CN105969518A - Preparation method and application of walnut distillate oil - Google Patents
Preparation method and application of walnut distillate oil Download PDFInfo
- Publication number
- CN105969518A CN105969518A CN201610532220.8A CN201610532220A CN105969518A CN 105969518 A CN105969518 A CN 105969518A CN 201610532220 A CN201610532220 A CN 201610532220A CN 105969518 A CN105969518 A CN 105969518A
- Authority
- CN
- China
- Prior art keywords
- semen juglandis
- distilling
- oil
- heating
- distilling oil
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/12—Production of fats or fatty oils from raw materials by melting out
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/52—Juglandaceae (Walnut family)
Landscapes
- Health & Medical Sciences (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Microbiology (AREA)
- Wood Science & Technology (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Alternative & Traditional Medicine (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Botany (AREA)
- Medical Informatics (AREA)
- Medicinal Chemistry (AREA)
- Organic Chemistry (AREA)
- Mycology (AREA)
- Pharmacology & Pharmacy (AREA)
- Epidemiology (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Medicines Containing Material From Animals Or Micro-Organisms (AREA)
Abstract
The invention discloses a preparation method of walnut distillate oil and application of the walnut distillate oil, belonging to the technical field of Chinese traditional medicine extraction. The method comprises the following steps of heating walnut kernels to 150 DEG C or more, beginning collecting the walnut distillate oil when liquid flows out, continuously heating up to 392 DEG C, and collecting the walnut distillate oil generated in the temperature rising process. The walnut distillate oil prepared according to the preparation method disclosed by the invention has the advantage of higher curative effects of treating gynecological diseases, such as leukorrhagia, yellow leucorrhea, lower abdomen bearing-down pain, lumbosacral pain and cervical erosion.
Description
Technical field
The present invention relates to the preparation method and application of a kind of Semen Juglandis distilling oil, belong to technical field of extraction of Chinese traditional medicine.
Background technology
To Semen Juglandis vegetable oil in the Semen Juglandis that the methods such as squeezing, organic solvent dissolving obtain walnut oil (walnut oil treatment mark
Accurate: GB/22327-2008).And Semen Juglandis flows out produced walnut oil the most naturally Semen Juglandis distilling oil (country's food
Product Drug Administration standard: YBZ00492008).
Semen Juglandis distilling oil treatment gynaecopathia is in elm ditch group of clear gully people's commune of short report Kuan Dian county medical station: " Semen Juglandis distilling oil is controlled
Treat cervical erosion " the middle preparation stating Semen Juglandis distilling oil, but the Semen Juglandis distilling oil prepared according to its method only can prepare cervical erosion,
Therapeutic effect is single, and effective percentage need to improve further.
Summary of the invention
For solving the deficiencies in the prior art, the invention provides the preparation method of a kind of Semen Juglandis distilling oil, the technical scheme of employing is as follows:
It is an object of the invention to provide the preparation method of a kind of Semen Juglandis distilling oil, the method is that Semen Juglandis is heated to more than 150 DEG C,
Start to collect Semen Juglandis distilling oil in time having liquid to flow out, be continuously heating to 392 DEG C, collect the Semen Juglandis distilling oil produced in temperature-rise period.
Preferably, described mode of heating is electrical heating, electromagnetism, infrared, microwave, gas heating.
Preferably, described method is that Semen Juglandis is heated to more than 150 DEG C, starts to collect Semen Juglandis distilling oil, continue in time having liquid to flow out
Continue and be warming up to 392 DEG C, collect the Semen Juglandis distilling oil produced in temperature-rise period；Described heating rate is 0.1 DEG C/min-15 DEG C/min.
Preferably, described method, it is characterised in that step is as follows:
1) Semen Juglandis is heated to more than 150 DEG C, starts to collect Semen Juglandis distilling oil in time having liquid to flow out；
2) being continuously heating to T1, heating rate is 0.1 DEG C/min-15 DEG C/min, collects all Semen Juglandiss produced in temperature-rise period and evaporates
Oil；Described T1 is 200 DEG C-350 DEG C；
3) continuing to be warming up to T2 by T1, heating rate is 0.1 DEG C/min-15 DEG C/min, collects generation in T1 to T2 temperature-rise period
All Semen Juglandis distilling oils, stop when flowing out without Semen Juglandis distilling oil collecting；Described T2 is 350 DEG C-392 DEG C；
4) by during all Semen Juglandis distilling oils of producing be uniformly mixed after seal preserve stand-by.
Preferably, heating rate is 1 DEG C/min-10 DEG C/min；It is highly preferred that heating rate is 1 DEG C/min-5 DEG C/min.
Preferably, described T1 is 300 DEG C-350 DEG C.
It is highly preferred that described method, step is as follows:
1) Semen Juglandis is heated to more than 150 DEG C, starts to collect Semen Juglandis distilling oil in time having liquid to flow out；
2) being continuously heating to T1, heating rate is 0.5 DEG C/min-5 DEG C/min, collects all Semen Juglandis distilling oils produced in temperature-rise period；
Described T1 is 300 DEG C-350 DEG C；
3) continuing to be warming up to T2 by T1, heating rate is 0.5 DEG C/min-5 DEG C/min, collects generation in T1 to T2 temperature-rise period
All Semen Juglandis distilling oils, stop when flowing out without Semen Juglandis distilling oil collecting；Described T2 is 350 DEG C-392 DEG C；
4) by during all Semen Juglandis distilling oils of producing be uniformly mixed after seal preserve stand-by.
Present invention also offers Semen Juglandis distilling oil prepared by a kind of described either method application in preparing gynecopathy therapeutic medicine.
Preferably, described pharmaceutical dosage form is suppository.
It is highly preferred that above-mentioned suppository is shaped as Duckbill type, column type, bullet-shaped.
Present invention determine that having extraordinary therapeutic effect to gynaecopathia prepares the temperature range (150 DEG C of Semen Juglandis distilling oil
-392℃).This patent determines 150 DEG C of-392 DEG C of intervals first and prepares the Semen Juglandis distilling oil preparation method of mixed collection continuously,
The Semen Juglandis distilling oil that this preparation method obtains is to gynecological such as profuse leukorrhea, leucorrhea with yellow discharge, lower abdomen pendant pain, lumbus sacrum pain and cervical erosion
Disease treatment has higher curative effect.
The method have the benefit that
1, the present invention is by controlling technique mistake, determines that Semen Juglandis distilling oil is prepared mixed in 150 DEG C of 392 DEG C of intervals continuously first
Closing the method collected, the Semen Juglandis distilling oil that this preparation method obtains improves curative effect, adds gynaecopathia gynecopathy therapeutic
Therapeutic domain, improves the oil yield of Semen Juglandis, reduces product cost.
2, Semen Juglandis distilling oil and 200 DEG C and the 250 DEG C Semen Juglandis distilling oils extracted that prepared by the present invention are compared, and have widely therapeutic domain,
With more preferable therapeutic effect, the gynaecopathias such as profuse leukorrhea, leucorrhea with yellow discharge, lower abdomen pendant pain, lumbus sacrum pain and cervical erosion are controlled
Treating and all have higher curative effect, wholistic therapy has effective percentage to be up to 89.50%.
3, the present invention improves the oil yield of Semen Juglandis, and the Semen Juglandis distilling oil oil yield extracted when experiments verify that 200 DEG C is 21.5%,
Preparation method of the present invention improves the oil yield 37.5% of Semen Juglandis, reduces production cost.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention will be further described, but the present invention should not be limited by the examples.
Embodiment 1
Present embodiments provide the preparation method of a kind of Semen Juglandis distilling oil, method for Semen Juglandis is heated to more than 150 DEG C, liquid to be had
Body starts to collect Semen Juglandis distilling oil when flowing out, and is continuously heating to 392 DEG C, collects the Semen Juglandis distilling oil produced in temperature-rise period.Heating side
Formula is electrical heating.
The Semen Juglandis distilling oil prepared according to the method described above and polyoxyethylene stearate (40) ester are mixed and made into 2.5g suppository, by every 2.5g
Suppository containing 0.4g Semen Juglandis distilling oil make, vagina administration, one time one, once-a-day, within 7th, be a course for the treatment of, continuous two courses for the treatment of.
Experimental result is as follows:
The therapeutic outcome of table 1 Semen Juglandis distilling oil
Embodiment 2
Present embodiments providing the preparation method of a kind of Semen Juglandis distilling oil, method is:
1) Semen Juglandis is heated to more than 150 DEG C, starts to collect Semen Juglandis distilling oil in time having liquid to flow out；
2) being continuously heating to T1, heating rate is 0.1 DEG C/min-1 DEG C/min, collects all Semen Juglandis distilling oils produced in temperature-rise period；
Described T1 is 200 DEG C-350 DEG C；
3) continuing to be warming up to T2 by T1, heating rate is 0.1 DEG C/min-1 DEG C/min, collects generation in T1 to T2 temperature-rise period
All Semen Juglandis distilling oils, stop when flowing out without Semen Juglandis distilling oil collecting；Described T2 is 350 DEG C-392 DEG C；
4) by during all Semen Juglandis distilling oils of producing be uniformly mixed after seal preserve stand-by.
Mode of heating can be electrical heating, electromagnetism, infrared, microwave or gas heating.
The Semen Juglandis distilling oil prepared according to the method described above and polyoxyethylene stearate (40) ester are mixed and made into 2.5g suppository, by every 2.5g
Suppository containing 0.4g Semen Juglandis distilling oil make, vagina administration, one time one, once-a-day, within 7th, be a course for the treatment of, continuous two courses for the treatment of.
Experimental result is as follows:
The therapeutic outcome of table 2 Semen Juglandis distilling oil
Embodiment 3
Present embodiments providing the preparation method of a kind of Semen Juglandis distilling oil, step is:
1) Semen Juglandis is heated to more than 150 DEG C, starts to collect Semen Juglandis distilling oil in time having liquid to flow out；
2) being continuously heating to T1, heating rate is 1 DEG C/min-5 DEG C/min, collects all Semen Juglandis distilling oils produced in temperature-rise period；
Described T1 is 250 DEG C-300 DEG C；
3) continuing to be warming up to T2 by T1, heating rate is 1 DEG C/min-5 DEG C/min, collects the institute produced in T1 to T2 temperature-rise period
There is Semen Juglandis distilling oil, stop when flowing out without Semen Juglandis distilling oil collecting；Described T2 is 350 DEG C-392 DEG C；
4) by during all Semen Juglandis distilling oils of producing be uniformly mixed after seal preserve stand-by.
Above-mentioned mode of heating can be electrical heating, electromagnetism, infrared, microwave or gas heating.
The therapeutic outcome of table 6 Semen Juglandis distilling oil
Embodiment 4
Present embodiments providing the preparation method of a kind of Semen Juglandis distilling oil, step is:
1) Semen Juglandis is heated to more than 150 DEG C, starts to collect Semen Juglandis distilling oil in time having liquid to flow out；
2) being continuously heating to T1, heating rate is 1 DEG C/min-5 DEG C/min, collects all Semen Juglandis distilling oils produced in temperature-rise period；
Described T1 is 300 DEG C-350 DEG C；
3) continuing to be warming up to T2 by T1, heating rate is 1 DEG C/min-5 DEG C/min, collects the institute produced in T1 to T2 temperature-rise period
There is Semen Juglandis distilling oil, stop when flowing out without Semen Juglandis distilling oil collecting；Described T2 is 350 DEG C-392 DEG C；
4) by during all Semen Juglandis distilling oils of producing be uniformly mixed after seal preserve stand-by.
The Semen Juglandis distilling oil prepared according to the method described above and polyoxyethylene stearate (40) ester are mixed and made into 2.5g suppository, by every 2.5g
Suppository containing 0.4g Semen Juglandis distilling oil make, vagina administration, one time one, once-a-day, within 7th, be a course for the treatment of, continuous two courses for the treatment of.
Experimental result is as follows:
The therapeutic outcome of table 7 Semen Juglandis distilling oil
Understand from the above: Semen Juglandis distilling oil prepared by the inventive method is to profuse leukorrhea, leucorrhea with yellow discharge, lumbus sacrum pain, lower abdomen
The symptoms such as pendant pain, cervical erosion all have higher curative effect, and wherein embodiment 7 is optimum embodiment, and effect is best, to five kinds of symptoms
Total treatment rate be up to 89.50%.
Embodiment 5
Present embodiments providing the preparation method of a kind of Semen Juglandis distilling oil, method is:
1) Semen Juglandis is heated to more than 150 DEG C, starts to collect Semen Juglandis distilling oil in time having liquid to flow out；
2) being continuously heating to T1, heating rate is 5 DEG C/min-10 DEG C/min, collects all Semen Juglandis distilling oils produced in temperature-rise period；
Described T1 is 200 DEG C-350 DEG C；
3) continuing to be warming up to T2 by T1, heating rate is 5 DEG C/min-10 DEG C/min, collects the institute produced in T1 to T2 temperature-rise period
There is Semen Juglandis distilling oil, stop when flowing out without Semen Juglandis distilling oil collecting；Described T2 is 350 DEG C-392 DEG C；
4) by during all Semen Juglandis distilling oils of producing be uniformly mixed after seal preserve stand-by.
Mode of heating can be electrical heating, electromagnetism, infrared, microwave or gas heating.
The therapeutic outcome of table 4 Semen Juglandis distilling oil
Embodiment 5
Present embodiments providing the preparation method of a kind of Semen Juglandis distilling oil, method is:
1) Semen Juglandis is heated to more than 150 DEG C, starts to collect Semen Juglandis distilling oil in time having liquid to flow out；
2) being continuously heating to T1, heating rate is 10 DEG C/min-15 DEG C/min, collects all Semen Juglandiss produced in temperature-rise period and evaporates
Oil；Described T1 is 200 DEG C-350 DEG C；
3) continuing to be warming up to T2 by T1, heating rate is 10 DEG C/min-15 DEG C/min, collects generation in T1 to T2 temperature-rise period
All Semen Juglandis distilling oils, stop when flowing out without Semen Juglandis distilling oil collecting；Described T2 is 350 DEG C-392 DEG C；
4) by during all Semen Juglandis distilling oils of producing be uniformly mixed after seal preserve stand-by.
Mode of heating can be any one in electrical heating, electromagnetism, infrared, microwave, gas heating.
The Semen Juglandis distilling oil prepared according to the method described above and polyoxyethylene stearate (40) ester are mixed and made into 2.5g suppository, by every 2.5g
Suppository containing 0.4g Semen Juglandis distilling oil make, vagina administration, one time one, once-a-day, within 7th, be a course for the treatment of, continuous two courses for the treatment of.
Experimental result is as follows:
The therapeutic outcome of table 5 Semen Juglandis distilling oil
Embodiment 8
The present embodiment has carried out gynaecopathia treatment effectiveness evaluation to the Semen Juglandis distilling oil of preparation at 200 DEG C and 250 DEG C, and concrete packet is such as
Under:
The Semen Juglandis distilling oil that during test group 1:200 DEG C, constant temperature is collected, heating rate is 0.1 DEG C/min-15 DEG C/min；
The Semen Juglandis distilling oil that during test group 2:250 DEG C, constant temperature is collected, heating rate is 0.1 DEG C/min-15 DEG C/min；
The Semen Juglandis distilling oil of preparation is made 2.5g suppository, by every 2.5g suppository Semen Juglandis Han 0.4g with polyoxyethylene stearate (40) ester
Evaporate oil making, vagina administration, one time one, once-a-day, within 7th, be a course for the treatment of, continuous two courses for the treatment of.Its comparing result is such as
Under:
Table 8 test group 1 therapeutic effect
Table 9 test group 2 therapeutic effect
By table 12-13 it can be seen that experimental group 1 (200 DEG C of Semen Juglandis distilling oils extracted) and the experimental group 2 (Semen Juglandiss of 250 DEG C of extractions
Evaporate oil) only cervical erosion is had obvious therapeutic effect, and the Semen Juglandis distilling oil prepared according to the inventive method, to profuse leukorrhea, band
Lower yellow skin, lower abdomen pendant pain, lumbus sacrum pain and cervical erosion all have higher treatment to imitate, and are all remarkably higher than the treatment of experimental group 1-2
Efficiency.
The Semen Juglandis distilling oil oil yield extracted when experiments verify that 200 DEG C and 250 DEG C is 21.5%, and preparation method of the present invention is fuel-displaced for rate
37.5%, the present invention improves the oil yield of Semen Juglandis, reduces production cost.
The Semen Juglandis distilling oil prepared according to the inventive method adds the therapeutic domain to other gynaecopathia, improves going out of Semen Juglandis
Oil rate, and significantly improve the therapeutic effect to gynaecopathia, during checking curative effect, not finding toxic and side effects, safety can
Lean on, evident in efficacy.
Preparation method of the present invention by being prepared for the Semen Juglandis distilling oil with treatment gynaecopathia to the control of technical process, to leukorrhagia amount
The gynecopathy therapeutics such as many, leucorrhea with yellow discharge, lower abdomen pendant pain, lumbus sacrum pain and cervical erosion all have higher curative effect.
Although the present invention is open the most as above with preferred embodiment, but it is not limited to the present invention, any is familiar with this technology
People, without departing from the spirit and scope of the present invention, can do various change and modification, and therefore protection scope of the present invention should
Should be with being as the criterion that claims are defined.
Claims (6)
1. the preparation method of a Semen Juglandis distilling oil, it is characterised in that Semen Juglandis is heated to more than 150 DEG C, opens in time having liquid to flow out
Begin to collect Semen Juglandis distilling oil, be continuously heating to 392 DEG C, collect the Semen Juglandis distilling oil produced in temperature-rise period.
Method the most according to claim 1, it is characterised in that Semen Juglandis is heated to more than 150 DEG C, starts in time having liquid to flow out
Collect Semen Juglandis distilling oil, be continuously heating to 392 DEG C, collect the Semen Juglandis distilling oil produced in temperature-rise period；Described heating rate is 0.1 DEG C
/min-15℃/min。
Method the most according to claim 1, it is characterised in that step is as follows:
1) Semen Juglandis is heated to more than 150 DEG C, starts to collect Semen Juglandis distilling oil in time having liquid to flow out；
2) being continuously heating to T1, heating rate is 0.1 DEG C/min-15 DEG C/min, collects all Semen Juglandiss produced in temperature-rise period and evaporates
Oil；Described T1 is 200 DEG C-350 DEG C；
3) continuing to be warming up to T2 by T1, heating rate is 0.1 DEG C/min-15 DEG C/min, collects generation in T1 to T2 temperature-rise period
All Semen Juglandis distilling oils, stop when flowing out without Semen Juglandis distilling oil collecting；Described T2 is 350 DEG C-392 DEG C；
4) by during all Semen Juglandis distilling oils of producing be uniformly mixed after seal preserve stand-by.
4. according to either method described in claim 1-3, it is characterised in that described mode of heating is electrical heating, electromagnetism, infrared, micro-
Ripple, gas heating.
5. the Semen Juglandis distilling oil that prepared by either method described in claim 1-4 application in preparing gynecopathy therapeutic medicine.
Apply the most according to claim 5, it is characterised in that described pharmaceutical dosage form is suppository.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610532220.8A CN105969518A (en) | 2016-07-07 | 2016-07-07 | Preparation method and application of walnut distillate oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610532220.8A CN105969518A (en) | 2016-07-07 | 2016-07-07 | Preparation method and application of walnut distillate oil |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105969518A true CN105969518A (en) | 2016-09-28 |
Family
ID=56954064
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610532220.8A Pending CN105969518A (en) | 2016-07-07 | 2016-07-07 | Preparation method and application of walnut distillate oil |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105969518A (en) |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101502576A (en) * | 2007-05-31 | 2009-08-12 | 北京凯瑞创新医药科技有限公司 | Application of dry distillation liquid from cherry core in preparing medicament for treating or preventing fungal disease |
| CN103520264A (en) * | 2013-10-11 | 2014-01-22 | 哈尔滨欧替药业有限公司 | Fukang expandable vaginal suppository, and preparation method and detection method thereof |
| CN105038947A (en) * | 2015-06-24 | 2015-11-11 | 洛阳国花坊牡丹生物科技有限公司 | Supercritical extraction method of walnut oil |
-
2016
- 2016-07-07 CN CN201610532220.8A patent/CN105969518A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101502576A (en) * | 2007-05-31 | 2009-08-12 | 北京凯瑞创新医药科技有限公司 | Application of dry distillation liquid from cherry core in preparing medicament for treating or preventing fungal disease |
| CN103520264A (en) * | 2013-10-11 | 2014-01-22 | 哈尔滨欧替药业有限公司 | Fukang expandable vaginal suppository, and preparation method and detection method thereof |
| CN105038947A (en) * | 2015-06-24 | 2015-11-11 | 洛阳国花坊牡丹生物科技有限公司 | Supercritical extraction method of walnut oil |
Non-Patent Citations (4)
| Title |
|---|
| 宽甸县清山沟公社榆树沟大队医疗站: "核桃馏油治疗宫颈糜烂", 《辽宁中级医刊》 * |
| 左言富: "《简明中成药辞典》", 31 October 2002, 上海科学技术出版社 * |
| 辽宁宽甸县青山沟地区医院等: "核桃馏油治疗黄水疮", 《中草药通讯》 * |
| 辽宁省药品检验所: "中草药核桃馏油", 《中草药通讯》 * |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104352811A (en) | Plaster for curing bone injury and preparation method thereof | |
| CN103933129B (en) | Plaster for treating pain | |
| CN103830428B (en) | A kind of Chinese medicine preparation for the treatment of hordeolum | |
| CN105687587A (en) | Ointment for warming channels and dredging collaterals as well as alleviating pain | |
| CN104815114A (en) | Traditional Chinese medicine ointment for treating bone fracture and production method thereof | |
| CN104288533A (en) | Black plaster for treating bone injuries and preparation method thereof | |
| CN105969518A (en) | Preparation method and application of walnut distillate oil | |
| CN104771678A (en) | Drug for treating thrombophlebitis and preparation method thereof | |
| CN103977367A (en) | Traditional Chinese medicament for treating qi-stagnation blood-aggregation type bedsore and preparation method thereof | |
| CN104288417A (en) | Traditional Chinese medicine composition for treating dysmenorrhea and preparation method thereof | |
| CN106177508A (en) | The Chinese medicine external ointment for the treatment of radioactive skin injury | |
| CN103127444A (en) | Phlegm-qi stagnation type psychosis treatment traditional Chinese medicine | |
| CN104352683A (en) | Black plaster for curing bone injury and preparation method thereof | |
| CN104491254A (en) | Black plaster for treating bone injury and preparation method of black plaster | |
| CN104225318A (en) | Traditional Chinese medicine preparation for treating infantile convulsions | |
| CN105796673A (en) | Traditional Chinese medicine composition for rehabilitation after replantation of amputated finger and preparation method and application method of traditional Chinese medicine composition | |
| CN105726834A (en) | Black plaster for treating bone fracture and preparation method thereof | |
| CN104013840A (en) | Traditional Chinese medicine composition for treating epilepsy | |
| CN104888147A (en) | Traditional Chinese medicine ointment for shoulder periarthritis and preparation method thereof | |
| CN104288230A (en) | Plaster for treating bone injury and preparation method of plaster | |
| CN104147159A (en) | Medicine for treating varicosity | |
| CN104771531A (en) | Traditional Chinese medicine capsule for treating prosopalgia and preparation method thereof | |
| CN105687424A (en) | Ointment for treating traumatic injuries | |
| CN102920894B (en) | Medicament for treating arthralgia and myalgia and preparation method thereof | |
| CN104288535A (en) | Black plaster for treating bone injury and preparation method of black plaster |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20160928 |