CN106085235A - A kind of novel Waterproof corrosion modified coating and preparation thereof and application process - Google Patents
A kind of novel Waterproof corrosion modified coating and preparation thereof and application process Download PDFInfo
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- CN106085235A CN106085235A CN201610553301.6A CN201610553301A CN106085235A CN 106085235 A CN106085235 A CN 106085235A CN 201610553301 A CN201610553301 A CN 201610553301A CN 106085235 A CN106085235 A CN 106085235A
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- novel waterproof
- modified coating
- waterproof corrosion
- corrosion modified
- coating
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D195/00—Coating compositions based on bituminous materials, e.g. asphalt, tar, pitch
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/08—Anti-corrosive paints
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
Abstract
The invention provides a kind of novel Waterproof corrosion modified coating and the preparation of this novel Waterproof corrosion modified coating and application process.Novel Waterproof corrosion modified coating the most of the present invention, including fluorine-containing epoxy resin, Oleum Verniciae fordii, Colophonium, dimethylbenzene, butylene phthalate, nano titanium oxide, barium sulfate, zinc oxide, copper chloride, Pulvis Talci and gasoline.Novel Waterproof corrosion modified coating of the present invention, its component is reasonable, and water-fast, wearability, the weatherability of coating and rotproofness are excellent, and product stability is good.The preparation method of novel Waterproof corrosion modified coating of the present invention, simple for process, production efficiency is high, and application cost is low, simple to operate, be easily achieved, the constant product quality of production, and application is convenient, and adaptability is good, has higher application value.
Description
Technical field
The invention belongs to paint production field, in particular it relates to a kind of novel Waterproof corrosion modified coating, and this is novel
The preparation method and application method of Waterproof corrosion modified coating.
Background technology
Paint, in general, it is simply that coated article surface can be coated in and the continuous film of firm attachment can be formed
Material, the most traditional coating products with natural materials as raw material, or in modern development to synthesize chemical products
For the coating products of raw material, broadly falling into organic chemical industry's macromolecular material, the film formed belongs to macromolecular compound type, presses
According to the classification of the chemical products that the modern times pass through, coating belongs to fine chemical product, and it is many that modern coating the most progressively becomes a class
Functional engineering material, is an important industry in chemical industry.
For many special equipments or be applied to special harshness corrosive environment in appliance arrangement, the corrosion resistant to coating
Erosion, the performance requirement such as waterproof, weather-proof, wear-resisting are high.Common coating of the prior art is difficult to meet requirement, therefore, is badly in need of wanting
A kind of corrosion resistant coating, is suitable under the use environment of harshness applying.
Summary of the invention
Goal of the invention: in order to overcome above deficiency, the invention provides a kind of novel Waterproof corrosion modified coating and this is novel
The preparation of Waterproof corrosion modified coating and application process.
Technical scheme: in order to overcome the deficiencies in the prior art, the invention provides a kind of novel Waterproof corrosion and changes
Property coating, by weight part, including following components:
Fluorine-containing epoxy resin 20-35 part
Oleum Verniciae fordii 15-30 part
Colophonium 40-60 part
Dimethylbenzene 30-70 part
Butylene phthalate 2-5 part
Nano titanium oxide 0.5-1.2 part
Barium sulfate 2-12 part
Zinc oxide 4-16 part
Copper chloride 8-14 part
Pulvis Talci 3-8 part
Gasoline 40-60 part.
Novel Waterproof corrosion modified coating of the present invention, its component is reasonable, and product stability is good.Coating water-fast,
Wearability, weatherability and rotproofness are excellent, for the anticorrosion of chemical industry equipment and pipeline etc., are producing ammonia, sulfur dioxide, three oxidations
During the chemicals such as sulfur, nitrogen oxide, the antisepsis of equipment is become apparent from.Wherein epoxy resin is as the gluing in coating
Agent, to metal with nonmetal be respectively provided with good bonding force, makes coating have excellent water proofing property, resistance to soiling, thermostability, insulation
Property, hardness and pliability.Oleum Verniciae fordii oil film is dried rapidly, firm does not glues, can water-fast, alkaline-resisting, fast light and atmospheric corrosion resistance, simultaneously its
Also as preservative and solvent.Additionally, Colophonium is as preservative, adhesive, and butylene phthalate is as plasticizer, and
Nano titanium oxide filling epoxy resin, can be effectively improved the wearability of coating, hot strength and anti-swelling, and product is steady
Qualitative good.
Further, above-mentioned novel Waterproof corrosion modified coating, described Colophonium is asphalt.Asphalt has excellent
Good cementability, water-resistance and anti-corrosive properties, as preservative, adhesive, it is ensured that the stable performance of coating.
Further, above-mentioned novel Waterproof corrosion modified coating, described gasoline is No. 120 industrial napthas.Industrial naptha
Low without lead tetraethyl, sulfur content, it is ensured that the quality of modified coating.
The present invention also provides for the preparation method of a kind of novel Waterproof corrosion modified coating, comprises the steps:
(1) by 2,4-diisocyanate joins in reactor, drips ten difluoro enanthol, with 1 DEG C/min under the conditions of 40-80 DEG C
Speed be warming up to 85 DEG C, and react 1.5-3h；
(2) instill epoxy resin, be warming up to 100-120 DEG C with the speed of 1 DEG C/min, and react 1.5-3h；
(3) described fluorine-containing epoxy resin is cooled down to obtain；
(4) fluorine-containing epoxy resin and Oleum Verniciae fordii are joined in reactor, are warming up to 150-180 DEG C, stir, be dehydrated after add nanometer
Titanium dioxide, barium sulfate, zinc oxide, copper chloride and Pulvis Talci stirring 30-60min；
(5) adding Colophonium after being warming up to 220-260 DEG C, stirring is also warming up to 280 DEG C with the speed of 2 DEG C/min, adds adjacent benzene two
Formic acid fourth diester, after stirring and evenly mixing, stops heating；
(6) temperature is down to 70-90 DEG C, adds dimethylbenzene and stirs, adds gasoline, stir；
(7) through 100-150 mesh sieve, described novel Waterproof corrosion modified coating is obtained.
The preparation method of novel Waterproof corrosion modified coating of the present invention, simple for process, production efficiency is high, should
By low cost, simple to operate, be easily achieved.Wherein with fluorine-containing epoxy resin, Oleum Verniciae fordii, Colophonium, dimethylbenzene, phthalic acid fourth two
The raw material such as ester, gasoline, blended, heat, the modulation of the operation such as dissolving forms, have resistance to water, chemical-resistant, corrosion resistance with
And the advantage such as adhesion property is excellent.
Further, the preparation method of above-mentioned novel Waterproof corrosion modified coating, described nano titanium oxide, sulphuric acid
Barium, zinc oxide, copper chloride and Pulvis Talci use front grind into powder, and through 100-150 mesh sieve.Ensure the coating property of preparation
Stable, quality is high.
Further, the preparation method of above-mentioned novel Waterproof corrosion modified coating, described nano titanium oxide, sulphuric acid
Grind into powder in dispersion machine or three-roller put into by barium, zinc oxide, copper chloride and Pulvis Talci.Good crushing effect, efficiency is high.
Further, the preparation method of above-mentioned novel Waterproof corrosion modified coating, the rotating speed of described stirring is 2500-
2800r/min.The high-speed stirred of 2500-2800r/min is easily achieved, and makes material stirring uniform simultaneously.
The present invention also provides for the application process of a kind of novel Waterproof corrosion modified coating, before application, is cleaned up in painting face,
Remove surface and oil contaminant；During application, add the benzene dimethylamine of described novel Waterproof corrosion modified coating 3-7%, brush after mix homogeneously
Or spraying or roller coating 2-3 time.Using method is simple, convenient, benzene dimethylamine firming agent, and solidification is rapidly and solidification effect is good.
Beneficial effect: compared with prior art, the invention have the advantages that novel Waterproof corrosion of the present invention changes
Property coating, product is water-fast, wearability, weatherability and rotproofness is good and stability is high.Novel Waterproof corrosion of the present invention changes
Property coating preparation method, simple for process, production efficiency is high, and application cost is low, simple to operate, be easily achieved, production
Constant product quality, application is convenient, and the compatibility is good, has higher application value.
Detailed description of the invention
The present invention will be further elucidated with by several specific embodiments below, these embodiments simply to illustrate that problem,
It is not a kind of restriction.
Embodiment 1
A kind of novel Waterproof corrosion modified coating, by weight part, including following components:
Fluorine-containing epoxy resin 20 parts
Oleum Verniciae fordii 15 parts
40 parts of asphalt
Dimethylbenzene 30 parts
Butylene phthalate 2 parts
Nano titanium oxide 0.5 part
2 parts of barium sulfate
Zinc oxide 4 parts
Copper chloride 8 parts
Pulvis Talci 3 parts
No. 120 industrial napthas 40 parts.
The preparation method of above-mentioned novel Waterproof corrosion modified coating, comprises the steps:
(1) by 2,4-diisocyanate joins in reactor, drips ten difluoro enanthol, with 1 DEG C/min's under the conditions of 40 DEG C
Speed is warming up to 85 DEG C, and reacts 1.5h；
(2) instill epoxy resin, be warming up to 100 DEG C with the speed of 1 DEG C/min, and react 1.5h；
(3) described fluorine-containing epoxy resin is cooled down to obtain；
(4) fluorine-containing epoxy resin and Oleum Verniciae fordii are joined in reactor, are warming up to 150 DEG C, stir, be dehydrated after add be dispersed through machine
Middle grind into powder through nano titanium oxide, barium sulfate, zinc oxide, copper chloride and the Pulvis Talci of 100 mesh sieves, with
The mixing speed stirring 30min of 2500r/min；
(5) adding Colophonium after being warming up to 220 DEG C, stirring is also warming up to 280 DEG C with the speed of 2 DEG C/min, adds phthalic acid
Fourth diester, after the mixing speed stirring and evenly mixing of 2500r/min, stops heating；
(6) temperature is down to 70 DEG C, adds dimethylbenzene, stirs with the mixing speed of 2500r/min, add gasoline, stirring
Uniformly；
(7) through 100 mesh sieves, described novel Waterproof corrosion modified coating is obtained.
The application process of above-mentioned novel Waterproof corrosion modified coating, before application, cleans up painting face, removes surface oil
Dirty；During application, add the benzene dimethylamine of described novel Waterproof corrosion modified coating 3%, brush 2 times after mix homogeneously.
Embodiment 2
A kind of novel Waterproof corrosion modified coating, by weight part, including following components:
Fluorine-containing epoxy resin 35 parts
Oleum Verniciae fordii 30 parts
60 parts of asphalt
Dimethylbenzene 70 parts
Butylene phthalate 5 parts
Nano titanium oxide 1.2 parts
12 parts of barium sulfate
Zinc oxide 16 parts
Copper chloride 14 parts
Pulvis Talci 8 parts
No. 120 industrial napthas 60 parts.
The preparation method of above-mentioned novel Waterproof corrosion modified coating, comprises the steps:
(1) by 2,4-diisocyanate joins in reactor, drips ten difluoro enanthol, with 1 DEG C/min's under the conditions of 80 DEG C
Speed is warming up to 85 DEG C, and reacts 3h；
(2) instill epoxy resin, be warming up to 120 DEG C with the speed of 1 DEG C/min, and react 3h；
(3) described fluorine-containing epoxy resin is cooled down to obtain；
(4) fluorine-containing epoxy resin and Oleum Verniciae fordii are joined in reactor, are warming up to 180 DEG C, stir, be dehydrated after add through three-roller
Middle grind into powder through nano titanium oxide, barium sulfate, zinc oxide, copper chloride and the Pulvis Talci of 150 mesh sieves, with
The mixing speed stirring 60min of 2800r/min；
(5) adding Colophonium after being warming up to 260 DEG C, stirring is also warming up to 280 DEG C with the speed of 2 DEG C/min, adds phthalic acid
Fourth diester, after the mixing speed stirring and evenly mixing of 2800r/min, stops heating；
(6) temperature is down to 90 DEG C, adds dimethylbenzene, stirs with the mixing speed of 2800r/min, add gasoline, stirring
Uniformly；
(7) through 150 mesh sieves, described novel Waterproof corrosion modified coating is obtained.
The application process of above-mentioned novel Waterproof corrosion modified coating, before application, cleans up painting face, removes surface oil
Dirty；During application, add the benzene dimethylamine of described novel Waterproof corrosion modified coating 7%, spray 3 times after mix homogeneously.
Embodiment 3
A kind of novel Waterproof corrosion modified coating, by weight part, including following components:
Fluorine-containing epoxy resin 30 parts
Oleum Verniciae fordii 18 parts
50 parts of asphalt
Dimethylbenzene 50 parts
Butylene phthalate 3 parts
Nano titanium oxide 0.9 part
5 parts of barium sulfate
Zinc oxide 10 parts
Copper chloride 12 parts
Pulvis Talci 5 parts
No. 120 industrial napthas 50 parts.
The preparation method of above-mentioned novel Waterproof corrosion modified coating, comprises the steps:
(1) by 2,4-diisocyanate joins in reactor, drips ten difluoro enanthol, with 1 DEG C/min's under the conditions of 60 DEG C
Speed is warming up to 85 DEG C, and reacts 2h；
(2) instill epoxy resin, be warming up to 110 DEG C with the speed of 1 DEG C/min, and react 2h；
(3) described fluorine-containing epoxy resin is cooled down to obtain；
(4) fluorine-containing epoxy resin and Oleum Verniciae fordii are joined in reactor, are warming up to 160 DEG C, stir, be dehydrated after add through three-roller
Middle grind into powder through nano titanium oxide, barium sulfate, zinc oxide, copper chloride and the Pulvis Talci of 120 mesh sieves, with
The mixing speed stirring 40min of 2600r/min；
(5) adding Colophonium after being warming up to 250 DEG C, stirring is also warming up to 280 DEG C with the speed of 2 DEG C/min, adds phthalic acid
Fourth diester, after the mixing speed stirring and evenly mixing of 2600r/min, stops heating；
(6) temperature is down to 80 DEG C, adds dimethylbenzene, stirs with the mixing speed of 2600r/min, add gasoline, stirring
Uniformly；
(7) through 120 mesh sieves, described novel Waterproof corrosion modified coating is obtained.
The application process of above-mentioned novel Waterproof corrosion modified coating, before application, cleans up painting face, removes surface oil
Dirty；During application, add the benzene dimethylamine of described novel Waterproof corrosion modified coating 5%, roller coating 2 times after mix homogeneously.
Embodiment 4
A kind of novel Waterproof corrosion modified coating, by weight part, including following components:
Fluorine-containing epoxy resin 35 parts
Oleum Verniciae fordii 30 parts
45 parts of asphalt
Dimethylbenzene 55 parts
Butylene phthalate 2 parts
Nano titanium oxide 0.5 part
12 parts of barium sulfate
Zinc oxide 16 parts
Copper chloride 8 parts
Pulvis Talci 5 parts
No. 120 industrial napthas 40 parts.
The preparation method of above-mentioned novel Waterproof corrosion modified coating, comprises the steps:
(1) by 2,4-diisocyanate joins in reactor, drips ten difluoro enanthol, with 1 DEG C/min's under the conditions of 70 DEG C
Speed is warming up to 85 DEG C, and reacts 1.5h；
(2) instill epoxy resin, be warming up to 120 DEG C with the speed of 1 DEG C/min, and react 3h；
(3) described fluorine-containing epoxy resin is cooled down to obtain；
(4) fluorine-containing epoxy resin and Oleum Verniciae fordii are joined in reactor, are warming up to 150 DEG C, stir, be dehydrated after add dispersion machine or
Grind into powder nano titanium oxide, barium sulfate, zinc oxide, copper chloride and Pulvis Talci through 150 mesh sieves in three-roller,
50min is stirred with the mixing speed of 2800r/min；
(5) adding Colophonium after being warming up to 220 DEG C, stirring is also warming up to 280 DEG C with the speed of 2 DEG C/min, adds phthalic acid
Fourth diester, after the mixing speed stirring and evenly mixing of 2800r/min, stops heating；
(6) temperature is down to 70 DEG C, adds dimethylbenzene, stirs with the mixing speed of 2800r/min, add gasoline, stirring
Uniformly；
(7) through 150 mesh sieves, described novel Waterproof corrosion modified coating is obtained.
The application process of above-mentioned novel Waterproof corrosion modified coating, before application, cleans up painting face, removes surface oil
Dirty；During application, add the benzene dimethylamine of described novel Waterproof corrosion modified coating 4%, brush after mix homogeneously or spray or roller coating
3 times.
The above is only several embodiments of invention, it is noted that for those skilled in the art
For, on the premise of without departing from inventive principle, it is also possible to make some improvement, these improve the protection that also should be regarded as the present invention
Scope.
Claims (8)
1. a novel Waterproof corrosion modified coating, it is characterised in that: by weight part, including following components:
Fluorine-containing epoxy resin 20-35 part
Oleum Verniciae fordii 15-30 part
Colophonium 40-60 part
Dimethylbenzene 30-70 part
Butylene phthalate 2-5 part
Nano titanium oxide 0.5-1.2 part
Barium sulfate 2-12 part
Zinc oxide 4-16 part
Copper chloride 8-14 part
Pulvis Talci 3-8 part
Gasoline 40-60 part.
Novel Waterproof corrosion modified coating the most according to claim 1, it is characterised in that: described Colophonium is asphalt.
Novel Waterproof corrosion modified coating the most according to claim 1, it is characterised in that: described gasoline is No. 120 solvents
Gasoline.
4. the preparation method of the novel Waterproof corrosion modified coating as described in any one of claim 1-3, it is characterised in that:
Comprise the steps:
(1) by 2,4-diisocyanate joins in reactor, drips ten difluoro enanthol, with 1 DEG C/min under the conditions of 40-80 DEG C
Speed be warming up to 85 DEG C, and react 1.5-3h；
(2) instill epoxy resin, be warming up to 100-120 DEG C with the speed of 1 DEG C/min, and react 1.5-3h；
(3) described fluorine-containing epoxy resin is cooled down to obtain；
(4) fluorine-containing epoxy resin and Oleum Verniciae fordii are joined in reactor, are warming up to 150-180 DEG C, stir, be dehydrated after add nanometer
Titanium dioxide, barium sulfate, zinc oxide, copper chloride and Pulvis Talci stirring 30-60min；
(5) adding Colophonium after being warming up to 220-260 DEG C, stirring is also warming up to 280 DEG C with the speed of 2 DEG C/min, adds adjacent benzene two
Formic acid fourth diester, after stirring and evenly mixing, stops heating；
(6) temperature is down to 70-90 DEG C, adds dimethylbenzene and stirs, adds gasoline, stir；
(7) through 100-150 mesh sieve, described novel Waterproof corrosion modified coating is obtained.
The preparation method of novel Waterproof corrosion modified coating the most according to claim 4, it is characterised in that: described nanometer two
Titanium oxide, barium sulfate, zinc oxide, copper chloride and Pulvis Talci use front grind into powder, and through 100-150 mesh sieve.
The preparation method of novel Waterproof corrosion modified coating the most according to claim 4, it is characterised in that: described nanometer two
Grind into powder in dispersion machine or three-roller put into by titanium oxide, barium sulfate, zinc oxide, copper chloride and Pulvis Talci.
The preparation method of novel Waterproof corrosion modified coating the most according to claim 4, it is characterised in that: described stirring
Rotating speed is 2500-2800r/min.
8. the application process of the novel Waterproof corrosion modified coating as described in claim 1 or 4, it is characterised in that: application
Before, painting face is cleaned up, removes surface and oil contaminant；During application, add the benzene two of described novel Waterproof corrosion modified coating 3-7%
Methylamine, brushes after mix homogeneously or sprays or roller coating 2-3 time.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201610553301.6A CN106085235A (en) | 2016-07-14 | 2016-07-14 | A kind of novel Waterproof corrosion modified coating and preparation thereof and application process |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610553301.6A CN106085235A (en) | 2016-07-14 | 2016-07-14 | A kind of novel Waterproof corrosion modified coating and preparation thereof and application process |
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| CN109135503A (en) * | 2018-07-12 | 2019-01-04 | 山东联星能源集团有限公司 | A kind of stone protectant of containing graphene and tourmaline |
| CN110746855A (en) * | 2019-11-18 | 2020-02-04 | 樊福生 | Wall coating and preparation method thereof |
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| CN110746855A (en) * | 2019-11-18 | 2020-02-04 | 樊福生 | Wall coating and preparation method thereof |
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Application publication date: 20161109 |