CN106140028A - Reactor quantitative liquid feeding device and using method thereof - Google Patents

Reactor quantitative liquid feeding device and using method thereof Download PDF

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Publication number
CN106140028A
CN106140028A CN201610690069.0A CN201610690069A CN106140028A CN 106140028 A CN106140028 A CN 106140028A CN 201610690069 A CN201610690069 A CN 201610690069A CN 106140028 A CN106140028 A CN 106140028A
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China
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liquid
post
sealing
storage container
quantitative
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CN201610690069.0A
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CN106140028B (en
Inventor
余建龙
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Jiangsu Sanpeng Biochemical Co Ltd
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00Feed or outlet devices; Feed or outlet control devices
    • B01J4/001Feed or outlet devices as such, e.g. feeding tubes
    • B01J4/007Feed or outlet devices as such, e.g. feeding tubes provided with moving parts
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/0066Stirrers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00Feed or outlet devices; Feed or outlet control devices
    • B01J4/02Feed or outlet devices; Feed or outlet control devices for feeding measured, i.e. prescribed quantities of reagents
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2204/00Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices
    • B01J2204/002Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices the feeding side being of particular interest

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Devices For Dispensing Beverages (AREA)

Abstract

The invention discloses reactor quantitative liquid feeding device and using method thereof.Including housing, case top connects liquid injecting pipeline, and housing arranges quantitative liquor charging assembly and lifting assembly, and quantitative liquor charging assembly includes flexible liquid storage container and liquid collecting container, quantitatively cooperating between liquor charging assembly and lifting assembly, device is also connected with a stirring structure simultaneously.The present invention is by merging liquid component equivalent bigger for accounting joining in reactor in batches with stirring with other compositions again, add the small amount of liquids composition of equivalent i.e. while stirring, thus promote stirring efficiency, ensure that stirring is merged uniformly, increase product percent of pass, also there is the effect avoiding waste simultaneously.

Description

Reactor quantitative liquid feeding device and using method thereof
Technical field
The present invention relates to perfume production reactor technical field, especially reactor quantitative liquid feeding device and use thereof Method.
Background technology
Need when prepared by perfume to use reactor, stir in heterogeneity is joined reactor according to certain ratio Draw after mixing, and be fixing with this ratio of a perfume.
At present frequently with agitating mode, be directly to stir in various deployed compositions are implanted sequentially reactor Mixing, although this agitating mode is simple to operate, but stirring efficiency is relatively low, such as by direct for liquid component bigger for a kind of accounting When all injecting in the liquid in reactors, generally requiring the stirring long period can both merge uniform completely, and stirs Mix uneven meeting and directly influence the whole structure of perfume, produce substandard product.
Content of the invention
The present invention is directed to deficiency of the prior art, provide reactor quantitative liquid feeding device and using method thereof, its By liquid component equivalent bigger for accounting joining in reactor in batches is merged stirring with other compositions again, i.e. limit is stirred Mix limit and add the small amount of liquids composition of equivalent, thus promote stirring efficiency, it is ensured that stirring is merged uniformly, increases product qualified Rate, also has the effect avoiding waste simultaneously.
For solving above-mentioned technical problem, the present invention is addressed by following technical proposals: reactor is filled by quantitative liquor charging Putting, including inside offers the housing of cavity, described case top is connected with liquid injecting pipeline, described housing is provided with and quantitatively send Liquid assembly and the lifting assembly coordinating with described quantitative liquor charging assembly, described quantitative liquor charging assembly includes being arranged on described housing Interior flexible liquid storage container and the some liquid collectings being arranged on described housing exterior walls and connecting with described flexible liquid storage container are held Device, described flexible liquid storage container is positioned at immediately below described liquid injecting pipeline, offers liquid outlet, described liter bottom described liquid collecting container Part of coming down to a lower group includes the connection post being slidably connected in described inner walls, the connecting rod being arranged on described connection capital face, sets Put the black box in described connecting rod end and control some magnet combination that described connection post rises or falls, described magnetic Iron combination includes being slidably connected in described inner walls and is connected the connected slide block of post with described, is fixedly installed on described slide block Magnet on bottom surface and the electromagnet being fixedly installed in described inner walls, when described electromagnet is energized, described electromagnetism Iron repels each other with described magnet, described connecting rod is provided with the jacking block coordinating with described flexible liquid storage container, in described connecting rod Offering cell body, described black box is arranged on described cell body inwall, and described black box includes from outside toward inner side successively A number tooth bar of engagement, gear and sealing-plug assembly, a described tooth bar is slidably connected on described cell body inwall, and described A number tooth bar lower end is provided with contiguous block, is provided with a spring, institute between described contiguous block and described connecting rod bottom surface Stating pinion rotation to be connected on described cell body inwall, described sealing-plug assembly includes be slidably connected on described cell body inwall two Number tooth bar and the sealing-plug being arranged on described No. two tooth bar tops, be provided with on described liquid collecting container outer wall simultaneously with described The push rod component that number tooth bar coordinates, fixed block that described push rod component includes being fixedly installed on described liquid collecting container outer wall, Be opened in the through hole on described fixed block, the push rod being plugged in described through hole, some grooves of being opened on described push rod with And it is rotatably connected on described fixed block bottom surface and the clamping block with described groove fit, described push rod upper end end is provided with connection It is provided with No. two springs, described clamping block and described fixed block bottom surface between piece, and described connection piece and described fixed block end face Link position at be provided with torsion spring, when described jacking block is bottom the rising of described connection post with described flexible liquid storage container During contact, described sealing-plug seals up described liquid outlet, offers cavity and form cavity body, at described cavity inside described connection post The internal motor that is provided with, described motor is connected with being arranged on the described stirring vane being connected immediately below post.
In technique scheme, it is preferred that described sealing-plug and described liquid outlet interference fit.
In technique scheme, it is preferred that described sealing-plug top is provided with circular arc projection.Due to liquid outlet out Liquid can directly be flushed to sealing-plug top, therefore arranges circular arc projection and ensure that sealing-plug top not residual liquid, it is ensured that Actual ratio and the uniformity of desired proportions, improving product qualification rate.
In technique scheme, it is preferred that described case top is provided with some support bars.By arrange support bar by Whole device is fixed in reactor.
In technique scheme, it is preferred that be coated with waterproof coating on described black box outer surface.Avoid liquid close Remain on sealing assembly outer surface, affect overall ratio.
Using the reactor described above method of quantitative liquid feeding device, its step is as follows: 1., by liquid injecting pipeline toward soft Property liquid storage container in inject need add liquid;2., start electromagnet and motor, connect post and repelled each other with magnet by electromagnet Rising after power effect, stirring vane is persistently mixed motion by motor control;3., with connecting the rising of post, sealing-plug assembly Rising therewith, after a tooth bar is blocked by push rod, a tooth bar moves relative to connecting post, promotes gear to rotate, meanwhile, No. two tooth bars of gear driven up move, and sealing-plug rises therewith;4., bottom the jacking block in connecting rod with flexible liquid storage container During contact, sealing-plug seals up liquid outlet;5., jacking block continues the liquid level rising of the liquid in rising promotes flexible liquid storage container, The liquid exceeding the position with flexible liquid storage container connector for the liquid collecting container is flowed in liquid collecting container, now electromagnet and magnetic The mutual expelling force of iron makes to connect post held stationary state;6. after, electromagnet is energized 30 seconds, close electromagnet power supply, connect under post Move;7., connecting in post folding process, first, in liquid collecting container, redundance liquid is back in flexible liquid storage container, and liquid collecting is held In device, liquid level keeps level consistent with above-mentioned connector bottom surface, reaches quantitative;Secondly, sealing-plug leaves liquid outlet, liquid collecting container Interior liquid is flowed in reactor from liquid outlet, mixes with other liquid;8. after, electromagnet stops energising 2 minutes, again right Electromagnet is energized, and so circulates.
The invention has the beneficial effects as follows: the present invention is by by anti-for liquid component equivalent bigger for accounting joining in batches Merge stirring with other compositions again in answering kettle, add the small amount of liquids composition of equivalent i.e. while stirring, thus promote stirring effect Rate, it is ensured that stirring is merged uniformly, increases product percent of pass, also has the effect avoiding waste simultaneously.
Brief description
Fig. 1 is schematic cross-section of the present invention.
Fig. 2 is jacking block of the present invention and schematic cross-section when contacting bottom flexible liquid storage container.
Fig. 3 be the flexible liquid storage container of the present invention in schematic cross-section when flowing to liquid collecting container for the liquid.
Fig. 4 is the schematic cross-section of connecting rod of the present invention.
Detailed description of the invention
With detailed description of the invention, the present invention is described in further detail below in conjunction with the accompanying drawings: see Fig. 1-Fig. 4, reactor Using quantitative liquid feeding device, including inside offers the housing 1 of cavity, described housing 1 top is connected with liquid injecting pipeline 2, described shell It is provided with quantitative liquor charging assembly and the lifting assembly coordinating with described quantitative liquor charging assembly on body 1.
Described quantitative liquor charging assembly includes the flexible liquid storage container 3 being arranged in described housing 1 and is arranged on described shell The some liquid collecting containers 4 connecting on body 1 outer wall and with described flexible liquid storage container 3, described flexible liquid storage container 3 is positioned at described note Immediately below liquid pipeline 2, bottom described liquid collecting container 4, offer liquid outlet 41.
Described lifting assembly include the connection post being slidably connected on described housing 1 inwall the 5th, be arranged on described connection post 5 Connecting rod on end face the 51st, be arranged on the black box 52 of described connecting rod 51 end and control described connection post 5 rise or The some magnet combination declining, the combination of described magnet includes being slidably connected on described housing 1 inwall and is connected post 5 phase with described The 531st, slide block even is fixedly installed on the magnet 532 on described slide block 531 bottom surface and is fixedly installed on described housing 1 inwall Electromagnet 533, when described electromagnet 533 is energized, described electromagnet 533 repels each other with described magnet 532, described connecting rod 51 On be provided with the jacking block 511 coordinating with described flexible liquid storage container 3, described connecting rod 51 offers cell body 512, described sealing Assembly 52 is arranged on described cell body 512 inwall.
Described black box 52 includes a tooth bar the 521st, gear 522 and the sealing-plug being engaged successively from outside toward inner side Assembly, a described tooth bar 521 is slidably connected on described cell body 512 inwall, and described tooth bar 521 lower end is arranged There is contiguous block 5211, between described contiguous block 5211 and described connecting rod 51 bottom surface, be provided with a spring 5212, described gear 522 are rotatably connected on described cell body 512 inwall.
Described sealing-plug assembly includes No. two tooth bars 523 being slidably connected on described cell body 512 inwall and is arranged on The sealing-plug 524 at described No. two tooth bar 523 tops, described sealing-plug 524 and described liquid outlet 41 interference fit, simultaneously described It is provided with the push rod component 6 coordinating with a described tooth bar 521 on liquid collecting container 4 outer wall.
Described push rod component 6 include the fixed block being fixedly installed on described liquid collecting container 4 outer wall the 61st, be opened in described solid The 62nd, the push rod determine the through hole on block 61, being plugged in described through hole is opened in some grooves 63 on described push rod 62 and turns Being automatically connected in described fixed block 61 bottom surface and the clamping block 64 coordinating with described groove 63, described push rod 62 upper end end is provided with Connect and be provided with No. two springs 66 between piece 65, and described connection piece 65 and described fixed block 61 end face, described clamping block 64 with Be provided with torsion spring at the link position of described fixed block 61 bottom surface, when described jacking block 511 with described connection post 5 rising and with Bottom described flexible liquid storage container 3 during contact, described sealing-plug 524 seals up described liquid outlet 41, and described connection post 5 is internal to be opened If cavity forms cavity body 54, being provided with motor 55 in described cavity body 54, described motor 55 described is connected post 5 with being arranged on The stirring vane 56 of underface is connected.
Described sealing-plug 524 top is provided with circular arc projection 5241.Owing to liquid outlet liquid out can directly be flushed to Sealing-plug top, therefore arranges circular arc projection and ensure that sealing-plug top not residual liquid, it is ensured that actual ratio and ideal The uniformity of ratio, improving product qualification rate.
Described housing 1 top is provided with some support bars 7.By arranging support bar, whole device is fixed on reactor In.
It is coated with waterproof coating on described black box 52 outer surface.Liquid is avoided to remain on black box outer surface, Affect overall ratio.
Using the reactor described above method of quantitative liquid feeding device, its step is as follows: 1., by liquid injecting pipeline toward soft Property liquid storage container in inject need add liquid;2., start electromagnet and motor, connect post and repelled each other with magnet by electromagnet Rising after power effect, stirring vane is persistently mixed motion by motor control;3., with connecting the rising of post, sealing-plug assembly Rising therewith, after a tooth bar is blocked by push rod, a tooth bar moves relative to connecting post, promotes gear to rotate, meanwhile, No. two tooth bars of gear driven up move, and sealing-plug rises therewith;4., bottom the jacking block in connecting rod with flexible liquid storage container During contact, sealing-plug seals up liquid outlet;5., jacking block continues the liquid level rising of the liquid in rising promotes flexible liquid storage container, The liquid exceeding the position with flexible liquid storage container connector for the liquid collecting container is flowed in liquid collecting container, now electromagnet and magnetic The mutual expelling force of iron makes to connect post held stationary state;6. after, electromagnet is energized 30 seconds, close electromagnet power supply, connect under post Move;7., connecting in post folding process, first, in liquid collecting container, redundance liquid is back in flexible liquid storage container, and liquid collecting is held In device, liquid level keeps level consistent with above-mentioned connector bottom surface, reaches quantitative;Secondly, sealing-plug leaves liquid outlet, liquid collecting container Interior liquid is flowed in reactor from liquid outlet, mixes with other liquid;8. after, electromagnet stops energising 2 minutes, again right Electromagnet is energized, and so circulates.
Arrange sealing-plug assembly to be because joining the amount in flexible liquid storage container with the fit system cause of push rod component The different positions that can change bottom flexible liquid storage container.
The principle of this fit system is the position by adjusting push rod, changes the position of sealing-plug, thus according to reality Join the amount of liquid in flexible liquid storage container to control the position of sealing-plug, it is ensured that connecting at the bottom of post and flexible liquid storage container When portion's contact, it can be ensured that sealing-plug seals up liquid outlet, it is to avoid liquid outlet leakage causes excessive fluid injection.
The fundamental prerequisite of this fit system is that the position of push rod is adjustable.

Claims (6)

1. the quantitative liquid feeding device of reactor, it is characterised in that: include that inside offers the housing (1) of cavity, described housing (1) Top is connected with liquid injecting pipeline (2), described housing (1) is provided with quantitative liquor charging assembly and joins with described quantitative liquor charging assembly The lifting assembly closing, described quantitative liquor charging assembly includes flexible liquid storage container (3) and the setting being arranged in described housing (1) The some liquid collecting containers (4) connecting on described housing (1) outer wall and with described flexible liquid storage container (3), described flexible liquid storage Container (3) is positioned at immediately below described liquid injecting pipeline (2), and described liquid collecting container (4) bottom offers liquid outlet (41), described lifting Assembly includes the connection post (5) being slidably connected on described housing (1) inwall, the company being arranged on described connection post (5) end face Extension bar (51), be arranged on the black box (52) of described connecting rod (51) end and control described connection post (5) rise or under Some magnet combination of fall, the combination of described magnet includes being slidably connected on described housing (1) inwall and is connected post (5) with described Be connected slide block (531), the magnet (532) being fixedly installed on described slide block (531) bottom surface and be fixedly installed on described shell Electromagnet (533) on body (1) inwall, when described electromagnet (533) is energized, described electromagnet (533) and described magnet (532) repel each other, described connecting rod (51) is provided with the jacking block (511) coordinating with described flexible liquid storage container (3), described connection Offering cell body (512) on bar (51), described black box (52) is arranged on described cell body (512) inwall, described sealing group Part (52) includes a tooth bar (521), gear (522) and the sealing-plug assembly being engaged successively from outside toward inner side, described one Number tooth bar (521) is slidably connected on described cell body (512) inwall, and described tooth bar (521) lower end is provided with even Connect block (5211), between described contiguous block (5211) and described connecting rod (51) bottom surface, be provided with a spring (5212), described Gear (522) is rotatably connected on described cell body (512) inwall, and described sealing-plug assembly includes being slidably connected at described cell body (512) No. two tooth bars (523) on inwall and the sealing-plug (524) being arranged on described No. two tooth bar (523) tops, exists simultaneously It is provided with the push rod component (6) coordinating with a described tooth bar (521), described push rod component on described liquid collecting container (4) outer wall (6) include the fixed block (61) being fixedly installed on described liquid collecting container (4) outer wall, be opened on described fixed block (61) logical Hole, the push rod (62) being plugged in described through hole, the some grooves (63) being opened on described push rod (62) and rotation connect At described fixed block (61) bottom surface and the clamping block (64) coordinating with described groove (63), described push rod (62) upper end end is arranged Have and be provided with No. two springs (66) between connection piece (65), and described connection piece (65) and described fixed block (61) end face, described It is provided with torsion spring, when described jacking block (511) is with described at the link position of clamping block (64) and described fixed block (61) bottom surface When connecting the rising of post (5) and contact with described flexible liquid storage container (3) bottom, described sealing-plug (524) seal up described in go out Liquid mouth (41), the internal cavity of offering of described connection post (5) forms cavity body (54), is provided with motor in described cavity body (54) (55), described motor (55) is connected with being arranged on the described stirring vane (56) being connected immediately below post (5).
2. the quantitative liquid feeding device of reactor according to claim 1, it is characterised in that: described sealing-plug (524) and institute State liquid outlet (41) interference fit.
3. the quantitative liquid feeding device of reactor according to claim 1, it is characterised in that: described sealing-plug (524) top It is provided with circular arc projection (5241).
4. the quantitative liquid feeding device of reactor according to claim 1, it is characterised in that: described housing (1) top is arranged Have some support bars (7).
5. the quantitative liquid feeding device of reactor according to claim 1, it is characterised in that: described black box (52) appearance It is coated with waterproof coating on face.
6. using the reactor method of quantitative liquid feeding device as claimed in claim 1, its step is as follows: 1., pass through fluid injection Pipeline (2) injects, in flexible liquid storage container (3), the liquid needing to add;2., electromagnet (533) and motor (55) are started, even Connecing post (5) to be risen by after the mutual expelling force effect of electromagnet (533) and magnet (532), stirring vane (56) is controlled by motor (55) Persistently mix motion;3., with connecting the rising of post (5), sealing-plug assembly rises therewith, when a tooth bar (521) is pushed up After bar (62) blocks, a tooth bar (521) is mobile relative to connecting post (5), promotes gear (522) to rotate, meanwhile, and gear (522) driving No. two tooth bars (523) up to move, sealing-plug (524) rises therewith;4., when the jacking block in connecting rod (51) (511), when contacting with flexible liquid storage container (3) bottom, sealing-plug (524) seals up liquid outlet (41);5., jacking block (511) continues The liquid level rising the liquid promoting in flexible liquid storage container (3) rises, and exceedes liquid collecting container (4) with flexible liquid storage container (3) even The liquid of the position of interface is flowed in liquid collecting container (4), and now electromagnet (533) and the mutual expelling force of magnet (532) make Connect post (5) held stationary state;6. after, electromagnet (533) is energized 30 seconds, close electromagnet (533) power supply, connect post (5) Move down;7., connecting in post (5) folding process, first, the interior redundance liquid of liquid collecting container (4) is back to flexible liquid storage container (3), in, the interior liquid level of liquid collecting container (4) keeps level consistent with above-mentioned connector bottom surface, reaches quantitative;Secondly, sealing-plug (524) Leaving liquid outlet (41), the liquid in liquid collecting container (4) is flowed in reactor from liquid outlet (41), mixes with other liquid; 8., after, electromagnet (533) stops energising 2 minutes, again electromagnet (533) is energized, so circulates.
CN201610690069.0A 2016-08-19 2016-08-19 Reaction kettle quantitative liquid feeding device and its application method Active CN106140028B (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107537416A (en) * 2017-10-09 2018-01-05 岑森参 A kind of chemical reagent device
CN110559946A (en) * 2019-09-05 2019-12-13 宁波润爵科技有限公司 Feeding device for mixing two liquids in batches
CN112191216A (en) * 2020-09-16 2021-01-08 湖州卓瑞化工科技有限公司 A processingequipment for preparing paratoluensulfonyl chloride
WO2023044215A1 (en) * 2021-09-14 2023-03-23 Exxonmobil Chemical Patents Inc. Catalyst feeder and processes thereof

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH06190264A (en) * 1992-12-24 1994-07-12 Shimadzu Corp Simultaneous chemical reaction apparatus for multiple grades
CN203635187U (en) * 2013-10-16 2014-06-11 抚顺市禄通化工有限公司 High-efficiency reaction kettle

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH06190264A (en) * 1992-12-24 1994-07-12 Shimadzu Corp Simultaneous chemical reaction apparatus for multiple grades
CN203635187U (en) * 2013-10-16 2014-06-11 抚顺市禄通化工有限公司 High-efficiency reaction kettle

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107537416A (en) * 2017-10-09 2018-01-05 岑森参 A kind of chemical reagent device
CN110559946A (en) * 2019-09-05 2019-12-13 宁波润爵科技有限公司 Feeding device for mixing two liquids in batches
CN112191216A (en) * 2020-09-16 2021-01-08 湖州卓瑞化工科技有限公司 A processingequipment for preparing paratoluensulfonyl chloride
CN112191216B (en) * 2020-09-16 2022-04-01 湖州卓瑞化工科技有限公司 A processingequipment for preparing paratoluensulfonyl chloride
WO2023044215A1 (en) * 2021-09-14 2023-03-23 Exxonmobil Chemical Patents Inc. Catalyst feeder and processes thereof

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