CN106116408A - A kind of antioxidation construction material and preparation method thereof - Google Patents

A kind of antioxidation construction material and preparation method thereof Download PDF

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Publication number
CN106116408A
CN106116408A CN201610456620.5A CN201610456620A CN106116408A CN 106116408 A CN106116408 A CN 106116408A CN 201610456620 A CN201610456620 A CN 201610456620A CN 106116408 A CN106116408 A CN 106116408A
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China
Prior art keywords
powder
mixing
antioxidation
weight
gypsum fibrosum
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CN201610456620.5A
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Chinese (zh)
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不公告发明人
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Hefei Qiteng Agricultural Science And Technology Co Ltd
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Hefei Qiteng Agricultural Science And Technology Co Ltd
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Priority to CN201610456620.5A priority Critical patent/CN106116408A/en
Publication of CN106116408A publication Critical patent/CN106116408A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B28/00Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
    • C04B28/14Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing calcium sulfate cements

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Organic Chemistry (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)

Abstract

The invention discloses a kind of antioxidation construction material and preparation method thereof, by weight, its constitutive material is, polyvinyl resin 80 110, Gypsum Fibrosum powder 45 55, artificial zeolite's powder 30 40, calcium stearate 10 15, Radix Gentianae grass meal 56, punching Nelumbo nucifera Gaertn. Powder 24, hydroxyethyl cellulose 56, diphenylguanidine TDM 12, anti-aging agent RD 13, n-BMA 34, zinc stearate 46, vinyl methyl siloxane 48, sodium tripolyphosphate 24, boronation two molybdenum 34;Insulation material prepared by the present invention is with polyvinyl resin, Gypsum Fibrosum powder, artificial zeolite's powder as main material, multiple ingredients of arranging in pairs or groups is made, formula is reasonable, preparation method is simple, and the insulation material prepared is nonpoisonous and tasteless, environmental protection, there is light weight, mechanical strength is high, and high insulating effect characteristic can be widely applied to the energy-saving heat preserving field of building energy-saving heat-insulating material and other high-temperature service outer layers.

Description

A kind of antioxidation construction material and preparation method thereof
Technical field
The present invention relates to a kind of antioxidation construction material and preparation method thereof, belong to insulation material technical field.
Background technology
At present, the insulation material that China's wall thermal insulating is used remains based on organic insulation material, but, in Nanjing Ring International Square, 360 degree of Gemini mansions of Harbin longitude and latitude, the Olympic Sports Center, Jinan, attached cultural center, Beijing CCTV new address, on The architecture exterior wall insulating materials fire of the generations such as sea teacher apartment, Jiangzhou, Shenyang feudal dynasty ten thousand prosperous mansion all causes serious personnel Injures and deaths and property loss, create ill effect, therefore researchs and develops new inorganic heat insulation material imperative, a kind of source Extensively, cheap raw material has obtained paying close attention to widely.
Summary of the invention
In order to alleviate the deficiencies in the prior art, it is an object of the invention to provide a kind of antioxidation construction material and making thereof Method.
To achieve these goals, the present invention adopts the following technical scheme that
Antioxidation construction material, by weight, its constitutive material is, polyvinyl resin 80-110, Gypsum Fibrosum powder 45-55, artificial Zeolite powder 30-40, calcium stearate 10-15, Radix Gentianae grass meal 5-6, punching Nelumbo nucifera Gaertn. Powder 2-4, hydroxyethyl cellulose 5-6, diphenylguanidine TDM 1-2, anti-aging agent RD 1-3, n-BMA 3-4, zinc stearate 4-6, vinyl methyl siloxane 4-8, tripolyphosphate Sodium 2-4, boronation two molybdenum 3-4.
Antioxidation construction material, by weight, its constitutive material is, polyvinyl resin 100, Gypsum Fibrosum powder 50, manually boils Stone powder 35, calcium stearate 12, Radix Gentianae grass meal 5.5, punching Nelumbo nucifera Gaertn. Powder 3, hydroxyethyl cellulose 5.5, diphenylguanidine TDM 1.5, age resistor RD 2, n-BMA 3.5, zinc stearate 5, vinyl methyl siloxane 6, sodium tripolyphosphate 3, boronation two molybdenum 3.5.
The manufacture method of antioxidation construction material, including herein below:
(1) weigh each raw material by the weight portion of constitutive material, first Radix Gentianae grass meal, punching Nelumbo nucifera Gaertn. Powder are fully pulverized, then with methyl N-butyl acrylate, zinc stearate add in blender in the lump, and mixing and stirring is standby;
(2) weigh polyvinyl resin, Gypsum Fibrosum powder, artificial zeolite's powder by weight, add and mix on mixer, mixing 10~ 15min, mixing rotating speed is 100~200r/min, then adds and states step (1) mixture mixing 20~30min, mixes rotating speed It is 200~300r/min, is eventually adding calcium stearate, hydroxyethyl cellulose, diphenylguanidine TDM, anti-aging agent RD, vinyl methyl Other residue constitutive materials such as siloxanes, sodium tripolyphosphate, boronation two molybdenum continue mixing, mix 30~40min, mix rotating speed It is 400~500r/min, expectation must be mixed;
(3) temperature 400~600 DEG C, pressure 1~3MPa, temperature retention time 20~30min are put in above-mentioned steps (2) mixing expectation Under the conditions of compressing, obtain moulding material, place into muffle furnace calcining, calcining heat is 400~500 DEG C, temperature retention time 1~ 2h;After cooling and get final product.
Beneficial effects of the present invention:
Insulation material prepared by the present invention with polyvinyl resin, Gypsum Fibrosum powder, artificial zeolite's powder as main material, multiple ingredients system of arranging in pairs or groups Becoming, formula is reasonable, and preparation method is simple, and the insulation material prepared is nonpoisonous and tasteless, environmental protection, has light weight, machinery Intensity is high, and high insulating effect characteristic can be widely applied to the energy-conservation guarantor of building energy-saving heat-insulating material and other high-temperature service outer layers Temperature field.
Detailed description of the invention
Embodiment 1: antioxidation construction material, by weight (kg) meter, its constitutive material is, polyvinyl resin 100, Gypsum Fibrosum powder 50, artificial zeolite's powder 35, calcium stearate 12, Radix Gentianae grass meal 5.5, punching Nelumbo nucifera Gaertn. Powder 3, hydroxyethyl cellulose 5.5, diphenylguanidine TDM 1.5, anti-aging agent RD 2, n-BMA 3.5, zinc stearate 5, vinyl methyl siloxane 6, sodium tripolyphosphate 3, boron Change two molybdenums 3.5.
The manufacture method of antioxidation construction material, including herein below:
(1) weigh each raw material by the weight portion of constitutive material, first Radix Gentianae grass meal, punching Nelumbo nucifera Gaertn. Powder are fully pulverized, then with methyl N-butyl acrylate, zinc stearate add in blender in the lump, and mixing and stirring is standby;
(2) weigh polyvinyl resin, Gypsum Fibrosum powder, artificial zeolite's powder by weight, add and mix on mixer, mix 12min, Mixing rotating speed is 150r/min, then adds and states step (1) mixture mixing 25min, and mixing rotating speed is 250r/min, finally Add calcium stearate, hydroxyethyl cellulose, diphenylguanidine TDM, anti-aging agent RD, vinyl methyl siloxane, sodium tripolyphosphate, boron Changing other residue constitutive materials such as two molybdenums and continue mixing, mix 35min, mixing rotating speed is 450r/min, must mix expectation;
(3) temperature 500 DEG C, pressure 2MPa are put in above-mentioned steps (2) mixing expectation, be pressed under the conditions of temperature retention time 25min Type, obtains moulding material, places into muffle furnace calcining, and calcining heat is 450 DEG C, temperature retention time 1.5h;After cooling and get final product.

Claims (3)

1. an antioxidation construction material, it is characterised in that by weight, its constitutive material is, polyvinyl resin 80-110, Gypsum Fibrosum powder 45-55, artificial zeolite powder 30-40, calcium stearate 10-15, Radix Gentianae grass meal 5-6, punching Nelumbo nucifera Gaertn. Powder 2-4, hydroxy ethyl fiber Element 5-6, diphenylguanidine TDM 1-2, anti-aging agent RD 1-3, n-BMA 3-4, zinc stearate 4-6, vinyl methyl Siloxanes 4-8, sodium tripolyphosphate 2-4, boronation two molybdenum 3-4.
Antioxidation construction material the most according to claim 1, it is characterised in that by weight, its constitutive material is, poly- Vinyl 100, Gypsum Fibrosum powder 50, artificial zeolite's powder 35, calcium stearate 12, Radix Gentianae grass meal 5.5, punching Nelumbo nucifera Gaertn. Powder 3, hydroxy ethyl fiber Element 5.5, diphenylguanidine TDM 1.5, anti-aging agent RD 2, n-BMA 3.5, zinc stearate 5, vinyl methyl silica Alkane 6, sodium tripolyphosphate 3, boronation two molybdenum 3.5.
3. the manufacture method of an antioxidation construction material as claimed in claim 1, it is characterised in that include herein below:
(1) weigh each raw material by the weight portion of constitutive material, first Radix Gentianae grass meal, punching Nelumbo nucifera Gaertn. Powder are fully pulverized, then with methyl N-butyl acrylate, zinc stearate add in blender in the lump, and mixing and stirring is standby;
(2) weigh polyvinyl resin, Gypsum Fibrosum powder, artificial zeolite's powder by weight, add and mix on mixer, mixing 10~ 15min, mixing rotating speed is 100~200r/min, then adds and states step (1) mixture mixing 20~30min, mixes rotating speed It is 200~300r/min, is eventually adding calcium stearate, hydroxyethyl cellulose, diphenylguanidine TDM, anti-aging agent RD, vinyl methyl Other residue constitutive materials such as siloxanes, sodium tripolyphosphate, boronation two molybdenum continue mixing, mix 30~40min, mix rotating speed It is 400~500r/min, expectation must be mixed;
(3) temperature 400~600 DEG C, pressure 1~3MPa, temperature retention time 20~30min are put in above-mentioned steps (2) mixing expectation Under the conditions of compressing, obtain moulding material, place into muffle furnace calcining, calcining heat is 400~500 DEG C, temperature retention time 1~ 2h;After cooling and get final product.
CN201610456620.5A 2016-06-23 2016-06-23 A kind of antioxidation construction material and preparation method thereof Pending CN106116408A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610456620.5A CN106116408A (en) 2016-06-23 2016-06-23 A kind of antioxidation construction material and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610456620.5A CN106116408A (en) 2016-06-23 2016-06-23 A kind of antioxidation construction material and preparation method thereof

Publications (1)

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CN106116408A true CN106116408A (en) 2016-11-16

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CN (1) CN106116408A (en)

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101274836A (en) * 2008-05-21 2008-10-01 昆明理工大学 Polymer reinforced light gypsum decorative material
CN103342531A (en) * 2013-07-05 2013-10-09 李奕 Building exterior wall thermal insulation material and preparation process thereof
CN104177041A (en) * 2013-05-24 2014-12-03 青岛极致节能环保有限公司 Environmentally friendly high efficiency energy saving building material
CN104310936A (en) * 2014-10-20 2015-01-28 青岛锦绣水源商贸有限公司 Thermal insulation material of house building
CN104876525A (en) * 2015-05-14 2015-09-02 青岛百千川海洋生态科技有限公司 Lightweight building exterior-wall thermal insulation material

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101274836A (en) * 2008-05-21 2008-10-01 昆明理工大学 Polymer reinforced light gypsum decorative material
CN104177041A (en) * 2013-05-24 2014-12-03 青岛极致节能环保有限公司 Environmentally friendly high efficiency energy saving building material
CN103342531A (en) * 2013-07-05 2013-10-09 李奕 Building exterior wall thermal insulation material and preparation process thereof
CN104310936A (en) * 2014-10-20 2015-01-28 青岛锦绣水源商贸有限公司 Thermal insulation material of house building
CN104876525A (en) * 2015-05-14 2015-09-02 青岛百千川海洋生态科技有限公司 Lightweight building exterior-wall thermal insulation material

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Application publication date: 20161116