CN106190530A - A kind of plant sterol Camellia oil that can prevent cardiovascular disease and preparation method thereof - Google Patents

A kind of plant sterol Camellia oil that can prevent cardiovascular disease and preparation method thereof Download PDF

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CN106190530A
CN106190530A CN201610657766.6A CN201610657766A CN106190530A CN 106190530 A CN106190530 A CN 106190530A CN 201610657766 A CN201610657766 A CN 201610657766A CN 106190530 A CN106190530 A CN 106190530A
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plant sterol
oil
camellia
nata
cardiovascular disease
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余方成
叶六韬
叶松柏
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Anhui Future Agricultural Development Co Ltd
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Anhui Future Agricultural Development Co Ltd
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    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00—Production of fats or fatty oils from raw materials
    • C11B1/02—Pretreatment
    • C11B1/04—Pretreatment of vegetable raw material
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
    • A61K36/287—Chrysanthemum, e.g. daisy
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
    • A61K36/481—Astragalus (milkvetch)
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/82—Theaceae (Tea family), e.g. camellia
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00—Production of fats or fatty oils from raw materials
    • C11B1/06—Production of fats or fatty oils from raw materials by pressing
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00—Production of fats or fatty oils from raw materials
    • C11B1/06—Production of fats or fatty oils from raw materials by pressing
    • C11B1/08—Production of fats or fatty oils from raw materials by pressing by hot pressing
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00—Production of fats or fatty oils from raw materials
    • C11B1/10—Production of fats or fatty oils from raw materials by extracting
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00—Refining fats or fatty oils
    • C11B3/001—Refining fats or fatty oils by a combination of two or more of the means hereafter
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00—Refining fats or fatty oils
    • C11B3/008—Refining fats or fatty oils by filtration, e.g. including ultra filtration, dialysis
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00—Refining fats or fatty oils
    • C11B3/02—Refining fats or fatty oils by chemical reaction
    • C11B3/04—Refining fats or fatty oils by chemical reaction with acids
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00—Refining fats or fatty oils
    • C11B3/02—Refining fats or fatty oils by chemical reaction
    • C11B3/06—Refining fats or fatty oils by chemical reaction with bases
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/30—Extraction of the material
    • A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
    • A61K2236/331—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation, decoction
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/30—Extraction of the material
    • A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
    • A61K2236/333—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using mixed solvents, e.g. 70% EtOH

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
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  • Alternative & Traditional Medicine (AREA)
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  • Pharmacology & Pharmacy (AREA)
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  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
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  • Veterinary Medicine (AREA)
  • General Chemical & Material Sciences (AREA)
  • Medicines Containing Plant Substances (AREA)
  • Edible Oils And Fats (AREA)

Abstract

The invention discloses a kind of plant sterol Camellia oil that can prevent cardiovascular disease, including following parts by weight of component: camellia seed kernels 120 125, the Radix Astragali 35 40, Bellis perennis leaf 30 35 plant sterol 23, Nata24 26, pure soda powder 0.42 0.43, acetic acid 0.55 0.56, appropriate pure water, appropriate water, the ethanol of appropriate concentration 3%.The present invention uses the Radix Astragali, Bellis perennis leaf, plant sterol to coordinate camellia seed kernels to prepare Camellia oil, Folium daisy gentisin in Astragaloside IV in Radix Astragali, Bellis perennis leaf and activate readily soluble plant sterol and work in coordination with the effect enhancing goods in terms of prevention cardiovascular disease.

Description

A kind of plant sterol Camellia oil that can prevent cardiovascular disease and preparation method thereof
Technical field
The present invention relates to Camellia oil technical field, particularly relate to a kind of plant sterol Flos Camelliae Japonicae that can prevent cardiovascular disease Oil and preparation method thereof.
Background technology
Oil tea is the distinctive woody oleiferous plants of China, the oil crop that Ye Shi China greatly develops, containing abundant unsaturation The bioactive substances such as fatty acid, monounsaturated fatty acid, vitamin E, Squalene, tea polyphenols, have the highest nutriture value Value, along with masses are to the increase of high-quality oil tea demand and day by day increasing of requirement, the processing of high-quality nourishing healthy oil tea is more Send out important.
For a long time, the Oleum Camelliae of market sale has the oils and fats of hot moulding and extraction gained to be main more, but hot moulding Oleum Camelliae contains greatly The impurity of amount or undesirable substance, not only perception is poor, is of low nutritive value, and mouthfeel is poor, easily becomes sour, and affects storage stability, is unfavorable for Health；Meanwhile, the most inevitably there is solvent and retain in extraction Oleum Camelliae so that Oleum Camelliae range of application is extremely restricted, Potential economic benefit could not give full play to, and Guan Jihua, Liu Xiongmin etc. are in " camellia oleosa seed cold-press produces Oleum Camelliae technical study ", application Work, 2015 volume 44 the 12nd, propose to use cold-press to be prepared for keeping nutritional labeling and the Oleum Camelliae of original local flavor, method in this Directly camellia oleosa seed is dried during preparing Oleum Camelliae or oven drying at low temperature, physics shelling, remove impurity, direct physical are squeezed and then filtered Preparing camellia oleosa seed crude oil, although this preparation technology maintains Oleum Camelliae nutritional labeling and original local flavor, but also existing one is Oil rate is low, and less than 30%, two is crude oil not to be carried out polish, and this preparation method can not meet the efficient of industry Oleum Camelliae Processing request, it is thus achieved that crude oil can not meet the demand of Oleum Camelliae of people's high-quality height nutrition.
The polish of crude oil refers to that crude oil is prepared as stable uniform color through several steps such as degumming, deacidification, decolouring, deodorizes The process of the quintessence oil that pool is good.Wherein deacidifying process mainly uses the way of alkali-refining deacidification, and alkali-refining deacidification is by adding alkali liquor, making Free fatty in oils and fats generates salt with alkali with reaction and separates further, thus reaches to remove free fatty, reduction The effect of acid number.But the salt generated due to acid-base neutralization is more difficult and separating of oil, but also the step that need to wash (reduces the residual of alkali Stay), oil-water separation will cause the further loss of oil.It addition, the Oleum Camelliae that alkali-refining deacidification processes contains one " alkali taste ", after needs The step of continuous deodorize removes remove impurity taste, and this finishing step is loaded down with trivial details, and power consumption is big, retains problem many.A kind of lean of exploitation is the most smart Processing technique coordinates the crude oil processing technique of high oil recovery to have the efficient industrial processes realizing high-quality height nutrition Camellia oil Significance.
Summary of the invention
The object of the invention is contemplated to make up the defect of prior art, it is provided that a kind of plant that can prevent cardiovascular disease Sterol Camellia oil and preparation method thereof.
The present invention is achieved by the following technical solutions:
A kind of plant sterol Camellia oil that can prevent cardiovascular disease, including following parts by weight of component: camellia seed kernels 120- 125, Radix Astragali 35-40, Bellis perennis leaf 30-35 plant sterol 2-3, Nata24-26, pure soda powder 0.42-0.43, acetic acid 0.55- 0.56, appropriate pure water, appropriate water, the ethanol of appropriate concentration 3%.
A kind of plant sterol Camellia oil that can prevent cardiovascular disease, is made up of following steps:
(1), by after the Radix Astragali, Bellis perennis leaf co-grinding, after adding the water mixing of gross weight 2-3 times, little fiery infusion 3h, mistake Filter, obtain filtrate and filtering residue, camellia seed kernels is put into big fire in pot stir-fry process 40min, during stir-frying, be uniformly sprinkled into 2-3 time Filtrate, is sprinkled into amount of filtrate every time and makes camellia seed kernels surface just moistening the best, and waiting to have stir-fried obtains modified Camellia afterwards Core is standby；
(2), by modified camellia oleosa seed put in the screw extruder of sectional temperature control, the first paragraph work of sectional temperature control screw extruder Controlling at 80 DEG C as temperature, second segment operating temperature controls at 40 DEG C, and the pressure of two sections is 60Mpa, from screw extruder In crude oil out flow into oil trap, from screw extruder, tea seed cake out is again introduced into segmentation temperature after quick micronizing Control screw extruder, the most uniformly sprays filtrate that step (1) obtains and stirs, keeping with the above work bar when of input Part, crude oil is collected in squeezing again, repeats 6-8 time, obtains crude oil standby；
(3) filtering residue, by step (1) obtained, bakes through little fire, after micronizing, adds the second of the concentration 3% of gross weight 4 times Alcohol mix and blend 30-40min, filters to obtain alcohol extract and alcohol extraction slag, by this alcohol extract, after step (1) and (2) use remaining The pure water mixing of filtrate, plant sterol, half Nata, pure soda powder and gross weight 10 times, heats under high temperature of 120 DEG C and stirs Mixing process 30min, afterwards in refrigerator after-20 DEG C of freezing processing, in vacuum 600kPa, to carry out vacuum under the conditions of-70 DEG C cold The dry 48h of lyophilizing must be standby rich in the Nata aeroge of the fortification alkalescence regular shape of high molten plant sterol；
(4), the pure water of second half Nata, acetic acid and gross weight 15-16 times is mixed, heated and stirred under high temperature of 120 DEG C Process 30min, after addition alcohol extraction slag stirs, put in Muffle furnace anti-150 DEG C of agitating heating stirrings under n 2 atmosphere Answer 5.5h, obtain acid Nata-plant slag carbon aerogels standby；
(5), will be enriched in the Nata aeroge of the fortification alkalescence regular shape of high molten plant sterol and hair that step (1) obtains Oil mixing, is sufficiently stirred for reacting 4h at 70 DEG C, filters, obtain fortification refined oil, afterwards toward in this fortification refined oil Again add acid Nata-plant slag carbon aerogels, at 50 DEG C, be sufficiently stirred for reacting 4h, centrifugal, centrifugal filtration, degassing, cold But vacuum barreled and get final product.
The invention have the advantage that the present invention uses the Radix Astragali, Bellis perennis leaf, plant sterol to coordinate camellia seed kernels to prepare Camellia oil, Folium daisy gentisin in Astragaloside IV in Radix Astragali, Bellis perennis leaf and activate that readily soluble plant sterol is collaborative enhances goods in advance Effect in terms of anti-cardiovascular disease；In preparation process, the water of the Radix Astragali, Bellis perennis leaf is endured extracting solution and adds camellia seed kernels In stir-frying, enhance the medicinal efficacy of camellia seed kernels, afterwards to the camellia seed kernels stir-fried by repeatedly squeezing preparation Flos Camelliae Japonicae hair Oil, in preparation process, uses the sectional temperature control Technology in Pressing of high temperature 80 DEG C and low temperature 40 DEG C, improves the oil yield of crude oil Decrease the loss of nutritional labeling simultaneously, meanwhile, at hot stage, again add the Radix Astragali, the water of Bellis perennis leaf endures extracting solution, strengthening Nutrition, improves effect of goods further；For the crude oil tentatively prepared, have employed homemade rich in high molten plant steroid The Nata aeroge of the fortification alkalescence regular shape of alcohol and acid Nata-plant slag carbon aerogels carry out degumming, deacidification, Decolouring, the process of deodorize, it is achieved that the refine of crude oil, technique is simple, and efficiency is high；The battalion rich in high molten plant sterol used Support the Nata aeroge of strengthening alkalescence regular shape be use the Radix Astragali, Bellis perennis alcohol extracts from the leaves and water cooking liquid, plant sterol and The reaction under alkalescence hot conditions of Nata cellulose aquagel is prepared from, and rich in amino-reactive site, has good taking off Acid effect, meanwhile, simplifies the Radix Astragali, the preparation process of Bellis perennis folic alcohol extract functional mass, it is achieved that the battalion of Nata aeroge Support strengthening；The acid Nata-plant slag carbon aerogels used is to use Nata to combine alcohol extraction slag through inert gas environment heating system For obtain, Stability Analysis of Structures, there is abundant aperture and good adsorption effect, the alkali neutralizing oil can be further functioned as simultaneously Effect of property.
Detailed description of the invention
A kind of plant sterol Camellia oil that can prevent cardiovascular disease, including following parts by weight of component: camellia seed kernels 120, the Radix Astragali 35, Bellis perennis leaf 30 plant sterol 2, Nata24, pure soda powder 0.42, acetic acid 0.55, appropriate pure water, appropriate Water, the ethanol of appropriate concentration 3%.
A kind of plant sterol Camellia oil that can prevent cardiovascular disease, is made up of following steps:
(1), by after the Radix Astragali, Bellis perennis leaf co-grinding, after adding the water mixing of gross weight 2 times, little fire infusion 3h, filter, Filtrate and filtering residue, camellia seed kernels is put into big fire in pot stir-fry process 40min, during stir-frying, be uniformly sprinkled into 2 filtrates, Be sprinkled into amount of filtrate makes camellia seed kernels surface just moistening the best every time, and waiting to have stir-fried, it is standby to obtain modified camellia seed kernels afterwards With；
(2), by modified camellia oleosa seed put in the screw extruder of sectional temperature control, the first paragraph work of sectional temperature control screw extruder Controlling at 80 DEG C as temperature, second segment operating temperature controls at 40 DEG C, and the pressure of two sections is 60Mpa, from screw extruder In crude oil out flow into oil trap, from screw extruder, tea seed cake out is again introduced into segmentation temperature after quick micronizing Control screw extruder, the most uniformly sprays filtrate that step (1) obtains and stirs, keeping with the above work bar when of input Part, crude oil is collected in squeezing again, repeats 6 times, obtains crude oil standby；
(3) filtering residue, by step (1) obtained, bakes through little fire, after micronizing, adds the second of the concentration 3% of gross weight 4 times Alcohol mix and blend 30min, filters to obtain alcohol extract and alcohol extraction slag, by this alcohol extract, remaining filter after step (1) and (2) use The pure water mixing of liquid, plant sterol, half Nata, pure soda powder and gross weight 10 times, heated and stirred under high temperature of 120 DEG C Process 30min, afterwards in refrigerator after DEG C freezing processing, vacuum 600kPa, DEG C under the conditions of carry out vacuum lyophilization 48h Must be standby rich in the Nata aeroge of the fortification alkalescence regular shape of high molten plant sterol；
(4), being mixed by the pure water of second half Nata, acetic acid and gross weight 15 times, under high temperature of 120 DEG C, heated and stirred processes 30min, after addition alcohol extraction slag stirs, puts in Muffle furnace under n 2 atmosphere 150 DEG C of agitating heating stirring reactions 5.5h, obtains acid Nata plant slag carbon aerogels standby；
(5), will be enriched in the Nata aeroge of the fortification alkalescence regular shape of high molten plant sterol and hair that step (1) obtains Oil mixing, is sufficiently stirred for reacting 4h at 70 DEG C, filters, obtain fortification refined oil, afterwards toward in this fortification refined oil Again add acid Nata plant slag carbon aerogels, at 50 DEG C, be sufficiently stirred for reacting 4h, centrifugal, centrifugal filtration, deaerate, cool down Vacuum barreled and get final product.

Claims (2)

1. the plant sterol Camellia oil that can prevent cardiovascular disease, it is characterised in that include following parts by weight of component: mountain Camellia oleosa seed 120-125, Radix Astragali 35-40, Bellis perennis leaf 30-35 plant sterol 2-3, Nata24-26, pure soda powder 0.42-0.43, second Acid 0.55-0.56, appropriate pure water, appropriate water, the ethanol of appropriate concentration 3%.
A kind of plant sterol Camellia oil that can prevent cardiovascular disease the most according to claim 1, it is characterised in that by Following steps are made:
(1), by after the Radix Astragali, Bellis perennis leaf co-grinding, after adding the water mixing of gross weight 2-3 times, little fiery infusion 3h, mistake Filter, obtain filtrate and filtering residue, camellia seed kernels is put into big fire in pot stir-fry process 40min, during stir-frying, be uniformly sprinkled into 2-3 time Filtrate, is sprinkled into amount of filtrate every time and makes camellia seed kernels surface just moistening the best, and waiting to have stir-fried obtains modified Camellia afterwards Core is standby；
(2), by modified camellia oleosa seed put in the screw extruder of sectional temperature control, the first paragraph work of sectional temperature control screw extruder Controlling at 80 DEG C as temperature, second segment operating temperature controls at 40 DEG C, and the pressure of two sections is 60Mpa, from screw extruder In crude oil out flow into oil trap, from screw extruder, tea seed cake out is again introduced into segmentation temperature after quick micronizing Control screw extruder, the most uniformly sprays filtrate that step (1) obtains and stirs, keeping with the above work bar when of input Part, crude oil is collected in squeezing again, repeats 6-8 time, obtains crude oil standby；
(3) filtering residue, by step (1) obtained, bakes through little fire, after micronizing, adds the second of the concentration 3% of gross weight 4 times Alcohol mix and blend 30-40min, filters to obtain alcohol extract and alcohol extraction slag, by this alcohol extract, after step (1) and (2) use remaining The pure water mixing of filtrate, plant sterol, half Nata, pure soda powder and gross weight 10 times, heats under high temperature of 120 DEG C and stirs Mixing process 30min, afterwards in refrigerator after-20 DEG C of freezing processing, in vacuum 600kPa, to carry out vacuum under the conditions of-70 DEG C cold The dry 48h of lyophilizing must be standby rich in the Nata aeroge of the fortification alkalescence regular shape of high molten plant sterol；
(4), the pure water of second half Nata, acetic acid and gross weight 15-16 times is mixed, heated and stirred under high temperature of 120 DEG C Process 30min, after addition alcohol extraction slag stirs, put in Muffle furnace anti-150 DEG C of agitating heating stirrings under n 2 atmosphere Answer 5.5h, obtain acid Nata-plant slag carbon aerogels standby；
(5), will be enriched in the Nata aeroge of the fortification alkalescence regular shape of high molten plant sterol and hair that step (1) obtains Oil mixing, is sufficiently stirred for reacting 4h at 70 DEG C, filters, obtain fortification refined oil, afterwards toward in this fortification refined oil Again add acid Nata-plant slag carbon aerogels, at 50 DEG C, be sufficiently stirred for reacting 4h, centrifugal, centrifugal filtration, degassing, cold But vacuum barreled and get final product.
CN201610657766.6A 2016-08-12 2016-08-12 A kind of plant sterol Camellia oil that can prevent cardiovascular disease and preparation method thereof Pending CN106190530A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111528294A (en) * 2020-06-11 2020-08-14 咸宁市兴鑫农业开发有限公司 A nutritious health camellia oil and its preparation method

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CN103493904A (en) * 2013-08-29 2014-01-08 潘逸东 Preparation method of stomach strengthening and qi regulating camellia oil
CN103923740A (en) * 2014-03-11 2014-07-16 安徽亿宏生物科技有限公司 Preparation method of strong aroma camellia oil
CN103989991A (en) * 2014-05-12 2014-08-20 深圳市恒昇启泰进出口有限公司 A camellia oil liquid preparation used for preventing and treating oral diseases

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
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Application publication date: 20161207