CN105938139A - Tail gas detection and absorption device for nitric acid production and installation method thereof - Google Patents

Tail gas detection and absorption device for nitric acid production and installation method thereof Download PDF

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Publication number
CN105938139A
CN105938139A CN201610488059.9A CN201610488059A CN105938139A CN 105938139 A CN105938139 A CN 105938139A CN 201610488059 A CN201610488059 A CN 201610488059A CN 105938139 A CN105938139 A CN 105938139A
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China
Prior art keywords
connects
detection
microcontroller
pipeline
probe
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CN201610488059.9A
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Chinese (zh)
Inventor
孙世全
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Tianjin City Po Moist Chemical Co Ltd
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Tianjin City Po Moist Chemical Co Ltd
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Priority to CN201610488059.9A priority Critical patent/CN105938139A/en
Publication of CN105938139A publication Critical patent/CN105938139A/en
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/0004Gaseous mixtures, e.g. polluted air
    • G01N33/0009General constructional details of gas analysers, e.g. portable test equipment
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/0004Gaseous mixtures, e.g. polluted air
    • G01N33/0009General constructional details of gas analysers, e.g. portable test equipment
    • G01N33/0011Sample conditioning
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/0004Gaseous mixtures, e.g. polluted air
    • G01N33/0009General constructional details of gas analysers, e.g. portable test equipment
    • G01N33/0027General constructional details of gas analysers, e.g. portable test equipment concerning the detector
    • G01N33/0031General constructional details of gas analysers, e.g. portable test equipment concerning the detector comprising two or more sensors, e.g. a sensor array
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/0004Gaseous mixtures, e.g. polluted air
    • G01N33/0009General constructional details of gas analysers, e.g. portable test equipment
    • G01N33/0062General constructional details of gas analysers, e.g. portable test equipment concerning the measuring method or the display, e.g. intermittent measurement or digital display
    • G01N33/0063General constructional details of gas analysers, e.g. portable test equipment concerning the measuring method or the display, e.g. intermittent measurement or digital display using a threshold to release an alarm or displaying means

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Food Science & Technology (AREA)
  • Medicinal Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Combustion & Propulsion (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
  • Sampling And Sample Adjustment (AREA)

Abstract

The invention discloses a tail gas detection and absorption device for nitric acid production and an installation method thereof. Two gas outlets of a three way pipe are connected to a detection pipeline and an absorption pipeline respectively. The detection pipeline is connected to a gas drier. The gas drier is connected to a mixing box. The mixing box is externally provided with a thermal insulation jacket. The mixing box is connected to a booster pump. The booster pump is connected to a detection cavity. A pressure stabilizing valve is arranged on the pipeline that connects the booster pump and the detection cavity. A nitrogen monoxide probe and a nitrogen dioxide probe are arranged in the detection cavity. The nitrogen monoxide probe and the nitrogen dioxide probe are connected to a micro controller. A wireless module is arranged on the micro controller. The micro controller is connected to a display screen through the wireless module. The absorption pipeline is connected to an alkali liquid absorbing box. An electromagnetic valve is arranged on the absorption pipeline. The electromagnetic valve is connected to the micro controller. A communication pipe is arranged between the absorption pipeline and the detection cavity. A non-return valve is arranged on the communication pipe. The structure is simple, the device is user-friendly, the detected data is accurate, the detection and absorption are combined, the absorbing effect is good, and the pollutant discharge is reduced.

Description

The Tail gas measuring absorption plant of a kind of nitric acid production and installation method thereof
Technical field
The present invention relates to nitric acid production technical field, more particularly, it relates to the Tail gas measuring of a kind of nitric acid production Absorption plant and installation method thereof and installation method thereof and installation method thereof.
Background technology
Containing certain density nitrogen oxides in the tail gas of nitric acid production, its concentration usually has been out the discharge of country Standard, needs to carry out denitration process, therefore monitors exhaust gas component in real time for grasping emissions data to closing Important.Additionally, by the oxygen in reaction end gas, ammonia, the on-line checking analysis of nitrogen oxides, can obtain Obtain course of reaction parameter to be used for evaluating nitric acid synthesis efficiency.At present the on-line checking of tail gas oil, chemical industry, The aspects such as metallurgy, environmental protection, automobile are widely used, but are exclusively used in the industrialization of nitric acid production tail gas Online detection instrument is the most fewer, has researcher to use mass spectrograph, but the Tail gas measuring for industrialized production becomes This is higher, maintenance complexity, and the suitability is the strongest.In prior art, the Tail gas measuring equipment of use is usually directly Tail gas is passed in test chamber, owing to gas mixing is uneven, causes detection data fluctuated, inaccurate. Further, detection equipment can't be realized and be combined with tail gas absorption equipment, cause detecting data delayed, cause Data obtain inaccurate, affect creation data statistics.And can not be according to real-time emission data to absorbing alkali liquor amount It is adjusted, causes assimilation effect poor, cause exhaust emissions to exceed standard, affect air ambient.
Accordingly, because prior art exists above-mentioned technological deficiency, it is that those skilled in that art are urgently to be resolved hurrily Technical problem.
Summary of the invention
The purpose of the present invention is for providing Tail gas measuring absorption plant and the installation method thereof of a kind of nitric acid production, it is intended to Present in solution prior art, nitric acid tail gas detection is inaccurate, and can not be tied mutually with tail gas absorption by Tail gas measuring Close, cause the tail gas absorption thorough problem discharging the environmental pollution caused.
For achieving the above object, the present invention provides following technical scheme:
The Tail gas measuring absorption plant of a kind of nitric acid production and installation method thereof, including air inlet pipe, tee T, inspection Test tube road, extraction duct, gas dryer, blending bin, thermal-insulation coat, force (forcing) pump, pressure maintaining valve, test chamber, Nitric oxide probe, nitrogen dioxide probe, alkali liquor absorption case, microcontroller, wireless module, display screen, company Siphunculus, check valve and electromagnetic valve, described air inlet pipe connecting tee pipe, two gas outlets of described tee T connect respectively Connecing detection pipeline and extraction duct, described detection pipeline connects gas dryer, and described gas dryer connects mixed Mould assembling, described blending bin is externally provided with thermal-insulation coat, and described blending bin connects force (forcing) pump, and described force (forcing) pump connects inspection Survey chamber, described force (forcing) pump and test chamber connection pipeline and be provided with pressure maintaining valve, in described test chamber, be provided with nitric oxide Probe and nitrogen dioxide are popped one's head in, and described nitric oxide probe and nitrogen dioxide probe connect microcontroller, described micro- Controller is provided with wireless module, and described microcontroller connects display screen, described extraction duct by wireless module Connecting alkali liquor absorption case, described extraction duct is provided with electromagnetic valve, and described electromagnetic valve connects described microcontroller, It is communicated with pipe between described extraction duct and test chamber, described communicating pipe is provided with check valve.
Preferably, described alkali liquor absorption case includes casing, feed tube, drain pipe and liquid feeding pump, described absorption tube End, road is stretched in described casing below liquid level, and described casing one lower sidewall is provided with feed tube, and described casing is another One side wall upper part is provided with drain pipe, and described feed tube is provided with liquid feeding pump, and described liquid feeding pump connects described microcontroller Device.
Preferably, also including audible-visual annunciator, described audible-visual annunciator connects described microcontroller.
The invention have benefit that: by arranging blending bin in detection equipment, it is possible to by air inlet in mixing Carry out mix homogeneously in advance in case, prevent detecting data fluctuated;Detection equipment is combined with absorption equipment and makes With, it is possible to after the data of on-line real-time measuremen are analyzed, by the electricity in microprocessor controls extraction duct Magnet valve, is controlled feed rate;And by the liquid feeding pump on microprocessor controls feed tube, can be according to entering Gas speed controls the feed liquor speed of alkali liquor, it is achieved organic control;The setting of audible-visual annunciator, it is possible to when an oxygen The detected value of change nitrogen and nitrogen dioxide, beyond after pre-set value, carries out sound and light alarm, reminds operator.The present invention Simple in construction, easy to use, detection data are accurate, detect and combine with absorption, good absorbing effect, discharge dirt Contaminate little.
Accompanying drawing explanation
In order to be illustrated more clearly that the embodiment of the present invention or technical scheme of the prior art, below will be to embodiment Or the required accompanying drawing used is briefly described in description of the prior art, it should be apparent that, in describing below Accompanying drawing is only some embodiments of the present invention, for those of ordinary skill in the art, is not paying creation Property work on the premise of, it is also possible to obtain other accompanying drawing according to these accompanying drawings.
Fig. 1 is the structural representation of the present invention;
In figure: 1 air inlet pipe;2 tee Ts;3 detection pipelines;4 extraction duct;5 gas dryers;6 mix Mould assembling;7 thermal-insulation coats;8 force (forcing) pumps;9 pressure maintaining valves;10 test chamber;11 nitric oxide probes;12 dioxies Change nitrogen probe;13 alkali liquor absorption casees;131 casings;132 feed tubes;133 drain pipes;134 liquid feeding pumps; 14 microcontrollers;15 wireless modules;16 display screens;17 communicating pipes;18 check valves;19 electromagnetic valves;20 Audible-visual annunciator.
Detailed description of the invention
The invention provides Tail gas measuring absorption plant and installation method, the present configuration of a kind of nitric acid production Simply, easy to use, detection data are accurate, detect and combine with absorption, and good absorbing effect, exhaust emission is little.
Below in conjunction with the accompanying drawing in the embodiment of the present invention, the technical scheme in the embodiment of the present invention is carried out clear and Detailed description, it is clear that described embodiment is only a part of embodiment rather than all of the present invention Embodiment.Based on the embodiment in the present invention, those of ordinary skill in the art are not before making creative work Put all other embodiments obtained, broadly fall into the scope of protection of the invention.
The Tail gas measuring absorption plant of a kind of nitric acid production as shown in Figure 1 and installation method thereof, including air inlet pipe 1, tee T 2, detection pipeline 3, extraction duct 4, gas dryer 5, blending bin 6, thermal-insulation coat 7, Force (forcing) pump 8, pressure maintaining valve 9, test chamber 10, nitric oxide probe 11, nitrogen dioxide probe 12, alkali liquor are inhaled Receive case 13, microcontroller 14, wireless module 15, display screen 16, communicating pipe 17, check valve 18 and electromagnetism Valve 19, described air inlet pipe 1 connecting tee pipe 2,2 two gas outlets of described tee T connect detection pipeline respectively 3 and extraction duct 4, described detection pipeline 3 connects gas dryer 5, and described gas dryer 5 connects mixed Mould assembling 6, described blending bin 6 is externally provided with thermal-insulation coat 7, and described blending bin 6 connects force (forcing) pump 8, described in add Press pump 8 connects test chamber 10, and described force (forcing) pump 8 and test chamber 10 connect pipeline and be provided with pressure maintaining valve 9, institute Nitric oxide probe 11 and nitrogen dioxide probe 12, described nitric oxide probe 11 it is provided with in stating test chamber 10 With nitrogen dioxide probe 12 connection microcontroller 14, described microcontroller 14 is provided with wireless module 15, institute Stating microcontroller 14 and connect display screen 16 by wireless module 15, described extraction duct 4 connects alkali liquor absorption Case 13, described extraction duct 4 is provided with electromagnetic valve 19, and described electromagnetic valve 19 connects described microcontroller 14, It is communicated with pipe 17 between described extraction duct 4 and test chamber 10, described communicating pipe 17 is provided with check valve 18.The microcontroller 14 used in this technical scheme can be single-chip microcomputer, can be to list according to difference use environment The use model of sheet machine is changed.Display screen is wirelessly connected with microcontroller, it is achieved display merit Can, its position can arbitrarily be arranged, as long as conveniently observing, the most specific is fixed on a certain position.
Further, described alkali liquor absorption case 13 includes casing 131, feed tube 132, drain pipe 133 With liquid feeding pump 134, described extraction duct 4 end is stretched in described casing 131 below liquid level, described casing 131 One lower sidewall is provided with feed tube 132, and described another side wall upper part of casing 131 is provided with drain pipe 133, described Feed tube 132 is provided with liquid feeding pump 134, and described liquid feeding pump 134 connects described microcontroller 14.
Further, also include that audible-visual annunciator 20, described audible-visual annunciator 20 connect described microcontroller 14。
The use principle of the present invention is as follows:
Air inlet pipe 1 connecting tee pipe 2, connects detection pipeline 3 and extraction duct 4 respectively, and detection pipeline 3 enters Gas connects blending bin 6, carries out air inlet in blending bin 6 buffering and from mixing, and when can make to give vent to anger, gas becomes Divide mix homogeneously, prevent prohibited data detection true, test chamber 10 arranges nitric oxide probe 11 and dioxy Change nitrogen probe 12, by detection data feedback to microcontroller 14, microcontroller 14 detection data are passed through nothing Line mode sends display screen 16 to, it is achieved data detect display in real time, extraction duct 4 is by most nitre Acid produces tail gas and is passed in alkali liquor absorption case 13, it is achieved the absorption of tail gas, and arranges in extraction duct 4 Electromagnetic valve 19, is controlled electromagnetic valve 19 according to detection data by microcontroller 14, so that air inflow Mate with alkali liquor in lye tank, and liquid feeding pump 134 be set on the feed tube 132 of alkali liquor absorption case 13, The feed liquor speed of liquid feeding pump 134 is controlled so that it is can be with the air inflow of extraction duct 4 by microcontroller 14 Match, it is achieved thereby that organically mate, prevent tail gas absorption the most thorough;Microcontroller 14 is arranged Audible-visual annunciator 20, it is possible to when detected value is beyond pre-set value, send sound and light alarm, remind operator Take measures.
The invention have benefit that: by arranging blending bin in detection equipment, it is possible to by air inlet in mixing Carry out mix homogeneously in advance in case, prevent detecting data fluctuated;Detection equipment is combined with absorption equipment and makes With, it is possible to after the data of on-line real-time measuremen are analyzed, by the electricity in microprocessor controls extraction duct Magnet valve, is controlled feed rate;And by the liquid feeding pump on microprocessor controls feed tube, can be according to entering Gas speed controls the feed liquor speed of alkali liquor, it is achieved organic control;The setting of audible-visual annunciator, it is possible to when an oxygen The detected value of change nitrogen and nitrogen dioxide, beyond after pre-set value, carries out sound and light alarm, reminds operator.The present invention Simple in construction, easy to use, detection data are accurate, detect and combine with absorption, good absorbing effect, discharge dirt Contaminate little.
In this specification, each embodiment uses the mode gone forward one by one to describe, what each embodiment stressed is with The difference of other embodiments, between each embodiment, identical similar portion sees mutually.
Described above to the disclosed embodiments, makes professional and technical personnel in the field be capable of or uses this Bright.Multiple amendment to these embodiments is apparent from, herein for those skilled in the art Defined in General Principle can without departing from the spirit or scope of the present invention, in other embodiments Middle realization.Therefore, the present invention is not intended to be limited to the embodiments shown herein, and is to fit to and this Principle disclosed in literary composition and the consistent the widest scope of features of novelty.

Claims (3)

1. the Tail gas measuring absorption plant of a nitric acid production and installation method thereof, it is characterised in that: include into Trachea, tee T, detection pipeline, extraction duct, gas dryer, blending bin, thermal-insulation coat, force (forcing) pump, Pressure maintaining valve, test chamber, nitric oxide probe, nitrogen dioxide probe, alkali liquor absorption case, microcontroller, wireless Module, display screen, communicating pipe, check valve and electromagnetic valve, described air inlet pipe connecting tee pipe, described tee T Two gas outlets connect detection pipeline and extraction duct respectively, and described detection pipeline connects gas dryer, described Gas dryer connects blending bin, and described blending bin is externally provided with thermal-insulation coat, and described blending bin connects force (forcing) pump, Described force (forcing) pump connects test chamber, described force (forcing) pump and test chamber connection pipeline and is provided with pressure maintaining valve, described detection Intracavity is provided with nitric oxide probe and nitrogen dioxide is popped one's head in, and described nitric oxide probe and nitrogen dioxide probe connect Microcontroller, described microcontroller is provided with wireless module, and described microcontroller connects display by wireless module Screen, described extraction duct connects alkali liquor absorption case, and described extraction duct is provided with electromagnetic valve, and described electromagnetic valve is even Connect described microcontroller, be communicated with pipe between described extraction duct and test chamber, described communicating pipe be provided with list To valve.
2. the Tail gas measuring absorption plant of nitric acid production as claimed in claim 1 and installation method thereof, it is special Levy and be: described alkali liquor absorption case includes casing, feed tube, drain pipe and liquid feeding pump, described extraction duct end Portion stretches in described casing below liquid level, and described casing one lower sidewall is provided with feed tube, described casing opposite side Wall top is provided with drain pipe, and described feed tube is provided with liquid feeding pump, and described liquid feeding pump connects described microcontroller.
3. the Tail gas measuring absorption plant of nitric acid production as claimed in claim 2 and installation method thereof, it is special Levying and be: also include audible-visual annunciator, described audible-visual annunciator connects described microcontroller.
CN201610488059.9A 2016-06-27 2016-06-27 Tail gas detection and absorption device for nitric acid production and installation method thereof Pending CN105938139A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610488059.9A CN105938139A (en) 2016-06-27 2016-06-27 Tail gas detection and absorption device for nitric acid production and installation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610488059.9A CN105938139A (en) 2016-06-27 2016-06-27 Tail gas detection and absorption device for nitric acid production and installation method thereof

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CN105938139A true CN105938139A (en) 2016-09-14

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107024444A (en) * 2017-02-15 2017-08-08 武汉启呈环保技术有限公司 A kind of diesel engine denitration the escaping of ammonia tests reponse system
CN107561230A (en) * 2017-10-31 2018-01-09 电子科技大学中山学院 Air detection mechanism based on electric signal or wireless control
CN109030725A (en) * 2018-06-20 2018-12-18 佛山市川东磁电股份有限公司 A kind of connection structure of nitrogen dioxide sensor

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107024444A (en) * 2017-02-15 2017-08-08 武汉启呈环保技术有限公司 A kind of diesel engine denitration the escaping of ammonia tests reponse system
CN107561230A (en) * 2017-10-31 2018-01-09 电子科技大学中山学院 Air detection mechanism based on electric signal or wireless control
CN109030725A (en) * 2018-06-20 2018-12-18 佛山市川东磁电股份有限公司 A kind of connection structure of nitrogen dioxide sensor

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Application publication date: 20160914