CN106192543A - A kind of by the preparation method that purple willow skin is raw material made weaving paper using - Google Patents

A kind of by the preparation method that purple willow skin is raw material made weaving paper using Download PDF

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Publication number
CN106192543A
CN106192543A CN201610597627.9A CN201610597627A CN106192543A CN 106192543 A CN106192543 A CN 106192543A CN 201610597627 A CN201610597627 A CN 201610597627A CN 106192543 A CN106192543 A CN 106192543A
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CN
China
Prior art keywords
purple willow
raw material
skin
semen maydis
preparation
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201610597627.9A
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Chinese (zh)
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CN106192543B (en
Inventor
孟祥荣
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FUNAN TENGXIANG ARTS AND CRAFTS Co Ltd
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FUNAN TENGXIANG ARTS AND CRAFTS Co Ltd
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Priority to CN201610597627.9A priority Critical patent/CN106192543B/en
Publication of CN106192543A publication Critical patent/CN106192543A/en
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Classifications

    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H11/00Pulp or paper, comprising cellulose or lignocellulose fibres of natural origin only
    • D21H11/12Pulp from non-woody plants or crops, e.g. cotton, flax, straw, bagasse
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21CPRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C5/00Other processes for obtaining cellulose, e.g. cooking cotton linters ; Processes characterised by the choice of cellulose-containing starting materials
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H17/00Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
    • D21H17/02Material of vegetable origin
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H17/00Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
    • D21H17/20Macromolecular organic compounds
    • D21H17/33Synthetic macromolecular compounds
    • D21H17/46Synthetic macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D21H17/47Condensation polymers of aldehydes or ketones
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H17/00Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
    • D21H17/71Mixtures of material ; Pulp or paper comprising several different materials not incorporated by special processes
    • D21H17/74Mixtures of material ; Pulp or paper comprising several different materials not incorporated by special processes of organic and inorganic material
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H21/00Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
    • D21H21/14Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
    • D21H21/16Sizing or water-repelling agents
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H27/00Special paper not otherwise provided for, e.g. made by multi-step processes

Abstract

The invention discloses a kind of by the preparation method that purple willow skin is raw material made weaving paper using, including: prepare raw material, Feedstock treating, prepared by oleo stock, several step is prepared and manufactured paper with pulp to mixed slurry.The present invention has the advantage that in the present invention compared to existing technology with the fiber in mallee bark infusion liquid size degradation purple willow skin and purple willow leaf bar, can strengthen its tensile strength;Glutinous Semen Maydis serosity can improve tenacity of fibre, in infiltrated fiber hole, to combine with fiber in processing procedure;Utilize Lauxite and other raw material synergism, improve the water proofing property of product;In product preparation process, raw material availability is high, and products obtained therefrom has higher intensity and toughness, it is easy to braiding, Stability Analysis of Structures, and weatherability is strong, is difficult to go mouldy.

Description

A kind of by the preparation method that purple willow skin is raw material made weaving paper using
Technical field
The invention belongs to baskets craft technical field, relate to a kind of braiding paper using, being specifically related to one by purple willow skin is The preparation method of raw material made weaving paper using.
Background technology
Purple willow is widely distributed in China, and along with the development of woven product industry, the demand of purple willow is increasing, gradually by Wild being converted to unifies plantation, and the wicker products that purple willow is made is fashionable, of a great variety, is liked by consumer, purple willow Purple willow skin can be peelled off at the process initial stage, it will usually discarded or burning disposal, although have raiser at present by purple willow crust ensiling Being used as feedstuff afterwards, but utilization rate is relatively low, major part purple willow skin is not utilized effectively, and the kind of woven product is the most increasingly Variation, the requirement to braiding paper using is more and more higher, including weatherability, toughness and the water proofing property of paper, therefore needs Want a kind of and can reach the paper that braiding requires.
Summary of the invention
It is an object of the invention to for existing problem, it is provided that a kind of is raw material made weaving paper using by purple willow skin Preparation method.
The present invention is achieved by the following technical solutions: a kind of by the system that purple willow skin is raw material made weaving paper using Preparation Method, comprises the following steps:
(1) prepare raw material: purple willow skin 38-45 part, mallee bark 8-12 part, purple willow leaf bar 12-16 part, Glutinous Semen Maydis serosity 16-22 part, Sorbitan fatty acid ester 3-6 part, Pentachorophenol 1-2 part, Semen Lini oil 3-4 part, alumina sol 3-5 part, styrene sulfonic acid Sodium 2-4 part, polyoxyethylene polyoxy propanol amidogen ether 2-3 part, polyacrylamide 1-2 part, Lauxite 1-2 part;
Wherein, the preparation method of Glutinous Semen Maydis serosity is: collect the seed of Glutinous Semen Maydis, with blister 3-4 hour, is then placed in being equivalent to The boiling water of its weight portion 5 times boils 12-15 minute, natural cooling after completing, by the soup of infusion Glutinous Semen Maydis seed and Glutinous Semen Maydis seed Grain is put in beater and is pulled an oar, and to obtain final product;
(2) Feedstock treating: put into exchange views after purple willow skin, purple willow leaf bar pulverizer being pulverized and wear into crude fibre in vermicelli machine, eucalyptus globulus Bark powder is broken into the particle diameter fragment less than 1cm;
(3) prepared by oleo stock: mallee bark is put into infusion 2-2.5 hour in the water being equivalent to its weight portion 8 times, is subsequently adding purple willow The crude fibre that skin and purple willow leaf bar are made continues infusion 1.5-2 hour, adds Glutinous Semen Maydis serosity, make in fiberizer after completing Slurry, proceeds to disperser and processes 5-8 minute with the Rate Dispersion of 500-800r/min, obtain oleo stock;
(4) prepared by mixed slurry: after above-mentioned oleo stock is heated to 55-60 DEG C, is sequentially added into the urea of corresponding weight portion in oleo stock Urea formaldehyde, alumina sol, Sodium styrene sulfonate, sorbitan fatty acid ester and polyoxyethylene polyoxy propanol amidogen ether, stirring Processing 20-30 minute, be subsequently adding the water being equivalent to its gross weight equivalent, again defibrination in fiberizer, defibrination carries after completing To arrest reaction tower, react 20 minutes under conditions of 80 DEG C, after going the removal of impurity, obtain mixed slurry;
(5) manufacture paper with pulp: after being diluted by Semen Lini oil, Pentachorophenol and the polyacrylamide water being equivalent to its gross weight 5 times, add mixing In slurry, manufacture paper with pulp after stirring, drying.
As further improvement of these options, described purple willow skin, the water content of purple willow leaf bar are 20-36%, described eucalyptus globulus The water content of bark is 8-15%.
As further improvement of these options, the beating degree of described oleo stock is 28.5 ° of SR, the beating degree of mixed slurry It is 48.3 ° of SR.
The present invention has the advantage that in the present invention compared to existing technology with mallee bark infusion liquid size degradation purple willow skin and purple willow Fiber in leaf bar, can strengthen its tensile strength;Glutinous Semen Maydis serosity can be with in infiltrated fiber hole in processing procedure, with fiber Combine, improve tenacity of fibre;Utilize Lauxite and other raw material synergism, improve the water proofing property of product;In product system During Bei, raw material availability is high, and products obtained therefrom has higher intensity and toughness, it is easy to braiding, Stability Analysis of Structures, weatherability By force, it is difficult to go mouldy.
Detailed description of the invention
Embodiment
A kind of by the preparation method that purple willow skin is raw material made weaving paper using, comprise the following steps:
(1) raw material is prepared: purple willow skin 40 parts, mallee bark 10 parts, 12 parts of purple willow leaf bar, 18 parts of Glutinous Semen Maydis serosity, anhydrous sorbitol Fatty acid ester 5 parts, Pentachorophenol 1 part, Semen Lini oil 3 parts, alumina sol 4 parts, Sodium styrene sulfonate 3 parts, polyoxyethylene polyoxy Propanol amidogen ether 2 parts, polyacrylamide 1 part, Lauxite 1 part;
Wherein, the preparation method of Glutinous Semen Maydis serosity is: collect the seed of Glutinous Semen Maydis, with blister 3-4 hour, is then placed in being equivalent to The boiling water of its weight portion 5 times boils 12-15 minute, natural cooling after completing, by the soup of infusion Glutinous Semen Maydis seed and Glutinous Semen Maydis seed Grain is put in beater and is pulled an oar, and to obtain final product;
(2) Feedstock treating: put into exchange views after purple willow skin, purple willow leaf bar pulverizer being pulverized and wear into crude fibre in vermicelli machine, eucalyptus globulus Bark powder is broken into the particle diameter fragment less than 1cm;
(3) prepared by oleo stock: mallee bark is put into infusion 2-2.5 hour in the water being equivalent to its weight portion 8 times, is subsequently adding purple willow The crude fibre that skin and purple willow leaf bar are made continues infusion 1.5-2 hour, adds Glutinous Semen Maydis serosity, make in fiberizer after completing Slurry, proceeds to disperser and processes 5-8 minute with the Rate Dispersion of 500-800r/min, obtain oleo stock;
(4) prepared by mixed slurry: after above-mentioned oleo stock is heated to 55-60 DEG C, is sequentially added into the urea of corresponding weight portion in oleo stock Urea formaldehyde, alumina sol, Sodium styrene sulfonate, sorbitan fatty acid ester and polyoxyethylene polyoxy propanol amidogen ether, stirring Processing 20-30 minute, be subsequently adding the water being equivalent to its gross weight equivalent, again defibrination in fiberizer, defibrination carries after completing To arrest reaction tower, react 20 minutes under conditions of 80 DEG C, after going the removal of impurity, obtain mixed slurry;
(5) manufacture paper with pulp: after being diluted by Semen Lini oil, Pentachorophenol and the polyacrylamide water being equivalent to its gross weight 5 times, add mixing In slurry, manufacture paper with pulp after stirring, drying.
Wherein, described purple willow skin, the water content of purple willow leaf bar are 20-36%, and the water content of described mallee bark is 8-15%, institute The beating degree stating oleo stock is 28.5 ° of SR, and the beating degree of mixed slurry is 48.3 ° of SR.
The present embodiment is prepared gained weaving paper using performance indications as follows: wet strength is 47.5%, machine direction tensile strength For 2.67KN/m, bursting strength is 4.3KPa*/g, and antifungal rate is 98.5%.

Claims (3)

1. one kind by the preparation method that purple willow skin is raw material made weaving paper using, it is characterised in that comprise the following steps:
(1) prepare raw material: purple willow skin 38-45 part, mallee bark 8-12 part, purple willow leaf bar 12-16 part, Glutinous Semen Maydis serosity 16-22 part, Sorbitan fatty acid ester 3-6 part, Pentachorophenol 1-2 part, Semen Lini oil 3-4 part, alumina sol 3-5 part, styrene sulfonic acid Sodium 2-4 part, polyoxyethylene polyoxy propanol amidogen ether 2-3 part, polyacrylamide 1-2 part, Lauxite 1-2 part;
Wherein, the preparation method of Glutinous Semen Maydis serosity is: collect the seed of Glutinous Semen Maydis, with blister 3-4 hour, is then placed in being equivalent to The boiling water of its weight portion 5 times boils 12-15 minute, natural cooling after completing, by the soup of infusion Glutinous Semen Maydis seed and Glutinous Semen Maydis seed Grain is put in beater and is pulled an oar, and to obtain final product;
(2) Feedstock treating: put into exchange views after purple willow skin, purple willow leaf bar pulverizer being pulverized and wear into crude fibre in vermicelli machine, eucalyptus globulus Bark powder is broken into the particle diameter fragment less than 1cm;
(3) prepared by oleo stock: mallee bark is put into infusion 2-2.5 hour in the water being equivalent to its weight portion 8 times, is subsequently adding purple willow The crude fibre that skin and purple willow leaf bar are made continues infusion 1.5-2 hour, adds Glutinous Semen Maydis serosity, make in fiberizer after completing Slurry, proceeds to disperser and processes 5-8 minute with the Rate Dispersion of 500-800r/min, obtain oleo stock;
(4) prepared by mixed slurry: after above-mentioned oleo stock is heated to 55-60 DEG C, is sequentially added into the urea of corresponding weight portion in oleo stock Urea formaldehyde, alumina sol, Sodium styrene sulfonate, sorbitan fatty acid ester and polyoxyethylene polyoxy propanol amidogen ether, stirring Processing 20-30 minute, be subsequently adding the water being equivalent to its gross weight equivalent, again defibrination in fiberizer, defibrination carries after completing To arrest reaction tower, react 20 minutes under conditions of 80 DEG C, after going the removal of impurity, obtain mixed slurry;
(5) manufacture paper with pulp: after being diluted by Semen Lini oil, Pentachorophenol and the polyacrylamide water being equivalent to its gross weight 5 times, add mixing In slurry, manufacture paper with pulp after stirring, drying.
It is a kind of by the preparation method that purple willow skin is raw material made weaving paper using, it is characterised in that Described purple willow skin, the water content of purple willow leaf bar are 20-36%, and the water content of described mallee bark is 8-15%.
It is a kind of by the preparation method that purple willow skin is raw material made weaving paper using, it is characterised in that The beating degree of described oleo stock is 28.5 ° of SR, and the beating degree of mixed slurry is 48.3 ° of SR.
CN201610597627.9A 2016-07-27 2016-07-27 A kind of preparation method by purple willow skin for the made weaving paper of raw material Active CN106192543B (en)

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Cited By (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106958159A (en) * 2017-04-06 2017-07-18 霍邱县淮美奇工艺品有限公司 A kind of preparation method of modified purple willow hide fiber
CN108277681A (en) * 2017-10-07 2018-07-13 霍文慧 A kind of high tenacity rice paper material
CN108286205A (en) * 2017-10-07 2018-07-17 霍文慧 A kind of ageing-resistant rice paper material
CN108301250A (en) * 2017-10-07 2018-07-20 霍文慧 A kind of novel rice paper material
CN108342928A (en) * 2017-10-07 2018-07-31 谷文 A kind of fire prevention painting and calligraphy carrier material
CN108360284A (en) * 2017-10-07 2018-08-03 霍文慧 A kind of modified form rice paper material
CN108385432A (en) * 2017-10-07 2018-08-10 霍文慧 A kind of fire-retardant rice paper material
CN108385431A (en) * 2017-10-07 2018-08-10 谷文 A kind of ageing-resistant painting and calligraphy carrier material
CN108385433A (en) * 2017-10-07 2018-08-10 谷文 A kind of fire-retardant painting and calligraphy carrier material
CN108411703A (en) * 2017-10-07 2018-08-17 霍文慧 A kind of moisture-proof rice paper material
CN108411701A (en) * 2017-10-07 2018-08-17 谷文 A kind of moisture-proof painting and calligraphy carrier material
CN108411699A (en) * 2017-10-07 2018-08-17 谷文 A kind of modified form painting and calligraphy carrier material
CN108411700A (en) * 2017-10-07 2018-08-17 谷文 A kind of painting and calligraphy carrier material
CN108411702A (en) * 2017-10-07 2018-08-17 霍文慧 A kind of fire-retardant rice paper material
CN108729296A (en) * 2018-04-24 2018-11-02 阜南县宇翔工艺品有限公司 A kind of waterproof anti-fungicide paper rattan processing method
CN113173336A (en) * 2021-05-08 2021-07-27 滁州远达彩印包装有限公司 Printing packaging box capable of being recycled and production method thereof

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Cited By (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106958159A (en) * 2017-04-06 2017-07-18 霍邱县淮美奇工艺品有限公司 A kind of preparation method of modified purple willow hide fiber
CN108277681A (en) * 2017-10-07 2018-07-13 霍文慧 A kind of high tenacity rice paper material
CN108286205A (en) * 2017-10-07 2018-07-17 霍文慧 A kind of ageing-resistant rice paper material
CN108301250A (en) * 2017-10-07 2018-07-20 霍文慧 A kind of novel rice paper material
CN108342928A (en) * 2017-10-07 2018-07-31 谷文 A kind of fire prevention painting and calligraphy carrier material
CN108360284A (en) * 2017-10-07 2018-08-03 霍文慧 A kind of modified form rice paper material
CN108385432A (en) * 2017-10-07 2018-08-10 霍文慧 A kind of fire-retardant rice paper material
CN108385431A (en) * 2017-10-07 2018-08-10 谷文 A kind of ageing-resistant painting and calligraphy carrier material
CN108385433A (en) * 2017-10-07 2018-08-10 谷文 A kind of fire-retardant painting and calligraphy carrier material
CN108411703A (en) * 2017-10-07 2018-08-17 霍文慧 A kind of moisture-proof rice paper material
CN108411701A (en) * 2017-10-07 2018-08-17 谷文 A kind of moisture-proof painting and calligraphy carrier material
CN108411699A (en) * 2017-10-07 2018-08-17 谷文 A kind of modified form painting and calligraphy carrier material
CN108411700A (en) * 2017-10-07 2018-08-17 谷文 A kind of painting and calligraphy carrier material
CN108411702A (en) * 2017-10-07 2018-08-17 霍文慧 A kind of fire-retardant rice paper material
CN108729296A (en) * 2018-04-24 2018-11-02 阜南县宇翔工艺品有限公司 A kind of waterproof anti-fungicide paper rattan processing method
CN113173336A (en) * 2021-05-08 2021-07-27 滁州远达彩印包装有限公司 Printing packaging box capable of being recycled and production method thereof

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