CN106086452B - A kind of Palladium recovery device - Google Patents

A kind of Palladium recovery device Download PDF

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Publication number
CN106086452B
CN106086452B CN201610646324.1A CN201610646324A CN106086452B CN 106086452 B CN106086452 B CN 106086452B CN 201610646324 A CN201610646324 A CN 201610646324A CN 106086452 B CN106086452 B CN 106086452B
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China
Prior art keywords
reactive tank
motor
palladium
main shaft
agitating shaft
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CN201610646324.1A
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Chinese (zh)
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CN106086452A (en
Inventor
韦建敏
赵兴文
张晓蓓
张小波
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Honghua Technology Co ltd
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Chengdu Honghua Environmental Protection Technology Co Ltd
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Priority to CN201610646324.1A priority Critical patent/CN106086452B/en
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    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B11/00Obtaining noble metals
    • C22B11/04Obtaining noble metals by wet processes
    • C22B11/042Recovery of noble metals from waste materials
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00Technologies related to metal processing
    • Y02P10/20Recycling

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  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Chemically Coating (AREA)

Abstract

The invention discloses a kind of Palladium recovery device, it includes reactive tank(1), motor I(2), be arranged at reactive tank(1)The closure at top(3), be arranged at closure(3)On inlet(4), rotation be installed on reactive tank(1)Interior main shaft(5), described main shaft(5)On be provided with positioned at reactive tank(1)Interior suction palladium resin column(6), main shaft(5)With motor I(2)Output end between be provided with transmission device, reactive tank(1)Side wall on be provided with liquid outlet(8), agitating shaft(10)With motor II(9)Output end connection, agitating shaft(10)Run through reactive tank from lower to upper(1)Set, agitating shaft(10)Upper end be provided with positioned at reactive tank(1)Interior blade(7), the retracting device is also including controller, described controller and motor I(2)With motor II(9)Connection.The beneficial effects of the invention are as follows:Inhale palladium efficiency high, simple to operate, Palladium recovery amount big.

Description

A kind of Palladium recovery device
Technical field
The present invention relates to the technical field of Palladium recovery in electroplate liquid, particularly a kind of Palladium recovery device.
Background technology
In Du Ba manufacturing enterprises, to make surface of decoration more exquisite, it will usually plate a palladium layers on ornaments surface, electricity Generally also contain substantial amounts of palladium in the electroplate liquid used during plating, if plating liquid discharge is not only directly polluted into environment, and Also create waste.Therefore people are reclaimed using palladium resin column is inhaled to the palladium in electroplate liquid, because inhaling palladium resin column has Following characteristics, the adsorption rate for inhaling palladium resin column is fast, is more than five times of common coconut carbon adsorption rate;Inhale the choosing of palladium resin column Preferably, to other metals, the annoyance level of such as copper, nickel, iron and/or lead is small for selecting property;Inhale palladium resin column antifouling property compared with It is good, it can be cleaned with pure water or sodium chloride solution.However, palladium is largely deposited on the bottom for the treatment of trough, not There is the suction palladium resin column with being suspended in the middle part for the treatment of trough to contact, there is the low defect of absorption efficiency, and workman is difficult detect tank The content of interior palladium, after processing time arrives, plating liquid discharge to next process processing, is caused the waste of palladium by workman side.
The content of the invention
It is an object of the invention to the shortcoming for overcoming prior art, there is provided a kind of compact conformation, suction palladium efficiency high, operation letter The big Palladium recovery device of single, Palladium recovery amount.
The purpose of the present invention is achieved through the following technical solutions:A kind of Palladium recovery device, it include reactive tank, motor I, It is arranged at the closure at the top of reactive tank, the inlet being arranged on closure, rotates the main shaft being installed in reactive tank, it is described Main shaft on be provided with the suction palladium resin column in reactive tank, be provided with transmission device between main shaft and motor I output end, Liquid outlet is provided with the side wall of reactive tank, the retracting device also includes being located at the motor II and agitating shaft below reactive tank, stirs The output end that axle is mixed with motor II is connected, and agitating shaft is set through reactive tank from lower to upper, and the upper end of agitating shaft is provided with position In the blade in reactive tank, the retracting device also includes controller, and described controller is connected with motor I and motor II.
Described transmission device is made up of driving gear and driven gear, and driving gear is installed on motor I output end, from Moving gear is installed on main shaft, and driving gear is engaged with driven gear.
Described controller is PLC.
The bottom of described reactive tank is provided with multiple supporting legs.
The present invention has advantages below:Compact conformation of the present invention, suction palladium efficiency high, simple to operate, Palladium recovery amount are big.
Brief description of the drawings
Fig. 1 is structural representation of the invention;
In figure, 1- reactive tanks, 2- motors I, 3- closure, 4- inlets, 5- main shafts, 6- inhales palladium resin column, 7- blades, 8- Liquid outlet, 9- motors II, 10- agitating shaft, 11- driving gears, 12- driven gears, 13- supporting legs.
Embodiment
The present invention will be further described below in conjunction with the accompanying drawings, and protection scope of the present invention is not limited to as described below:
As shown in figure 1, a kind of Palladium recovery device, it includes reactive tank 1, motor I2, is arranged at the sealing at the top of reactive tank 1 Lid 3, the inlet 4 being arranged on closure 3, rotation, which are installed on main shaft 5 in reactive tank 1, described main shaft 5, is provided with position In the suction palladium resin column 6 in reactive tank 1, transmission device, the side of reactive tank 1 are provided between main shaft 5 and motor I2 output end Liquid outlet 8 is provided with wall, the retracting device also includes the motor II9 and agitating shaft 10 for being located at the lower section of reactive tank 1, agitating shaft 10 It is connected with motor II9 output end, agitating shaft 10 is set through reactive tank 1 from lower to upper, and the upper end of agitating shaft 10 is provided with Blade 7 in reactive tank 1, the retracting device also includes controller, and described controller connects with motor I2 and motor II9 Connect, controller is PLC, being capable of controller by controller
As shown in figure 1, transmission device is made up of driving gear 11 and driven gear 12, driving gear 11 is installed on motor I2 Output end, driven gear 12 is installed on main shaft 5, and driving gear 11 is engaged with driven gear 12.The bottom of described reactive tank 1 Portion is provided with multiple supporting legs 13.
The job step of Recover palladium of the present invention is as follows:
S1, it is passed through a certain amount of electroplate liquid into reactive tank 1 through inlet 4, when electroplate liquid floods suction palladium resin column 6, stops Only inject electroplate liquid;
S2, startup motor I2, motor I2 drive driving gear 11 to rotate, and driving gear 11 drives driven gear 12 to rotate, Driven gear 12 drives main shaft 5 to rotate, and main shaft 5 drives suction palladium resin column 6 to rotate;
S3, the agitated axles 10 of startup motor II9, motor II9 drive blade 7 to rotate, and blade 7 makes to be deposited on the bottom of reactive tank 1 The palladium in portion constantly rolls, and increases palladium with inhaling the contact frequency of palladium resin column 6, while inhale palladium resin column 6 is doing rotation fortune again It is dynamic, the utilization rate for inhaling palladium resin column 6 is increased, the absorption of palladium is realized, processed waste water is discharged through liquid outlet 8.Therefore this time Receiving apparatus greatly improves the efficiency for inhaling palladium, improves the yield of palladium, reduces the cost that ornaments plate palladium.

Claims (1)

1. a kind of Palladium recovery device, it is characterised in that:It includes reactive tank(1), motor I(2), be arranged at reactive tank(1)Top Closure(3), be arranged at closure(3)On inlet(4), rotation be installed on reactive tank(1)Interior main shaft(5), it is described Main shaft(5)On be provided with positioned at reactive tank(1)Interior suction palladium resin column(6), main shaft(5)With motor I(2)Output end between It is provided with transmission device, reactive tank(1)Side wall on be provided with liquid outlet(8), the retracting device is also including being located at reactive tank(1) The motor II of lower section(9)And agitating shaft(10), agitating shaft(10)With motor II(9)Output end connection, agitating shaft(10)Under Up run through reactive tank(1)Set, agitating shaft(10)Upper end be provided with positioned at reactive tank(1)Interior blade(7), the recovery Device also includes controller, described controller and motor I(2)With motor II(9)Connection, described transmission device is by driving tooth Wheel(11)And driven gear(12)Composition, driving gear(11)It is installed on motor I(2)Output end, driven gear(12)Install In main shaft(5)On, driving gear(11)With driven gear(12)Engagement, controller is PLC, reactive tank(1)Bottom It is provided with multiple supporting legs(13).
CN201610646324.1A 2016-08-09 2016-08-09 A kind of Palladium recovery device Active CN106086452B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610646324.1A CN106086452B (en) 2016-08-09 2016-08-09 A kind of Palladium recovery device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610646324.1A CN106086452B (en) 2016-08-09 2016-08-09 A kind of Palladium recovery device

Publications (2)

Publication Number Publication Date
CN106086452A CN106086452A (en) 2016-11-09
CN106086452B true CN106086452B (en) 2017-11-07

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CN201610646324.1A Active CN106086452B (en) 2016-08-09 2016-08-09 A kind of Palladium recovery device

Country Status (1)

Country Link
CN (1) CN106086452B (en)

Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1123843A (en) * 1994-11-30 1996-06-05 核工业北京化工冶金研究院 Recovery of platinum family elements from waste catalysts
CN2464331Y (en) * 2001-01-17 2001-12-12 吴懋芳 Large porous adsorption resin column
CN1493706A (en) * 2002-10-08 2004-05-05 ס�ѽ�����ɽ��ʽ���� Method for separating/ recovering platinum family metal
CN201321393Y (en) * 2008-12-31 2009-10-07 南京中电联环保股份有限公司 Magnetic resin adsorption reactor
CN102329959A (en) * 2011-09-05 2012-01-25 中南大学 Separation method of palladium from silver electrolyte
CN102906286A (en) * 2010-04-21 2013-01-30 上原春男 System and method for recycling rare metals
CN103882242A (en) * 2012-12-19 2014-06-25 沈阳有色金属研究院 Method for utilizing chelate resin to realize separation of platinum, palladium and rhodium
CN204224676U (en) * 2014-10-28 2015-03-25 天津三雄科技有限公司 Palladium recovery device
CN204752826U (en) * 2015-04-10 2015-11-11 李玉明 Resin electrolysis integration gold, palladium recovery system
CN205856571U (en) * 2016-08-09 2017-01-04 成都虹华环保科技股份有限公司 A kind of Palladium recovery device

Patent Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1123843A (en) * 1994-11-30 1996-06-05 核工业北京化工冶金研究院 Recovery of platinum family elements from waste catalysts
CN2464331Y (en) * 2001-01-17 2001-12-12 吴懋芳 Large porous adsorption resin column
CN1493706A (en) * 2002-10-08 2004-05-05 ס�ѽ�����ɽ��ʽ���� Method for separating/ recovering platinum family metal
CN201321393Y (en) * 2008-12-31 2009-10-07 南京中电联环保股份有限公司 Magnetic resin adsorption reactor
CN102906286A (en) * 2010-04-21 2013-01-30 上原春男 System and method for recycling rare metals
CN102329959A (en) * 2011-09-05 2012-01-25 中南大学 Separation method of palladium from silver electrolyte
CN103882242A (en) * 2012-12-19 2014-06-25 沈阳有色金属研究院 Method for utilizing chelate resin to realize separation of platinum, palladium and rhodium
CN204224676U (en) * 2014-10-28 2015-03-25 天津三雄科技有限公司 Palladium recovery device
CN204752826U (en) * 2015-04-10 2015-11-11 李玉明 Resin electrolysis integration gold, palladium recovery system
CN205856571U (en) * 2016-08-09 2017-01-04 成都虹华环保科技股份有限公司 A kind of Palladium recovery device

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Address after: 610000 Chengdu province high tech Zone, West core road, No. 4, No.

Patentee after: Honghua Technology Co.,Ltd.

Address before: 610000 Chengdu province high tech Zone, West core road, No. 4, No.

Patentee before: CHENGDU HONGHUA ENVIRONMENTAL SCIENCE & TECHNOLOGY Co.,Ltd.

PE01 Entry into force of the registration of the contract for pledge of patent right
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Denomination of invention: A palladium recovery device

Effective date of registration: 20220725

Granted publication date: 20171107

Pledgee: Zheshang Bank Co.,Ltd. Chengdu Branch

Pledgor: Honghua Technology Co.,Ltd.

Registration number: Y2022510000223