CN105950004A - Method for measuring temperature of electrical equipment through irreversible thermochromic material - Google Patents

Method for measuring temperature of electrical equipment through irreversible thermochromic material Download PDF

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Publication number
CN105950004A
CN105950004A CN201610565158.2A CN201610565158A CN105950004A CN 105950004 A CN105950004 A CN 105950004A CN 201610565158 A CN201610565158 A CN 201610565158A CN 105950004 A CN105950004 A CN 105950004A
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CN
China
Prior art keywords
electrical equipment
indicating material
irreversible
thermally indicating
irreversible thermally
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610565158.2A
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Chinese (zh)
Inventor
胡虔
吴雄
潘吉林
董中强
吴峰
朱晓东
何昌林
沈帆
柯锐
柳欢欢
梅端
林锋
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Auspicious Electric Power Project Engineering Equipment Ltd South Wuhan
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Auspicious Electric Power Project Engineering Equipment Ltd South Wuhan
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Auspicious Electric Power Project Engineering Equipment Ltd South Wuhan filed Critical Auspicious Electric Power Project Engineering Equipment Ltd South Wuhan
Priority to CN201610565158.2A priority Critical patent/CN105950004A/en
Publication of CN105950004A publication Critical patent/CN105950004A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D183/00Coating compositions based on macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon, with or without sulfur, nitrogen, oxygen, or carbon only; Coating compositions based on derivatives of such polymers
    • C09D183/04Polysiloxanes
    • C09D183/06Polysiloxanes containing silicon bound to oxygen-containing groups
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00Use of inorganic substances as compounding ingredients
    • C08K3/28Nitrogen-containing compounds
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00Use of inorganic substances as compounding ingredients
    • C08K3/30Sulfur-, selenium- or tellurium-containing compounds
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D183/00Coating compositions based on macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon, with or without sulfur, nitrogen, oxygen, or carbon only; Coating compositions based on derivatives of such polymers
    • C09D183/10Block or graft copolymers containing polysiloxane sequences
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/26Thermosensitive paints
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00Use of inorganic substances as compounding ingredients
    • C08K3/30Sulfur-, selenium- or tellurium-containing compounds
    • C08K2003/3045Sulfates
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00Specific properties of additives
    • C08K2201/014Additives containing two or more different additives of the same subgroup in C08K
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/02Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group

Abstract

The invention provides a detecting method for judging heating failure of an electric transmission line through an irreversible thermochromic material. The method comprises the steps of preparation of the irreversible thermochromic material, cleaning and drying of electrical equipment, coating and curing. Whether a short circuit happens to the electrical equipment or not is judged through the color changes of the irreversible thermochromic material. The irreversible thermochromic material is an environment-friendly product low in volatility and smell, has the advantages of being high in bonding strength, good in sun blocking and ageing resisting performance and the like, and is easy and convenient to operate, capable of being cured at normal temperature, high in bonding force and good in toughness. The temperature/color response speed is high, the advantages of being simple, fast, convenient, visual and the like are achieved, and the construction process is simple and convenient.

Description

A kind of method using irreversible thermally indicating material to measure electrical equipment temperature
Technical field
The present invention relates to technical field of electric equipment, be specifically related to the irreversible thermally indicating material of a kind of employing and measure electricity The method of gas device temperature.
Background technology
Due to residing high altitude environment, O&M maintenance is difficult to, therefore for the temperature prison of equipment on transmission line of electricity Survey and not in time.When having short circuit, the big electric current that is struck by lightning to pass through, ground operation maintenance personnel can not be informed, Cause a hidden trouble to equipment safety operation.For the equipment thermometric on transmission line of electricity typically have optical fiber monitoring and Two kinds of methods of hand-held infrared radiation thermometer thermometric.Lay optical fiber cost the highest, use hand-held infrared radiation thermometer needs Climb up shaft tower, and the temperature when temperature surveyed only is merely thermometric timing node, can not accurately reflect and be No suffer overcurrent or short trouble, can not effectively indicate.Accordingly, it would be desirable to a kind of low cost of exploitation, The temperature indicating means that accuracy is high is filled a hole in the market.
Summary of the invention
It is an object of the invention to provide a kind of method using irreversible thermally indicating material to measure electrical equipment temperature, Use irreversible thermally indicating material to show the change of electricity piece equipment, thus reach the purpose of thermometric, it is not necessary to specially The temperature measuring equipment of door, i.e. can observe whether there is short circuit generation with naked eyes, and the most efficiently, quick, safety can Lean on.
To achieve these goals, the technical solution used in the present invention is as follows:
A kind of method using irreversible thermally indicating material to measure electrical equipment temperature, comprises the steps:
1) fire resistant resin it is sufficiently mixed with irreversible temperature sensing material and stirs, utilizing solvent diformazan Benzene allocates viscosity with n-butyl acetate, prepares irreversible thermally indicating material mixed liquor;
2) it is dried after the substrate surface floating dust of electrical equipment, greasy dirt, foreign material being cleaned out;
3) irreversible thermally indicating material mixed liquor is uniformly coated on the substrate surface of electrical equipment;
4) electrical equipment having been coated with irreversible thermally indicating material mixed liquor is at room temperature solidified, and stand 24h Above, it is then mounted to desired location;
5) judge whether electrical equipment has short circuit generation by the color change of irreversible thermally indicating material.
According to above scheme, described fire resistant resin includes epoxy modified silicone resin, polyurethane-modified has Any one or more than one mixture in machine silicones.
According to above scheme, described irreversible thermally indicating material include lead, nickel, cobalt, ferrum, every, zinc, manganese, The sulfate of metal such as molybdenum, barium, magnesium, nitrate, phosphate, chromate, sulfide, oxide, with And AZOpigments, phthalocyanine color, arylmethane dyes etc..
According to above scheme, the heat discoloration temperature range of described irreversible thermally indicating material is: 150-1250 DEG C.
According to above scheme, described coating process includes brushing, spraying etc..
According to above scheme, the coating weight of described coating is according to the basal plane situation of coated article body, the difference of size Doing corresponding adjustment, thickness can the most freely determine, generally 20~50 μm.
According to above scheme, described solidification is carried out in a heated condition, to accelerate solidification.
According to above scheme, described irreversible thermally indicating material mixed liquor need to be coated in 1h after producing.
Described viscosity is: spray viscosity is 20-30 second (coating-4 viscosity meter, 25 DEG C), and brushing viscosity is 30-35 Second (coating-4 viscosity meter, 25 DEG C).
Special irreversible temperature indicating paint is a kind of novel sapecial coating, and it is to indicate object with color phenomenon A kind of coating of surface temperature, measures instruction temperature with thermo-color and has simple, fast and easy, directly perceived Etc. advantage, less than general glass-stem thermometer, thermocouple, thermal resistance thermometer.The present invention's is irreversible Thermally indicating material is Bi-component high-temperature resistant irreversible temperature indicating paint, and its discoloring temperature scope is 150-1250 DEG C.
The irreversible thermally indicating material of the present invention is mainly used in high voltage power transmission, transformator, electronic apparatus etc. as showing Thermo-paint, whether instruction electrical equipment has short circuit generation;It also is used as metallic paint, metal-to-metal adhesive, prevents Rotten material etc.;Insulant is also acted as in electrical equipment industry.
When the irreversible thermally indicating material mixed liquor of the present invention is not coated construction in preparing one hour after, many Remaining mixed liquor can not be refunded in tank, can only discard.Instrument after using should clean with dimethylbenzene immediately.
The invention has the beneficial effects as follows:
1) the irreversible thermally indicating material of the present invention is volatility abnormal smells from the patient environmentally friendly machine little, low, has high viscous Connect the feature such as intensity, good sun-proof and ageing resistace, adapted ratio width, easy and simple to handle, can room temperature solid Changing, bonding force is strong, good toughness;
2) by the color of irreversible thermally indicating material, the present invention can change whether instruction electrical equipment occurs short Road, and temperature changing speed is fast, has the advantages such as simple, fast and easy, directly perceived;
3) work progress of the present invention is simple, convenient.
Detailed description of the invention
Below in conjunction with embodiment, technical scheme is illustrated.
Embodiment 1:
The present invention provides a kind of method using irreversible thermally indicating material to measure electrical equipment temperature, including as follows Step:
1) 100g epoxy modified silicone resin it is sufficiently mixed with 300g nickel sulfate and stirs, profit Allocate viscosity with solvent xylene, prepare irreversible thermally indicating material mixed liquor;
2) it is dried after the substrate surface floating dust of busbar of transformer station's use, greasy dirt, foreign material being cleaned out;
3) irreversible thermally indicating material mixed liquor is uniformly coated on the substrate surface of busbar;
4) at room temperature being solidified by the busbar having been coated with irreversible thermally indicating material mixed liquor, coating thickness is 20 μm, and stand 40h, it is then mounted to desired location;
5) judge whether electrical equipment is short-circuited by the color change of irreversible thermally indicating material.
Embodiment 2:
The present invention provides a kind of method using irreversible thermally indicating material to measure electrical equipment temperature, including as follows Step:
1) polyurethane-modified for 100g organic siliconresin it is sufficiently mixed with 300g cobalt nitrate and stirs, Utilize solvent xylene to allocate viscosity, prepare irreversible thermally indicating material mixed liquor;
2) it is dried after the substrate surface floating dust of plug-in strip, greasy dirt, foreign material being cleaned out;
3) irreversible thermally indicating material mixed liquor is uniformly coated on the substrate surface of plug-in strip;
4) at 60 DEG C, the plug-in strip having been coated with irreversible thermally indicating material mixed liquor being accelerated solidification, coating thickness is 50 μm, and stand 35h, it is then mounted to desired location;
5) judge whether electrical equipment is short-circuited by the color change of irreversible thermally indicating material.
Embodiment 3:
The present invention provides a kind of method using irreversible thermally indicating material to measure electrical equipment temperature, including as follows Step:
1) by 50g oxygen modified organic silicone resin, the polyurethane-modified organic siliconresin of 50g and 100g azo face Material, 200g phthalocyanine color are sufficiently mixed and stir, and utilize solvent xylene to allocate viscosity, prepare not Reversible temperature indicating material mixed liquor;
2) it is dried after the substrate surface floating dust of transformator, greasy dirt, foreign material being cleaned out;
3) irreversible thermally indicating material mixed liquor is uniformly coated on the substrate surface of transformator;
4) at room temperature being solidified by the transformator having been coated with irreversible thermally indicating material mixed liquor, coating thickness is 30 μm, and stand 50h, it is then mounted to desired location;
5) judge whether electrical equipment is short-circuited by the color change of irreversible thermally indicating material.
Above example is only in order to illustrative not limiting technical scheme, although above-described embodiment is to this Invention has been described in detail, and the person skilled of this area is it is understood that can repair the present invention Change or replace on an equal basis, but any amendment and local without departing from spirit and scope of the invention is replaced and all should be contained In scope of the presently claimed invention.

Claims (8)

1. one kind uses the method that irreversible thermally indicating material measures electrical equipment temperature, it is characterised in that bag Include following steps:
1) fire resistant resin it is sufficiently mixed with irreversible temperature sensing material and stirs, utilizing solvent diformazan Benzene allocates viscosity with n-butyl acetate, prepares irreversible thermally indicating material mixed liquor;
2) it is dried after the substrate surface floating dust of electrical equipment, greasy dirt, foreign material being cleaned out;
3) irreversible thermally indicating material mixed liquor is uniformly coated on the substrate surface of electrical equipment;
4) electrical equipment having been coated with irreversible thermally indicating material mixed liquor is at room temperature solidified, and stand 24h Above, it is then mounted to desired location;
5) judge whether electrical equipment has short circuit generation by the color change of irreversible thermally indicating material.
The irreversible thermally indicating material of employing the most according to claim 1 measures the method for electrical equipment temperature, It is characterized in that, described fire resistant resin includes epoxy modified silicone resin, polyurethane-modified organosilicon tree Any one or more than one mixture in fat.
The irreversible thermally indicating material of employing the most according to claim 1 measures the method for electrical equipment temperature, It is characterized in that, described irreversible thermally indicating material include lead, nickel, cobalt, ferrum, every, zinc, manganese, molybdenum, barium, The sulfate of magnesium, nitrate, phosphate, chromate, sulfide, oxide and AZOpigments, phthalein Cyanine pigment, arylmethane dyes.
The irreversible thermally indicating material of employing the most according to claim 1 measures the method for electrical equipment temperature, It is characterized in that, the heat discoloration temperature range of described irreversible thermally indicating material is: 150-1250 DEG C.
The irreversible thermally indicating material of employing the most according to claim 1 measures the method for electrical equipment temperature, It is characterized in that, described coating process includes brushing, spraying.
The irreversible thermally indicating material of employing the most according to claim 1 measures the method for electrical equipment temperature, It is characterized in that, the thickness of described coating is 20~50 μm.
The irreversible thermally indicating material of employing the most according to claim 1 measures the method for electrical equipment temperature, It is characterized in that, described solidification is carried out in a heated condition, to accelerate solidification.
The irreversible thermally indicating material of employing the most according to claim 1 measures the method for electrical equipment temperature, It is characterized in that, described irreversible thermally indicating material mixed liquor is coated in 1h after producing.
CN201610565158.2A 2016-07-18 2016-07-18 Method for measuring temperature of electrical equipment through irreversible thermochromic material Pending CN105950004A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610565158.2A CN105950004A (en) 2016-07-18 2016-07-18 Method for measuring temperature of electrical equipment through irreversible thermochromic material

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610565158.2A CN105950004A (en) 2016-07-18 2016-07-18 Method for measuring temperature of electrical equipment through irreversible thermochromic material

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CN105950004A true CN105950004A (en) 2016-09-21

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106995632A (en) * 2017-05-22 2017-08-01 湖南省湘电试验研究院有限公司 The production method of fault diagnosis method and thermo colour and the coating
CN107987706A (en) * 2017-12-19 2018-05-04 中国铁路沈阳局集团有限公司沈阳动车段 A kind of method for monitoring EMU EEF bogie universal shaft and gear-box
CN110698953A (en) * 2019-11-16 2020-01-17 李煜阳 50-200 ℃ multi-color-changing irreversible temperature indicating material and preparation method and application thereof
CN111423724A (en) * 2020-03-26 2020-07-17 国网江西省电力有限公司电力科学研究院 Insulating material with visual flashover trace function and preparation method and application thereof
CN112409837A (en) * 2020-11-27 2021-02-26 中国航发四川燃气涡轮研究院 Isothermal line identification-based single-color-changing irreversible temperature indicating coating and coating manufacturing method
CN115011250A (en) * 2022-05-27 2022-09-06 中国航发四川燃气涡轮研究院 Isothermal line identification-based single-color-changing irreversible temperature indicating coating and coating manufacturing method

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JPH06256719A (en) * 1993-03-09 1994-09-13 Kansai Paint Co Ltd Heat-resistant coating composition
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CN101760111A (en) * 2009-11-30 2010-06-30 北方涂料工业研究设计院 300 DEG C-800 DEG C pleochromatic irreversible thermopaint
CN102492362A (en) * 2011-11-28 2012-06-13 北方涂料工业研究设计院 800DEG C-1250DEG C multi color-changing irreversible thermopaint
CN103911069A (en) * 2012-12-31 2014-07-09 南车戚墅堰机车车辆工艺研究所有限公司 Irreversible temperature indicating paint for brake discs and preparation method thereof
CN104277569A (en) * 2014-10-29 2015-01-14 国家电网公司 Temperature-indicating coating and insulator coated with same

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JPH06256719A (en) * 1993-03-09 1994-09-13 Kansai Paint Co Ltd Heat-resistant coating composition
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CN101760111A (en) * 2009-11-30 2010-06-30 北方涂料工业研究设计院 300 DEG C-800 DEG C pleochromatic irreversible thermopaint
CN102492362A (en) * 2011-11-28 2012-06-13 北方涂料工业研究设计院 800DEG C-1250DEG C multi color-changing irreversible thermopaint
CN103911069A (en) * 2012-12-31 2014-07-09 南车戚墅堰机车车辆工艺研究所有限公司 Irreversible temperature indicating paint for brake discs and preparation method thereof
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Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106995632A (en) * 2017-05-22 2017-08-01 湖南省湘电试验研究院有限公司 The production method of fault diagnosis method and thermo colour and the coating
CN106995632B (en) * 2017-05-22 2019-01-11 湖南省湘电试验研究院有限公司 The production method of fault diagnosis method and thermo colour and the coating
CN107987706A (en) * 2017-12-19 2018-05-04 中国铁路沈阳局集团有限公司沈阳动车段 A kind of method for monitoring EMU EEF bogie universal shaft and gear-box
CN107987706B (en) * 2017-12-19 2020-01-17 中国铁路沈阳局集团有限公司沈阳动车段 Method for monitoring universal shaft and gearbox of running gear of motor train unit
CN110698953A (en) * 2019-11-16 2020-01-17 李煜阳 50-200 ℃ multi-color-changing irreversible temperature indicating material and preparation method and application thereof
CN110698953B (en) * 2019-11-16 2021-02-09 李煜阳 50-200 ℃ multi-color-changing irreversible temperature indicating material and preparation method and application thereof
CN111423724A (en) * 2020-03-26 2020-07-17 国网江西省电力有限公司电力科学研究院 Insulating material with visual flashover trace function and preparation method and application thereof
CN112409837A (en) * 2020-11-27 2021-02-26 中国航发四川燃气涡轮研究院 Isothermal line identification-based single-color-changing irreversible temperature indicating coating and coating manufacturing method
CN115011250A (en) * 2022-05-27 2022-09-06 中国航发四川燃气涡轮研究院 Isothermal line identification-based single-color-changing irreversible temperature indicating coating and coating manufacturing method

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Application publication date: 20160921