can either evaluate the ability of slow-release solid release active substance, can observe again its in the wellbore molten
Solution state, makes the laboratory performance evaluation more closing to reality of slow-release solid rod, more convincing.
The using method of this invention: slow-releasing solid, to temperature required, is put into shaft drum form by the temperature of regulation heater
Intend in device.Opening liquid pump and current are modulated suitable flow, the flow injecting water can be detected by effusion meter, slow
The active substance content that the dissolution velocity of the property released solid flows out water by detection is determined;The dissolved state of slow-releasing solid can
To be observed by the observation window on pit shaft simulator.
In sum, present disclosure is not limited in the above embodiments, and the knowledgeable people in same area can
Can propose other embodiment within technological guidance's thought of the present invention easily, but this embodiment is included in this
Within the scope of bright.
Claims (7)
1. a slow-release solid solubility property Lab-evaluation device, it is characterised in that include that passing sequentially through connection pipeline is carried out
The liquid pump (1) of connection, effusion meter (2), heater (3), pit shaft simulator (4), analytical sampling mouth (6);Liquid pump (1) energy
Regulation injected media speed, flowmeter survey medium flows through the speed of pit shaft simulator (4), and heater (3) is scalable temperature
The firing equipment of degree.
Slow-release solid solubility property Lab-evaluation device the most according to claim 1, it is characterised in that described liquid pump
(1) it is the one in plunger displacement pump, screw pump, centrifugal pump.
Slow-release solid solubility property Lab-evaluation device the most according to claim 1, it is characterised in that described in add hot charging
The heating efficiency putting (3) is 0 DEG C-100 DEG C.
Slow-release solid solubility property Lab-evaluation device the most according to claim 1, it is characterised in that described shaft drum form
Intend device (4) to be made up of one or several in rustless steel, plastics, fiberglass, PVA.
Slow-release solid solubility property Lab-evaluation device the most according to claim 1, it is characterised in that described shaft drum form
The material intending device is opaque material, leaves on pit shaft simulator surface and is easy to observe slow-release solid in pit shaft simulator
The observation window (5) of dissolved state.
Slow-release solid solubility property Lab-evaluation device the most according to claim 1, it is characterised in that described connecting tube
Line is made up of rustless steel, PVA or plastic material, and pipeline inside diameter ranges is 6mm-50mm.
7. according to the slow-release solid solubility property Lab-evaluation device described in any one of claim 1-6, it is characterised in that institute
State connection pipeline exterior heat-insulation layer to wrap up.
Priority Applications (1)
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CN201610700271.7A CN106226198A (en) | 2016-08-19 | 2016-08-19 | Slow-release solid solubility property Lab-evaluation device |
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CN201610700271.7A CN106226198A (en) | 2016-08-19 | 2016-08-19 | Slow-release solid solubility property Lab-evaluation device |
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CN106226198A true CN106226198A (en) | 2016-12-14 |
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CN201610700271.7A Pending CN106226198A (en) | 2016-08-19 | 2016-08-19 | Slow-release solid solubility property Lab-evaluation device |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107677776A (en) * | 2017-10-12 | 2018-02-09 | 华北科技学院 | A kind of coal-bed flooding bar-shaped additive simulating test device and method |
CN112763244A (en) * | 2020-12-11 | 2021-05-07 | 中国石油天然气股份有限公司 | Simulation evaluation device and method for release effect of solid particle scale inhibitor shaft |
Citations (7)
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JP2825333B2 (en) * | 1990-10-09 | 1998-11-18 | 株式会社レアックス | Integral cone mirror for hole wall observation and lifting sonde using this |
CN2938071Y (en) * | 2006-04-21 | 2007-08-22 | 中国石油天然气股份有限公司 | Intelligent solid solution speed detector |
CN101819132A (en) * | 2010-04-09 | 2010-09-01 | 重庆大学 | Method for realizing rock salt dissolving characteristic test under triaxial stress condition |
CN101846668A (en) * | 2010-04-09 | 2010-09-29 | 重庆大学 | Device for implementing rock salt dissolution test under condition of triaxial stress |
CN105735965A (en) * | 2016-04-07 | 2016-07-06 | 中国地质大学(武汉) | Coal-bed gas well shaft drainage gas recovery visual simulation experiment device and simulation method |
CN105735966A (en) * | 2016-04-07 | 2016-07-06 | 中国地质大学(武汉) | Coal-bed gas well shaft drainage gas recovery coal dust migration simulation device and simulation method |
CN105910951A (en) * | 2016-04-06 | 2016-08-31 | 西南石油大学 | Measuring apparatus and measuring method for gas solubility in fluid in shaft of oil and gas well |
-
2016
- 2016-08-19 CN CN201610700271.7A patent/CN106226198A/en active Pending
Patent Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2825333B2 (en) * | 1990-10-09 | 1998-11-18 | 株式会社レアックス | Integral cone mirror for hole wall observation and lifting sonde using this |
CN2938071Y (en) * | 2006-04-21 | 2007-08-22 | 中国石油天然气股份有限公司 | Intelligent solid solution speed detector |
CN101819132A (en) * | 2010-04-09 | 2010-09-01 | 重庆大学 | Method for realizing rock salt dissolving characteristic test under triaxial stress condition |
CN101846668A (en) * | 2010-04-09 | 2010-09-29 | 重庆大学 | Device for implementing rock salt dissolution test under condition of triaxial stress |
CN105910951A (en) * | 2016-04-06 | 2016-08-31 | 西南石油大学 | Measuring apparatus and measuring method for gas solubility in fluid in shaft of oil and gas well |
CN105735965A (en) * | 2016-04-07 | 2016-07-06 | 中国地质大学(武汉) | Coal-bed gas well shaft drainage gas recovery visual simulation experiment device and simulation method |
CN105735966A (en) * | 2016-04-07 | 2016-07-06 | 中国地质大学(武汉) | Coal-bed gas well shaft drainage gas recovery coal dust migration simulation device and simulation method |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107677776A (en) * | 2017-10-12 | 2018-02-09 | 华北科技学院 | A kind of coal-bed flooding bar-shaped additive simulating test device and method |
CN112763244A (en) * | 2020-12-11 | 2021-05-07 | 中国石油天然气股份有限公司 | Simulation evaluation device and method for release effect of solid particle scale inhibitor shaft |
CN112763244B (en) * | 2020-12-11 | 2023-02-07 | 中国石油天然气股份有限公司 | Simulation evaluation device and method for solid particle scale inhibitor wellbore release effect |
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