CN106046543A - PP wood-plastic ground heating floor material and preparation method thereof - Google Patents

PP wood-plastic ground heating floor material and preparation method thereof Download PDF

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Publication number
CN106046543A
CN106046543A CN201610501641.4A CN201610501641A CN106046543A CN 106046543 A CN106046543 A CN 106046543A CN 201610501641 A CN201610501641 A CN 201610501641A CN 106046543 A CN106046543 A CN 106046543A
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China
Prior art keywords
wood
parts
ground heating
heating floor
floor material
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Pending
Application number
CN201610501641.4A
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Chinese (zh)
Inventor
王眈眈
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Wuhu Sandao Material Technology Co Ltd
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Wuhu Sandao Material Technology Co Ltd
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Publication date
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Priority to CN201610501641.4A priority Critical patent/CN106046543A/en
Publication of CN106046543A publication Critical patent/CN106046543A/en
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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L23/00—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
    • C08L23/02—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers not modified by chemical after-treatment
    • C08L23/10—Homopolymers or copolymers of propene
    • C08L23/12—Polypropene
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C48/00—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor
    • B29C48/25—Component parts, details or accessories; Auxiliary operations
    • B29C48/92—Measuring, controlling or regulating
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C2948/00—Indexing scheme relating to extrusion moulding
    • B29C2948/92—Measuring, controlling or regulating
    • B29C2948/92504—Controlled parameter
    • B29C2948/92704—Temperature
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2201/00—Properties
    • C08L2201/08—Stabilised against heat, light or radiation or oxydation
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00—Polymer mixtures characterised by other features
    • C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00—Polymer mixtures characterised by other features
    • C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Floor Finish (AREA)

Abstract

The invention provides a PP wood-plastic ground heating floor material and a preparation method thereof. The PP wood-plastic ground heating floor material is mainly prepared from the following raw materials: 100 parts of PP resin powder, 55-80 parts of poplar powder of 80 meshes, 40-60 parts of Al(OH)3, 5-6 parts of a silane coupling agent, 2-3 parts of barium stearate, 1.5-3 parts of zinc borate, 0.5-1.5 parts of an antioxidant, 0.2-0.5 part of acrylic acid (AA), 0.2-0.5 part of titanium dioxide and 1-2 parts of polyethylene wax. The invention further provides a preparation method of the PP wood-plastic ground heating floor material. With the combination of the formula and the preparation method, the problems that a conventional floor heating plate which is made of a wood-plastic material is generally poor in mechanical properties, thermal resistance and aging resistance can be solved.

Description

Ground heating floor material and preparation method thereof moulded by a kind of PP wood
Technical field
The invention belongs to heating materials technical field, be specifically related to a kind of PP wood and mould ground heating floor material and preparation side thereof Method.
Background technology
Ground heating floor refers to be applicable to the floor of low temperature hydraulic floor heating (abbreviation floor heating).Need to possess good breathability And while heat sinking function, possess thermostability and the feature of environmental protection.Ground heating floor optimal pavement material at present is solid wooden compound floor, but This floor needs to use a large amount of adhesive and paint in process of production, and both materials can discharge a large amount of formaldehyde.Current is general Although the floor that wooden supporter moulding material makes accomplished content of formaldehyde far below Standard, but when using as ground heating floor its Mechanical property, heat resistance, resistance to ag(e)ing all have problems.
Summary of the invention
The technical problem to be solved is to provide a kind of PP wood to mould ground heating floor material and preparation method thereof, energy Enough solving the floor heating floor that current Wood-plastic material makes, mechanical property, heat resistance and resistance to ag(e)ing are the most poor Problem.
In the present invention, " consumption ", " part " are all quality criterias, and the amount of each component is all on the basis of 100 parts of PP resins.
For solving above-mentioned existing technical problem, the present invention uses following scheme:
Ground heating floor material moulded by a kind of PP wood, mainly includes that following raw material is made: PP resin-oatmeal 100 parts, 80 mesh Poplar Powders 55-80 part, Al (OH)3 40-60 part, silane coupler 5-6 part, barium stearate 2-3 part, Firebrake ZB 1.5-3 part, antioxidant 0.5-1.5 part, acrylic acid (AA) 0.2-0.5 part, titanium dioxide 0.2-0.5, Tissuemat E 1-2 part.
As preferably, described 80 mesh Poplar Powder water content ＜ 2wt%.
As preferably, described antioxidant uses antioxidant 1076, and it is mainly composed of β-(3,5-di-t-butyl-4-hydroxyls Base phenyl)-propanoic acid positive octadecanol ester.
The preparation method of ground heating floor material moulded by this PP wood, comprises the following steps:
(1) according to proportioning raw materials, PP resin-oatmeal, 80 mesh Poplar Powders, silane coupler, barium stearate are added in blender mixed Closing, rotating speed is 450 revs/min, and the time is 8-10 minute, and temperature is 90 DEG C, obtains mixture standby；
(2) batch mixing step (1) obtained, adds Al (OH)3, Firebrake ZB, antioxidant, acrylic acid (AA), titanium dioxide, poly-second Alkene wax continues stirring, and rotating speed is 1200 revs/min, and the time is 10-12 minute, and temperature is 115 DEG C, obtains mixture standby；
(3) pelletize is carried out at a temperature of the mixture obtained in step (2) being joined comminutor 130 DEG C, by cold for the pellet obtained But, after, obtain a kind of PP wood and mould ground heating floor material former material granule；
(4) the granular Wood-plastic material obtained in step (3) being passed through extruding production line, extrusion temperature controls at 165 DEG C-185 DEG C Between, ground heating floor material moulded by the PP wood that extruding production line makes different size according to difform mould.
The invention have benefit that: the present invention uses technique scheme to provide a kind of PP wood to mould ground heating floor material And preparation method thereof, it is possible to solve the floor heating floor that current Wood-plastic material makes, mechanical property, heat resistance and resistance to always The problem that the property changed is the most poor.
Detailed description of the invention
The present invention is described in detail, in illustrative examples and the explanation of this present invention below in conjunction with specific embodiment It is used for explaining the present invention, but not as a limitation of the invention.
Embodiment 1
Ground heating floor material moulded by a kind of PP wood, mainly includes that following raw material is made: PP resin-oatmeal 100 parts, 80 mesh Poplar Powders 55 parts, Al (OH)3 40 parts, silane coupler 5 parts, barium stearate 2 parts, Firebrake ZB 1.5 parts, antioxidant 1 part, acrylic acid (AA) 0.2 part, titanium dioxide 0.2, Tissuemat E 1 part；Described 80 mesh Poplar Powder water content ＜ 2wt%；Described antioxidant uses antioxidant 1076, it is mainly composed of β-(3,5-di-tert-butyl-hydroxy phenyl)-propanoic acid positive octadecanol ester.
The preparation method of ground heating floor material moulded by this PP wood, comprises the following steps:
(1) according to proportioning raw materials, PP resin-oatmeal, 80 mesh Poplar Powders, silane coupler, barium stearate are added in blender mixed Closing, rotating speed is 450 revs/min, and the time is 8 minutes, and temperature is 90 DEG C, obtains mixture standby；
(2) batch mixing step (1) obtained, adds Al (OH)3, Firebrake ZB, antioxidant, acrylic acid (AA), titanium dioxide, poly-second Alkene wax continues stirring, and rotating speed is 1200 revs/min, and the time is 10 minutes, and temperature is 115 DEG C, obtains mixture standby；
(3) pelletize is carried out at a temperature of the mixture obtained in step (2) being joined comminutor 130 DEG C, by cold for the pellet obtained But, after, obtain a kind of PP wood and mould ground heating floor material former material granule；
(4) the granular Wood-plastic material obtained in step (3) being passed through extruding production line, extrusion temperature controls at 165 DEG C-185 DEG C Between, ground heating floor material moulded by the PP wood that extruding production line makes different size according to difform mould.
Embodiment 2
Ground heating floor material moulded by a kind of PP wood, mainly includes that following raw material is made: PP resin-oatmeal 100 parts, 80 mesh Poplar Powders 70 parts, Al (OH)3 50 parts, silane coupler 6 parts, barium stearate 2.5 parts, Firebrake ZB 2 parts, antioxidant 1 part, acrylic acid (AA) 0.4 part, titanium dioxide 0.3, Tissuemat E 1.5 parts；Described 80 mesh Poplar Powder water content ＜ 2wt%；Described antioxidant uses antioxygen Agent 1076, it is mainly composed of β-(3,5-di-tert-butyl-hydroxy phenyl)-propanoic acid positive octadecanol ester.
The preparation method of ground heating floor material moulded by this PP wood, comprises the following steps:
(1) according to proportioning raw materials, PP resin-oatmeal, 80 mesh Poplar Powders, silane coupler, barium stearate are added in blender mixed Closing, rotating speed is 450 revs/min, and the time is 9 minutes, and temperature is 90 DEG C, obtains mixture standby；
(2) batch mixing step (1) obtained, adds Al (OH)3, Firebrake ZB, antioxidant, acrylic acid (AA), titanium dioxide, poly-second Alkene wax continues stirring, and rotating speed is 1200 revs/min, and the time is 11 minutes, and temperature is 115 DEG C, obtains mixture standby；
(3) pelletize is carried out at a temperature of the mixture obtained in step (2) being joined comminutor 130 DEG C, by cold for the pellet obtained But, after, obtain a kind of PP wood and mould ground heating floor material former material granule；
(4) the granular Wood-plastic material obtained in step (3) being passed through extruding production line, extrusion temperature controls at 165 DEG C-185 DEG C Between, ground heating floor material moulded by the PP wood that extruding production line makes different size according to difform mould.
Embodiment 3
Ground heating floor material moulded by a kind of PP wood, mainly includes that following raw material is made: PP resin-oatmeal 100 parts, 80 mesh Poplar Powders 80 parts, Al (OH)3 60 parts, silane coupler 6 parts, barium stearate 3 parts, Firebrake ZB 3 parts, antioxidant 1.5 parts, acrylic acid (AA) 0.5 part, titanium dioxide 0.5, Tissuemat E 2 parts；Described 80 mesh Poplar Powder water content ＜ 2wt%；Described antioxidant uses antioxidant 1076, it is mainly composed of β-(3,5-di-tert-butyl-hydroxy phenyl)-propanoic acid positive octadecanol ester.
The preparation method of ground heating floor material moulded by this PP wood, comprises the following steps:
(1) according to proportioning raw materials, PP resin-oatmeal, 80 mesh Poplar Powders, silane coupler, barium stearate are added in blender mixed Closing, rotating speed is 450 revs/min, and the time is 10 minutes, and temperature is 90 DEG C, obtains mixture standby；
(2) batch mixing step (1) obtained, adds Al (OH)3, Firebrake ZB, antioxidant, acrylic acid (AA), titanium dioxide, poly-second Alkene wax continues stirring, and rotating speed is 1200 revs/min, and the time is 12 minutes, and temperature is 115 DEG C, obtains mixture standby；
(3) pelletize is carried out at a temperature of the mixture obtained in step (2) being joined comminutor 130 DEG C, by cold for the pellet obtained But, after, obtain a kind of PP wood and mould ground heating floor material former material granule；
(4) the granular Wood-plastic material obtained in step (3) being passed through extruding production line, extrusion temperature controls at 165 DEG C-185 DEG C Between, ground heating floor material moulded by the PP wood that extruding production line makes different size according to difform mould.
The principle of above-described embodiment only illustrative present invention and effect thereof, not for limiting the present invention.Any ripe Above-described embodiment all can be modified under the spirit and the scope of the present invention or change by the personage knowing this technology.Cause This, have usually intellectual such as complete with institute under technological thought without departing from disclosed spirit in art All equivalences become are modified or change, and must be contained by the claim of the present invention.

Claims (2)

1. ground heating floor material and preparation method thereof moulded by a PP wood, it is characterised in that mainly include that following raw material is made: PP resin-oatmeal 100 parts, 80 mesh Poplar Powder 55-80 parts, Al (OH)3 40-60 part, silane coupler 5-6 part, barium stearate 2-3 part, Firebrake ZB 1.5-3 part, antioxidant 0.5-1.5 part, acrylic acid (AA) 0.2-0.5 part, titanium dioxide 0.2-0.5, Tissuemat E 1-2 Part；Described 80 mesh Poplar Powder water content ＜ 2wt%；Described antioxidant uses antioxidant 1076, and it is mainly composed of β-(3,5- Di-tert-butyl-hydroxy phenyl)-propanoic acid positive octadecanol ester.
The preparation method of ground heating floor material moulded by PP wood the most according to claim 1, it is characterised in that include following step Rapid:
(1) according to proportioning raw materials, PP resin-oatmeal, 80 mesh Poplar Powders, silane coupler, barium stearate are added in blender mixed Closing, rotating speed is 450 revs/min, and the time is 8-10 minute, and temperature is 90 DEG C, obtains mixture standby；
(2) batch mixing step (1) obtained, adds Al (OH)3, Firebrake ZB, antioxidant, acrylic acid (AA), titanium dioxide, poly-second Alkene wax continues stirring, and rotating speed is 1200 revs/min, and the time is 10-12 minute, and temperature is 115 DEG C, obtains mixture standby；
(3) pelletize is carried out at a temperature of the mixture obtained in step (2) being joined comminutor 130 DEG C, by cold for the pellet obtained But, after, obtain a kind of PP wood and mould ground heating floor material former material granule；
(4) the granular Wood-plastic material obtained in step (3) being passed through extruding production line, extrusion temperature controls at 165 DEG C-185 DEG C Between, extruding production line makes the ABS Wood-plastic material of different size according to difform mould.
CN201610501641.4A 2016-06-30 2016-06-30 PP wood-plastic ground heating floor material and preparation method thereof Pending CN106046543A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610501641.4A CN106046543A (en) 2016-06-30 2016-06-30 PP wood-plastic ground heating floor material and preparation method thereof

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Application Number Priority Date Filing Date Title
CN201610501641.4A CN106046543A (en) 2016-06-30 2016-06-30 PP wood-plastic ground heating floor material and preparation method thereof

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Publication Number Publication Date
CN106046543A true CN106046543A (en) 2016-10-26

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110028735A (en) * 2019-04-30 2019-07-19 陈兴权 A kind of preparation method of the ageing-resistant ground heating floor of high strength heat resistant

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102321374A (en) * 2011-07-29 2012-01-18 东北林业大学 Fire-retardant polyolefin based wood plastic composite material and preparation method thereof
CN104631758A (en) * 2015-01-13 2015-05-20 东北林业大学 Wood-plastic composite floor and manufacturing method thereof

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102321374A (en) * 2011-07-29 2012-01-18 东北林业大学 Fire-retardant polyolefin based wood plastic composite material and preparation method thereof
CN104631758A (en) * 2015-01-13 2015-05-20 东北林业大学 Wood-plastic composite floor and manufacturing method thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110028735A (en) * 2019-04-30 2019-07-19 陈兴权 A kind of preparation method of the ageing-resistant ground heating floor of high strength heat resistant

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Application publication date: 20161026