CN105937109A - Multi-pipeline quantitative medium tank filling system of supercritical fluid waterless dyeing machine - Google Patents

Multi-pipeline quantitative medium tank filling system of supercritical fluid waterless dyeing machine Download PDF

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Publication number
CN105937109A
CN105937109A CN201610368954.7A CN201610368954A CN105937109A CN 105937109 A CN105937109 A CN 105937109A CN 201610368954 A CN201610368954 A CN 201610368954A CN 105937109 A CN105937109 A CN 105937109A
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supercritical fluid
medium
pipeline
high pressure
pressure
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CN201610368954.7A
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CN105937109B (en
Inventor
龙家杰
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Zhongke Shouwang waterless dyeing intelligent equipment (Suzhou) Co.,Ltd.
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Suzhou University
Nantong Textile and Silk Industrial Technology Research Institute
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Priority to CN201610368954.7A priority Critical patent/CN105937109B/en
Priority to PCT/CN2016/085184 priority patent/WO2017206195A1/en
Priority to US15/557,105 priority patent/US10294598B2/en
Publication of CN105937109A publication Critical patent/CN105937109A/en
Priority to TW106117703A priority patent/TWI649473B/en
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    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06BTREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
    • D06B9/00Solvent-treatment of textile materials
    • D06B9/02Solvent-treatment of textile materials solvent-dyeing
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/94General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using dyes dissolved in solvents which are in the supercritical state
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06BTREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
    • D06B19/00Treatment of textile materials by liquids, gases or vapours, not provided for in groups D06B1/00 - D06B17/00
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06BTREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
    • D06B23/00Component parts, details, or accessories of apparatus or machines, specially adapted for the treating of textile materials, not restricted to a particular kind of apparatus, provided for in groups D06B1/00 - D06B21/00
    • D06B23/20Arrangements of apparatus for treating processing-liquids, -gases or -vapours, e.g. purification, filtration or distillation
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06BTREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
    • D06B23/00Component parts, details, or accessories of apparatus or machines, specially adapted for the treating of textile materials, not restricted to a particular kind of apparatus, provided for in groups D06B1/00 - D06B21/00
    • D06B23/20Arrangements of apparatus for treating processing-liquids, -gases or -vapours, e.g. purification, filtration or distillation
    • D06B23/205Arrangements of apparatus for treating processing-liquids, -gases or -vapours, e.g. purification, filtration or distillation for adding or mixing constituents of the treating material
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06BTREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
    • D06B9/00Solvent-treatment of textile materials
    • D06B9/06Solvent-treatment of textile materials with recovery of the solvent
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06BTREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
    • D06B23/00Component parts, details, or accessories of apparatus or machines, specially adapted for the treating of textile materials, not restricted to a particular kind of apparatus, provided for in groups D06B1/00 - D06B21/00
    • D06B23/10Devices for dyeing samples

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Treatment Of Fiber Materials (AREA)

Abstract

The present invention relates to a multi-pipeline quantitative medium tank filling system of a supercritical fluid waterless dyeing machine. The multi-pipeline quantitative medium tank filling system comprises a supercritical fluid medium reservoir, a stop valve and a medium filter which are successively connected through a high-pressure main pipe, and at least two and more than two tank filling branches which are mutually independent and simultaneously connected with the medium filter. Each tank filling branch comprises a booster pump, a supercritical fluid high-pressure mass flowmeter, a high-pressure ball valve and a dyeing unit which are successively connected in a medium forward direction through a high-pressure branch pipe. By adoption of the mutually independent multi-branch tank filling systems in a mass metering manner, accurate quantitative medium tank filling can be simultaneously carried out for a plurality of independent dyeing units effectively, differentiation tank filling of different medium masses of different dyeing units can also be achieved, the disadvantages of unreliability, inaccuracy and low service efficiency of a traditional method are overcome, and the dyeing operation process becomes simple, scientific and feasible.

Description

A kind of multi-pipeline quantitative medium tank charging system of supercritical fluid non-aqueous dyeing machine
Technical field
The invention belongs to pressure vessel and textile dyeing and finishing equipment manufacturing technology field, particularly relate to a kind of supercritical The multi-pipeline quantitative medium tank charging system of liquid waterless staining machine.
Background technology
Supercritical CO2Fluid is a kind of environmental protection, safe, green fluid media (medium).Traditional water bath is replaced with it Textile is carried out pre-treatment, dyeing or Final finishing processing, thoroughly realize from source textile green, Environmental protection, ecology produce, and the most also have the advantages such as energy-conservation.Therefore, with supercritical CO2Fluid is representative The anhydrous dyeing and finishing technique of supercritical fluid and the research and development of change system, be to traditional textile dyeing Secondary technological revolution, to realizing the sustainable development of industry and preserving the ecological environment etc. the most significant.
Recently as the development of technology, the supercritical CO of textile2Waterless staining technique has started to enter into Commercialization stage.Its applicable change system have also been obtained to be greatly developed, as successively occurred in that supercritical CO2Stream Vertical or the horizontal beam dyeing of body, and the cooked mode such as the dye gigging of twin shaft pattern and rope form.
Wherein, " a kind of production system using supercritical fluid to carry out continuous dyeing and production technology thereof " (CN101024922A) Chinese invention patent reports a kind of integrated form dyeing caldron and system, including mutually Supercritical fluid feeding mechanism, dye cycle device and the supercritical fluid retracting device of connection, wherein dyes Circulating device includes at least two integrated dyeing kettle, and integrated dyeing kettle makes in same still Can complete the dissolving of dyestuff simultaneously, and can be 10-45Mpa at supercritical fluid pressures, temperature be The Colour Difference of fabric is completed under the conditions of 100-180 DEG C.
The Chinese invention of " with the method and apparatus for the treatment of with supercritical fluid textile substrates " (CN1200153A) In patent, describe a kind of for packing resultant yarn cylinder or the vertical warp beam high pressure dyeing of package endless fabric dyeing Still and system, and processing temperature and time can be controlled regulation, can constant pressure such as 280 bar with Dye under the conditions of the treatment temperature raised.
Chinese invention patent " one supercritical carbon dioxide fluid in Publication No. CN101824716A Device and method to textile dyeing " in, disclose the special seamless warp beam being made up of inside and outside two-layer, and The wound fabric outermost layer suit netted infantees of seamless knitted cylinder, at supercritical carbon dioxide fluid pressure be Under the conditions of 10MPa~30Mpa, temperature are 90 DEG C~140 DEG C, use fluid circulation alternate with hydrostatic Dyeing, to realize the level dyeing processing of piece dyeing fabric in supercritical carbon dioxide fluid.Open Number for Chinese invention patent " a kind of knitting with supercritical carbon dioxide fluid as medium of CN102747566A Thing rope dyeing machine and colouring method " in, disclose and be arranged on carrying cloth wheel system in color jar, and pass through The draw of selvage guide rope drives fabric in rope form to carry out order cycle motion, and conservative control dyeing fluid jointly The technological parameters such as circular flow, fabric circulation speed, dyeing temperature and pressure, to realize supercritical dioxy Change the fabric in rope form piece dyeing in carbon fluid media (medium).Additionally, at the middle promulgated by the State Council of Publication No. CN101760914A In bright patent " supercritical dyeing machine ", also disclose that containing dye cycle system, enter distribution system, separation and recovery The fabrics in roped form piece dyeing staining machine of the composition such as system, the non-aqueous dyeing that fabric realizes pine formula tension-free state adds Work.
But, the process unit system such as all kinds of supercritical fluid non-aqueous dyeings disclosed above, it is typically all and exists The dissolving of dyestuff, upper dye behavior is controlled by regulation system medium pressure under the conditions of uniform temperature, thus Realize the processing such as the dyeing to textile.In other words, these change systems are all to set the goal dye one at present During color temperature, indirectly control the number of required dyeing medium with the height of system pressure.But in practical operation During, especially during to system boost, it is generally not capable of accurately realizing a supercharging and enters system Medium, right up to required dyeing pressure or required dyeing medium when system is warmed up to target coloration temperature Amount.Thus, generally on the basis of combining early stage experience, and reach at system temperature or be i.e. up to dyeing During temperature, the mode continuing to carry out system repeatedly supercharging or decompression realizes.It is obvious that it is this to system The tank of medium fills or boost mode, has the biggest unreliability and inaccuracy, not only makes dyeing course Operation becomes complicated and loaded down with trivial details, and what is more important can make dyeing condition during repeatedly pressure regulation There is fluctuation and change, especially during pressure regulation, easily cause the change of dyeing temperature and time, so that product Cylinder difference becomes big, and repeatability becomes to be difficult to control to.Also thus significantly impact non-aqueous dyeing product the percentage of A-class goods and The application that its industrialization produces.Additionally, the supercharging of the most general supercritical fluid non-aqueous dyeing machine or Tank charging system, is all that its service efficiency is low with fixing dye vat one to one, be not suitable for industrialization produce, Especially commercialization colour combination such as is drawn a design at high efficiency and the differential demand.
Because above-mentioned defect, the design people, the most in addition research and innovation, to founding a kind of novel knot The multi-pipeline quantitative medium tank charging system of the supercritical fluid non-aqueous dyeing machine of structure so that it is have more in industry Value.
Summary of the invention
For solving above-mentioned technical problem, it is an object of the invention to provide a kind of supercritical fluid non-aqueous dyeing machine Multi-pipeline quantitative medium tank charging system, for the multi-pipeline quantitative medium tank charging system of mass metrology pattern, can be real Now independent dye unit multiple to supercritical fluid non-aqueous dyeing machine carry out disposable accurately tank simultaneously and fill supercharging Or differential tank fills supercharging, and have efficiency high, easy and simple to handle, on dyeing condition without impact, product The advantages such as cylinder difference is little, repeatability good, reliable and stable, wide accommodation.
The multi-pipeline quantitative medium tank charging system of the supercritical fluid non-aqueous dyeing machine of the present invention, including by height Supercritical fluid media bin that pressure main pipeline is sequentially connected with, stop valve, medium filter, and at least Article two, and above tank separate, that be simultaneously connected with described medium filter fills branch road, each described tank fills Road all includes by high pressure bypass line successively along booster pump, the shooting flow height of the connection of medium direction of advance Pressure mass flowmenter, high-pressure ball valve and dye unit, wherein
-described supercritical fluid media bin has medium entrance and media outlet, described medium entrance and gas Source connects, and described media outlet is connected with described stop valve by described high voltage charge road;
The entrance point of-each described booster pump all with described high voltage charge road connection be connected described medium filter, The port of export connects with each described supercritical fluid high pressure mass flowmenter respectively, and respectively by each described supercritical Fluid high-pressure mass flowmenter controls its start and stop;
The entrance point of-each described supercritical fluid high pressure mass flowmenter by described high pressure bypass line respectively with The connection of each described booster pump, the port of export are connected with each described high-pressure ball valve respectively by described high pressure bypass line, Each described supercritical fluid high pressure mass flowmenter is connected with each described booster pump coordinated signals the most respectively, and leads to Cross the measurement of shooting flow weight, density and temperature flowed through, transmission, and to required fluid mass The coordinated signals signal such as predetermined set control the start and stop of each described booster pump;
One end of-each described high-pressure ball valve by described high pressure bypass line respectively with each described shooting flow height Pressure mass flowmenter connection, the other end is connected with each dye unit respectively, needed for respectively to each dye unit The quantitative pot of dyeing medium fills.
Further, described source of the gas enters described super after being processed by pressure piping, stop valve condensed device Critical fluids media reservoir.
Further, described medium entrance is arranged on away from described supercritical fluid media bin top 10-50cm Place, described media outlet is arranged on bottom described supercritical fluid media bin at 5-50cm.
Further, described supercritical fluid high pressure mass flowmenter be suitable for pressure be 0-70MPa, temperature be -50℃-150℃。
Further, described booster pump is gas boosting pump, liquid booster pump, high-pressure plunger pump, membrane pump In one.
Further, each described dye unit is connected with separating and reclaiming device also by high voltage charge road simultaneously, Described separating and reclaiming device is connected with described condenser by stop valve.
Further, in order to be passed through the cut-off that the stop valve of described source of the gas is connected with described separating and reclaiming device Valve is connected with described condenser by Highpressure Tee pipeline.
Further, described dye unit is fixing high pressure dye vat or the high pressure processing vessels of movable type.
By such scheme, the present invention at least has the advantage that
Owing to have employed mass metrology pattern, separate, multiple branch circuit tank charging system, can effectively realize Multiple independent dye unit are carried out accurate quantitative analysis medium tank to fill simultaneously, and different Jie of coloured differently unit Matter qualitative difference tank fills, thus overcomes the unreliability of traditional method, inaccuracy, and uses The shortcomings such as efficiency is low, also make dying operation process become easy simultaneously and science are feasible;Additionally, use this Bright tank charging system, can avoid existing and traditional method to be made dyeing condition during repeatedly pressure regulation The fluctuation become and change, also thus can effectively alleviate or to reduce cylinder poor, the repeatability of raising product;Meanwhile, The present invention is also adapted to the industrialization of supercritical fluid non-aqueous dyeing and produces, and particularly commercialization colour combination is drawn a design High efficiency and differential accurate tank fill demand.Thus, the present invention is remarkably improved supercritical fluid non-aqueous dyeing Production and processing efficiency and the percentage of A-class goods of non-aqueous dyeing product, on source solve textile printing and dyeing industry pollute The generation of thing and discharge, it is achieved the saving energy, lowering energy consumption and reducing pollutants discharge of textile printing and dyeing industry, cleaning produce, and have the widest Wealthy application prospect and important practical significance.
Described above is only the general introduction of technical solution of the present invention, in order to better understand the technology of the present invention Means, and can being practiced according to the content of description, below with presently preferred embodiments of the present invention and coordinate attached After figure describes in detail such as.
Accompanying drawing explanation
Fig. 1 is the supercritical fluid dyeing machine operation principle schematic diagram that the embodiment of the present invention provides.
In figure: 1, supercritical fluid media bin, 1-1, media outlet, 1-2, medium entrance, (2,9, 10,12,13), stop valve, 3, medium filter, 4, booster pump, 5, supercritical fluid high pressure quality Effusion meter, the coordinated signals signal of 5-1, mass flowmenter and booster pump, 6, ball valve, 7, dye unit, 8, Separating and reclaiming device, 10-1, Highpressure Tee pipeline, 11, condenser, 14, high voltage charge road, (n1、n2..., ni-1、ni, i 2), tank fill branch road.
Detailed description of the invention
Below in conjunction with the accompanying drawings and embodiment, the detailed description of the invention of the present invention is described in further detail.With Lower embodiment is used for illustrating the present invention, but is not limited to the scope of the present invention.
See Fig. 1, the multi-pipeline of a kind of supercritical fluid non-aqueous dyeing machine described in a preferred embodiment of the present invention Quantitatively medium tank charging system, it includes that the supercritical fluid media being sequentially connected with by high voltage charge road 14 is stored Device 1, stop valve 2, medium filter 3, and at least two and above separate, simultaneously with medium mistake The tank that filter 3 connects fills branch road, and each tank is filled branch road and all includes being advanced along medium successively by high pressure bypass line Booster pump 4, supercritical fluid high pressure mass flowmenter 5, high-pressure ball valve 6 and the dye unit 7 that direction connects.
Separate tank fills branch road n1、n2、…、ni-1、ni(i 2), sequentially with high voltage charge road 14 Connection, each independent tank fills the booster pump 4 in branch road, supercritical fluid high pressure mass flowmenter 5, high-pressure ball valve 6 are sequentially connected by high pressure bypass line along medium direction of advance respectively with dye unit 7.The most each booster pump The entrance point of 4 all connects with high voltage charge road 14, the port of export the most respectively with supercritical fluid high pressure mass flow Meter 5 is connected;The port of export of supercritical fluid high pressure mass flowmenter 5 is by high pressure bypass line and height simultaneously Pressure ball valve 6 connects, and high-pressure ball valve 6 is connected with dye unit 7 by high pressure bypass line.Wherein surpass and face Boundary's fluid high-pressure mass flowmenter 5 can be directly realized by shooting flow weight, the density flowing through place branch road With temperature survey and display, and the predetermined set to required fluid mass can be realized, and then pass through shooting flow Height pressure mass flowmenter 5 and the coordinated signals signal 5-1 of booster pump 4 are real to start and stop and the flow of booster pump 4 Existing coordinated signals, to reach to fill the quantitative quality tank of supercritical fluid media in each independent dye unit 7.
Medium filter 3 on high voltage charge road 14 and the media outlet 1-1 of supercritical fluid media bin 1 It is connected.Wherein medium filter 3, can realize and ensure to treat purification and the remove impurity process of filling medium.
Separate tank fills branch road n1、n2、…、ni-1、ni(i 2), at the supercritical fluid of its correspondence Under the high pressure mass flowmenter 5 coordinated signals to booster pump 4, can realize simultaneously to multiple independent dye unit 7 Carry out accurate quantitative analysis medium tank to fill, and the different medium qualitative difference tank of coloured differently unit 7 fills.
Medium source of the gas needed for the system of the present invention is accessed by Highpressure Tee pipeline 10-1, stop valve 10, and Condensed device 11 process laggard enter supercritical fluid media reservoir 1 standby.
Each branch road mesohigh ball valve 6 is connected with dye unit 7 by high pressure bypass line one end, the other end and Supercritical fluid high pressure mass flowmenter 5 is connected, opened by it make supercritical fluid media bin 1 with Dye unit 7 connects, thus realizes filling the quantitative pot of dyeing medium needed for dye unit 7.
In each branch road, booster pump 4 can use gas boosting pump or liquid booster pump, or high-pressure plunger pump, barrier film Pump, its outlet is connected with supercritical fluid high pressure mass flowmenter 5 by high pressure bypass line.Its start and stop and Flow is controlled by the output signal of front supercritical fluid high pressure mass flowmenter 5, to realize dye unit 7 Quantitative pot fill.
Supercritical fluid media bin 1 is provided with media outlet 1-1 and medium entrance 1-2, and its medium goes out Mouth 1-1 is arranged on bottom supercritical fluid media bin 1 at 5-50cm, and by high voltage charge road 14 Being connected with stop valve 2, stop valve 2 is connected with medium filter 3 again simultaneously, and medium entrance 1-2 is arranged on At supercritical fluid media bin 1 top 10-50cm, and by high voltage charge road and stop valve 12, Condenser 11 order is connected, and reaching the acceptance to medium source of the gas, stores and the function such as output.
Each separate dye unit 7 can be fixing all kinds of multi-forms, difformity and different appearance The high pressure dye vat of amount, it is possible to be that portable textile dyeing, pre-treatment or Final finishing process HIGH PRESSURE TREATMENT Container.Its one end is connected with high-pressure ball valve 6, the other end on-demand can or not with separating and reclaiming device 8, stop valve 9, condenser 11 order is connected.
When the multi-pipeline quantitative medium tank charging system of the supercritical fluid non-aqueous dyeing machine of the present invention works, first Close stop valve 9,13,2, and opening stop valve 10,12 and condenser 11, by Highpressure Tee pipeline The tank that 10-1 makes medium source of the gas that supercritical fluid media bin 1 is carried out storage medium fills, and closes after completing Stop valve 10, disconnects source of the gas.To treat that each dye unit 7 that tank fills accesses each tank by high pressure bypass line and fills Branch road n1、n2、…、ni-1、ni(i 2), and be connected with branch road mesohigh ball valve 6 respectively, distinguish simultaneously Corresponding supercritical fluid high pressure mass flowmenter 5 is preset the quality of the required medium of dyeing, is then turned on Stop valve 2 in high voltage charge road 14, and open each branch road mesohigh ball valve 6, start super in each branch road facing The quantitative pot that boundary's fluid high-pressure mass flowmenter 5 carries out dyeing medium to each dye unit 7 fills;Meanwhile, respectively The supercritical fluid high pressure mass flowmenter 5 medium temperature to being flowed through, density, instantaneous and accumulation in branch road Flow is monitored and shows, and will treat that filling medium quality information is transferred to correspondence by coordinated signals signal 5-1 Booster pump 4, to realize the coordinated signals of its start and stop and flow, thus reach each corresponding dye unit 7 institute The disposable accurate quantitative analysis tank needing supercritical fluid media fills.Predetermined tank filling medium is reached when there being dye unit 7 During quality, booster pump 4 pump trip of its correspondence, the high-pressure ball valve 6 being then shut off in this branch road, it is right to complete The quantitative pot of this dye unit 7 fills.
For fixed dye unit, tank then can be according to predetermined dyeing after filling end, directly to each dye Color element carries out heating up and completing dyeing course;And to portable dye unit, then itself and tank can be filled branch road Disconnect, be then transported in suitable device carry out the dyeing that heats up;Meanwhile, to fill branch road the most repeatable for each tank Said process continues other dye unit to be filled are carried out quantitative pot to fill, and fills the efficient of pressure charging system realizing tank Utilize.
Additionally, the most each fixed dye unit or portable dye unit, dyeing all can be on-demand after terminating It is connected with separating and reclaiming device 8, to complete dyeing medium and the separation of residual dye and recycling, with And the dye post processing etc. of product.
The above is only the preferred embodiment of the present invention, is not limited to the present invention, it is noted that For those skilled in the art, on the premise of without departing from the technology of the present invention principle, also Can make some improvement and modification, these improve and modification also should be regarded as protection scope of the present invention.

Claims (8)

1. the multi-pipeline quantitative medium tank charging system of a supercritical fluid non-aqueous dyeing machine, it is characterised in that: Including the supercritical fluid media bin being sequentially connected with by high voltage charge road, stop valve, medium filter, And at least two and above tank separate, that be connected with described medium filter fill branch road, each institute simultaneously State tank to fill branch road and all include the booster pump connected along medium direction of advance successively by high pressure bypass line, super face Boundary's fluid high-pressure mass flowmenter, high-pressure ball valve and dye unit, wherein
-described supercritical fluid media bin has medium entrance and media outlet, described medium entrance and gas Source connects, and described media outlet is connected with described stop valve by described high voltage charge road;
The entrance point of-each described booster pump all with described high voltage charge road connection be connected described medium filter, The port of export connects with each described supercritical fluid high pressure mass flowmenter respectively, and respectively by each described supercritical Fluid high-pressure mass flowmenter controls its start and stop;
The entrance point of-each described supercritical fluid high pressure mass flowmenter is by described high pressure bypass line respectively Connect with each described booster pump, the port of export is connected with each described high-pressure ball valve respectively by described high pressure bypass line Logical, each described supercritical fluid high pressure mass flowmenter is connected with each described booster pump coordinated signals the most respectively, And pass through the measurement of shooting flow weight, density and temperature flowed through, transmission, and to required fluid The coordinated signals signals such as the predetermined set of quality control the start and stop of each described booster pump;
One end of-each described high-pressure ball valve by described high pressure bypass line respectively with each described supercritical fluid High pressure mass flowmenter connects, and the other end is connected with each dye unit respectively, with respectively to each dye unit institute The quantitative pot needing dyeing medium fills.
The quantitative medium tank of multi-pipeline of supercritical fluid non-aqueous dyeing machine the most according to claim 1 is filled and is System, it is characterised in that: described source of the gas enters described after being processed by pressure piping, stop valve condensed device Supercritical fluid media bin.
The quantitative medium tank of multi-pipeline of supercritical fluid non-aqueous dyeing machine the most according to claim 1 and 2 Charging system, it is characterised in that: described medium entrance is arranged on away from described supercritical fluid media bin top At 10-50cm, described media outlet is arranged on bottom described supercritical fluid media bin at 5-50cm.
The quantitative medium tank of multi-pipeline of supercritical fluid non-aqueous dyeing machine the most according to claim 1 is filled and is System, it is characterised in that: it is 0-70MPa, temperature that described supercritical fluid high pressure mass flowmenter is suitable for pressure For-50 DEG C-150 DEG C.
The quantitative medium tank of multi-pipeline of supercritical fluid non-aqueous dyeing machine the most according to claim 1 is filled and is System, it is characterised in that: described booster pump is gas boosting pump, liquid booster pump, high-pressure plunger pump, barrier film One in pump.
The quantitative medium tank of multi-pipeline of supercritical fluid non-aqueous dyeing machine the most according to claim 2 is filled and is System, it is characterised in that: each described dye unit also by high voltage charge road even with separating and reclaiming device simultaneously Connecing, described separating and reclaiming device is connected with described condenser by stop valve.
The quantitative medium tank of multi-pipeline of supercritical fluid non-aqueous dyeing machine the most according to claim 6 is filled and is System, it is characterised in that: in order to be passed through that the stop valve of described source of the gas is connected with described separating and reclaiming device section Only valve is connected with described condenser by Highpressure Tee pipeline.
The quantitative medium tank of multi-pipeline of supercritical fluid non-aqueous dyeing machine the most according to claim 7 is filled and is System, it is characterised in that: described dye unit is fixing high pressure dye vat or the high pressure processing vessels of movable type.
CN201610368954.7A 2016-05-30 2016-05-30 A kind of quantitative medium tank charging system of multi-pipeline of supercritical fluid non-aqueous dyeing machine Active CN105937109B (en)

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CN201610368954.7A CN105937109B (en) 2016-05-30 2016-05-30 A kind of quantitative medium tank charging system of multi-pipeline of supercritical fluid non-aqueous dyeing machine
PCT/CN2016/085184 WO2017206195A1 (en) 2016-05-30 2016-06-08 Multi-pipe quantitative medium refill system of supercritical fluid anhydrous dyeing machine
US15/557,105 US10294598B2 (en) 2016-05-30 2016-06-08 Multi-pipe quantitative medium filling system of supercritical fluid dyeing machine
TW106117703A TWI649473B (en) 2016-05-30 2017-05-26 Multi-channel quantitative medium tank filling system for supercritical fluid waterless dyeing machine

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CN106801308A (en) * 2016-11-21 2017-06-06 大连工业大学 A kind of anhydrous dyeing and finishing system and method for intelligent supercritical carbon dioxide fluid
CN110899248A (en) * 2019-06-21 2020-03-24 杭州杭氧股份有限公司 System and method for cleaning ultrahigh-purity gas steel cylinders in batch by using supercritical fluid

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CN105937113B (en) * 2016-05-30 2018-03-30 南通纺织丝绸产业技术研究院 A kind of separation and recovery and Self-cleaning system of supercritical fluid non-aqueous dyeing machine
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