CN106216085A - A kind of ultra-fine grade mine tailing method for separating - Google Patents

A kind of ultra-fine grade mine tailing method for separating Download PDF

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Publication number
CN106216085A
CN106216085A CN201610668909.3A CN201610668909A CN106216085A CN 106216085 A CN106216085 A CN 106216085A CN 201610668909 A CN201610668909 A CN 201610668909A CN 106216085 A CN106216085 A CN 106216085A
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CN
China
Prior art keywords
cylinder
ultra
separating
mine tailing
overhead stream
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Pending
Application number
CN201610668909.3A
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Chinese (zh)
Inventor
马跃
王鞍山
高飞
张勇
高树龙
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Dalian Earth Environment Technology Co., Ltd.
Original Assignee
DALIAN DITUO HEAVY INDUSTRY Co Ltd
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Priority to CN201610668909.3A priority Critical patent/CN106216085A/en
Publication of CN106216085A publication Critical patent/CN106216085A/en
Pending legal-status Critical Current

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B03SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
    • B03BSEPARATING SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS
    • B03B9/00General arrangement of separating plant, e.g. flow sheets
    • B03B9/06General arrangement of separating plant, e.g. flow sheets specially adapted for refuse

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  • Separation Of Suspended Particles By Flocculating Agents (AREA)

Abstract

The invention provides the method for separating of a kind of ultra-fine grain, can sort for ultra-fine grade mine tailing, there is the features such as the response rate is high, efficiency of separation high cost is low.Solve conventional flotation technology and cannot sort a difficult problem for ultra-fine grade mine tailing.And technological process is simple, apparatus processing is convenient, workable.Conventional oil reunion separation method is flotation or screening, and the present invention, without flotation or screening, uses the form of heating evaporation to reclaim neutral oil, has the highest response rate, be dried concentrate simultaneously.

Description

A kind of ultra-fine grade mine tailing method for separating
Technical field
The present invention relates to tailings glass field, be specifically related to a kind of ultra-fine grade mine tailing method for separating.
Background technology
Submicron-sized particulate mine tailing, generally include that disseminated grain size is tiny, useful constituent be difficult to even cannot the material of monomer dissociation, Or material is by over grind during monomer dissociation, part useful constituent, presented in submicron-sized particulate, uses routine Isolation technics is difficult to its resource reclaim.On ordinary meaning, the disseminated grain size that submicron-sized particulate material refers generally to useful constituent is remote Material much smaller than 75 μm.
Along with the progress of science and technology, the such as magnetic separation, flotation of the conventional means of resources processing, gravity treatment all start to fine Sorting infiltration, and make some progress.As a example by flotation, traditional view think fine mineral can not flotation, and A lot of operator also pay special attention to the overground of material to be avoided or " argillization ".Submicron-sized particulate material commonly uses separation method for carrying Flotation body, this technique is to utilize other easily floating more rough grain to do carrier, optionally adheres to micro-, particulate target minreal therewith The method of emersion together, and spontaneous carrier flotation technique is the floatation process utilizing same mineral to make carrier.
Summary of the invention
In order to solve above technical problem, the invention provides the method for separating of a kind of ultra-fine grain, comprise the following steps:
Ultra-fine grade mine tailing containing concentrate granule and gangue mineral adds mixing drum together with neutral oil;
Enter cylinder after sufficiently mixing, concentrate granule float together with neutral oil formed overhead stream flow into add hot charging Putting, gangue mineral and water are formed after underflow adds flocculant and enter Paste thickener;
The overhead stream comprising concentrate granule and neutral oil is clean by regenerating unit through the dried neutral oil of heating devices heat Change, return to described mixing drum and recycle, collect remaining concentrate granular powder, neutral oil and concentrate granule and pass through heating, Both can reclaim neutral oil, mineral can be dried again;
After the underflow comprising gangue mineral and water enters Paste thickener, through flocculant effect, it is achieved solid-liquid separation, overflow Primary water returns, and recycles, and underflow is flowed out, and underflow stone-like pulse tailings concentration, up to 70%~80%, is applied directly to building materials deep In processing.
The method for separating of ultra-fine grain provided by the present invention, wherein cylinder preferred multiple stage separation cylinder, can be by one-level Cylinder, two poles separate and three grades separate composition, two, three grades of buckets be mainly further Separation of Neutral oil float the water brought out and Gangue mineral, ultra-fine grade mine tailing and the blended cylinder of neutral oil enter flash trapping stage cylinder, the generation of flash trapping stage cylinder after being sufficiently mixed Overhead stream flow into the second-order separation cylinder, three grades of cylinders of inflow that the second-order separation cylinder produces, the overhead stream that three grades of cylinders produce flows into Heater, the underflow of flash trapping stage cylinder, the second-order separation cylinder and three grades of cylinders adds flocculant and enters Paste thickener.
The method for separating of ultra-fine grain provided by the present invention, uses the method for oil aggregation to be enriched with ultra-fine grade mine tailing, oil Reunion is to add collecting agent in ore pulp to make ultra-fine grade mineral hydrophobic, then adds neutral oil, and neutral oil is at hydrophobic granule table Face is sprawled, and promotes subparticle to be gathered in oil phase formation group, thus increases the apparent particle diameter of fine-grained particles.Pass through profit again Separate, reach the purpose of sorting, finally reclaim neutral oil, recycle after purification.
Oil aggregation neutral oil used in invention is hydro carbons, has and selects and the character of overseas Chinese federation.According to the difference of mineral, choosing Selecting different medicaments, the activity order of hydro carbons is: aromatic hydrocarbons > alkene > isoparaffin > cycloalkane > n-alkane;Polycyclic aromatic hydrocarbon > mononuclear aromatics;The non-alkylaromatic hydrocarbon of many alkylaromatic hydrocarbons >, selectivity is contrary.It is simultaneously introduced the collecting agent such as kerosene, diesel oil.
The method for separating of ultra-fine grain provided by the present invention sorts for ultra-fine grade mine tailing, has response rate height, divides Select the features such as efficiency high cost is low.Solve conventional flotation technology and cannot sort a difficult problem for ultra-fine grade mine tailing.And technique stream Journey is simple, and apparatus processing is convenient, workable.Conventional oil reunion separation method is flotation or screening, and the present invention is without flotation Or screening, use the form of heating evaporation to reclaim neutral oil, there is the highest response rate, concentrate is dried simultaneously.
Accompanying drawing explanation
Fig. 1 is the method for separating schematic flow sheet of ultra-fine grain provided by the present invention.
Detailed description of the invention
Below in conjunction with accompanying drawing, the present invention is further illustrated.
The method for separating of ultra-fine grain as described in Figure 1, comprises the following steps:
Ultra-fine grade mine tailing containing concentrate granule and gangue mineral adds mixing drum 1 together with neutral oil;
Entering cylinder 2 after sufficiently mixing, concentrate granule the formed overhead stream that floats together with neutral oil flows into two fraction From cylinder 3, three grades of cylinders 4 of inflow that the second-order separation cylinder 3 produces, the overhead stream that three grades of cylinders 4 produce flows into heater 5, and one The underflow of level cylinder 2, the second-order separation cylinder 3 and three grades of cylinders 4 adds flocculant and enters Paste thickener 7;
The overhead stream comprising concentrate granule and neutral oil neutral oil after heater 5 heat drying passes through regenerating unit 6 Purify, return to described mixing drum 1 and recycle, collect remaining concentrate granular powder;
After the underflow comprising gangue mineral and water enters Paste thickener 7, through flocculant effect, it is achieved solid-liquid separation, overflow Stream primary water returns, and recycles, and underflow is flowed out, and underflow stone-like pulse tailings concentration, up to 70%~80%, is applied directly to building materials In deep processing.
The method for separating of this ultra-fine grain sorts for ultra-fine grade mine tailing, has response rate height, efficiency of separation high cost The feature such as low.Solve conventional flotation technology and cannot sort a difficult problem for ultra-fine grade mine tailing.And technological process is simple, and equipment adds Work is convenient, workable.Conventional oil reunion separation method is flotation or screening, and the present invention adds without flotation or screening, employing The form of thermal evaporation reclaims neutral oil, has the highest response rate, is dried concentrate simultaneously.

Claims (2)

1. the method for separating of a ultra-fine grain, it is characterised in that comprise the following steps:
Ultra-fine grade mine tailing adds mixing drum together with neutral oil;
Entering cylinder after sufficiently mixing, the overhead stream that described cylinder produces flows into heater, and described cylinder produces Underflow adds flocculant and enters Paste thickener;
Flowing into oil body and powder body that the described overhead stream of described heater produces after drying, described oil body is clean by regenerating unit After change, return to described mixing drum and recycle, collect described powder body;
After described underflow enters described Paste thickener, through flocculant effect, it is achieved solid-liquid separation, overflow primary water returns, and follows Ring utilizes, and underflow is flowed out.
2. the method for separating of a ultra-fine grain, it is characterised in that described cylinder is separated and three grades by flash trapping stage cylinder, two poles Separating composition, described ultra-fine grade mine tailing and described neutral oil enter described flash trapping stage after described mixing drum is sufficiently mixed Cylinder, the overhead stream that described flash trapping stage cylinder produces flows into described the second-order separation cylinder, and the overhead stream that described the second-order separation cylinder produces flows into institute Stating three grades of cylinders, the overhead stream that described three grades of cylinders produce flows into described heater, described flash trapping stage cylinder, the second-order separation The underflow of cylinder and three grades of cylinders adds flocculant and enters Paste thickener.
CN201610668909.3A 2016-08-15 2016-08-15 A kind of ultra-fine grade mine tailing method for separating Pending CN106216085A (en)

Priority Applications (1)

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CN201610668909.3A CN106216085A (en) 2016-08-15 2016-08-15 A kind of ultra-fine grade mine tailing method for separating

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Application Number Priority Date Filing Date Title
CN201610668909.3A CN106216085A (en) 2016-08-15 2016-08-15 A kind of ultra-fine grade mine tailing method for separating

Publications (1)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107051750A (en) * 2017-03-31 2017-08-18 太原理工大学 The device and technique of a kind of use waste oil flotation
CN111659707A (en) * 2020-06-16 2020-09-15 太原理工大学 Gasification fine slag carbon-ash separation and high-carbon product dehydration integrated device and method
CN115211582A (en) * 2021-04-21 2022-10-21 重庆中烟工业有限责任公司 Smoking particles for heating cigarettes and preparation method thereof

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CN86105760A (en) * 1986-07-17 1988-03-23 中南工业大学 Branch carrier flotation and perforated baffle stirring tank
WO2002083316A1 (en) * 2001-04-12 2002-10-24 Wmc Resources Ltd Process for sulphide concentration
CN101507950A (en) * 2009-03-20 2009-08-19 中南大学 Mineral separation process capable of recovering micro scheelite from scheelite flotation tailings
CN101642731A (en) * 2009-06-29 2010-02-10 金堆城钼业股份有限公司 Deoiling treatment method of molybdenum concentrate after floatation
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CN103194623A (en) * 2013-03-29 2013-07-10 嵩县开拓者钼业有限公司 Method and device for purifying molybdenum concentrate
CN103949353A (en) * 2014-05-14 2014-07-30 中国矿业大学 Method and device for reinforcing oil bubble column floatation process of low-order coal
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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107051750A (en) * 2017-03-31 2017-08-18 太原理工大学 The device and technique of a kind of use waste oil flotation
CN107051750B (en) * 2017-03-31 2019-01-15 太原理工大学 A kind of device and technique using waste oil flotation
CN111659707A (en) * 2020-06-16 2020-09-15 太原理工大学 Gasification fine slag carbon-ash separation and high-carbon product dehydration integrated device and method
CN115211582A (en) * 2021-04-21 2022-10-21 重庆中烟工业有限责任公司 Smoking particles for heating cigarettes and preparation method thereof

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Address after: 116200 Zhenxing street, Pulandian Bay Industrial Zone, Dalian, Liaoning, China, No. 16

Applicant after: Dalian Earth Environment Technology Co., Ltd.

Address before: 116299 Zhenxing street, Pulandian Bay Industrial Zone, Dalian, Liaoning, China, No. 16

Applicant before: DALIAN DITUO HEAVY INDUSTRY CO., LTD.

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Application publication date: 20161214

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