CN106215500A - A kind of freon purifier using distillation mode - Google Patents

A kind of freon purifier using distillation mode Download PDF

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Publication number
CN106215500A
CN106215500A CN201610693949.3A CN201610693949A CN106215500A CN 106215500 A CN106215500 A CN 106215500A CN 201610693949 A CN201610693949 A CN 201610693949A CN 106215500 A CN106215500 A CN 106215500A
Authority
CN
China
Prior art keywords
evaporator
freon
collecting tank
magnetic drive
drive pump
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610693949.3A
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Chinese (zh)
Inventor
余中军
王东
王永青
郭云珺
程思为
易新强
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Naval University of Engineering PLA
Original Assignee
Naval University of Engineering PLA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Naval University of Engineering PLA filed Critical Naval University of Engineering PLA
Priority to CN201610693949.3A priority Critical patent/CN106215500A/en
Publication of CN106215500A publication Critical patent/CN106215500A/en
Pending legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D36/00Filter circuits or combinations of filters with other separating devices
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D1/00Evaporating
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D1/00Evaporating
    • B01D1/30Accessories for evaporators ; Constructional details thereof
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/42Regulation; Control

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Abstract

The invention discloses a kind of freon purifier using distillation mode.It includes air compressor machine, filter, the first magnetic drive pump, evaporator, collecting tank and condenser, on described evaporator, water influent pipeline is set, described air compressor machine connection evaporator or collecting tank, described evaporator, the first magnetic drive pump and filter are sequentially connected from head to tail to form filtration cycle system, in described evaporator, heater is set, evaporator is connected with collecting tank top by pipeline, and described condenser is arranged at collecting tank inside top.Present configuration is simple, good purification, easy to operate, maintenance cost is low, treatment effeciency is high.

Description

A kind of freon purifier using distillation mode
Technical field
The present invention relates to a kind of for the purifier of liquid freon under normal temperature and pressure, be specifically related to a kind of employing and distill The freon purifier of mode.
Background technology
It is in the application industrially of the Freon medium of liquid under normal temperature and pressure quite varied, is applied especially to evaporate cold But, after motor, for ensureing the insulating properties of Freon medium, the impurity contained in Freon medium and moisture have all been had tighter The requirement of lattice, but the most inevitably mix impurity and moisture, if not processing, then can be cold to evaporation But the safety of motor brings hidden danger, if more renewing Freon medium, then the discharge of the freon liquid containing impurity exists Problem, not only causes waste economically, more can bring problem of environmental pollution.At present, freon purifier is both for low The Freon medium of boiling point (-30 DEG C), is not suitable for the Freon medium of high boiling point (48 DEG C).
Summary of the invention
The purpose of the present invention is contemplated to solve the deficiency that above-mentioned background technology exists, it is provided that a kind of good purification, behaviour Make the freon purifier using distillation mode simple, that maintenance cost is low.
The technical solution used in the present invention is: a kind of freon purifier using distillation mode, including air compressor machine, mistake Filter, the first magnetic drive pump, evaporator, collecting tank and condenser, described evaporator arranges water influent pipeline, and described air compressor machine connects Evaporator or collecting tank, described evaporator, the first magnetic drive pump and filter are sequentially connected from head to tail to form filtration cycle system, described Arranging heater in evaporator, evaporator is connected with collecting tank top by pipeline, and described condenser is arranged at inside collecting tank Top.
Further, described evaporator and collecting tank are respectively equipped with the first liquidometer and the second liquidometer.
Further, also including controller, described controller is electrically connected with air compressor machine, the first magnetic drive pump and heater respectively Connect.
Further, described evaporator and collecting tank are respectively equipped with the first pressure transducer and the second pressure transducer, Described first pressure transducer and the second pressure transducer are electrically connected with the controller respectively.
Further, described evaporator and collecting tank are respectively equipped with the first temperature sensor and the second temperature sensor, Described first temperature sensor and the second temperature sensor are electrically connected with the controller respectively.
Further, the second magnetic drive pump of freon liquid in discharging collecting tank, the second magnetic drive pump and control are also included Device processed electrically connects, and described second magnetic drive pump is connected with bottom collecting tank, and the drain line of the second magnetic drive pump arranges dry filter Device.
Further, the drain line of described second magnetic drive pump connects with evaporator.
The present invention utilizes air compressor machine that evaporator and collecting tank are pumped into negative pressure state, then water influent pipeline is inserted to be clean Freon liquid in, utilize negative-pressure liquid suction principle to be sucked in evaporator by freon liquid, for the fluorine that impurity content is more Leon liquid first carries out circulating filtration, restarts heater and the freon liquid of high temperature boiling point carries out distil(l), structure letter List, good purification, easy to operate, maintenance cost is low, treatment effeciency is high.
Accompanying drawing explanation
Fig. 1 is the theory structure schematic diagram of the present invention.
Fig. 2 is circuit part connection diagram of the present invention.
In figure: 1. water influent pipeline, 2. air compressor machine, 3. filter, 4. relief valve, 5. heater, 6. the first magnetic drive pump, 7. steaming Send out tank, 8. pipeline valve, 9. collecting tank, 10. the first liquidometer, 11. second liquidometers, 12. second magnetic drive pumps, 13. dried Filter, 14. draining valves, 15. controllers, 16. condensers, 17. first pressure transducers, 18. second pressure transducers, 19. First temperature sensor, 20. second temperature sensors, 21. collection devices.
Detailed description of the invention
The present invention is described in further detail with specific embodiment below in conjunction with the accompanying drawings, it is simple to is well understood to this Bright, but they do not constitute restriction to the present invention.
As shown in Figure 1 and Figure 2, the present invention includes air compressor machine 2, filter the 3, first magnetic drive pump 6, evaporator 7, collecting tank 9 and Condenser 16, described evaporator 7 arranges water influent pipeline 1 and relief valve 4, and described air compressor machine 2 connects evaporator 7 or collecting tank 9, In the present embodiment, air compressor machine 2 connects evaporator 7, and described evaporator the 7, first magnetic drive pump 6 and filter 3 are sequentially connected from head to tail to form Filtration cycle system, arranges heater 5 in described evaporator 7, evaporator 7 is connected, on pipeline with collecting tank 9 top by pipeline Pipeline valve 8 is set.It is corresponding with pipe outlet that described condenser 16 is arranged at collecting tank 9 inside top, and condenser 16 is positioned at receipts Collection tank top and heat exchange area are relatively large, it is ensured that major part freon steam becomes liquid after condenser and flows into In collecting tank.
Utilize air compressor machine 2 that evaporator 7 and collecting tank 9 are pumped into negative pressure state, then water influent pipeline 1 is inserted to be clean In freon liquid, open water influent pipeline valve, utilize negative-pressure liquid suction principle to be sucked in evaporator 7 by freon liquid.For Freon liquid advanced person's row circulating filtration that impurity content is more, restarts heater 5 and heats freon liquid;For Impurity content less freon liquid can directly initiate heater 5 and heat freon liquid.Control heater heating Temperature is higher than the cold high boiling temperature of fluorine, and the gas that Freon liquid evacuator body is formed flows in condenser 16, becomes the most again Liquid is become to enter in collecting tank 9, after the liquid of 9 reach a certain height in collecting tank, after being purified by the second magnetic drive pump 12 Freon liquid discharge after device for drying and filtering 13, so complete distillation type purification process, it is miscellaneous that freon liquid contains Matter all can remain in evaporator.
In such scheme, evaporator 7 and collecting tank 9 are respectively equipped with the first liquidometer 10 and the second liquidometer 11.Pass through First liquidometer 10 and the second liquidometer 11 can observe liquid height in evaporator 7 and collecting tank 9, it is ensured that processing procedure more and Time.
In such scheme, also include controller 15, described controller 15 respectively with air compressor machine the 2, first magnetic drive pump 6 and heating Device 5 electrically connects.The start and stop of air compressor machine the 2, first magnetic drive pump 6 and heater 5 are controlled by controller 15, easy to operate, safeguard letter Single, treatment effeciency is high.Controller 15 controls the temperature of heater 5 and is slightly above the cold high boiling temperature of fluorine, can reduce the steaming of moisture Send out, to ensure freon purity liquid.
In such scheme, evaporator 7 and collecting tank 9 are respectively equipped with the first pressure transducer 17 and the second pressure transducer 18, described first pressure transducer 17 and the second pressure transducer 18 electrically connect with controller 15 respectively.Evaporator 7 and collecting tank The first temperature sensor 19 and the second temperature sensor 20, described first temperature sensor 19 and the second temperature it is respectively equipped with on 9 Sensor 20 electrically connects with controller 15 respectively.The pressure in evaporator 7, collecting tank 9, temperature can be automatically monitored by controller 15 Degree change, automaticity is high.
In such scheme, also include the second magnetic drive pump 12 of freon liquid in discharging collecting tank, the second magnetic drive pump 12 electrically connect with controller 15, and described second magnetic drive pump 12 is connected bottom collecting tank 9, in the drain line of the second magnetic drive pump 12 Device for drying and filtering 13 and draining valve 14, drain line connection freon fluid collection device 21 are set.Drain line is installed There is device for drying and filtering, can removal moisture solution to freon liquid further.
In such scheme, the drain line of the second magnetic drive pump 12 can also connect with evaporator 7, can as required, to steaming Evaporate in the freon liquid after purification is transported to evaporator and carry out distil(l) again.
The process that employing said apparatus realizes freon purification is as follows:
Start air compressor machine 2 and pipe valve thereof, opening conduits valve 8, negative pressure (ratio will be pumped in evaporator 7, collecting tank 9 As for-50kPa, can set), water influent pipeline 1 is inserted in freon liquid, utilizes principle of negative pressure to be sucked by external world's freon and steam Send out in tank 7, observed the freon capacity poured into by the first liquidometer 10.
If containing relatively multimedium in freon liquid, before distillation, first carry out circulating filtration, start the first magnetic drive pump 6 and Its pipe valve, is pumped into the freon liquid in evaporator 7 in filter 3, then is back in evaporator 7, so circulates Close after a period of time.
Freon liquid is carried out distillation process, opens heater 5 power supply and the freon liquid in evaporator 7 is added Heat, heater surface temperatures controls 55 DEG C of scopes, in running, by the pressure in controller 15 moment monitoring evaporator 7 Power and variations in temperature, and the speed of evaporation capacity is realized by controlling the heating power of heater 5;Freon heated liquid gasifies Flow in condenser 16 by pipeline, valve 8 afterwards, become liquid after condensation, then flow in collecting tank 9.By the second liquidometer 11 observe the liquid level in collecting tank 9, after reaching to a certain degree, can be discharged by liquid, utilize the second magnetic drive pump 2 by collecting tank 9 Freon liquid discharge after device for drying and filtering 14.
These are only present pre-ferred embodiments, not in order to limit the present invention, all spirit in the present invention and former Any amendment, equivalent and the improvement etc. made within then, should be included within the scope of the present invention.This specification In the content that is not described in detail belong to prior art known to professional and technical personnel in the field.

Claims (7)

1. the freon purifier using distillation mode, it is characterised in that: include air compressor machine (2), filter (3), One magnetic drive pump (6), evaporator (7), collecting tank (9) and condenser (16), described evaporator (7) arranges water influent pipeline (1), institute State air compressor machine (2) connection evaporator or collecting tank, described evaporator (7), the first magnetic drive pump (6) and filter (3) head and the tail successively Connecting and form filtration cycle system, arrange heater (5) in described evaporator (7), evaporator (7) passes through pipeline and collecting tank (9) top connection, described condenser (16) is arranged at collecting tank (9) inside top.
A kind of freon purifier using distillation mode the most according to claim 1, it is characterised in that: described evaporation The first liquidometer (10) and the second liquidometer (11) it is respectively equipped with on tank (7) and collecting tank (9).
A kind of freon purifier using distillation mode the most according to claim 1, it is characterised in that: also include control Device processed (15), described controller (15) electrically connects with air compressor machine (2), the first magnetic drive pump (6) and heater (5) respectively.
A kind of freon purifier using distillation mode the most according to claim 3, it is characterised in that: described evaporation The first pressure transducer (17) and the second pressure transducer (18), described first pressure it is respectively equipped with on tank (7) and collecting tank (9) Sensor (17) and the second pressure transducer (18) electrically connect with controller (15) respectively.
A kind of freon purifier using distillation mode the most according to claim 3, it is characterised in that: described evaporation The first temperature sensor (19) and the second temperature sensor (20), described first temperature it is respectively equipped with on tank (7) and collecting tank (9) Sensor (19) and the second temperature sensor (20) electrically connect with controller (15) respectively.
A kind of freon purifier using distillation mode the most according to claim 1, it is characterised in that: also include using Second magnetic drive pump (12) of freon liquid in discharging collecting tank, the second magnetic drive pump (12) electrically connects with controller (15), institute State the second magnetic drive pump (12) to be connected with collecting tank (9) bottom, the drain line of the second magnetic drive pump (12) arranges device for drying and filtering (13)。
A kind of freon purifier using distillation mode the most according to claim 6, it is characterised in that: described second The drain line of magnetic drive pump (12) connects with evaporator (4).
CN201610693949.3A 2016-08-19 2016-08-19 A kind of freon purifier using distillation mode Pending CN106215500A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108031178A (en) * 2017-12-22 2018-05-15 武汉船用电力推进装置研究所(中国船舶重工集团公司第七二研究所) One kind boiling cryogen purifier

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4770748A (en) * 1987-02-24 1988-09-13 Roncell, Inc. Vacuum distillation system
JPH0435701A (en) * 1990-05-31 1992-02-06 Otsuka Giken Kogyo Kk Method for recovering exhausted fluorocarbon solvent
US5377499A (en) * 1994-05-10 1995-01-03 Hudson Technologies, Inc. Method and apparatus for refrigerant reclamation
CN2268024Y (en) * 1996-10-10 1997-11-19 王金堂 Freon recovering-purifying device
JP2005009715A (en) * 2003-06-17 2005-01-13 Oei Kaihatsu Kogyo Kk Reproduction method of recovered chlorofluorocarbon
US20100218552A1 (en) * 2009-02-27 2010-09-02 Ideal Fluids, Inc. Apparatus and process for the separation and purification of ideal and non-ideal refrigerant mixtures
CN103453703A (en) * 2012-05-28 2013-12-18 易科泰克尼克公司 Method and apparatus for recovering the refrigerant from an air conditioning system

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4770748A (en) * 1987-02-24 1988-09-13 Roncell, Inc. Vacuum distillation system
JPH0435701A (en) * 1990-05-31 1992-02-06 Otsuka Giken Kogyo Kk Method for recovering exhausted fluorocarbon solvent
US5377499A (en) * 1994-05-10 1995-01-03 Hudson Technologies, Inc. Method and apparatus for refrigerant reclamation
CN2268024Y (en) * 1996-10-10 1997-11-19 王金堂 Freon recovering-purifying device
JP2005009715A (en) * 2003-06-17 2005-01-13 Oei Kaihatsu Kogyo Kk Reproduction method of recovered chlorofluorocarbon
US20100218552A1 (en) * 2009-02-27 2010-09-02 Ideal Fluids, Inc. Apparatus and process for the separation and purification of ideal and non-ideal refrigerant mixtures
CN103453703A (en) * 2012-05-28 2013-12-18 易科泰克尼克公司 Method and apparatus for recovering the refrigerant from an air conditioning system

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108031178A (en) * 2017-12-22 2018-05-15 武汉船用电力推进装置研究所(中国船舶重工集团公司第七二研究所) One kind boiling cryogen purifier

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Application publication date: 20161214

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