CN106148750A - The process equipment of silver copper oxide and processing technique thereof - Google Patents

The process equipment of silver copper oxide and processing technique thereof Download PDF

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Publication number
CN106148750A
CN106148750A CN201610487276.6A CN201610487276A CN106148750A CN 106148750 A CN106148750 A CN 106148750A CN 201610487276 A CN201610487276 A CN 201610487276A CN 106148750 A CN106148750 A CN 106148750A
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China
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powder
casing
connects
copper oxide
smelting apparatus
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CN201610487276.6A
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CN106148750B (en
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孙珂杨
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NINGBO KEYANG PRECIOUS METAL ALLOYS TECHNOLOGY Co Ltd
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NINGBO KEYANG PRECIOUS METAL ALLOYS TECHNOLOGY Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C1/00Making non-ferrous alloys
    • C22C1/10Alloys containing non-metals

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Manufacture And Refinement Of Metals (AREA)
  • Apparatuses For Bulk Treatment Of Fruits And Vegetables And Apparatuses For Preparing Feeds (AREA)

Abstract

The invention discloses process equipment and the processing technique thereof of silver copper oxide, including smelting apparatus and PLC control system, smelting apparatus connects atomising device, it is provided with valve between smelting apparatus and atomising device, connect on atomising device and have pressurizer and vacuum extractor, powder ejiction opening it is provided with bottom atomising device, powder ejiction opening connects powder collection screen screening device, powder collection screen screening device includes casing, casing is separated into coarse fodder chamber and fines chamber by dividing plate, casing is provided with fumarole at powder ejiction opening, both sides, institute's coarse fodder chamber connect feed back pipeline, feed back pipeline forms loop and connects smelting apparatus.The process equipment of this kind of silver copper oxide and processing technique thereof can reduce oarse-grained metal dust, so that oxidization of metal powder is more abundant, product quality improves.

Description

The process equipment of silver copper oxide and processing technique thereof
Technical field
The invention belongs to process equipment and the processing technique thereof in metal fabrication techniques field, specifically silver copper oxide.
Background technology
Along with the development of science and technology, industry manufacture field is increasing to the demand of electromechanical compo, also refers to its performance simultaneously Mark requires more and more higher.Silver copper oxide contact material is development in recent years Novel non-toxic electrical contact material quickly, has heat steady The advantage such as reserve, resistance to arc erosion and resistance fusion welding are strong, be the ideal material at present in catalyst, relay field.
Existing silver copper oxide processing technique step is: by silver ingot, copper is placed in melting ingot casting in smelting furnace, then by gold Belong to ingot and be processed into chip, obtain the mixing material based on silver copper oxide through High Temperature High Pressure oxidation, crush through machining, By chip extrusion forming in punching block, the most at high temperature it is squeezed into bar, band, then obtains silver copper oxide bar, band through drawing Material.
The existing method that ingot is made chip is usually and uses ball mill ball milling or use nebulization, ball mill In mechanical milling process, it may be acted on by grinding compressive stress repeatedly, cause be present in intrinsic on this particle surface or newborn The crack extesion become, and then it is directed at its broken or generation plastic deformation.When this granule is the most crushed. certain one-level of generation New granule dyschezia is with the most levigate, this is because the crackle on new grain surface is relatively thin, and a certain minimum fracture occurs The cause that the crackle probability of stress also reduces.When shattering process proceeds, required finished breaking stress may increase Greatly to the degree making granule produce plastic deformation.Now, along with the generation of plastic deformation, granule just will not be by levigate.Cause This, have a granularity ultimate value during grinding material, say, that when the grinding of material enters into the scope of superfine grinding, The pulverization of ball mill is the most more and more difficult.An actual grinding limit is all there is in most of grinding systems, this One limit depends on that grinding product granule produces the tendency again built up mainly, and is set up between building up and being broken The physical equilibrium come.Long prolongation Ball-milling Time is skimble-skamble, only results in the increase of energy consumption, because meticulous granule Cannot effectively store the elastic energy made needed for crack extesion, the powder particle that therefore ball-milling method prepares is relatively large, rear Continuous oxidizing process is difficult to fully oxidized.Nebulization more advantage by contrast, nebulization is to be led to by melted metal liquid Crossing high pressure to spray from shower nozzle, the method forming powder after the drop cooling of ejection, the powder of nebulization ejection is relative to ball milling Machine ball milling powder out is less, can aoxidize more abundant, and the granule of nebulization shower nozzle ejection also has during subsequent oxidation Size, one is due to ejection some oarse-grained drops of the uneven existence caused, and two is owing to the drop of ejection is not also coagulating Form big liquid after contact before knot, thus have oarse-grained powder after causing the droplet formation powder that nebulization sprays End, causes subsequent oxidation process to be difficult to fully oxidized.
Summary of the invention
The present invention is directed to prior art not enough, it is provided that the process equipment of silver copper oxide and processing technique thereof, this kind of silver oxidation The process equipment of copper and processing technique thereof can reduce oarse-grained metal dust, so that oxidization of metal powder is more filled Point, product quality improves.
In order to solve above-mentioned technical problem, the present invention is addressed by following technical proposals: the processing of silver copper oxide sets Standby, including smelting apparatus and PLC control system, described smelting apparatus connects atomising device, described smelting apparatus and institute Stating and be provided with valve between atomising device, described atomising device connects pressurizer and vacuum extractor, described atomization Bottom of device is provided with powder ejiction opening, and described powder ejiction opening connects powder collection screen screening device, described powder collection screen Screening device includes casing, is vertically arranged with the dividing plate keeping the connection of casing upper end in the middle part of described casing, and casing is divided by described dividing plate Being divided into coarse fodder chamber and fines chamber, described casing is provided with fumarole at described powder ejiction opening, and described fumarole connects There are air jet system, described air jet system to include motor and impeller, are provided with out on the casing of described fumarole opposite side Pore, described venthole connects outlet pipe, and described outlet pipe connects the air inlet of described air jet system, described fines chamber Bottom is provided with discharging opening, and described coarse fodder chamber connects feeding back device, and described feeding back device connects described smelting apparatus.This equipment Prevent the motlten metal in atomising device oxidized by the air in vacuum extractor evacuation atomising device, blow when colluding and make Obtaining oarse-grained powder and drop into coarse fodder intracavity, short grained powder drops into fines intracavity, and oarse-grained powder is from feed back pipe Road backs into refuse in smelting apparatus, so that be all fine powder, beneficially later stage from discharging opening powder out Oxidation.
In technique scheme, it is preferred that described feeding back device includes feed back pipeline, described feed back pipeline forms loop also Connect described smelting apparatus, be provided with the chain that head and the tail connect in described feed back pipeline, described chain be provided with and described time The delivery board of pipe material match of pipe diameter, described feed back pipeline is provided with the sprocket wheel mated with described chain, on described motor Connecting on output shaft and have described sprocket wheel, when described electric motor starting, described sprocket wheel rotates with described impeller simultaneously.By impeller and chain Wheel controls to open so that chain will run when blowing device works by motor simultaneously, prevents the coarse fodder in coarse fodder chamber Pile up and too much fall in fines case.
In technique scheme, it is preferred that be provided with chiller on described outlet pipe.Apparatus for supercooling and jet Device coordinates ejection cold air so that the motlten metal fast setting of atomising device ejection, thus prevents motlten metal after ejection Contact bonding forms bulky grain powder.
In technique scheme, it is preferred that be provided with on described outlet pipe and add QI KOU for be filled with protective gas.If Put protective gas and add entrance, when discharging opening opens discharging, be filled with nitrogen thus prevent air from entering casing.
The processing technique of the process equipment of application silver copper oxide, comprises the following steps: 1, put into described molten by silver ingot, copper ingot Melt in refining device;2, starting described vacuum extractor and evacuate the air in described atomising device, opening described valve will be melted Metal put in atomising device and close described valve;3, start described motor and make described impeller and described chain round Dynamic, start described pressurizer and atomising device is filled with nitrogen supercharging.
In technique scheme, it is preferred that also include between step 2 and step 3 and be filled with in the nitrogen described casing of replacement The step of air.
The present invention compared with prior art, has the advantages that this equipment evacuates atomization dress by vacuum extractor Putting interior air prevents the motlten metal in atomising device oxidized, and blowing when colluding makes oarse-grained powder drop into coarse fodder Intracavity, short grained powder drops into fines intracavity, and oarse-grained powder backs in smelting apparatus from feed back pipeline and again melts Change, so that be all fine powder from discharging opening powder out, beneficially later stage oxidation.
Accompanying drawing explanation
Fig. 1 is the structural representation of the embodiment of the present invention.
Fig. 2 is the left view of Fig. 1.
Fig. 3 is the attachment structure schematic diagram of chain and delivery board.
Detailed description of the invention
With detailed description of the invention, the present invention is described in further detail below in conjunction with the accompanying drawings: see Fig. 1 to Fig. 3, silver oxygen Changing the process equipment of copper, including smelting apparatus 1 and PLC control system, described smelting apparatus 1 connects atomising device 2, described Be provided with valve 3 between smelting apparatus 1 and described atomising device 2, on described atomising device 2 connect have pressurizer 4 and Vacuum extractor 5, is provided with powder ejiction opening 21 bottom described atomising device 2, described powder ejiction opening 21 connects has powder to receive Collection screening plant 6, described powder collection screen screening device 6 includes casing 7, is vertically arranged with on holding casing 7 in the middle part of described casing 7 The dividing plate 71 of end connection, casing 7 is separated into coarse fodder chamber 72 and fines chamber 73 by described dividing plate 71, and described casing 7 is near described Being provided with fumarole 74 at powder ejiction opening 21, described fumarole 74 connects has air jet system 8, described air jet system 8 to include electricity Being provided with venthole 75 on machine and impeller, with the casing 7 of described fumarole 74 opposite side, described venthole 75 connects to be had Feed channel 76, described outlet pipe 76 connects the air inlet of described air jet system 8, is provided with discharging opening bottom described fines chamber 73 77, described coarse fodder chamber 72 connects has feeding back device 10, described feeding back device 10 to connect described smelting apparatus 1.This equipment is by taking out Air in vacuum equipment evacuation atomising device prevents the motlten metal in atomising device oxidized, blows and make big when colluding The powder of grain drops into coarse fodder intracavity, and short grained powder drops into fines intracavity, and oarse-grained powder backs into from feed back pipeline Refuse in smelting apparatus, so that be all fine powder from discharging opening powder out, beneficially later stage oxidation.
Described feeding back device 10 includes that feed back pipeline 78, described feed back pipeline 78 form loop and connect described smelting apparatus 1, it is provided with the chain 79 that head and the tail connect in described feed back pipeline 78, described chain 79 is provided with and manages with described feed back pipeline 78 The delivery board 710 of footpath coupling, described feed back pipeline 78 is provided with the sprocket wheel mated with described chain 79, defeated on described motor Connecting on shaft and have described sprocket wheel, when described electric motor starting, described sprocket wheel rotates with described impeller simultaneously.By impeller and sprocket wheel Control to open by motor so that chain will run when blowing device works simultaneously, prevent the coarse fodder heap in coarse fodder chamber Amass and too much fall in fines case.
It is provided with chiller 9 on described outlet pipe 76.Apparatus for supercooling and air jet system coordinate ejection cold air, make Obtain the motlten metal fast setting of atomising device ejection, thus prevent motlten metal to be followed by contact bonding knot in ejection and form bulky grain powder End.
It is provided with on described outlet pipe 76 and adds QI KOU 711 for be filled with protective gas.Protective gas is set and adds entrance, When discharging opening opens discharging, it is filled with nitrogen thus prevents air from entering casing.
Comprise the following steps: 1, silver ingot, copper ingot are put into described smelting apparatus 1 and melted;2, described vacuum means is started Put the air in the 5 described atomising devices of evacuation 2, open in melted metal is put into atomising device 2 by described valve 3 and close Described valve 3;3, starting described motor makes described impeller and described sprocket wheel rotate, and starts described pressurizer 4 to atomization Device 2 is filled with nitrogen supercharging.
Also include between step 2 and step 3 and be filled with nitrogen and replace the step of air in described casing 7.

Claims (6)

1. the process equipment of silver copper oxide, including smelting apparatus (1) and PLC control system, described smelting apparatus (1) connects to be had Atomising device (2), it is characterised in that: it is provided with valve (3), institute between described smelting apparatus (1) and described atomising device (2) Stating the upper connection of atomising device (2) has pressurizer (4) and vacuum extractor (5), described atomising device (2) bottom to be provided with powder Material ejiction opening (21), described powder ejiction opening (21) connects powder collection screen screening device (6), described powder collection screen screening device (6) including casing (7), described casing (7) middle part is vertically arranged with the dividing plate (71) keeping the connection of casing (7) upper end, described every Casing (7) is separated into coarse fodder chamber (72) and fines chamber (73) by plate (71), and described casing (7) is near described powder ejiction opening (21) place is provided with fumarole (74), and described fumarole (74) connects has air jet system (8), described air jet system (8) to include electricity Venthole (75), described venthole (75) it is provided with on machine and impeller, with the casing (7) of described fumarole (74) opposite side Connecting has outlet pipe (76), described outlet pipe (76) to connect the air inlet of described air jet system (8), described fines chamber (73) Bottom is provided with discharging opening (77), and described coarse fodder chamber (72) connects feeding back device (10), and described feeding back device (10) connects institute State smelting apparatus (1).
2. the process equipment of silver copper oxide as claimed in claim 1, it is characterised in that: described feeding back device (10) includes feed back Pipeline (78), described feed back pipeline (78) forms loop and connects described smelting apparatus (1), arranges in described feed back pipeline (78) The chain (79) having head and the tail to connect, described chain (79) is provided with and the delivery board of described feed back pipeline (78) match of pipe diameter (710), described feed back pipeline (78) is provided with the sprocket wheel mated with described chain (79), the output shaft on described motor connects Being connected to described sprocket wheel, when described electric motor starting, described sprocket wheel rotates with described impeller simultaneously.
3. the process equipment of silver copper oxide as claimed in claim 1, it is characterised in that: described outlet pipe is provided with on (76) Chiller (9).
4. the process equipment of silver copper oxide as claimed in claim 1, it is characterised in that: described outlet pipe is provided with on (76) QI KOU (711) is added for be filled with protective gas.
5. apply the processing technique of the process equipment of silver copper oxide as claimed in claim 2, it is characterised in that include following step Rapid: 1, silver ingot, copper ingot to be put into described smelting apparatus (1) and melted;2, start described vacuum extractor (5) and evacuate described atomization Air in device (2), opens in melted metal is put into atomising device (2) by described valve (3) and closes described valve (3);3, starting described motor makes described impeller and described sprocket wheel rotate, and starts described pressurizer (4) to atomising device (2) it is filled with nitrogen supercharging.
6. the processing technique of the process equipment of silver copper oxide as claimed in claim 5, it is characterised in that: step 2 and step 3 it Between also include be filled with nitrogen replace described casing (7) interior air step.
CN201610487276.6A 2016-06-29 2016-06-29 The process equipment and its processing technology of silver copper oxide Active CN106148750B (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111922352A (en) * 2020-07-27 2020-11-13 安徽旭晶粉体新材料科技有限公司 Efficient preparation device and preparation method of spherical copper alloy powder

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101362206A (en) * 2008-10-09 2009-02-11 陈新国 Preparation method of continuous high quality soldering powder
CN201817055U (en) * 2010-09-25 2011-05-04 杭州华达喷射真空设备有限公司 Chain plate type sprocket driving and tensioning pipeline conveying appliance
CN102054598A (en) * 2011-01-13 2011-05-11 中希合金有限公司 Silver copper oxide/copper composite electrical contact material and preparation process thereof
CN102689015A (en) * 2012-06-21 2012-09-26 北京有色金属研究总院 Metal powder preparation device and method therefor
CN103611942A (en) * 2013-12-10 2014-03-05 河北联合大学 High-pressure smelting atomizing nitrogen-quenching device and method for utilizing device to produce samarium iron nitrogen alloy powder

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101362206A (en) * 2008-10-09 2009-02-11 陈新国 Preparation method of continuous high quality soldering powder
CN201817055U (en) * 2010-09-25 2011-05-04 杭州华达喷射真空设备有限公司 Chain plate type sprocket driving and tensioning pipeline conveying appliance
CN102054598A (en) * 2011-01-13 2011-05-11 中希合金有限公司 Silver copper oxide/copper composite electrical contact material and preparation process thereof
CN102689015A (en) * 2012-06-21 2012-09-26 北京有色金属研究总院 Metal powder preparation device and method therefor
CN103611942A (en) * 2013-12-10 2014-03-05 河北联合大学 High-pressure smelting atomizing nitrogen-quenching device and method for utilizing device to produce samarium iron nitrogen alloy powder

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111922352A (en) * 2020-07-27 2020-11-13 安徽旭晶粉体新材料科技有限公司 Efficient preparation device and preparation method of spherical copper alloy powder

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