CN106039197A - 草果二十一味丸及其鉴别方法 - Google Patents

草果二十一味丸及其鉴别方法 Download PDF

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CN106039197A
CN106039197A CN201610602124.6A CN201610602124A CN106039197A CN 106039197 A CN106039197 A CN 106039197A CN 201610602124 A CN201610602124 A CN 201610602124A CN 106039197 A CN106039197 A CN 106039197A
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fructus tsaoko
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陶淑霞
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Mongolian Medical Hospital of Fuxin Mongolian Autonomous County
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Fuxin Liaoning Mongolian Medicine Research Institute
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Abstract

本发明公开了草果二十一味丸及其鉴别方法，草果二十一味丸的配方为：草果45‑55g，石膏27‑36g，紫花地丁26‑32g，木鳖子24‑30g，青皮25‑35g，白豆蔻28‑35g，沉香20‑32g，茜草30‑40g，木香25‑35g，麦冬23‑30g，五灵脂26‑32g，石莲子25‑35g，栀子22‑32g，甘松28‑38g，诃子26‑35g，广枣20‑40g，紫檀香28‑32g，血竭26‑32g，西红花27‑36g，麝香5‑15g，三鲜红350‑450g。本发明配伍科学合理；能够健胃健脾，消食消肿，调和“三根”，解毒化瘀，进而养肝造血；对于再生障碍性贫血疗效显著。

Description

草果二十一味丸及其鉴别方法
技术领域
本发明涉及一种中药丸药及其鉴别方法，尤其是草果二十一味丸及其鉴别方法。
背景技术
草果有特异香气，味辛、微苦，是一种调味香料，具有特殊浓郁的辛辣香味。其干燥的果实被用作中餐调味料和中草药。草果辛辣香味能除腥气，增进食欲，是烹调佐料中的佳品，被人们誉为食品调味中的“五香之一”。草果用来烹调菜肴，可去腥除膻，增进菜肴味道，烹制鱼类和肉类时，有了草果其味更佳。草果还具有食疗作用，其味辛，性温；归脾、胃经；芳烈燥散具有燥湿温中，辟秽截疟的功效，主治胸膈痞满、脘腹冷痛、恶心呕吐、泄泻下痢、食积不消、霍乱、瘟疫、瘴疟，还能解酒毒，去口臭。草果还具有较高的药用价值，是药食两用中药材大宗品种之一，食用量大于药用量，主治脘腹胀满、反胃呕吐、食积疟疾等症；好多中成药离不开它的配方，如透骨搜风丸、益肾丸、开郁舒肝丸、宽胸利膈丸、洁白丸等。随着人们生活水平的提高和健康的需要，草果的用途和用量将越来越多。
目前未见有草果为主要成分治疗再生型贫血的中成药的相关文献报道。
发明内容
为解决以上现有难题，本发明公开了草果二十一味丸及其鉴别方法，其方案是这样实现的：
草果二十一味丸的配方为：
草果45-55g，石膏27-36g，紫花地丁26-32g，木鳖子24-30g，青皮25-35g，白豆蔻28-35g，沉香20-32g，茜草30-40g，木香25-35g，麦冬23-30g，五灵脂26-32g，石莲子25-35g，栀子22-32g，甘松28-38g，诃子26-35g，广枣20-40g，紫檀香28-32g，血竭26-32g，西红花27-36g，麝香5-15g，三鲜红350-450g。
进一步的，草果二十一味丸的配方为：
草果48-52g，石膏28-32g，紫花地丁29-31g，木鳖子26-30g，青皮28-33g，白豆蔻29-32g，沉香27-32g，茜草30-35g，木香28-32g，麦冬26-30g，五灵脂28-32g，石莲子28-33g，栀子28-32g，甘松29-33g，诃子28-32g，广枣29-42g，紫檀香29-31g，血竭28-32g，西红花28-33g，麝香8-12g，三鲜红380-420g。
进一步的，草果二十一味丸的配方为：
草果50g，石膏30g，紫花地丁30g，木鳖子30g，青皮30g，白豆蔻30g，沉香30g，茜草30g，木香30g，麦冬30g，五灵脂30g，石莲子30g，栀子30g，甘松30g，诃子30g，广枣30g，紫檀香30g，血竭30g，西红花30g，麝香10g，三鲜红400g。
草果二十一味丸的制备方法为：
以上二十一味药，麝香、西红花、血竭粉碎成细粉；其余草果等十八味粉碎成细粉，与上述细粉配研，过筛，混匀。每100g粉末用炼蜜100g制成大蜜丸，即得。
草果二十一味丸的鉴别方法为：
取本品10g，加硅藻土2g，研匀，加甲醇30ml，超声处理20分钟，过滤后将滤液蒸干，残渣加甲醇1ml使之溶解，作为供试品溶液。另取紫花地丁对照药材1g，同法制成对照药材溶液。照薄层色谱法(中国药典2005年版一部附录VI B)试验，吸取供试品溶液5-10μl、对照药材溶液5μl，分别点于同一以羧甲基纤维素钠为粘合剂的硅胶G薄层板上，以甲苯-乙酸乙酯-甲酸(体积比为5∶3∶1)的上层溶液为展开剂，展开、取出、晾干，置紫外光灯(365nm)下检视。供试品色谱中，在与对照药材色谱相应的位置上，显示相同颜色的荧光斑点。
有益效果：本发明配伍科学合理；能够健胃健脾，消食消肿，调和“三根”，解毒化瘀，进而养肝造血；对于再生障碍性贫血疗效显著。
具体实施方式
结合实施例，对本发明做进一步详细说明。
实施例1
草果二十一味丸及其鉴别方法，其方案是这样实现的：
草果二十一味丸的配方为：
草果45g，石膏27g，紫花地丁26g，木鳖子24g，青皮25g，白豆蔻28g，沉香20g，茜草30g，木香25g，麦冬23g，五灵脂26g，石莲子25g，栀子22g，甘松28g，诃子26g，广枣20g，紫檀香28g，血竭26g，西红花27g，麝香5g，三鲜红350g。
草果二十一味丸的制备方法为：
以上二十一味药，麝香、西红花、血竭粉碎成细粉；其余草果等十八味粉碎成细粉，与上述细粉配研，过筛，混匀。每100g粉末用炼蜜100g制成大蜜丸，即得。
草果二十一味丸的鉴别方法为：
取本品10g，加硅藻土2g，研匀，加甲醇30ml，超声处理20分钟，过滤后将滤液蒸干，残渣加甲醇1ml使之溶解，作为供试品溶液。另取紫花地丁对照药材1g，同法制成对照药材溶液。照薄层色谱法(中国药典2005年版一部附录VI B)试验，吸取供试品溶液5-10μl、对照药材溶液5μl，分别点于同一以羧甲基纤维素钠为粘合剂的硅胶G薄层板上，以甲苯-乙酸乙酯-甲酸(体积比为5∶3∶1)的上层溶液为展开剂，展开、取出、晾干，置紫外光灯(365nm)下检视。供试品色谱中，在与对照药材色谱相应的位置上，显示相同颜色的荧光斑点。
实施例2
草果二十一味丸及其鉴别方法，其方案是这样实现的：
草果二十一味丸的配方为：
草果55g，石膏36g，紫花地丁32g，木鳖子30g，青皮35g，白豆蔻35g，沉香32g，茜草40g，木香35g，麦冬30g，五灵脂32g，石莲子35g，栀子32g，甘松38g，诃子35g，广枣40g，紫檀香32g，血竭32g，西红花36g，麝香15g，三鲜红450g。
草果二十一味丸的制备方法为：
以上二十一味药，麝香、西红花、血竭粉碎成细粉；其余草果等十八味粉碎成细粉，与上述细粉配研，过筛，混匀。每100g粉末用炼蜜100g制成大蜜丸，即得。
草果二十一味丸的鉴别方法为：
取本品10g，加硅藻土2g，研匀，加甲醇30ml，超声处理20分钟，过滤后将滤液蒸干，残渣加甲醇1ml使之溶解，作为供试品溶液。另取紫花地丁对照药材1g，同法制成对照药材溶液。照薄层色谱法(中国药典2005年版一部附录VI B)试验，吸取供试品溶液5-10μl、对照药材溶液5μl，分别点于同一以羧甲基纤维素钠为粘合剂的硅胶G薄层板上，以甲苯-乙酸乙酯-甲酸(体积比为5∶3∶1)的上层溶液为展开剂，展开、取出、晾干，置紫外光灯(365nm)下检视。供试品色谱中，在与对照药材色谱相应的位置上，显示相同颜色的荧光斑点。
实施例3
草果二十一味丸及其鉴别方法，其方案是这样实现的：
草果二十一味丸的配方为：
草果50g，石膏30g，紫花地丁30g，木鳖子30g，青皮30g，白豆蔻30g，沉香30g，茜草30g，木香30g，麦冬30g，五灵脂30g，石莲子30g，栀子30g，甘松30g，诃子30g，广枣30g，紫檀香30g，血竭30g，西红花30g，麝香10g，三鲜红400g。
草果二十一味丸的制备方法为：
以上二十一味药，麝香、西红花、血竭粉碎成细粉；其余草果等十八味粉碎成细粉，与上述细粉配研，过筛，混匀。每100g粉末用炼蜜100g制成大蜜丸，即得。
草果二十一味丸的鉴别方法为：
取本品10g，加硅藻土2g，研匀，加甲醇30ml，超声处理20分钟，过滤后将滤液蒸干，残渣加甲醇1ml使之溶解，作为供试品溶液。另取紫花地丁对照药材1g，同法制成对照药材溶液。照薄层色谱法(中国药典2005年版一部附录VI B)试验，吸取供试品溶液5-10μl、对照药材溶液5μl，分别点子同一以羧甲基纤维素钠为粘合剂的硅胶G薄层板上，以甲苯-乙酸乙酯-甲酸(体积比为5∶3∶1)的上层溶液为展开剂，展开、取出、晾干，置紫外光灯(365nm)下检视。供试品色谱中，在与对照药材色谱相应的位置上，显示相同颜色的荧光斑点。
上述具体实施方式仅仅是为清楚地说明本发明所作的举例，而并非对实施方式的限定。对于所属领域的普通技术人员来说，在上述说明的基础上还可以做出其它不同形式的变化或变动，这里无需也无法对所有的实施方式予以穷举，而由此所引申出的显而易见的变化或变动仍处于本发明的保护范围中。

Claims (4)

1.草果二十一味丸及其鉴别方法，其特征在于，草果二十一味丸是这样得到的：
草果二十一味丸的配方为：
草果45-55g，石膏27-36g，紫花地丁26-32g，木鳖子24-30g，青皮25-35g，白豆蔻28-35g，沉香20-32g，茜草30-40g，木香25-35g，麦冬23-30g，五灵脂26-32g，石莲子25-35g，栀子22-32g，甘松28-38g，诃子26-35g，广枣20-40g，紫檀香28-32g，血竭26-32g，西红花27-36g，麝香5-15g，三鲜红350-450g；
草果二十一味丸的制备方法为：
以上二十一味药，麝香、西红花、血竭粉碎成细粉；其余草果等十八味粉碎成细粉，与上述细粉配研，过筛，混匀。每100g粉末用炼蜜100g制成大蜜丸，即得。
2.根据权利要求1所述的草果二十一味丸及其鉴别方法，其特征在于，
草果二十一味丸的配方为：
草果48-52g，石膏28-32g，紫花地丁29-31g，木鳖子26-30g，青皮28-33g，白豆蔻29-32g，沉香27-32g，茜草30-35g，木香28-32g，麦冬26-30g，五灵脂28-32g，石莲子28-33g，栀子28-32g，甘松29-33g，诃子28-32g，广枣29-42g，紫檀香29-31g，血竭28-32g，西红花28-33g，麝香8-12g，三鲜红380-420g。
3.根据权利要求1所述的草果二十一味丸及其鉴别方法，其特征在于，
草果二十一味丸的配方为：
草果50g，石膏30g，紫花地丁30g，木鳖子30g，青皮30g，白豆蔻30g，沉香30g，茜草30g，木香30g，麦冬30g，五灵脂30g，石莲子30g，栀子30g，甘松30g，诃子30g，广枣30g，紫檀香30g，血竭30g，西红花30g，麝香10g，三鲜红400g。
4.根据权利要求1所述的草果二十一味丸及其鉴别方法，其特征在于，
草果二十一味丸的鉴别方法为：
取本品10g，加硅藻土2g，研匀，加甲醇30ml，超声处理20分钟，过滤后将滤液蒸干，残渣加甲醇1ml使之溶解，作为供试品溶液。另取紫花地丁对照药材1g，同法制成对照药材溶液。照薄层色谱法(中国药典2005年版一部附录VI B)试验，吸取供试品溶液5-10μl、对照药材溶液5μl，分别点于同一以羧甲基纤维素钠为粘合剂的硅胶G薄层板上，以甲苯-乙酸乙酯-甲酸(体积比为5∶3∶1)的上层溶液为展开剂，展开、取出、晾干，置紫外光灯(365nm)下检视。供试品色谱中，在与对照药材色谱相应的位置上，显示相同颜色的荧光斑点。
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