CN106094452A - A kind of environment-friendly type powdered ink and preparation method thereof - Google Patents
A kind of environment-friendly type powdered ink and preparation method thereof Download PDFInfo
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- CN106094452A CN106094452A CN201610607212.5A CN201610607212A CN106094452A CN 106094452 A CN106094452 A CN 106094452A CN 201610607212 A CN201610607212 A CN 201610607212A CN 106094452 A CN106094452 A CN 106094452A
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- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03G—ELECTROGRAPHY; ELECTROPHOTOGRAPHY; MAGNETOGRAPHY
- G03G9/00—Developers
- G03G9/08—Developers with toner particles
- G03G9/0827—Developers with toner particles characterised by their shape, e.g. degree of sphericity
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- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03G—ELECTROGRAPHY; ELECTROPHOTOGRAPHY; MAGNETOGRAPHY
- G03G9/00—Developers
- G03G9/08—Developers with toner particles
- G03G9/0802—Preparation methods
- G03G9/0804—Preparation methods whereby the components are brought together in a liquid dispersing medium
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- General Physics & Mathematics (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The invention discloses a kind of environment-friendly type powdered ink, described environment-friendly type powdered ink is counted by weight and is included that following material is made: styrenated acrylic resin 50 80 parts, pigment carbon black 5 10 parts, nano ferriferrous oxide 0.5 1 parts, nano-titanium oxide 0.5 1 parts, nanoscale molybdenum oxide 0.5 1 parts, citric acid 0.1 0.5 parts, modified hydrogenated Oleum Ricini 38 parts, nano-silicon dioxide modified acrylic ester 5 10 parts, Tissuemat E 12 parts, sodium laurylsulfate 12 parts, 2,6 di-t-butyl 4 methylphenols 25 parts, catechin 0.5 1 parts；Powdered ink of the present invention has scattered, and grain diameter is uniform, and during printing, powdered ink fusing completely, along with printing paper out will not substantially reduce powdered ink content in air, play environmental-protection function；The function admirable of powdered ink the most of the present invention, tack is good, clear patterns after printing, be difficult to oxidized, good light stability, colour-fast variable color.
Description
Technical field
The present invention relates to printing consumable material technical field, be specifically related to a kind of printer environment-friendly type powdered ink and preparation side thereof
Method.
Background technology
Powdered ink is the one in printing consumable material, is generally used for printer and photocopier, and the main component of powdered ink is not carbon, and
Great majority are made up of resin and white carbon black, electric charge agent, magnetic powder etc..For different demands, carbon dust produces to becoming more meticulous, colored
Change, high speed direction is developed.But generally there is following point in current powdered ink: toner particle diameter has a very wide distribution, and causes powdered ink
There is the toner particles that part is big non-fusible in use, so that the uneven and infusible powdered ink of the color of image printed
Granule results in blockage and along with printing paper out, suspends and pollute air in atmosphere, and be easily absorbed by the body, to human body
Health works the mischief.
Summary of the invention
It is an object of the invention to for the problems referred to above, it is provided that a kind of printer environment-friendly type powdered ink, powdered ink of the present invention
Having scattered, grain diameter is uniform, and during printing, powdered ink fusing completely, will not along with printing paper out substantially reduce in air
Powdered ink content, plays environmental-protection function；The function admirable of powdered ink the most of the present invention, tack is good, clear patterns after printing, be difficult to by
Oxidation, good light stability, colour-fast variable color.
The technical scheme that the present invention provides is:
A kind of environment-friendly type powdered ink, described environment-friendly type powdered ink counts by weight and includes that following material is made: phenylethene modified
Acrylic resin 50-80 part, pigment carbon black 5-10 part, nano ferriferrous oxide 0.5-1 part, nano-titanium oxide 0.5-1 part, nanometer
Molybdenum oxide 0.5-1 part, citric acid 0.1-0.5 part, modified hydrogenated Oleum Ricini 3-8 part, nano-silicon dioxide modified acrylic ester 5-
10 parts, Tissuemat E 1-2 part, sodium laurylsulfate 1-2 part, 2,6-di-tert-butyl-4-methy phenol 2-5 part, catechin 0.5-1
Part；The preparation method of environment-friendly type powdered ink comprises the following steps:
1) by styrenated acrylic resin, pigment carbon black, nano ferriferrous oxide, nano-titanium oxide, nano oxidized
Mo, citric acid join in reactor, add deionized water, ethanol as solvent, start the dispersion machine in reactor,
Rotating speed is transferred to 2000rmp, carries out dispersion 20-30 minute, closes dispersion machine；
2) add modified hydrogenated Oleum Ricini, nano-silicon dioxide modified acrylic ester, start the dispersion machine in reactor, turn
Velocity modulation, to 4000rmp, carries out disperseing 20 minutes, and rotating speed is transferred to 2000rmp, adds 2,6-di-tert-butyl-4-methy phenol, catechu
Element, carries out disperseing 10 minutes, and rotating speed is transferred to 1000rmp, adds sodium laurylsulfate, Tissuemat E, carries out disperseing 30 minutes, stop
Only after dispersion, obtain described environment-friendly type powdered ink through filtering, being spray-dried.
Preferably, described environment-friendly type powdered ink is counted by weight and is included that following material is made: styrenated acrylic
Resin 60 parts, pigment carbon black 6 parts, nano ferriferrous oxide 0.5 part, nano-titanium oxide 0.5 part, nanoscale molybdenum oxide 1 part, citric acid
0.4 part, modified hydrogenated Oleum Ricini 6 parts, nano-silicon dioxide modified acrylic ester 7 parts, Tissuemat E 2 parts, sodium laurylsulfate 1
Part, 2,6-di-tert-butyl-4-methy phenol 4 parts, catechin 0.5 part；The preparation method of environment-friendly type powdered ink comprises the following steps:
1) by styrenated acrylic resin, pigment carbon black, nano ferriferrous oxide, nano-titanium oxide, nano oxidized
Mo, citric acid join in reactor, add deionized water, ethanol as solvent, start the dispersion machine in reactor,
Rotating speed is transferred to 2000rmp, carries out dispersion 20-30 minute, closes dispersion machine；
2) add modified hydrogenated Oleum Ricini, nano-silicon dioxide modified acrylic ester, start the dispersion machine in reactor, turn
Velocity modulation, to 4000rmp, carries out disperseing 20 minutes, and rotating speed is transferred to 2000rmp, adds 2,6-di-tert-butyl-4-methy phenol, catechu
Element, carries out disperseing 10 minutes, and rotating speed is transferred to 1000rmp, adds sodium laurylsulfate, Tissuemat E, carries out disperseing 30 minutes, stop
Only after dispersion, obtain described environment-friendly type powdered ink through filtering, being spray-dried.
Preferably, described nano ferriferrous oxide particle diameter is 50-100 nanometer.
Preferably, described nano-titanium oxide particle diameter is 50-100 nanometer.
Preferably, described nanoscale molybdenum oxide particle diameter is 50-100 nanometer.
Preferably, described pigment carbon black is nano dye carbon black, and the particle diameter of described nano dye carbon black is that 50-100 receives
Rice.
Beneficial effects of the present invention is as follows:
First, the present invention adds nanoscale molybdenum oxide, sodium laurylsulfate, nano-silicon dioxide modified acrylic ester as breast
Agent and molecular weight regulator, can regulate the particle size distribution controlling powdered ink, makes the toner particle size distribution collection of the present invention
In at 5-8 micron, improve the tack of powdered ink simultaneously, make not fugitive color after powdered ink printing；2,6-di-t-butyl-4-methylbenzene
Phenol, catechin can improve the oxidation resistance of powdered ink as antioxidant, extend the shelf-life of powdered ink；The interpolation of titanium oxide increases
The light stability of powdered ink so that the middle pigment of powdered ink and resin Composition, under conditions of illumination, do not react, after keeping printing
The stability of image color；Citric acid energy chelated iron ion regulation in powdered ink is as the charge adjusting agent of powdered ink；In sum
Compared with prior art, powdered ink of the present invention has scattered, and grain diameter is uniform, and during printing, powdered ink fusing is completely, will not be along with
Printing paper out, substantially reduces powdered ink content in air, plays environmental-protection function；The function admirable of powdered ink the most of the present invention, attachment
Property good, printing after clear patterns, be difficult to oxidized, good light stability, colour-fast variable color.
Second, processing technology of the present invention is carried out at relatively low temperature, it is to avoid the high temperature destruction to the performance of raw material,
And the performance of itself uses different temperature to add for raw material, different rate of dispersions, carry out emulsifying synthesis, the ink of making
Powder particles is distributed concentration, exquisiteness, good dispersion, is suitable to printer use, does not bites, and printed patterns is clear.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is described in further detail, to make those skilled in the art with reference to saying
Bright book word can be implemented according to this.
Embodiment 1:
Environment-friendly type powdered ink is counted by weight and is included that following material is made: styrenated acrylic resin 50 parts, pigment
Carbon black 5 parts, nano ferriferrous oxide 0.5 part, nano-titanium oxide 0.5 part, nanoscale molybdenum oxide 0.5 part, citric acid 0.1 part, modification
Castor oil hydrogenated 3 parts, nano-silicon dioxide modified acrylic ester 5 parts, Tissuemat E 1 part, sodium laurylsulfate 1 part, 2,6-bis-
Tert-butyl-4-methyl-Phenol 2 parts, catechin 0.5 part；The preparation method of environment-friendly type powdered ink comprises the following steps:
1) by styrenated acrylic resin, pigment carbon black, nano ferriferrous oxide, nano-titanium oxide, nano oxidized
Molybdenum, citric acid material join in reactor, add 4 times of heavy deionized waters of material and ethanol as solvent, deionized water
Proportioning any with ethanol, the preferred deionized water of the present embodiment and ethanol weight ratio 2: 1, start the dispersion machine in reactor, rotating speed
It is transferred to 2000rmp, carries out disperseing 20 minutes, close dispersion machine；
2) add modified hydrogenated Oleum Ricini, nano-silicon dioxide modified acrylic ester, start the dispersion machine in reactor, turn
Velocity modulation, to 4000rmp, carries out disperseing 20 minutes, and rotating speed is transferred to 2000rmp, adds 2,6-di-tert-butyl-4-methy phenol, catechu
Element, carries out disperseing 10 minutes, and rotating speed is transferred to 1000rmp, adds sodium laurylsulfate, Tissuemat E, carries out disperseing 30 minutes, stop
Only after dispersion, obtain described environment-friendly type powdered ink through filtering, being spray-dried.
Embodiment 2
Environment-friendly type powdered ink is counted by weight and is included that following material is made: styrenated acrylic resin 80 parts, nanometer
Pigment carbon black 10 parts, nano ferriferrous oxide 1 part, nano-titanium oxide 1 part, nanoscale molybdenum oxide 1 part, citric acid 0.5 part, modified hydrogen
Change Oleum Ricini 8 parts, nano-silicon dioxide modified acrylic ester 10 parts, Tissuemat E 2 parts, sodium laurylsulfate 2 parts, 2,6-bis-uncle
Butyl-4-methylphenol 5 parts, catechin 1 part；Nano ferriferrous oxide particle diameter is 50-100 nanometer, and nano-titanium oxide particle diameter is
50-100 nanometer, described nanoscale molybdenum oxide particle diameter is 50-100 nanometer, and the particle diameter of nano dye carbon black is 50-100 nanometer；
The preparation method of environment-friendly type powdered ink comprises the following steps:
1) by styrenated acrylic resin, nano dye carbon black, nano ferriferrous oxide, nano-titanium oxide, nanometer
Molybdenum oxide, citric acid material join in reactor, add material twice weight deionized water and ethanol as solvent, go from
Sub-water and any proportioning of ethanol, the preferred deionized water of the present embodiment and ethanol weight ratio 1: 2, start the dispersion machine in reactor,
Rotating speed is transferred to 2000rmp, carries out dispersion 20-30 minute, closes dispersion machine；
2) add modified hydrogenated Oleum Ricini, nano-silicon dioxide modified acrylic ester, start the dispersion machine in reactor, turn
Velocity modulation, to 4000rmp, carries out disperseing 20 minutes, and rotating speed is transferred to 2000rmp, adds 2,6-di-tert-butyl-4-methy phenol, catechu
Element, carries out disperseing 10 minutes, and rotating speed is transferred to 1000rmp, adds sodium laurylsulfate, Tissuemat E, carries out disperseing 30 minutes, stop
Only after dispersion, obtain described environment-friendly type powdered ink through filtering, being spray-dried.
Embodiment 3
Environment-friendly type powdered ink is counted by weight and is included that following material is made: styrenated acrylic resin 60 parts, pigment
Carbon black 6 parts, nano ferriferrous oxide 0.5 part, nano-titanium oxide 0.5 part, nanoscale molybdenum oxide 1 part, citric acid 0.4 part, modified hydrogen
Change Oleum Ricini 6 parts, nano-silicon dioxide modified acrylic ester 7 parts, Tissuemat E 2 parts, sodium laurylsulfate 1 part, 2,6-bis-uncle
Butyl-4-methylphenol 4 parts, catechin 0.5 part；Nano ferriferrous oxide particle diameter is 50-100 nanometer, nano-titanium oxide particle diameter
For 50-100 nanometer, described nanoscale molybdenum oxide particle diameter is 50-100 nanometer；
The preparation method of environment-friendly type powdered ink comprises the following steps:
1) by styrenated acrylic resin, pigment carbon black, nano ferriferrous oxide, nano-titanium oxide, nano oxidized
Molybdenum, citric acid material join in reactor, add the heavy deionized water of material twice and ethanol as solvent, deionized water
Proportioning any with ethanol, the preferred deionized water of the present embodiment and ethanol weight ratio 1: 2, start the dispersion machine in reactor, rotating speed
It is transferred to 2000rmp, carries out disperseing 25 minutes, close dispersion machine；
2) add modified hydrogenated Oleum Ricini, nano-silicon dioxide modified acrylic ester, start the dispersion machine in reactor, turn
Velocity modulation, to 4000rmp, carries out disperseing 20 minutes, and rotating speed is transferred to 2000rmp, adds 2,6-di-tert-butyl-4-methy phenol, catechu
Element, carries out disperseing 10 minutes, and rotating speed is transferred to 1000rmp, adds sodium laurylsulfate, Tissuemat E, carries out disperseing 30 minutes, stop
Only after dispersion, obtain described environment-friendly type powdered ink through filtering, being spray-dried.
Although embodiment of the present invention are disclosed as above, but it is not restricted in description and embodiment listed
Using, it can be applied to various applicable the field of the invention completely, for those skilled in the art, and can be easily
Realizing other amendment, therefore under the general concept limited without departing substantially from claim and equivalency range, the present invention does not limit
In specific details with shown here as the embodiment with description.
Claims (6)
1. an environment-friendly type powdered ink, it is characterised in that described environment-friendly type powdered ink is counted by weight and included that following material is made: benzene
Ethylene modified acrylic resin 50-80 part, pigment carbon black 5-10 part, nano ferriferrous oxide 0.5-1 part, nano-titanium oxide 0.5-
1 part, nanoscale molybdenum oxide 0.5-1 part, citric acid 0.1-0.5 part, modified hydrogenated Oleum Ricini 3-8 part, nano-silicon dioxide modified third
Olefin(e) acid ester 5-10 part, Tissuemat E 1-2 part, sodium laurylsulfate 1-2 part, 2,6-di-tert-butyl-4-methy phenol 2-5 part, youngster
Theine 0.5-1 part；The preparation method of environment-friendly type powdered ink comprises the following steps:
1) by styrenated acrylic resin, pigment carbon black, nano ferriferrous oxide, nano-titanium oxide, nano oxidized molybdenum materials
Material, citric acid join in reactor, add deionized water, ethanol as solvent, the dispersion machine in startup reactor, rotating speed
It is transferred to 2000rmp, carries out dispersion 20-30 minute, close dispersion machine；
2) adding modified hydrogenated Oleum Ricini, nano-silicon dioxide modified acrylic ester, start the dispersion machine in reactor, rotating speed is adjusted
To 4000rmp, carrying out disperseing 20 minutes, rotating speed is transferred to 2000rmp, adds 2,6-di-tert-butyl-4-methy phenol, catechin,
Carrying out disperseing 10 minutes, rotating speed is transferred to 1000rmp, adds sodium laurylsulfate, Tissuemat E, carries out disperseing 30 minutes, stops
After dispersion, obtain described environment-friendly type powdered ink through filtering, being spray-dried.
2. environment-friendly type powdered ink as claimed in claim 1, it is characterised in that described environment-friendly type powdered ink count by weight include as
Lower material is made: styrenated acrylic resin 60 parts, pigment carbon black 6 parts, nano ferriferrous oxide 0.5 part, nano oxidized
Titanium 0.5 part, nanoscale molybdenum oxide 1 part, citric acid 0.4 part, modified hydrogenated Oleum Ricini 6 parts, nano-silicon dioxide modified acrylic ester 7
Part, Tissuemat E 2 parts, sodium laurylsulfate 1 part, 2,6-di-tert-butyl-4-methy phenol 4 parts, catechin 0.5 part；Environment-friendly type
The preparation method of powdered ink comprises the following steps:
1) by styrenated acrylic resin, pigment carbon black, nano ferriferrous oxide, nano-titanium oxide, nano oxidized molybdenum materials
Material, citric acid join in reactor, add deionized water, ethanol as solvent, the dispersion machine in startup reactor, rotating speed
It is transferred to 2000rmp, carries out dispersion 20-30 minute, close dispersion machine；
2) adding modified hydrogenated Oleum Ricini, nano-silicon dioxide modified acrylic ester, start the dispersion machine in reactor, rotating speed is adjusted
To 4000rmp, carrying out disperseing 20 minutes, rotating speed is transferred to 2000rmp, adds 2,6-di-t-butyl-4 monomethyl phenol, catechin,
Carrying out disperseing 10 minutes, rotating speed is transferred to 1000rmp, adds sodium laurylsulfate, Tissuemat E, carries out disperseing 30 minutes, stops
After dispersion, obtain described environment-friendly type powdered ink through filtering, being spray-dried.
3. environment-friendly type powdered ink as claimed in claim 1, it is characterised in that described nano ferriferrous oxide particle diameter is that 50-100 receives
Rice.
4. environment-friendly type powdered ink as described in claim 1, it is characterised in that described nano-titanium oxide particle diameter is that 50-100 receives
Rice.
5. environment-friendly type powdered ink as claimed in claim 1, it is characterised in that described nanoscale molybdenum oxide particle diameter is 50-100 nanometer.
6. environment-friendly type powdered ink as claimed in claim 1, it is characterised in that described pigment carbon black is nano dye carbon black, described
The particle diameter of nano dye carbon black is 50-100 nanometer.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610607212.5A CN106094452A (en) | 2016-07-28 | 2016-07-28 | A kind of environment-friendly type powdered ink and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610607212.5A CN106094452A (en) | 2016-07-28 | 2016-07-28 | A kind of environment-friendly type powdered ink and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113185866A (en) * | 2021-04-01 | 2021-07-30 | 浙江工业大学 | Carbon ink prepared from waste kelp residues and preparation method thereof |
| CN117761982A (en) * | 2024-01-20 | 2024-03-26 | 广州市三横信息科技有限公司 | Preparation method of modified carbon powder and carbon powder box |
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| CN102736455A (en) * | 2011-04-13 | 2012-10-17 | 柯尼卡美能达商用科技株式会社 | Toner for electrostatic image development |
| CN104160339A (en) * | 2012-03-07 | 2014-11-19 | 佳能株式会社 | Yellow toner and process for producing the yellow toner |
| CN104181783A (en) * | 2013-05-23 | 2014-12-03 | 施乐公司 | Toner composition |
| CN104950609A (en) * | 2014-03-27 | 2015-09-30 | 佳能株式会社 | Method for producing toner particle |
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- 2016-07-28 CN CN201610607212.5A patent/CN106094452A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1318775A (en) * | 2000-02-21 | 2001-10-24 | 佳能株式会社 | Magnetic toner and imaging method using the same |
| CN1338664A (en) * | 2000-07-28 | 2002-03-06 | 佳能株式会社 | Magnetic color tuner |
| JP2002123038A (en) * | 2000-10-17 | 2002-04-26 | Konica Corp | Electrophotographic toner and method for manufacturing the same |
| CN102736455A (en) * | 2011-04-13 | 2012-10-17 | 柯尼卡美能达商用科技株式会社 | Toner for electrostatic image development |
| CN104160339A (en) * | 2012-03-07 | 2014-11-19 | 佳能株式会社 | Yellow toner and process for producing the yellow toner |
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| CN113185866A (en) * | 2021-04-01 | 2021-07-30 | 浙江工业大学 | Carbon ink prepared from waste kelp residues and preparation method thereof |
| CN113185866B (en) * | 2021-04-01 | 2023-04-07 | 浙江工业大学 | Carbon ink prepared from waste kelp residues and preparation method thereof |
| CN117761982A (en) * | 2024-01-20 | 2024-03-26 | 广州市三横信息科技有限公司 | Preparation method of modified carbon powder and carbon powder box |
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