CN106226198A - Slow-release solid solubility property Lab-evaluation device - Google Patents

Slow-release solid solubility property Lab-evaluation device Download PDF

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Publication number
CN106226198A
CN106226198A CN201610700271.7A CN201610700271A CN106226198A CN 106226198 A CN106226198 A CN 106226198A CN 201610700271 A CN201610700271 A CN 201610700271A CN 106226198 A CN106226198 A CN 106226198A
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CN
China
Prior art keywords
slow
lab
release solid
evaluation device
solubility property
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Pending
Application number
CN201610700271.7A
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Chinese (zh)
Inventor
袁青
毕研霞
李风光
陈挺
牛增前
李军
贾红站
李文杰
王云云
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CNPC Bohai Drilling Engineering Co Ltd
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CNPC Bohai Drilling Engineering Co Ltd
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Publication date
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Priority to CN201610700271.7A priority Critical patent/CN106226198A/en
Publication of CN106226198A publication Critical patent/CN106226198A/en
Pending legal-status Critical Current

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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N13/00Investigating surface or boundary effects, e.g. wetting power; Investigating diffusion effects; Analysing materials by determining surface, boundary, or diffusion effects

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  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Sampling And Sample Adjustment (AREA)

Abstract

The invention discloses a kind of slow-release solid solubility property Lab-evaluation device, including pass sequentially through connect pipeline and be attached liquid pump, effusion meter, heater, pit shaft simulator, analytical sampling mouth;Liquid pump can regulate injected media speed, and flowmeter survey medium flows through the speed of pit shaft simulator, and heater is the firing equipment of temperature-adjustable.The present invention can the impact on solid rate of release with simulation wellbore hole temperature and water velocity, solid course of dissolution in the wellbore can be observed again, can more efficiently evaluate slow-release solid state in the wellbore.

Description

Slow-release solid solubility property Lab-evaluation device
Technical field
The present invention relates to mechanical design field, especially a kind of slow-release solid solubility property Lab-evaluation device.
Background technology
Along with the development of oil & gas industry, the slow-release solid class material with slow solubility property is constantly researched and developed and throws Enter to use, the products such as such as spacetabs type anti-scale rod, slow-release solid are sour.At present, to the Essential Performance Requirements of slow-release solid it is There is under media flow state good slow-release capability, course of dissolution will not produce solid impurity affect equipment run or Blocking stratum.
But indoor do not have a kind of experimental evaluation device evaluated its release performance and observe its dissolved state at present.
Summary of the invention
The technical problem to be solved is to provide a kind of release performance that can simulate slow-release solid, again can Observe the slow-release solid solubility property Lab-evaluation device of its dissolved state.
In order to solve above-mentioned technical problem, the technical solution used in the present invention is: a kind of slow-release solid solubility property room Inner evaluation device, including pass sequentially through connect pipeline be attached liquid pump, effusion meter, heater, pit shaft simulator, point Analysis sample tap;Liquid pump can regulate injected media speed, and flowmeter survey medium flows through the speed of pit shaft simulator, heater Firing equipment for temperature-adjustable.
Described liquid pump is the one in plunger displacement pump, screw pump, centrifugal pump.
The heating efficiency of described heater is 0 DEG C-100 DEG C.
Described pit shaft simulator is made up of one or several in rustless steel, plastics, fiberglass, PVA.
The material of described pit shaft simulator is opaque material, leaves on pit shaft simulator surface and is easy to observe spacetabs type admittedly The observation window of body dissolved state in pit shaft simulator.
Described connection pipeline is made up of rustless steel, PVA or plastic material, and pipeline inside diameter ranges is 6mm-50mm.
Described connection pipeline exterior heat-insulation layer wraps up, and reduces medium as far as possible and flows through the heat damage caused in pipeline process Lose.
The invention has the beneficial effects as follows: can the impact on solid rate of release with simulation wellbore hole temperature and water velocity, again Solid course of dissolution in the wellbore can be observed, can more efficiently evaluate slow-release solid state in the wellbore.
Accompanying drawing explanation
Fig. 1 is the structural representation of the slow-release solid solubility property Lab-evaluation device of the present invention.
Detailed description of the invention
With detailed description of the invention, the present invention is described in further detail below in conjunction with the accompanying drawings:
As it is shown in figure 1, the slow-release solid solubility property Lab-evaluation device of the present invention, including passing sequentially through connection pipeline The liquid pump 1 that is attached, effusion meter 2, heater 3, pit shaft simulator 4, analytical sampling mouth 6;Liquid pump 1 can regulate injection Medium velocity, flowmeter survey medium flows through the speed of pit shaft simulator 4, and heater 3 is the firing equipment of temperature-adjustable.
Described liquid pump 1 is the one in plunger displacement pump, screw pump, centrifugal pump.The effect of liquid pump is to inject in pipeline Fluid, this fluid is probably oily substance and is also likely to be water.
Heater is by the firing equipment of a kind of temperature-adjustable, it is ensured that medium can be heated to design temperature, Simulation slow-release solid course of dissolution under temperature in wellbore, the heating efficiency of heater is 0 DEG C-100 DEG C.
Described pit shaft simulator 4 is made up of one or several in rustless steel, plastics, fiberglass, PVA.
The material of described pit shaft simulator is opaque material, leaves on pit shaft simulator surface and is easy to observe spacetabs type admittedly The observation window 5 of body dissolved state in pit shaft simulator.
Described connection pipeline is made up of rustless steel, PVA or plastic material, and pipeline inside diameter ranges is 6mm-50mm.
Described connection pipeline exterior heat-insulation layer wraps up, and reduces medium as far as possible and flows through the heat damage caused in pipeline process Lose.
There is sample tap in pipeline outlet position, the liquid taken out can be carried out active substance detection in sample tap.
The present invention can either evaluate the ability of slow-release solid release active substance, can observe again its in the wellbore molten Solution state, makes the laboratory performance evaluation more closing to reality of slow-release solid rod, more convincing.
The using method of this invention: slow-releasing solid, to temperature required, is put into shaft drum form by the temperature of regulation heater Intend in device.Opening liquid pump and current are modulated suitable flow, the flow injecting water can be detected by effusion meter, slow The active substance content that the dissolution velocity of the property released solid flows out water by detection is determined;The dissolved state of slow-releasing solid can To be observed by the observation window on pit shaft simulator.
In sum, present disclosure is not limited in the above embodiments, and the knowledgeable people in same area can Can propose other embodiment within technological guidance's thought of the present invention easily, but this embodiment is included in this Within the scope of bright.

Claims (7)

1. a slow-release solid solubility property Lab-evaluation device, it is characterised in that include that passing sequentially through connection pipeline is carried out The liquid pump (1) of connection, effusion meter (2), heater (3), pit shaft simulator (4), analytical sampling mouth (6);Liquid pump (1) energy Regulation injected media speed, flowmeter survey medium flows through the speed of pit shaft simulator (4), and heater (3) is scalable temperature The firing equipment of degree.
Slow-release solid solubility property Lab-evaluation device the most according to claim 1, it is characterised in that described liquid pump (1) it is the one in plunger displacement pump, screw pump, centrifugal pump.
Slow-release solid solubility property Lab-evaluation device the most according to claim 1, it is characterised in that described in add hot charging The heating efficiency putting (3) is 0 DEG C-100 DEG C.
Slow-release solid solubility property Lab-evaluation device the most according to claim 1, it is characterised in that described shaft drum form Intend device (4) to be made up of one or several in rustless steel, plastics, fiberglass, PVA.
Slow-release solid solubility property Lab-evaluation device the most according to claim 1, it is characterised in that described shaft drum form The material intending device is opaque material, leaves on pit shaft simulator surface and is easy to observe slow-release solid in pit shaft simulator The observation window (5) of dissolved state.
Slow-release solid solubility property Lab-evaluation device the most according to claim 1, it is characterised in that described connecting tube Line is made up of rustless steel, PVA or plastic material, and pipeline inside diameter ranges is 6mm-50mm.
7. according to the slow-release solid solubility property Lab-evaluation device described in any one of claim 1-6, it is characterised in that institute State connection pipeline exterior heat-insulation layer to wrap up.
CN201610700271.7A 2016-08-19 2016-08-19 Slow-release solid solubility property Lab-evaluation device Pending CN106226198A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610700271.7A CN106226198A (en) 2016-08-19 2016-08-19 Slow-release solid solubility property Lab-evaluation device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610700271.7A CN106226198A (en) 2016-08-19 2016-08-19 Slow-release solid solubility property Lab-evaluation device

Publications (1)

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CN106226198A true CN106226198A (en) 2016-12-14

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107677776A (en) * 2017-10-12 2018-02-09 华北科技学院 A kind of coal-bed flooding bar-shaped additive simulating test device and method
CN112763244A (en) * 2020-12-11 2021-05-07 中国石油天然气股份有限公司 Simulation evaluation device and method for release effect of solid particle scale inhibitor shaft

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2825333B2 (en) * 1990-10-09 1998-11-18 株式会社レアックス Integral cone mirror for hole wall observation and lifting sonde using this
CN2938071Y (en) * 2006-04-21 2007-08-22 中国石油天然气股份有限公司 Intelligent solid solution speed detector
CN101819132A (en) * 2010-04-09 2010-09-01 重庆大学 Method for realizing rock salt dissolving characteristic test under triaxial stress condition
CN101846668A (en) * 2010-04-09 2010-09-29 重庆大学 Device for implementing rock salt dissolution test under condition of triaxial stress
CN105735965A (en) * 2016-04-07 2016-07-06 中国地质大学(武汉) Coal-bed gas well shaft drainage gas recovery visual simulation experiment device and simulation method
CN105735966A (en) * 2016-04-07 2016-07-06 中国地质大学(武汉) Coal-bed gas well shaft drainage gas recovery coal dust migration simulation device and simulation method
CN105910951A (en) * 2016-04-06 2016-08-31 西南石油大学 Measuring apparatus and measuring method for gas solubility in fluid in shaft of oil and gas well

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2825333B2 (en) * 1990-10-09 1998-11-18 株式会社レアックス Integral cone mirror for hole wall observation and lifting sonde using this
CN2938071Y (en) * 2006-04-21 2007-08-22 中国石油天然气股份有限公司 Intelligent solid solution speed detector
CN101819132A (en) * 2010-04-09 2010-09-01 重庆大学 Method for realizing rock salt dissolving characteristic test under triaxial stress condition
CN101846668A (en) * 2010-04-09 2010-09-29 重庆大学 Device for implementing rock salt dissolution test under condition of triaxial stress
CN105910951A (en) * 2016-04-06 2016-08-31 西南石油大学 Measuring apparatus and measuring method for gas solubility in fluid in shaft of oil and gas well
CN105735965A (en) * 2016-04-07 2016-07-06 中国地质大学(武汉) Coal-bed gas well shaft drainage gas recovery visual simulation experiment device and simulation method
CN105735966A (en) * 2016-04-07 2016-07-06 中国地质大学(武汉) Coal-bed gas well shaft drainage gas recovery coal dust migration simulation device and simulation method

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107677776A (en) * 2017-10-12 2018-02-09 华北科技学院 A kind of coal-bed flooding bar-shaped additive simulating test device and method
CN112763244A (en) * 2020-12-11 2021-05-07 中国石油天然气股份有限公司 Simulation evaluation device and method for release effect of solid particle scale inhibitor shaft
CN112763244B (en) * 2020-12-11 2023-02-07 中国石油天然气股份有限公司 Simulation evaluation device and method for solid particle scale inhibitor wellbore release effect

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