CN106045183A - High salinity wastewater evaporation device - Google Patents
High salinity wastewater evaporation device Download PDFInfo
- Publication number
- CN106045183A CN106045183A CN201610635467.2A CN201610635467A CN106045183A CN 106045183 A CN106045183 A CN 106045183A CN 201610635467 A CN201610635467 A CN 201610635467A CN 106045183 A CN106045183 A CN 106045183A
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- separation chamber
- pump
- condensed
- enters
- tank
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F9/00—Multistage treatment of water, waste water or sewage
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/02—Treatment of water, waste water, or sewage by heating
- C02F1/04—Treatment of water, waste water, or sewage by heating by distillation or evaporation
- C02F1/048—Purification of waste water by evaporation
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/52—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/66—Treatment of water, waste water, or sewage by neutralisation; pH adjustment
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2301/00—General aspects of water treatment
- C02F2301/08—Multistage treatments, e.g. repetition of the same process step under different conditions
Abstract
The invention discloses a high salinity wastewater evaporation device. The device comprises a raw material metering tank, a feeding pump, a condensate liquid heat exchanger, a steam heat exchanger, a forced circulating pump, a vertical type heater, a separation chamber, an overflow pump, a buffer tank, a separation tank, a sedimentation tank, a discharging pump, a suspension separator, a thickener, a centrifuge, a compressor, a steam condensate pot and a vacuum-pumping device. The high salinity wastewater evaporation device realizes economy maximization and energy consumption minimization.
Description
Technical field
The present invention relates to industrial waste water treatment, and in particular to a kind of high-salt wastewater vaporising device.
Background technology
At present, the processing method of the industrial wastewater that the chemical field such as chlor-alkali, papermaking, plating produces mainly includes chemical precipitation
Method, oxidation-reduction method, membrane separation process and ion exchange, but these traditional handicrafts are extremely difficult to the requirement of zero-emission.So-called
Zero-emission, for its content, on the one hand haves no alternative but the waste discharge produced, is reduced in production process to be controlled
Zero;On the other hand the garbage haveing no alternative but discharge is made full use of, finally stop the generation of non-renewable resources and the energy.Zero-emission
Discharge technique is integrated application membrance separation, evaporative crystallization or be dried etc. physics, chemistry, biochemical process, by miscellaneous for the solid in the middle of waste water
Matter is concentrated into very high concentration, and major part water has returned circulating and recovering, and remaining a small amount of water with solid waste can be by steaming
Send out/crystallize, evaporate/be dried, the approach such as waste material absorption processes and recycles, and does not discharge system.
In commercial production in the past frequently with processing method have multiple-effect evaporation after carry out sheeting or mist projection granulating with flaker
It is dried with fluid bed afterwards, but these methods generally require the substantial amounts of steam of consumption, electricity or coal homenergic, production cost
Height, and finally inorganic salt after evaporation is often with water of crystallization, and impurity content is higher, it is difficult to effectively utilize, final discharge
Waste water also is difficult to up to standard.
Industrial processes often contain in the waste water of discharge the inorganic salt of high concentration, particularly nothing in chemical process
With a large amount of inorganic salts produced in machine salt by-product or regulation solution acid alkalinity, inorganic salt in the waste water finally discharged all can be made
Concentration is higher.High-salt wastewater has discharge capacity big, strong toxicity, the feature that intractability is high.
For high salt organic waste water, although through pretreatment and biochemical treatment, but the most still contain a certain amount of
Organic substance, utilize above strong brine evaporation liquid zero emission device or process high-salt wastewater evaporation crystallization equipment to high salt
Waste water is evaporated crystallization, and obtained crystal salt includes substantial amounts of Organic substance, it is difficult to processes further and recycles, can only
Special filling up is carried out as solid waste.As a example by a certain medium-and-large-sized coal chemical industry enterprises, one produces 20 billion cubic meter coal systems per year
The enterprise of natural gas, the solid waste produced per hour is more than 3 tons, based on dangerous solid waste landfill per ton needs 3000 yuan
Calculating, annual landfill expense is 72,000,000 (running based on 8000 hours by annual), and this is for enterprise, can not bear.
Summary of the invention
For solving the problems referred to above, the present invention proposes a kind of high-salt wastewater vaporising device, it is possible to realize economy maximize,
Energy resource consumption minimizes.
For reaching above-mentioned purpose, the present invention proposes a kind of high-salt wastewater vaporising device, including 1, a kind of high-salt wastewater evaporation dress
Put, it is characterised in that including: raw material measuring tank, feed pump, condensed heat transfer fluid device, vapor heat exchanger, forced circulation pump, vertical
Heater, separation chamber, flood pump, buffer tank, knockout drum, stillpot, discharging pump, suspension separator, thickener, centrifuge, pressure
Contracting machine, vapor condensed water tank and vacuum extractor.
Material in raw material measuring tank by feed pump pump into condensed heat transfer fluid device (condensed fluid from system properly functioning time
The condensed fluid that System Heater condenses out, makes full use of system energy, reaches the purpose of energy-saving and emission-reduction), material temperature out
Degree raises more than 30 DEG C;
Material after condensed liquid heat exchanger enters vapor heat exchanger, and thermal source is made a living steam, by raw steam heated material
To evaporating temperature, then material enters forced circulation pump discharge;
Forced circulation pump forced circulation material, by entering separation chamber, two evaporated in separation chamber after standing heater
Secondary steam enters compressor, and material constantly circulates between circulating pump, heater, separation chamber, after indirect steam enters compressor
Standing heater shell side import be connected by compression to standing heater heat supply after being heated up;
At forced circulation pump import department connection pipeline to discharging pump (17) import, when in separation chamber, densimeter shows close to going out
During material strip part, material is pumped into thickener by discharging pump, bypasses out sample tap simultaneously, utilize beaker, graduated cylinder etc. on discharge pipe
Mode samples observation, and to determine whether to reach discharging condition, if not arriving discharging condition, discharging pump bypass is returned separation chamber and continued
Continuous circulating and evaporating.
Discharging pump is up to the material of condition and pumps into suspension separator (18), removes upper strata moisture, enters back into thickener not
Then disconnected stirring flows into centrifuge, realizes pure crystal by centrifuge and is centrifuged out, can directly pack.
Native system runs and all carries out under negative pressure state, and vacuum extractor (6) is essential, efficient vacuum extractor
(6) incoagulable gas is not contained in guaranteeing system, it is ensured that material evaporation is near best efficiency point, and vacuum extractor was running
Cheng Zhonghui produces condensed fluid and flows into vapor condensed water tank (5), and the liquid that standing heater (2) condenses out simultaneously also flows into vapor condensed water tank
(5), water pot serves collection condensed fluid effect, and the condensed fluid of high-quality also pumps into condensed heat transfer fluid device (7) simultaneously, as thermal source
It it is that the material having just enter into system heats, it is provided that heat utilization ratio;
For there being partial suspended thing to separate without pretreatment, this device separation chamber set up special groove for locating
The materials such as reason float, such as resin.Be internally provided with the groove (in Tu Zhong separation chamber at A) of a circle in separation chamber, material is not
Breaking and go out from horn mouth rolling, the continuous overflow of float more than liquid level enters in the groove of the internal circle in separation chamber, work people
Member is observed, when in groove, float opens overflow when being full of groove by multiple visors on distance learners' characteristics and separation chamber's device
Float in groove is pumped out by pump, enters in buffer tank, and after the buffered tank of float, gravity stream enters knockout drum, sinks through secondary
Float behind shallow lake enters in stillpot again, removes insoluble float eventually through the artificial mode salvaged;
In sum, there is advantages that
Improved vertical separation chamber can process the high-salt wastewater containing partial suspended thing;
The repeatedly high efficiency energy saving heat exchanging such as condensed heat transfer fluid device, vapor heat exchanger;
Electric energy inexpensively is converted to heat energy by mechanical recompression, and system under normal operating conditions, need not substantially
External supplementary steam;
Efficient vacuumizing device maintains system to run under vacuum conditions, without on-condensible gas in system;
Float by overflow, pump out, repeatedly the mode system such as natural sedimentation and gravity stream removed;
Material is increased its density by thickener, suspension separator again, eventually through centrifuge discharging crystal, reaches crystallization
Purpose.
Accompanying drawing explanation
Fig. 1 is the process chart of the high-salt wastewater vaporising device of the present invention.
Detailed description of the invention
In order to know more about the technology contents of the present invention, especially exemplified by specific embodiment and coordinate institute's accompanying drawings to be described as follows.
Fig. 1 is the process chart of the high-salt wastewater vaporising device of the present invention.As it is shown in figure 1, high-salt wastewater vaporising device
Including: 1. separation chamber 2. heater 3. compressor 4. forced circulation pump 5. vapor condensed water tank 6. vacuum extractor 7. condensed heat transfer fluid device
8. vapor heat exchanger 9. raw material measuring tank 10.PH regulation tank 11. buffer tank 12. knockout drum 13. stillpot 14. thickener 15. from
Scheming 16. condensate pump 17. discharging pump 18. suspension separator
Material liquid needs to detect pH value before entrance system, if meta-acid or meta-alkali, enters in raw material measuring tank, by gradually
Acid adding or add alkali and stir and regulate pH value and reach neutral degree, subsequently into vapo(u)rization system;If neutrality is then without dosing, directly
Tap into into vapo(u)rization system.
Material in raw material measuring tank by feed pump pump into condensed heat transfer fluid device (condensed fluid from system properly functioning time
The condensed fluid that System Heater condenses out, makes full use of system energy, reaches the purpose of energy-saving and emission-reduction), material temperature out
Degree raises more than 30 DEG C.
Material after condensed liquid heat exchanger enters vapor heat exchanger, and thermal source is made a living steam, by raw steam heated material
To evaporating temperature, then material enters forced circulation pump discharge.
By forced circulation pump forced circulation material, by entering separation chamber after standing heater, evaporate in separation chamber
Indirect steam enter compressor, material constantly circulates between circulating pump, heater, separation chamber, indirect steam enter compression
Heater shell side import be connected by compression to heater heat supply after being heated up after machine.
In separation chamber, material constantly goes out from horn mouth rolling, and the continuous overflow of float more than liquid level enters and separates
In the groove of chamber interior one circle, staff is observed by multiple visors on distance learners' characteristics and separation chamber's device, works as groove
Middle float is opened flood pump and float in groove is pumped out when being full of groove, enter in buffer tank, after the buffered tank of float
Gravity stream enters knockout drum, and the float after secondary precipitation enters in stillpot again, eventually through the artificial mode salvaged
Remove insoluble float.
At forced circulation pump import department connection pipeline to discharging pump import, when in separation chamber, densimeter shows close to going out material strip
During part, material is pumped into thickener by discharging pump, bypasses out sample tap simultaneously, utilize the mode such as beaker, graduated cylinder on discharge pipe
Sampling is observed, and to determine whether to reach discharging condition, if not arriving discharging condition, discharging pump bypass is returned separation chamber and continued to follow
Ring evaporates.
Discharging pump is up to the material of condition and pumps into suspension separator, removes upper strata moisture, enters back into thickener and constantly stir
Mix and then flow into centrifuge, realize pure crystal by centrifuge and be centrifuged out, can directly pack.
In sum, the high-salt wastewater vaporising device of the present invention improves new evaporation on the basis of tradition multiple-effect evaporation
Mode, converts electrical energy into heat energy, maximizes and saves the energy, it is achieved that economy maximizes, energy resource consumption minimizes.
Although the present invention is disclosed above with preferred embodiment, so it is not limited to the present invention.Skill belonging to the present invention
Art field has usually intellectual, without departing from the spirit and scope of the present invention, when being used for a variety of modifications and variations.Cause
This, protection scope of the present invention is when being as the criterion depending on those as defined in claim.
Claims (2)
1. a high-salt wastewater vaporising device, it is characterised in that including: raw material measuring tank, feed pump, condensed heat transfer fluid device, steaming
Vapour heat exchanger, forced circulation pump, standing heater, separation chamber, flood pump, buffer tank, knockout drum, stillpot, discharging pump, suspension
Separator, thickener, centrifuge, compressor, vapor condensed water tank and vacuum extractor.
Material in raw material measuring tank (9) pumps into condensed heat transfer fluid device (7) by feed pump (19), and (condensed fluid is normal from system
The condensed fluid that runtime system heater condenses out, makes full use of system energy, reaches the purpose of energy-saving and emission-reduction), out
Temperature of charge raises more than 30 DEG C;
Material after condensed liquid heat exchanger (7) enters vapor heat exchanger (8), and thermal source is made a living steam, by raw steam heating thing
Material is to evaporating temperature, and then material enters forced circulation pump (4) outlet;
Forced circulation pump (4) forced circulation material, enters separation chamber (1) afterwards by standing heater (2), in separation chamber (1)
The indirect steam of evaporation enters compressor (3), and material constantly circulates between forced circulation pump, heater, separation chamber, and two
Secondary steam connects standing heater shell side import to standing heater heat supply after being heated up by compression after entering compressor;
At forced circulation pump (4) import department connection pipeline to discharging pump (17) import, when in separation chamber (1), densimeter shows close
During discharging condition, material is pumped into thickener (14) by discharging pump (17), bypasses out sample tap on discharge pipe simultaneously, utilizes and burns
The modes such as cup, graduated cylinder sample observation, and to determine whether to reach discharging condition, if not arriving discharging condition, discharging pump (17) bypasses
Return separation chamber (1) to continue cycling through, evaporate;
Discharging pump is up to the material of condition and pumps into suspension separator (18), removes upper strata moisture, enters back into thickener (14) no
Then disconnected stirring flows into centrifuge (15), realizes pure crystal by centrifuge and is centrifuged out, finished product of can directly packing;
Native system runs and all carries out under negative pressure state, and vacuum extractor (6) is essential, efficient vacuum extractor (6)
Condensable gas is not contained, it is ensured that material evaporation is near best efficiency point, and vacuum extractor is at running in guaranteeing system
In can produce condensed fluid flow into vapor condensed water tank (5), the liquid that standing heater (2) condenses out simultaneously also flows into vapor condensed water tank
(5), water pot serves collection condensed fluid effect, and the condensed fluid of high-quality also pumps into condensed heat transfer fluid device (7) simultaneously, as thermal source
It it is that the material having just enter into system heats, it is provided that heat utilization ratio;
For there being partial suspended thing to separate without pretreatment, this device separation chamber set up special groove outstanding for processing
The materials such as float, such as resin.Be internally provided with the groove (in Tu Zhong separation chamber at A) of a circle in separation chamber, material constantly from
Horn mouth rolls and goes out, and the continuous overflow of float more than liquid level enters in the groove of the internal circle in separation chamber, and staff is led to
Cross multiple visors on distance learners' characteristics and separation chamber's device to observe, when in groove, float opens flood pump general when being full of groove
In groove, float pumps out, and enters in buffer tank, and after the buffered tank of float, gravity stream enters knockout drum, after secondary precipitation
Float enter again in stillpot, remove insoluble float eventually through the artificial mode salvaged.
High-salt wastewater vaporising device the most according to claim 1, it is characterised in that also include that PH regulates tank, be connected to
State in raw material measuring tank.
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CN201610635467.2A CN106045183B (en) | 2016-08-04 | 2016-08-04 | A kind of high-salt wastewater vaporising device |
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CN201610635467.2A CN106045183B (en) | 2016-08-04 | 2016-08-04 | A kind of high-salt wastewater vaporising device |
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CN106045183A true CN106045183A (en) | 2016-10-26 |
CN106045183B CN106045183B (en) | 2019-01-08 |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112578017A (en) * | 2020-11-11 | 2021-03-30 | 威海职业学院 | Rapid detection method and detection device for organic matters in high-salinity water |
CN114832424A (en) * | 2022-03-31 | 2022-08-02 | 国家能源集团宁夏煤业有限责任公司 | Crystallization equipment, application thereof and method for preparing large-particle ammonium sulfate crystals |
Citations (3)
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CN104326612A (en) * | 2014-10-24 | 2015-02-04 | 南京科盛环保科技有限公司 | Method and system for recovering salt from waste water treatment system |
CN204973107U (en) * | 2015-07-06 | 2016-01-20 | 江苏德邦工程有限公司 | Industrial waste water's evaporation processing apparatus |
CN105502540A (en) * | 2016-01-27 | 2016-04-20 | 成都锐思环保技术股份有限公司 | Anti-scaling and anti-corrosion desulfurization waste water multi-effect evaporation, concentration and crystallization method |
-
2016
- 2016-08-04 CN CN201610635467.2A patent/CN106045183B/en active Active
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104326612A (en) * | 2014-10-24 | 2015-02-04 | 南京科盛环保科技有限公司 | Method and system for recovering salt from waste water treatment system |
CN204973107U (en) * | 2015-07-06 | 2016-01-20 | 江苏德邦工程有限公司 | Industrial waste water's evaporation processing apparatus |
CN105502540A (en) * | 2016-01-27 | 2016-04-20 | 成都锐思环保技术股份有限公司 | Anti-scaling and anti-corrosion desulfurization waste water multi-effect evaporation, concentration and crystallization method |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112578017A (en) * | 2020-11-11 | 2021-03-30 | 威海职业学院 | Rapid detection method and detection device for organic matters in high-salinity water |
CN114832424A (en) * | 2022-03-31 | 2022-08-02 | 国家能源集团宁夏煤业有限责任公司 | Crystallization equipment, application thereof and method for preparing large-particle ammonium sulfate crystals |
CN114832424B (en) * | 2022-03-31 | 2023-07-25 | 国家能源集团宁夏煤业有限责任公司 | Crystallization equipment and application thereof, and method for preparing large-particle ammonium sulfate crystals |
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