CN106106586A - 一种猕猴桃用桉树叶植物源农药 - Google Patents

一种猕猴桃用桉树叶植物源农药 Download PDF

Info

Publication number
CN106106586A
CN106106586A CN201610430321.4A CN201610430321A CN106106586A CN 106106586 A CN106106586 A CN 106106586A CN 201610430321 A CN201610430321 A CN 201610430321A CN 106106586 A CN106106586 A CN 106106586A
Authority
CN
China
Prior art keywords
solution
radix
parts
actinidiae chinensis
fructus actinidiae
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610430321.4A
Other languages
English (en)
Inventor
吴权明
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
ZONGYANG COUNTY BAIYUN ECOLOGICAL GARDEN Co Ltd
Original Assignee
ZONGYANG COUNTY BAIYUN ECOLOGICAL GARDEN Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by ZONGYANG COUNTY BAIYUN ECOLOGICAL GARDEN Co Ltd filed Critical ZONGYANG COUNTY BAIYUN ECOLOGICAL GARDEN Co Ltd
Priority to CN201610430321.4A priority Critical patent/CN106106586A/zh
Publication of CN106106586A publication Critical patent/CN106106586A/zh
Pending legal-status Critical Current

Links

Classifications

    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N31/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic oxygen or sulfur compounds
    • A01N31/04—Oxygen or sulfur attached to an aliphatic side-chain of a carbocyclic ring system
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/06—Unsaturated carboxylic acids or thio analogues thereof; Derivatives thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/36—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/36—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids
    • A01N37/38—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids having at least one oxygen or sulfur atom attached to an aromatic ring system
    • A01N37/40—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids having at least one oxygen or sulfur atom attached to an aromatic ring system having at least one carboxylic group or a thio analogue, or a derivative thereof, and one oxygen or sulfur atom attached to the same aromatic ring system
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
    • A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
    • A01N43/06—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom five-membered rings
    • A01N43/08—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom five-membered rings with oxygen as the ring hetero atom
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
    • A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
    • A01N43/14—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings
    • A01N43/16—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings with oxygen as the ring hetero atom
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/72—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with nitrogen atoms and oxygen or sulfur atoms as ring hetero atoms
    • A01N43/74—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with nitrogen atoms and oxygen or sulfur atoms as ring hetero atoms five-membered rings with one nitrogen atom and either one oxygen atom or one sulfur atom in positions 1,3
    • A01N43/78—1,3-Thiazoles; Hydrogenated 1,3-thiazoles
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/06—Aluminium; Calcium; Magnesium; Compounds thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/40—Liliopsida [monocotyledons]
    • A01N65/48—Zingiberaceae [Ginger family], e.g. ginger or galangal
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change

Landscapes

  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Environmental Sciences (AREA)
  • Zoology (AREA)
  • Plant Pathology (AREA)
  • Wood Science & Technology (AREA)
  • Dentistry (AREA)
  • Agronomy & Crop Science (AREA)
  • Pest Control & Pesticides (AREA)
  • Biotechnology (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical & Material Sciences (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Medicinal Preparation (AREA)

Abstract

本发明公开了一种猕猴桃用桉树叶植物源农药，由下列物质制成：桉树叶、雷公藤、苦楝叶、槐根、断肠草、地榆、生姜、八角、黄连、白芍、改性淀粉溶液。本发明农药主要成分是从中草药中提取而得，与传统有机农药相比，具有安全、低毒、无刺激性气味、不会产生抗药性的优点，经过合理的复配后，其杀菌除虫效果显著，配合改性淀粉的添加，其稳定性更好、不易分解，同时改性淀粉又能吸附药物中的过量成分，进一步减少果实的药物残留；此外，中草药的提取成分含有各种营养成分，又含有活性酶、抗氧化物、生长促进因子等成分，能改善猕猴桃质量，提高猕猴桃的挂果率，增强了其预防人体心血管疾病的效果。

Description

一种猕猴桃用桉树叶植物源农药
技术领域
本发明属于农药领域，具体涉及一种猕猴桃用桉树叶植物源农药。
背景技术
猕猴桃是一种营养价值丰富，经济价值极高的水果，被誉为“绿色金矿”、“水果之王”等美称，有很好的食用、医疗、美容和保健作用，在国内国际果品消费市场上均有很大的发展潜力。
现在大多数植物的生长均离不开农药的施加，农药广义的定义是指用于预防、消灭或者控制危害农业、林业的病、虫、草和其他有害生物以及有目的地调节植物、昆虫生长的化学合成或者来源于生物、其他天然物质的一种物质或者几种物质的混合物及其制剂。是指在农业生产中，为保障、促进植物和农作物的成长，所施用的杀虫、杀菌、杀灭有害动物（或杂草） 的一类药物统称。特指在农业上用于防治病虫以及调节植物生长、除草等药剂。猕猴桃植物的生长也不例外，合理农药的施加可增加产量，并能改善猕猴桃质量。不过现在农药多数为化学制剂，气味浓烈难闻，且容易危及人畜安全，严重影响了环境卫生和安全，从绿色、环保、生态来说，都非常不利。此外，长期施加此类农药易产生抗病性，降低农药的使用效果。
发明内容
本发明旨在提供一种猕猴桃用桉树叶植物源农药。
本发明通过以下技术方案来实现：
一种猕猴桃用桉树叶植物源农药，由如下重量份的物质制成：
12份桉树叶、6份雷公藤、8份苦楝叶、4份槐根、5份断肠草、3份地榆、4份生姜、4份八角、7份黄连、5份白芍、4份改性淀粉溶液；所述改性淀粉溶液由如下重量份的物质制成：35份淀粉、3份改性高岭土、0.3份羧甲基纤维素钠、0.5份山梨醇脂肪酸酯、0.4份没食子酸丙脂、0.5份维生素A、0.5份维生素B1、0.8份维生素C、0.5份甲壳素、1份酒石酸、0.5份山梨酸钾。
进一步的，所述改性高岭土的制备方法为：先将高岭土放入质量分数为5%的氢氧化钠溶液中浸泡清洗20min，取出后放入860℃环境下煅烧2h，取出后用球磨机粉碎至颗粒大小为450~550目即可。
进一步的，所述改性淀粉溶液的制备方法为：
（1）将淀粉与其总质量3倍的清水共同混合，加热保持水温为85~88℃，糊化30~40min后得溶液A备用，期间不断搅拌；
（2）将改性高岭土与其质量2.5倍的清水共同混合，加热保持水温为40~45℃，再加入羧甲基纤维素钠、山梨醇脂肪酸酯、没食子酸丙脂，混合搅拌20min后，再将维生素A、维生素B1、维生素C、甲壳素、酒石酸和山梨酸钾加入，继续搅拌20min，得溶液B备用；
（3）保持溶液B的温度为43~46℃，保持溶液A的温度为85~88℃，将溶液B加入到溶液A中，并以300~350转/min的转速进行搅拌，待溶液温度恒定、成分分散均匀后即得改性淀粉溶液。将溶液A、溶液B以不同温度进行混合对冲，利用温度差增强分子间的混合，增强了分子间的交联融合程度，进而提高了溶液的稳定性与均匀性。
一种猕猴桃用桉树叶植物源农药的制备方法，包括如下步骤：
（1）将桉树叶、雷公藤、苦楝叶、槐根、断肠草、地榆、生姜、八角、黄连和白芍共同放入地窖中，保持地窖的温度为43~45℃，放置5~7天后取出备用；将上述成分放入地窖中中温储藏一段时间，可祛除中药的刺激性以及有毒成分，同时又能避免对有益成分的损害；
（2）用清水对步骤（1）处理后的成分进行冲洗、晾干备用；
（3）将槐根、生姜和白芍共同放入盛有炒砂的砂锅中，加热保持温度为95~103℃，不断翻炒，15~18min后取出得炒制药A备用；
（4）将雷公藤、八角和黄连共同放入盛有黄心土的砂锅中，加热保持温度为98~105℃，不断翻炒，10~15min后取出得炒制药B备用；针对药物的药性进行砂炒和土炒，可改善、提升药物的药性，并有利于后续的提取操作；
（5）将桉树叶、苦楝叶、断肠草、地榆和炒制药A、炒制药B共同混合，粉碎后过80目，然后放入其总质量3倍的质量分数为80%的乙醇溶液中循环提取20~24h，得提取液备用；将药物粉碎后用乙醇溶液进行提取，不仅能提高有益成分的含量，又能避免传统水提损害有益成分的问题，进一步保证了提取物的使用效果；
（6）将步骤（5）所得的提取液与改性淀粉溶液共同混合均匀即得成品。
本发明具有如下有益效果：本发明农药主要成分是从中草药中提取而得，与传统有机农药相比，具有安全、低毒、无刺激性气味、不会产生抗药性的优点，经过合理的复配后，其杀菌除虫效果显著，配合改性淀粉的添加，其稳定性更好、不易分解，同时改性淀粉又能吸附药物中的过量成分，进一步减少果实的药物残留；此外，中草药的提取成分含有各种营养成分，又含有活性酶、抗氧化物、生长促进因子等成分，能改善猕猴桃质量，提高猕猴桃的挂果率，增强了其预防人体心血管疾病的效果。
具体实施方式
实施例1
一种猕猴桃用桉树叶植物源农药，由如下重量份的物质制成：
12份桉树叶、6份雷公藤、8份苦楝叶、4份槐根、5份断肠草、3份地榆、4份生姜、4份八角、7份黄连、5份白芍、4份改性淀粉溶液；所述改性淀粉溶液由如下重量份的物质制成：35份淀粉、3份改性高岭土、0.3份羧甲基纤维素钠、0.5份山梨醇脂肪酸酯、0.4份没食子酸丙脂、0.5份维生素A、0.5份维生素B1、0.8份维生素C、0.5份甲壳素、1份酒石酸、0.5份山梨酸钾。
进一步的，所述改性高岭土的制备方法为：先将高岭土放入质量分数为5%的氢氧化钠溶液中浸泡清洗20min，取出后放入860℃环境下煅烧2h，取出后用球磨机粉碎至颗粒大小为450~550目即可。
进一步的，所述改性淀粉溶液的制备方法为：
（1）将淀粉与其总质量3倍的清水共同混合，加热保持水温为85~88℃，糊化30~40min后得溶液A备用，期间不断搅拌；
（2）将改性高岭土与其质量2.5倍的清水共同混合，加热保持水温为40~45℃，再加入羧甲基纤维素钠、山梨醇脂肪酸酯、没食子酸丙脂，混合搅拌20min后，再将维生素A、维生素B1、维生素C、甲壳素、酒石酸和山梨酸钾加入，继续搅拌20min，得溶液B备用；
（3）保持溶液B的温度为43~46℃，保持溶液A的温度为85~88℃，将溶液B加入到溶液A中，并以300~350转/min的转速进行搅拌，待溶液温度恒定、成分分散均匀后即得改性淀粉溶液。
一种猕猴桃用桉树叶植物源农药的制备方法，包括如下步骤：
（1）将桉树叶、雷公藤、苦楝叶、槐根、断肠草、地榆、生姜、八角、黄连和白芍共同放入地窖中，保持地窖的温度为43~45℃，放置5~7天后取出备用；
（2）用清水对步骤（1）处理后的成分进行冲洗、晾干备用；
（3）将槐根、生姜和白芍共同放入盛有炒砂的砂锅中，加热保持温度为95~103℃，不断翻炒，15~18min后取出得炒制药A备用；
（4）将雷公藤、八角和黄连共同放入盛有黄心土的砂锅中，加热保持温度为98~105℃，不断翻炒，10~15min后取出得炒制药B备用；
（5）将桉树叶、苦楝叶、断肠草、地榆和炒制药A、炒制药B共同混合，粉碎后过80目，然后放入其总质量3倍的质量分数为80%的乙醇溶液中循环提取20~24h，得提取液备用；
（6）将步骤（5）所得的提取液与改性淀粉溶液共同混合均匀即得成品。
对比实施例1
本对比实施例1与实施例1相比，除了不含有改性淀粉溶液外，其余方法步骤均相同。
对照组
市售普通农药。
为了对比本发明使用效果，选择三块条件相同且适宜的试验田，试验田中种植的均是五年龄“金艳”品种猕猴桃，分别用上述三种农药进行病虫害管理，下表为相应的对比数据：
实施例1 对比实施例1 对照组
亩产量（kg） 780 760 700
每百克可食部维生素C含量（mg） 98 93 85
每百克可食部钙含量（mg） 37 33 28
猕猴桃叶枯病治愈率（%） 93.2 89.7 92.6
猕猴桃灰霉病治愈率（%） 93.8 91.2 94.5
由上表可以看出，本发明农药可很好的提升猕猴桃的产量与品质，其果实中的有益成分含量得到提高，增强了其食用价值，此外，其对猕猴桃常见病的治愈率与传统农药相比，效果相差无几，但又具有安全无残留的优点，且长期使用又不会产生抗药性；而未添加改性淀粉溶液的一组，其效果在各方面相比本发明农药均有所下降。

Claims (4)

1.一种猕猴桃用桉树叶植物源农药，其特征在于，由如下重量份的物质制成：
12份桉树叶、6份雷公藤、8份苦楝叶、4份槐根、5份断肠草、3份地榆、4份生姜、4份八角、7份黄连、5份白芍、4份改性淀粉溶液；所述改性淀粉溶液由如下重量份的物质制成：35份淀粉、3份改性高岭土、0.3份羧甲基纤维素钠、0.5份山梨醇脂肪酸酯、0.4份没食子酸丙脂、0.5份维生素A、0.5份维生素B1、0.8份维生素C、0.5份甲壳素、1份酒石酸、0.5份山梨酸钾。
2.根据权利要求1所述的一种猕猴桃用桉树叶植物源农药，其特征在于，所述改性高岭土的制备方法为：先将高岭土放入质量分数为5%的氢氧化钠溶液中浸泡清洗20min，取出后放入860℃环境下煅烧2h，取出后用球磨机粉碎至颗粒大小为450~550目即可。
3.根据权利要求1所述的一种猕猴桃用桉树叶植物源农药，其特征在于，所述改性淀粉溶液的制备方法为：
（1）将淀粉与其总质量3倍的清水共同混合，加热保持水温为85~88℃，糊化30~40min后得溶液A备用，期间不断搅拌；
（2）将改性高岭土与其质量2.5倍的清水共同混合，加热保持水温为40~45℃，再加入羧甲基纤维素钠、山梨醇脂肪酸酯、没食子酸丙脂，混合搅拌20min后，再将维生素A、维生素B1、维生素C、甲壳素、酒石酸和山梨酸钾加入，继续搅拌20min，得溶液B备用；
（3）保持溶液B的温度为43~46℃，保持溶液A的温度为85~88℃，将溶液B加入到溶液A中，并以300~350转/min的转速进行搅拌，待溶液温度恒定、成分分散均匀后即得改性淀粉溶液。
4.一种如权利要求1所述的猕猴桃用桉树叶植物源农药的制备方法，其特征在于，包括如下步骤：
（1）将桉树叶、雷公藤、苦楝叶、槐根、断肠草、地榆、生姜、八角、黄连和白芍共同放入地窖中，保持地窖的温度为43~45℃，放置5~7天后取出备用；
（2）用清水对步骤（1）处理后的成分进行冲洗、晾干备用；
（3）将槐根、生姜和白芍共同放入盛有炒砂的砂锅中，加热保持温度为95~103℃，不断翻炒，15~18min后取出得炒制药A备用；
（4）将雷公藤、八角和黄连共同放入盛有黄心土的砂锅中，加热保持温度为98~105℃，不断翻炒，10~15min后取出得炒制药B备用；
（5）将桉树叶、苦楝叶、断肠草、地榆和炒制药A、炒制药B共同混合，粉碎后过80目，然后放入其总质量3倍的质量分数为80%的乙醇溶液中循环提取20~24h，得提取液备用；
（6）将步骤（5）所得的提取液与改性淀粉溶液共同混合均匀即得成品。
CN201610430321.4A 2016-06-17 2016-06-17 一种猕猴桃用桉树叶植物源农药 Pending CN106106586A (zh)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610430321.4A CN106106586A (zh) 2016-06-17 2016-06-17 一种猕猴桃用桉树叶植物源农药

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610430321.4A CN106106586A (zh) 2016-06-17 2016-06-17 一种猕猴桃用桉树叶植物源农药

Publications (1)

Publication Number Publication Date
CN106106586A true CN106106586A (zh) 2016-11-16

Family

ID=57469703

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610430321.4A Pending CN106106586A (zh) 2016-06-17 2016-06-17 一种猕猴桃用桉树叶植物源农药

Country Status (1)

Country Link
CN (1) CN106106586A (zh)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106614786A (zh) * 2016-11-28 2017-05-10 东莞市联洲知识产权运营管理有限公司 一种用于瓜果种植中的杀菌剂组合物的制备方法

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1826905A (zh) * 2006-04-07 2006-09-06 浙江省农业科学院 一种雷公藤生物碱复配杀虫剂
CN103120192A (zh) * 2011-11-18 2013-05-29 大连得达科技发展有限公司 一种防治病虫害的农药及制备方法
CN105340884A (zh) * 2015-09-24 2016-02-24 叶集试验区观山猕猴桃种植专业合作社 一种猕猴桃天然防护药剂及其制备方法
CN105494476A (zh) * 2015-12-16 2016-04-20 胡彩军 一种小白菜病虫害防治药剂
CN105613631A (zh) * 2014-10-27 2016-06-01 重庆鸿谦农业开发有限责任公司 无公害农药及其制备方法

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1826905A (zh) * 2006-04-07 2006-09-06 浙江省农业科学院 一种雷公藤生物碱复配杀虫剂
CN103120192A (zh) * 2011-11-18 2013-05-29 大连得达科技发展有限公司 一种防治病虫害的农药及制备方法
CN105613631A (zh) * 2014-10-27 2016-06-01 重庆鸿谦农业开发有限责任公司 无公害农药及其制备方法
CN105340884A (zh) * 2015-09-24 2016-02-24 叶集试验区观山猕猴桃种植专业合作社 一种猕猴桃天然防护药剂及其制备方法
CN105494476A (zh) * 2015-12-16 2016-04-20 胡彩军 一种小白菜病虫害防治药剂

Non-Patent Citations (6)

* Cited by examiner, † Cited by third party
Title
中国土农药志编辑委员会 编: "《中国土农药志》", 31 May 1959, 科学出版社 *
张文青 等编: "《农药加工及使用技术》", 30 September 1998, 中国农业大学出版社 *
杨洪强: "《有机园艺》", 31 July 2005, 中国农业出版社 *
罗永明 主编: "《中药化学成分提取分离技术与方法》", 31 January 2016, 上海科学技术出版社 *
陈永安 主编: "《猕猴桃GAP生产技术》", 30 November 2013, 西北农林科技大学出版社 *
龚国强: "基于改性高岭土/海藻酸钠为载体的缓释农药制备及性能", 《中国优秀硕士学位论文全文数据库 工程科技I辑》 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106614786A (zh) * 2016-11-28 2017-05-10 东莞市联洲知识产权运营管理有限公司 一种用于瓜果种植中的杀菌剂组合物的制备方法

Similar Documents

Publication Publication Date Title
CN104365704A (zh) 一种绿色农用复方中草药杀菌剂
CN103265366A (zh) 一种拌种剂
CN103242107A (zh) 一种秸秆腐熟有机杀菌除草复混肥
CN105248476B (zh) 鸡皮果树专用植物杀虫剂及其生产方法
CN103265376A (zh) 一种植物无公害杀菌除草复混肥
CN105901038B (zh) 防治蔬菜根线虫的植物杀虫剂及其制备方法
CN104058880B (zh) 一种丹参gap标准种植用药肥及其生产方法
CN105284961A (zh) 一种可以提高玉米抗病能力的拌种剂及制备方法
CN104072302B (zh) 一种芝麻专用药肥及其生产方法
CN106116880A (zh) 一种花椒保花保果营养剂
CN105104457B (zh) 一种杀菌剂组合物
CN104814048A (zh) 一种中药材植物复合驱杀型无公害农药制剂的加工方法
CN104072242A (zh) 一种桔梗gap标准种植用药肥及其生产方法
CN106106586A (zh) 一种猕猴桃用桉树叶植物源农药
CN105360179A (zh) 苗木扦插基质专用环保消毒剂
CN106305861A (zh) 用于茄子的植物源杀虫剂及其制备方法
CN105685102A (zh) 环保型木焦油杀菌驱虫剂
CN106614838A (zh) 一种棉花种子拌种剂
CN1093377C (zh) 一种复合植物提取液农用杀菌剂
CN106070383A (zh) 一种瓜蒌种植用农药
CN106135314A (zh) 一种防治蚧壳虫的杀虫剂配方及生产方法
CN105941500A (zh) 一种高效复合生物绿色杀虫剂及其制备方法
CN101861885A (zh) 一种防治稻瘟病的植物药剂
CN104286057A (zh) 一种防治番茄蚜虫的植物药剂及其制备方法
CN105994422A (zh) 一种橄榄叶葡萄植物源农药

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication
RJ01 Rejection of invention patent application after publication

Application publication date: 20161116