CN106118493B - Button conditioning liquid and preparation method thereof - Google Patents
Button conditioning liquid and preparation method thereof Download PDFInfo
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- CN106118493B CN106118493B CN201610438525.2A CN201610438525A CN106118493B CN 106118493 B CN106118493 B CN 106118493B CN 201610438525 A CN201610438525 A CN 201610438525A CN 106118493 B CN106118493 B CN 106118493B
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09G—POLISHING COMPOSITIONS; SKI WAXES
- C09G1/00—Polishing compositions
- C09G1/04—Aqueous dispersions
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Abstract
The present invention relates to a kind of button conditioning liquid and preparation method thereof.It solves the problems such as prior art design is unreasonable.This button conditioning liquid includes the component of following portions by weight：Camellia oil 3% 5%, emulsifying agent 0.1% 0.15%, sorbitan fatty ester 0.2% 0.4%, polyoxyethylene sorbitan monooleate 0.05% 0.1%, stearic acid 0.04% 0.05%, anhydrosorbitol acid anhydride trioleate 0.05% 0.1%, anhydrous sorbitol laurate 0.1% 0.2%, polyoxyethylene sorbitan laurate 0.1% 0.2%, emulsifying liquid paraffin 30% 40%, antistatic additive 0.4% 0.6%, brightener 0.3% 0.5%, preservative 0.001% 0.002%, surplus is pure water.The advantage of the invention is that：Cost is low, can avoid blushing and more practical.
Description
Technical field
The invention belongs to conditioning liquid technical field, more particularly to a kind of button conditioning liquid and preparation method thereof.
Background technology
Because technical problem, resin button polishing dead angle have blushing in button production process.With traditional method
Oil and have greater environmental impacts.
For example, Chinese patent literature discloses a kind of embroidery article antibacterial and mouldproof conditioning liquid and preparation method thereof [application
Number：201210518993.2], for the mould proof processing before the embroider line in anglicanum manufacturing process, embroidered square and storage.The present invention
The shortcomings that overcoming prior art has：It is colourless, tasteless, to silk non-corrosiveness, to no skin irritation, anti-microbial property is notable,
With rear no decolouring phenomenon, the generation of bacterium mildew can be effectively prevented, easy to use, the advantages that technique is simple.The technology of the present invention
Scheme is as follows：The formula of selection is following (percentage by weight %)：Carboxymethyl chitosan 2.0-4.0；Algal polysaccharides 2.0-3.0；Sea
The biological lysozyme 6.0-8.0 in ocean；Pure water is to 100.Preparation method：It is first according to disclosed in Chinese patent CN200410097081
Cultural method, culture marine organisms lysozyme are standby.Carry out again emulsification whipping process (1, by be formulated needed for pure water add breast
Change in tank, be heated to 40 DEG C.2nd, stirred 45 minutes in filling carboxymethyl chitosan, algal polysaccharides, addition by formula rate.3rd, drop
During to 30 DEG C, add marine organisms lysozyme and stir 15 minutes.4th, dispensed after cooling down).
Above-mentioned scheme has many advantages, such as the above, and still, the program does not solve above-mentioned technical problem thoroughly, still
Blushing being present, the brightness of button is relatively low, and oxidation resistance is poor, secondly, also there is that greasy dirt is greasy and pollution problem,
Poor practicability.
The content of the invention
Regarding the issue above, the present invention provides a kind of cost is low, blushing and more practical can be avoided
Button conditioning liquid.
Another object of the present invention is in view of the above-mentioned problems, to provide a kind of technique simple, can avoid blushing
Button conditioning liquid preparation method.
To reach above-mentioned purpose, present invention employs following technical proposal：This button conditioning liquid includes following portions by weight
Component：Camellia oil 3%-5%, emulsifying agent 0.1%-0.15%, sorbitan fatty ester 0.2%-0.4%, polyoxy
Ethene Arlacel-80 0.05%-0.1%, stearic acid 0.04%-0.05%, anhydrosorbitol acid anhydride trioleate
0.05%-0.1%, anhydrous sorbitol laurate 0.1%-0.2%, polyoxyethylene sorbitan laurate 0.1%-
0.2%, emulsifying liquid paraffin 30%-40%, antistatic additive 0.4%-0.6%, brightener 0.3%-0.5%, preservative
0.001%-0.002%, surplus are pure water.
Emulsifying agent：Camellia oil is emulsified, is dispersed in pure water.
Sorbitan fatty ester：Camellia oil is emulsified, is dispersed in pure water.
Polyoxyethylene sorbitan monooleate：Mentioned emulsifier is aided in, to reach optimal emulsifying effectiveness.
Anhydrosorbitol acid anhydride trioleate：Mentioned emulsifier is aided in, to reach optimal emulsifying effectiveness.
Anhydrous sorbitol laurate：Mentioned emulsifier is aided in, to reach optimal emulsifying effectiveness.
In above-mentioned button conditioning liquid, described emulsifying liquid paraffin includes the component of following portions by weight：Liquid stone
Wax 8%-11%, sorbitan fatty ester 1%-1.5%, polyoxyethylene sorbitan monooleate 1%-1.5%,
Stearic acid 0.05%-0.08%, surplus are pure water.
In above-mentioned button conditioning liquid, described emulsifying agent is ZR-5 emulsifying agents.
The preparation method of this button conditioning liquid comprises the following steps：
A, emulsifying liquid paraffin is prepared, the emulsifying liquid paraffin includes the component of following portions by weight：Atoleine 8%-
11%, sorbitan fatty ester 1%-1.5%, polyoxyethylene sorbitan monooleate 1%-1.5%, stearic acid
0.05%-0.08%, surplus are pure water；
B, conditioning liquid is prepared, the conditioning liquid includes the component of following portions by weight：Camellia oil 3%-5%, emulsifying agent
0.1%-0.15%, sorbitan fatty ester 0.2%-0.4%, polyoxyethylene sorbitan monooleate
0.05%-0.1%, stearic acid 0.04%-0.05%, anhydrosorbitol acid anhydride trioleate 0.05%-0.1%, Sorbitan
Alcohol laurate 0.1%-0.2%, polyoxyethylene sorbitan laurate 0.1%-0.2%, emulsion made of step A
Body paraffin 30%-40%, antistatic additive 0.4%-0.6%, brightener 0.3%-0.5%, preservative 0.001%-0.002%,
Surplus is pure water；
C, it is filling, the conditioning liquid in step B is fitted into holding vessel and is packaged.
In above-mentioned button conditioning liquid, in above-mentioned step A, the emulsifying liquid paraffin processes shape by following steps
Into：
A1, the atoleine 3%-5% aforementioned proportion, sorbitan fatty ester 1%-1.5%, polyoxyethylene
Arlacel-80 1%-1.5%, stearic acid 0.05%-0.08% are added sequentially in mulser；
A2, mulser increase to 800-1000rpm in 1min, and stirring 5-10min fills the material in above-mentioned a1 steps
Divide well mixed；
A3, increase mulser rotating speed to 5000-6000rpm in 2min, and the at the same time slow breast into a2 steps
Pure water is added dropwise in change machine；
A4, when the emulsion retrogradation in a3 steps turns into paste, improve the rate of addition of pure water, and make mulser rotating speed
To 8000-10000rpm；
A5, mulser persistently emulsify 15-20min with 8000-10000rpm speed, complete standby after emulsifying；That is, it is made
Emulsifying liquid paraffin.
In the preparation method of above-mentioned button conditioning liquid, in above-mentioned step B, the emulsifying liquid paraffin is by following
Step processes to be formed：
B1, camellia oil 3-5%, ZR-5 the emulsifying agent 0.1%-0.15% aforementioned proportion, sorbitan fatty acid
Ester 0.2%-0.4%, polyoxyethylene sorbitan monooleate 0.05%-0.1%, stearic acid 0.04%-0.05%, dehydration
Sorbitan trioleate 0.05%-0.1%, anhydrous sorbitol laurate 0.1%-0.2%, polyoxyethylene sorbitan
Alcohol laurate 0.1%-0.2%, is added sequentially in mulser；
B2, mulser are slowly increased to 800-1000rpm, and stirring 5-10min makes the material in the above-mentioned steps of b 1 fully mixed
Close uniform；
B3, mulser rotating speed is slowly improved to 5000-6000rpm, and the at the same time slow mulser into b2 steps
Emulsifying liquid paraffin made of interior dropwise addition step A；
B4, when the emulsion retrogradation in b3 steps turns into paste, improve the speed that emulsifying liquid paraffin is added dropwise, and quickly
Increase mulser rotating speed to continue to emulsify 5-10 minutes with 8000-10000rpm speed to 8000-10000rpm, mulser,
Need remaining emulsifying liquid paraffin will all to be added into mulser during this；
B5, when the emulsion in b4 steps is in emulsification, pure water and mulser is persistently added dropwise and continues with 10000-
11000rpm speed emulsification 10-15min；
B6, above-mentioned antistatic additive 0.4%-0.6% and brightener 0.3%-0.5% be added sequentially in mulser,
And with 8000-10000rpm speed 3-5min, i.e. conditioning liquid is made.
Compared with prior art, it is the advantages of this button conditioning liquid and preparation method thereof：
1st, it is more reasonable to design, avoid button whiten edge the problem of, increase button brightness and oxidation resistance.
2nd, cost is cheap, easy to use, and evaporation rate is fast.
3rd, water prescription, solve in traditional handicraft greasy dirt is greasy and pollution problem.
4th, it is adapted to matt, frosted and the light type button of various unsaturated-resin materials and plastic material.
2nd, technique is simple and is easily manipulated.
Embodiment
It is the specific embodiment of invention below, technical scheme is further described, but the present invention is not
It is limited to these embodiments.
This button conditioning liquid includes the component of following portions by weight：Camellia oil 3%-5%, emulsifying agent 0.1%-0.15%,
Sorbitan fatty ester 0.2%-0.4%, polyoxyethylene sorbitan monooleate 0.05%-0.1%, stearic acid
0.04%-0.05%, anhydrosorbitol acid anhydride trioleate 0.05%-0.1%, anhydrous sorbitol laurate 0.1%-
0.2%, polyoxyethylene sorbitan laurate 0.1%-0.2%, emulsifying liquid paraffin 30%-40%, antistatic additive
0.4%-0.6%, brightener 0.3%-0.5%, preservative 0.001%-0.002%, surplus are pure water.Here emulsifying agent is
ZR-5 emulsifying agents.
Secondly, emulsifying liquid paraffin includes the component of following portions by weight：Atoleine 8%-11%, anhydrosorbitol
Fatty acid ester 1%-1.5%, polyoxyethylene sorbitan monooleate 1%-1.5%, stearic acid 0.05%-0.08% are remaining
Measure as pure water.
Embodiment one
Button conditioning liquid includes the component of following portions by weight：Camellia oil 4%, emulsifying agent 0.125%, anhydrosorbitol
Fatty acid ester 0.3%, polyoxyethylene sorbitan monooleate 0.075%, stearic acid 0.045%, anhydrosorbitol acid anhydride
Trioleate 0.075%, anhydrous sorbitol laurate 0.15%, polyoxyethylene sorbitan laurate 0.15%, breast
Change atoleine 35%, antistatic additive 0.5%, brightener 0.4%, preservative 0.0015%, surplus is pure water.
Emulsifying liquid paraffin includes the component of following portions by weight：Atoleine 9.5%, sorbitan fatty ester
1.25%, polyoxyethylene sorbitan monooleate 1.25%, stearic acid 0.065%, surplus is pure water.
Embodiment two
Button conditioning liquid includes the component of following portions by weight：Camellia oil 3%, emulsifying agent 0.1%, Sorbitan alcohol ester
Fat acid esters 0.2%, polyoxyethylene sorbitan monooleate 0.05%, stearic acid 0.04%, the oil of anhydrosorbitol acid anhydride three
Acid esters 0.05%, anhydrous sorbitol laurate 0.1%, polyoxyethylene sorbitan laurate 0.1%, emulsifying liquid stone
Wax 30%, antistatic additive 0.4%, brightener 0.3%, preservative 0.001%, surplus are pure water.
Emulsifying liquid paraffin includes the component of following portions by weight：Atoleine 8%, sorbitan fatty ester
1%, polyoxyethylene sorbitan monooleate 1%, stearic acid 0.05%, surplus is pure water.
Embodiment three
Button conditioning liquid includes the component of following portions by weight：Camellia oil 5%, emulsifying agent 0.15%, anhydrosorbitol
Fatty acid ester 0.4%, polyoxyethylene sorbitan monooleate 0.1%, stearic acid 0.05%, the oil of anhydrosorbitol acid anhydride three
Acid esters 0.1%, anhydrous sorbitol laurate 0.2%, polyoxyethylene sorbitan laurate 0.2%, emulsifying liquid stone
Wax 340%, antistatic additive 0.6%, brightener 0.5%, preservative 0.002%, surplus are pure water.
Secondly, emulsifying liquid paraffin includes the component of following portions by weight：Atoleine 11%, sorbitan fatty
Acid esters 1.5%, polyoxyethylene sorbitan monooleate 1.5%, stearic acid 0.08%, surplus are pure water.
The preparation method of this button conditioning liquid comprises the following steps：
A, emulsifying liquid paraffin is prepared, the emulsifying liquid paraffin includes the component of following portions by weight：Atoleine 8%-
11%, sorbitan fatty ester 1%-1.5%, polyoxyethylene sorbitan monooleate 1%-1.5%, stearic acid
0.05%-0.08%, surplus are pure water；
B, conditioning liquid is prepared, the conditioning liquid includes the component of following portions by weight：Camellia oil 3%-5%, emulsifying agent
0.1%-0.15%, sorbitan fatty ester 0.2%-0.4%, polyoxyethylene sorbitan monooleate
0.05%-0.1%, stearic acid 0.04%-0.05%, anhydrosorbitol acid anhydride trioleate 0.05%-0.1%, Sorbitan
Alcohol laurate 0.1%-0.2%, polyoxyethylene sorbitan laurate 0.1%-0.2%, emulsion made of step A
Body paraffin 30%-40%, antistatic additive 0.4%-0.6%, brightener 0.3%-0.5%, preservative 0.001%-0.002%,
Surplus is pure water；
C, it is filling, the conditioning liquid in step B is fitted into holding vessel and is packaged.
In above-mentioned step A, the emulsifying liquid paraffin is processed by following steps to be formed：
A1, the atoleine 3%-5% aforementioned proportion, sorbitan fatty ester 1%-1.5%, polyoxyethylene
Arlacel-80 1%-1.5%, stearic acid 0.05%-0.08% are added sequentially in mulser；
A2, mulser increase to 800-1000rpm in 1min, and stirring 5-10min fills the material in above-mentioned a1 steps
Divide well mixed；
A3, increase mulser rotating speed to 5000-6000rpm in 2min, and the at the same time slow breast into a2 steps
Pure water is added dropwise in change machine；
A4, when the emulsion retrogradation in a3 steps turns into paste, improve the rate of addition of pure water, and make mulser rotating speed
To 8000-10000rpm；
A5, mulser persistently emulsify 15-20min with 8000-10000rpm speed, complete standby after emulsifying；That is, it is made
Emulsifying liquid paraffin.
In above-mentioned step B, the emulsifying liquid paraffin is processed by following steps to be formed：
B1, camellia oil 3-5%, ZR-5 the emulsifying agent 0.1%-0.15% aforementioned proportion, sorbitan fatty acid
Ester 0.2%-0.4%, polyoxyethylene sorbitan monooleate 0.05%-0.1%, stearic acid 0.04%-0.05%, dehydration
Sorbitan trioleate 0.05%-0.1%, anhydrous sorbitol laurate 0.1%-0.2%, polyoxyethylene sorbitan
Alcohol laurate 0.1%-0.2%, is added sequentially in mulser；
B2, mulser are slowly increased to 800-1000rpm, and stirring 5-10min makes the material in above-mentioned b1 steps fully mixed
Close uniform；
B3, mulser rotating speed is slowly improved to 5000-6000rpm, and the at the same time slow mulser into b2 steps
Emulsifying liquid paraffin made of interior dropwise addition step A；
B4, when the emulsion retrogradation in b3 steps turns into paste, improve the speed that emulsifying liquid paraffin is added dropwise, and quickly
Increase mulser rotating speed to continue to emulsify 5-10 minutes with 8000-10000rpm speed to 8000-10000rpm, mulser,
Need remaining emulsifying liquid paraffin will all to be added into mulser during this；
B5, when the emulsion in b4 steps is in emulsification, pure water and mulser is persistently added dropwise and continues with 10000-
11000rpm speed emulsification 10-15min；
B6, above-mentioned antistatic additive 0.4%-0.6% and brightener 0.3%-0.5% be added sequentially in mulser,
And with 8000-10000rpm speed 3-5min, i.e. conditioning liquid is made.
It is the result of the test of the various component difference numbers of emulsifying liquid paraffin below：
It is the result of the test of the various component difference numbers of button conditioning liquid below：
Specific embodiment described herein is only to spirit explanation for example of the invention.Technology belonging to the present invention is led
The technical staff in domain can be made various modifications or supplement to described specific embodiment or be replaced using similar mode
Generation, but without departing from the spiritual of the present invention or surmount scope defined in appended claims.
Claims (4)
1. a kind of button conditioning liquid, it is characterised in that this conditioning liquid includes the component of following portions by weight：Camellia oil 3%-5%,
Emulsifying agent 0.1%-0.15%, sorbitan fatty ester 0.2%-0.4%, polyoxyethylene sorbitan monooleate
0.05%-0.1%, stearic acid 0.04%-0.05%, anhydrosorbitol acid anhydride trioleate 0.05%-0.1%, Sorbitan
Alcohol laurate 0.1%-0.2%, polyoxyethylene sorbitan laurate 0.1%-0.2%, emulsifying liquid paraffin 30%-
40%, antistatic additive 0.4%-0.6%, brightener 0.3%-0.5%, preservative 0.001%-0.002%, surplus are pure water；
Described emulsifying liquid paraffin includes the component of following portions by weight：Atoleine 8%-11%, Sorbitan alcohol ester
Fat acid esters 1%-1.5%, polyoxyethylene sorbitan monooleate 1%-1.5%, stearic acid 0.05%-0.08%, surplus
For pure water.
2. button conditioning liquid according to claim 1, it is characterised in that described emulsifying agent is ZR-5 emulsifying agents.
3. a kind of preparation method of button conditioning liquid, it is characterised in that this method comprises the following steps：
A, emulsifying liquid paraffin is prepared, the emulsifying liquid paraffin includes the component of following portions by weight：Atoleine 8%-11%,
Sorbitan fatty ester 1%-1.5%, polyoxyethylene sorbitan monooleate 1%-1.5%, stearic acid
0.05%-0.08%, surplus are pure water；
B, conditioning liquid is prepared, the conditioning liquid includes the component of following portions by weight：Camellia oil 3%-5%, emulsifying agent 0.1%-
0.15%, sorbitan fatty ester 0.2%-0.4%, polyoxyethylene sorbitan monooleate 0.05%-
0.1%, stearic acid 0.04%-0.05%, anhydrosorbitol acid anhydride trioleate 0.05%-0.1%, anhydrous sorbitol laurate
Ester 0.1%-0.2%, polyoxyethylene sorbitan laurate 0.1%-0.2%, emulsifying liquid paraffin made of step A
30%-40%, antistatic additive 0.4%-0.6%, brightener 0.3%-0.5%, preservative 0.001%-0.002%, surplus are
Pure water；
C, it is filling, the conditioning liquid in step B is fitted into holding vessel and is packaged；
In above-mentioned step A, the emulsifying liquid paraffin is processed by following steps to be formed：
A1, the atoleine 3%-5% aforementioned proportion, sorbitan fatty ester 1%-1.5%, polyoxyethylene
Sorbitol monooleate 1%-1.5%, stearic acid 0.05%-0.08% are added sequentially in mulser；
A2, mulser increase to 800-1000rpm in 1min, and stirring 5-10min makes the material in above-mentioned a1 steps fully mixed
Close uniform；
A3, increase mulser rotating speed to 5000-6000rpm in 2min, and the at the same time slow mulser into a2 steps
Interior dropwise addition pure water；
A4, when the emulsion retrogradation in a3 steps turns into paste, improve the rate of addition of pure water, and arrive mulser rotating speed
8000-10000rpm；
A5, mulser persistently emulsify 15-20min with 8000-10000rpm speed, complete standby after emulsifying；That is, emulsification is made
Atoleine.
4. the preparation method of button conditioning liquid according to claim 3, it is characterised in that described in above-mentioned step B
Conditioning liquid is processed by following steps and formed：
B1, camellia oil 3-5%, ZR-5 the emulsifying agent 0.1%-0.15% aforementioned proportion, sorbitan fatty ester
0.2%-0.4%, polyoxyethylene sorbitan monooleate 0.05%-0.1%, stearic acid 0.04%-0.05%, dehydration mountain
Pears sugar alcohol acid anhydride trioleate 0.05%-0.1%, anhydrous sorbitol laurate 0.1%-0.2%, polyoxyethylene sorbitan
Laurate 0.1%-0.2%, is added sequentially in mulser；
B2, mulser are slowly increased to 800-1000rpm, and stirring 5-10min makes the material in above-mentioned b1 steps be sufficiently mixed
It is even；
B3, mulser rotating speed is slowly improved to 5000-6000rpm, and at the same time slowly dripped in the mulser into b2 steps
Add emulsifying liquid paraffin made of step A；
B4, when the emulsion retrogradation in b3 steps turns into paste, improve the speed that emulsifying liquid paraffin is added dropwise, and quickly increase
Mulser rotating speed is to 8000-10000rpm, and mulser continues to emulsify 5-10 minutes with 8000-10000rpm speed, in this phase
Between need will remaining emulsifying liquid paraffin all add into mulser；
B5, when the emulsion in b4 steps is in emulsification, pure water and mulser is persistently added dropwise and continues with 10000-11000rpm's
Speed emulsifies 10-15min；
B6, above-mentioned antistatic additive 0.4%-0.6% and brightener 0.3%-0.5% be added sequentially in mulser, and with
8000-10000rpm speed 3-5min, i.e. conditioning liquid is made.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610438525.2A CN106118493B (en) | 2016-06-19 | 2016-06-19 | Button conditioning liquid and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610438525.2A CN106118493B (en) | 2016-06-19 | 2016-06-19 | Button conditioning liquid and preparation method thereof |
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| Publication Number | Publication Date |
|---|---|
| CN106118493A CN106118493A (en) | 2016-11-16 |
| CN106118493B true CN106118493B (en) | 2018-01-05 |
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ID=57470901
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|---|---|---|---|
| CN201610438525.2A Active CN106118493B (en) | 2016-06-19 | 2016-06-19 | Button conditioning liquid and preparation method thereof |
Country Status (1)
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101177005A (en) * | 2007-12-10 | 2008-05-14 | 杨旭东 | Curing agent for lithoid and xylary objects |
| CN101406429A (en) * | 2008-11-25 | 2009-04-15 | 上海应用技术学院 | Oil-in-water emulsion and preparation method thereof |
| CN102174292A (en) * | 2011-03-15 | 2011-09-07 | 西北大学 | Resin paint surface nursing emulsion and preparation method thereof |
| CN103695578A (en) * | 2013-12-30 | 2014-04-02 | 青昊环保科技（上海）有限公司 | Leather water-proof curing agent and preparing method thereof |
-
2016
- 2016-06-19 CN CN201610438525.2A patent/CN106118493B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101177005A (en) * | 2007-12-10 | 2008-05-14 | 杨旭东 | Curing agent for lithoid and xylary objects |
| CN101406429A (en) * | 2008-11-25 | 2009-04-15 | 上海应用技术学院 | Oil-in-water emulsion and preparation method thereof |
| CN102174292A (en) * | 2011-03-15 | 2011-09-07 | 西北大学 | Resin paint surface nursing emulsion and preparation method thereof |
| CN103695578A (en) * | 2013-12-30 | 2014-04-02 | 青昊环保科技（上海）有限公司 | Leather water-proof curing agent and preparing method thereof |
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| Publication number | Publication date |
|---|---|
| CN106118493A (en) | 2016-11-16 |
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