CN106145106A - A kind of preparation method of modified activated carbon - Google Patents

A kind of preparation method of modified activated carbon Download PDF

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Publication number
CN106145106A
CN106145106A CN201610498466.8A CN201610498466A CN106145106A CN 106145106 A CN106145106 A CN 106145106A CN 201610498466 A CN201610498466 A CN 201610498466A CN 106145106 A CN106145106 A CN 106145106A
Authority
CN
China
Prior art keywords
activated carbon
preparation
modified activated
active charcoal
oxygen
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610498466.8A
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Chinese (zh)
Inventor
钟华
梁明
张兵
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Anhui Tianshun Environmental Protection Equipment Ltd By Share Ltd
Original Assignee
Anhui Tianshun Environmental Protection Equipment Ltd By Share Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Anhui Tianshun Environmental Protection Equipment Ltd By Share Ltd filed Critical Anhui Tianshun Environmental Protection Equipment Ltd By Share Ltd
Priority to CN201610498466.8A priority Critical patent/CN106145106A/en
Publication of CN106145106A publication Critical patent/CN106145106A/en
Pending legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/28Treatment of water, waste water, or sewage by sorption
    • C02F1/281Treatment of water, waste water, or sewage by sorption using inorganic sorbents
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/28Treatment of water, waste water, or sewage by sorption
    • C02F1/283Treatment of water, waste water, or sewage by sorption using coal, charred products, or inorganic mixtures containing them
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/12Surface area

Abstract

The invention discloses the preparation method of a kind of modified activated carbon, it comprises the following steps: take suitable raw material, through crushed after being dried, crosses 40 mesh sieves, obtains carbon powder;In carbon powder add adhesive, compressing after activate, obtain activated carbon;Activated carbon is pre-oxidized, obtains surface oxygen-content active charcoal;Oxygen-content active charcoal is put in potassium hydroxide solution, regulates PH to 7 ~ 9, take out after standing and be dried, obtain modified activated carbon.The present invention utilizes the mode of modification to increase the surface area of activated carbon, improves using effect in organic solvent for the activated carbon, adds its activity, economic and practical, can be widely applied to water pollution process.

Description

A kind of preparation method of modified activated carbon
Technical field
The present invention relates to field of Environment Protection, particularly relate to the preparation method of a kind of modified activated carbon.
Background technology
At present, as economic develops rapidly, chemical enterprise also high speed development therewith, cause the use of chemicals to increase Many, the situation of harmful substance contaminant water environment by all means is also increasing, had both affected environment, and had damaged again health of people. And these pollutant kinds are various, this causes serious impact to the improvement of enterprise, too increases certain difficulty.At present for Acidity of Aikalinity pollutes the mode being mostly to use chemistry neutralisation treatment, virtually to enterprise with certain economic loss, thus a kind of Very popular by modified activated carbon.
Content of the invention
In order to overcome the defect of above-mentioned prior art, it is an object of the invention to provide the preparation side of a kind of modified activated carbon Method.
The present invention takes techniques below scheme to realize: the preparation method of a kind of modified activated carbon, and it includes following Step: take suitable raw material, through crushed after being dried, crosses 40 mesh sieves, obtains carbon powder;Adhesive, pressure is added in carbon powder Activate after making type, obtain activated carbon;Activated carbon is pre-oxidized, obtains surface oxygen-content active charcoal;By oxygen-content active Charcoal is put in potassium hydroxide solution, regulates PH to 7 ~ 9, takes out and is dried, obtain modified activated carbon after standing.
The preparation method of above-mentioned a kind of modified activated carbon, described raw material is the various carbonaceous material such as anthracite, coking coal.
The preparation method of above-mentioned a kind of modified activated carbon, described baking temperature is at 60 ~ 80 DEG C.
The preparation method of above-mentioned a kind of modified activated carbon, a length of 8 ~ 12h during described standing.
The preparation method of above-mentioned a kind of modified activated carbon, described activation temperature is 200 ~ 400 DEG C.
The method have the advantages that the present invention utilizes the mode of modification to increase the surface of activated carbon in sum Long-pending, improve using effect in organic solvent for the activated carbon, add its activity, economic and practical, can be widely applied to water dirty The advantages such as dye process.
Detailed description of the invention
A kind of preparation method of modified activated carbon, it comprises the following steps: take suitable raw material, through crushed after being dried, Cross 40 mesh sieves, obtain carbon powder;In carbon powder add adhesive, compressing after activate, obtain activated carbon;To activity Charcoal pre-oxidizes, and obtains surface oxygen-content active charcoal;Oxygen-content active charcoal is put in potassium hydroxide solution, regulates PH to 7 ~ 9, quiet Postpone taking-up to be dried, obtain modified activated carbon.
The preparation method of above-mentioned a kind of modified activated carbon, described raw material is the various carbonaceous material such as anthracite, coking coal.
The preparation method of above-mentioned a kind of modified activated carbon, described baking temperature is at 60 ~ 80 DEG C.
The preparation method of above-mentioned a kind of modified activated carbon, a length of 8 ~ 12h during described standing.
The preparation method of above-mentioned a kind of modified activated carbon, described activation temperature is 200 ~ 400 DEG C.
The method have the advantages that the present invention has raw material sources in sum wide, can be recycled, reduce money The advantages such as the waste in source, utilize modified mode to increase the surface area of activated carbon, improve activated carbon in organic solvent Using effect, adds its activity, economic and practical, can be widely applied to water pollution process.
The above is embodiments of the invention, therefore all according to the construction described in the present patent application scope, feature and principle institute The equivalence change done or modification, in the range of being all included in present patent application.

Claims (5)

1. the preparation method of a modified activated carbon, it is characterised in that it comprises the following steps: take suitable raw material, through overdrying Pulverize after dry, cross 40 mesh sieves, obtain carbon powder;In carbon powder add adhesive, compressing after activate, obtain activity Charcoal;Activated carbon is pre-oxidized, obtains surface oxygen-content active charcoal;Oxygen-content active charcoal is put in potassium hydroxide solution, regulation PH to 7 ~ 9, takes out after standing and is dried, obtain modified activated carbon.
2. the preparation method of a kind of modified activated carbon according to claim 1, it is characterised in that: described raw material is smokeless The various carbonaceous material such as coal, coking coal.
3. the preparation method of a kind of modified activated carbon according to claim 1, it is characterised in that: described baking temperature is 60 ~80℃。
4. the preparation method of a kind of modified activated carbon according to claim 1, it is characterised in that: described a length of 8 when standing ~ 12h。
5. the preparation method of a kind of modified activated carbon according to claim 1, it is characterised in that: described activation temperature is 200~400℃。
CN201610498466.8A 2016-06-30 2016-06-30 A kind of preparation method of modified activated carbon Pending CN106145106A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610498466.8A CN106145106A (en) 2016-06-30 2016-06-30 A kind of preparation method of modified activated carbon

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610498466.8A CN106145106A (en) 2016-06-30 2016-06-30 A kind of preparation method of modified activated carbon

Publications (1)

Publication Number Publication Date
CN106145106A true CN106145106A (en) 2016-11-23

Family

ID=57350468

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610498466.8A Pending CN106145106A (en) 2016-06-30 2016-06-30 A kind of preparation method of modified activated carbon

Country Status (1)

Country Link
CN (1) CN106145106A (en)

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103496699A (en) * 2013-10-21 2014-01-08 哈尔滨工业大学 Preparation method for modified activated carbon

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103496699A (en) * 2013-10-21 2014-01-08 哈尔滨工业大学 Preparation method for modified activated carbon

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
刘晓敏等: ""浸渍改性活性炭对正丁烷吸附性能的研究"", 《可再生能源》 *
朱晨等: ""氧化-活化处理的超级电容器用高比电容活性炭"", 《中南大学学报(自然科学版)》 *
甘琦等: ""成型活性炭的制备研究进展"", 《材料导报》 *

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Application publication date: 20161123

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