CN106046937A - Drying-resistant calligraphic ink and preparation method thereof - Google Patents

Drying-resistant calligraphic ink and preparation method thereof Download PDF

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Publication number
CN106046937A
CN106046937A CN201610517581.5A CN201610517581A CN106046937A CN 106046937 A CN106046937 A CN 106046937A CN 201610517581 A CN201610517581 A CN 201610517581A CN 106046937 A CN106046937 A CN 106046937A
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CN
China
Prior art keywords
ink
prepared chinese
chinese ink
dry
difficult
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Pending
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CN201610517581.5A
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Chinese (zh)
Inventor
叶文佳
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Individual
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Individual
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Priority to CN201610517581.5A priority Critical patent/CN106046937A/en
Publication of CN106046937A publication Critical patent/CN106046937A/en
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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00Inks
    • C09D11/16Writing inks
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00Inks
    • C09D11/16Writing inks
    • C09D11/17Writing inks characterised by colouring agents

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Inks, Pencil-Leads, Or Crayons (AREA)

Abstract

The invention relates to the ink field, in particular to drying-resistant calligraphic ink and a preparation method thereof. The drying-resistant calligraphic ink comprises the following components in percent by weight: 4.6-8.1% of Alpha-naphtholbenzein, 0.23-0.67% of 3,4,5-trihydroxybenzoic acid, 1.1-3.2% of tannic acid, 7.8-17% of ethanol, 0.1-0.8% of xanthan, 0.1-0.2% of ferrous sulfate, 0.02-0.07% of a surfactant, 0.01-0.03% of glycerol, and 78.0-86.0% of distilled water; the preparation method of the ink comprises the following steps: 1), adding the tannic acid and ethanol into water, and stirring for dissolving; 2), adding Alpha-naphtholbenzein and 3,4,5-trihydroxybenzoic acid, and stirring; 3), mixing xanthan mother liquid and ferrous sulfate mother liquid, adding the surfactant and glycerol, and stirring. The preparation method of the ink is simple, the ink is low in cost and free of toxic and irritating smell, and the glycerol is used as a moisture absorbent in the ink so that the ink is kept moist at a nib and interruption of the ink due to drying rarely occurs.

Description

A kind of it is difficult to dry and hard calligraphy prepared Chinese ink and preparation method thereof
Technical field
The present invention relates to prepared Chinese ink field, a kind of be difficult to dry and hard calligraphy prepared Chinese ink and preparation method thereof.
Background technology
Brush pen, is a kind of traditional writing implement coming from China, is increasingly becoming traditional drawing instrument.Peculiar as China A traditional art, Writing brush calligraphy can improve overall mastery, supports noble spirit, long-pending erudite just obtains world intelligence, receives all things on earth Essence, my concentric big border of wound thing.
In order to carry forward chinese tradition art, from 2011, the Ministry of Education began one's study and arranges middle and primary schools' calligraphy education course, And formally having put into effect " middle and primary schools' calligraphy education guiding outlines " in February, 2013, it is desired to each school to open from primary school's Third school grade If special Writing brush calligraphy class, it can be seen that Writing brush calligraphy is in the critical role of China.But, owing to traditional calligraphy prepared Chinese ink can not The shortcoming of degraded, the paper write is not easily recycled utilization, accidentally drips the ink blok spattering on medicated clothing and cleans difficulty greatly, and writes During produce a large amount of waste water, thus cause the huge wasting of resources and environmental pollution.
Summary of the invention
In order to make up the deficiencies in the prior art, the invention provides and a kind of be difficult to dry and hard calligraphy prepared Chinese ink and preparation side thereof Method, this prepared Chinese ink production technology is simple, and in prepared Chinese ink lovely luster, writing process, prepared Chinese ink is difficult to dry and astringent disconnected ink.
The technical solution adopted for the present invention to solve the technical problems is: a kind of be difficult to dry and hard calligraphy prepared Chinese ink, and component is pressed Percentage by weight meter includes:
Preferably, containing appropriate amount of essence in described component.
Preferably, described surfactant is dodecylbenzene sodium sulfonate, sodium lauryl sulphate or dodecyl sodium sulfonate Sodium.
A kind of preparation method being difficult to dry and hard calligraphy prepared Chinese ink, comprises the steps: by said components weight proportion,
1) tannic acid, ethanol are added to the water, make it be completely dissolved by stirring;
2) then alpha-Naphthol phenyl methanol, 3,4,5 trihydroxybenzoic acids are added thereto, stirring, complete chromogenic reaction;
3) xanthan gum mother solution and the ferrous sulfate mother solution of 1% of 1% are configured;By the amount of regulation by xanthan gum mother solution and sulphuric acid Ferrous mother solution mixing, adds surfactant, glycerol, is sufficiently stirred for making solution mix homogeneously, i.e. makes the calligraphy that can fade Exercise prepared Chinese ink.
Beneficial effect: this prepared Chinese ink preparation method is simple, with low cost.Abnormal smells from the patient nontoxic, non-stimulated, environmentally safe.Make For calligraphy prepared Chinese ink, this prepared Chinese ink and the feature having chance water bleeding, easily removing, the paper write easily recycles, meanwhile, sweet Oil is used as hygroscopic agent in the ink, makes ink keep moistening on nib, is difficult to dry and hard disconnected ink.
Detailed description of the invention
For the technological means making the present invention realize, creation characteristic, reach purpose and be easy to understand with effect, below knot Close embodiment, the present invention is expanded on further.
A kind of being difficult to dry and hard calligraphy prepared Chinese ink, component includes by weight percentage:
Preferably, containing appropriate amount of essence in described component.
Preferably, described surfactant is dodecylbenzene sodium sulfonate, sodium lauryl sulphate or dodecyl sodium sulfonate Sodium.
A kind of preparation method being difficult to dry and hard calligraphy prepared Chinese ink, comprises the steps: by said components weight proportion,
1) tannic acid, ethanol are added to the water, make it be completely dissolved by stirring;
2) then alpha-Naphthol phenyl methanol, 3,4,5 trihydroxybenzoic acids are added thereto, stirring, complete chromogenic reaction;
3) xanthan gum mother solution and the ferrous sulfate mother solution of 1% of 1% are configured;By the amount of regulation by xanthan gum mother solution and sulphuric acid Ferrous mother solution mixing, adds surfactant, glycerol, is sufficiently stirred for making solution mix homogeneously, i.e. makes the calligraphy that can fade Exercise prepared Chinese ink.
The ultimate principle of the present invention, principal character and advantage have more than been shown and described.The technical staff of the industry should Understanding, the present invention is not restricted to the described embodiments, the simply explanation present invention's of the description in above-described embodiment and description Principle, without departing from the spirit and scope of the present invention, the present invention also has various changes and modifications, and these change and change Enter to both fall within scope of the claimed invention.Claimed scope is by appended claims and equivalent circle thereof Fixed.

Claims (4)

1. one kind is difficult to dry and hard calligraphy prepared Chinese ink, it is characterised in that: component includes by weight percentage:
A kind of it is difficult to dry and hard calligraphy prepared Chinese ink, it is characterised in that: containing appropriate in described component Essence.
A kind of it is difficult to dry and hard calligraphy prepared Chinese ink, it is characterised in that: described surfactant is Dodecylbenzene sodium sulfonate, sodium lauryl sulphate or dodecyl sodium sulfate.
4. the preparation method being difficult to dry and hard calligraphy prepared Chinese ink, it is characterised in that: comprise the steps: by claim 1 institute State composition weight proportioning,
1) tannic acid, ethanol are added to the water, make it be completely dissolved by stirring;
2) then alpha-Naphthol phenyl methanol, 3,4,5 trihydroxybenzoic acids are added thereto, stirring, complete chromogenic reaction;
3) xanthan gum mother solution and the ferrous sulfate mother solution of 1% of 1% are configured;By the amount of regulation by xanthan gum mother solution and ferrous sulfate Mother solution mixes, and adds surfactant, glycerol, is sufficiently stirred for making solution mix homogeneously, i.e. makes the drills to improve one's handwriting that can fade Prepared Chinese ink.
CN201610517581.5A 2016-06-30 2016-06-30 Drying-resistant calligraphic ink and preparation method thereof Pending CN106046937A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610517581.5A CN106046937A (en) 2016-06-30 2016-06-30 Drying-resistant calligraphic ink and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610517581.5A CN106046937A (en) 2016-06-30 2016-06-30 Drying-resistant calligraphic ink and preparation method thereof

Publications (1)

Publication Number Publication Date
CN106046937A true CN106046937A (en) 2016-10-26

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610517581.5A Pending CN106046937A (en) 2016-06-30 2016-06-30 Drying-resistant calligraphic ink and preparation method thereof

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CN (1) CN106046937A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106009916A (en) * 2016-06-30 2016-10-12 叶文佳 Anti-dry calligraphy ink

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2006117880A (en) * 2004-10-25 2006-05-11 Pilot Ink Co Ltd Water-based ink composition for writing utensil and writing utensil using the same
CN105504985A (en) * 2016-01-06 2016-04-20 山西大学 Fadable calligraphy training ink and preparation method thereof
CN106009916A (en) * 2016-06-30 2016-10-12 叶文佳 Anti-dry calligraphy ink

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2006117880A (en) * 2004-10-25 2006-05-11 Pilot Ink Co Ltd Water-based ink composition for writing utensil and writing utensil using the same
CN105504985A (en) * 2016-01-06 2016-04-20 山西大学 Fadable calligraphy training ink and preparation method thereof
CN106009916A (en) * 2016-06-30 2016-10-12 叶文佳 Anti-dry calligraphy ink

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
齐浩然: "《迷幻的化学》", 31 May 2015, 金盾出版社 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106009916A (en) * 2016-06-30 2016-10-12 叶文佳 Anti-dry calligraphy ink

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Application publication date: 20161026