CN105926056A - Hydrogel fiber production technology and equipment - Google Patents

Hydrogel fiber production technology and equipment Download PDF

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Publication number
CN105926056A
CN105926056A CN201610505034.5A CN201610505034A CN105926056A CN 105926056 A CN105926056 A CN 105926056A CN 201610505034 A CN201610505034 A CN 201610505034A CN 105926056 A CN105926056 A CN 105926056A
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CN
China
Prior art keywords
hydrogel
aquagel fibre
raw material
material tank
equipment
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610505034.5A
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Chinese (zh)
Inventor
古元安
李秦龙
潘大庆
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Beijing Health Guangji Biotechnology Co Ltd
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Beijing Health Guangji Biotechnology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
Application filed by Beijing Health Guangji Biotechnology Co Ltd filed Critical Beijing Health Guangji Biotechnology Co Ltd
Priority to CN201610505034.5A priority Critical patent/CN105926056A/en
Publication of CN105926056A publication Critical patent/CN105926056A/en
Pending legal-status Critical Current

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Classifications

    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01DMECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
    • D01D5/00Formation of filaments, threads, or the like
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01DMECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
    • D01D13/00Complete machines for producing artificial threads

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  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Textile Engineering (AREA)
  • Spinning Methods And Devices For Manufacturing Artificial Fibers (AREA)

Abstract

The invention relates to a hydrogel fiber production technology and equipment, and belongs to the technical field of fiber preparation. The hydrogel fiber production equipment comprises a raw material tank, a drainage pipeline, a spinneret device, a radiation device, a conveying crawler and a pressurizing device, wherein one free end of the drainage pipeline is connected with the bottom part of the raw material tank, the pressurizing device is arranged in the drainage pipeline, and the spinneret device is arranged at the other free end of the drainage pipeline; the radiation device is an arc-shaped pipeline, a spinneret head is arranged in a first end of the arc-shaped pipeline, and the conveying crawler is arranged near a second end of the arc-shaped pipeline. The hydrogel fiber production technology and the equipment have the advantages that the operation is simple, the production efficiency is high, the continuous industrialized production is easily realized, and the pollution is avoided in the process; the dry toughness of prepared hydrogel fiber is good, the single spinning is realized, the water absorbing and remaining capability is strong, and the biological compatibility is good; prepared non-woven cloth can be directly attached to a wound, and the purpose of quickly stopping bleeding is realized.

Description

Aquagel fibre production technology and equipments
Technical field
The present invention relates to technical field prepared by fiber, it is more particularly related to a kind of aquagel fibre production technology and Equipment.
Background technology
In the prior art, aquagel fibre mainly has two classes, a class to be to be with vinyl hydrophilic polymers such as acrylate copolymers The water-absorption fiber of main body;Another kind of is the one-component based on natural biomass or multicomponent hydrophilic fibers.In the prior art, All using high temeperature chemistry crosslinking technological or pyrohydrolysis technology in aquagel fibre preparation process, high to equipment requirement, energy disappears Consumption is big, and production cost is high, easily causes environmental pollution.ZL200910100525 discloses a kind of double-network hydrogel, its with the moon from Subtype vinyl monomer is the first monomer, and ultraviolet lighting obtains single network aqueous gel, and this list network aqueous gel is containing acrylamide The aqueous solution of class vinyl monomer, crosslinking agent and initiator is swelling to balance, then obtains double-network hydrogel with ultraviolet light irradiation. But gained gel is limited by the shape and size of template, the most block hydrogel, it is impossible to being processed into fiber, production efficiency is low Under, it is difficulty with industrialization.
Summary of the invention
In order to solve above-mentioned technical problem of the prior art, it is an object of the invention to provide a kind of aquagel fibre production technology And equipment.
In order to solve to invent described technical problem and realize goal of the invention, a first aspect of the present invention have employed techniques below scheme:
A kind of aquagel fibre produces equipment, it is characterised in that including: raw material tank, drainage pipe, spinning appts, irradiation devices, Transmit crawler belt and pressue device;Described raw material tank is used for containing hydrogel stoste, and described drainage pipe is L-shaped and includes vertical Pipeline and horizontal pipeline, the free end of wherein said vertical duct is connected with the bottom of described raw material tank, described horizontal pipeline interior Portion is provided with pressue device, and the free end of described horizontal pipeline is provided with spinning appts;Described irradiation devices are with purple The arc pipe of outer light, described spinning head is arranged in the first end of described arc pipe, and described transmission crawler belt is arranged on described arc Near second end of shape pipeline.
Wherein, described spinning appts is multi-holed jet or porous spinneret.
Wherein, described arc pipe is provided with recirculated cooling water pipeline.
A second aspect of the present invention further relates to a kind of aquagel fibre production technology, it is characterised in that comprise the following steps:
(1) ready hydrogel stoste is contained in described raw material tank;
(2) described hydrogel stoste is entered in horizontal pressue device by drainage pipe after stirring;
(3) described hydrogel stoste is sprayed by spinning appts after pressurization, and enters in irradiation devices, through hardening with radiation After shaping, form aquagel fibre through transmitting crawling traction.
Wherein, described aquagel fibre is single fiber finished product.
Wherein, being provided with fiber in the hole of described multi-holed jet or porous spinneret, the product obtained is hydrogel covered fiber.
Compared with immediate prior art, aquagel fibre production technology and equipments of the present invention has the advantages that
The aquagel fibre production technology and equipments of this method is simple to operate, and production efficiency is high, easily realizes continuous industrial production, Process is pollution-free;And the aquagel fibre dry state good toughness prepared, can individually spin, there is the strongest water suction and water conservation Ability, and good biocompatibility, the non-woven fabrics made can directly stick on wound, it is possible to reaches the purpose of quick-acting haemostatic powder.
Accompanying drawing explanation
Fig. 1 is the structural representation of the aquagel fibre production equipment of the present invention.
Detailed description of the invention
Below with reference to specific embodiment, aquagel fibre production technology and equipments of the present invention is further elaborated, with Help those skilled in the art that inventive concept, the technical scheme of the present invention are had more complete, accurate and deep understanding;Need It is pointed out that in embodiment that the description about structure, function and material etc. is all exemplary, and does not implies that invention protection The restriction of scope.
As it is shown in figure 1, the aquagel fibre of the present invention produces equipment, including: raw material tank 1, drainage pipe 2, spinning appts 3, Irradiation devices 4, transmission crawler belt 5 and pressue device 6.Described raw material tank is used for containing hydrogel stoste, described drainage pipe 2 in L-shaped and include vertical duct 21 and horizontal pipeline 22, the free end 23 of wherein said vertical duct 21 and described raw material tank Bottom connects, described horizontal pipeline 22 be internally provided with pressue device 6, and at the free end 24 of described horizontal pipeline 22 It is provided with spinning appts 3.Described irradiation devices 4 are the arc pipe with ultraviolet light, and described spinning appts 3 is arranged on described In first end 41 of arc pipe, described transmission crawler belt 5 is arranged near the second end 42 of described arc pipe.Described spinneret Device is multi-holed jet or porous spinneret, and described arc pipe is provided with recirculated cooling water pipeline (not shown).Adopt Produce equipment with above-mentioned aquagel fibre and prepare the technique of aquagel fibre, comprise the following steps: (1) is by ready hydrogel Stoste is contained in described raw material tank;(2) described hydrogel stoste enters horizontal pressue device by drainage pipe after stirring In;(3) described hydrogel stoste is sprayed by spinning appts after pressurization, and enters in irradiation devices, becomes through hardening with radiation After shape, form aquagel fibre through transmitting crawling traction.Described aquagel fibre can be single fiber finished product, when water-setting to be prepared During glue covered fiber, pre-set fiber as sandwich layer using arranging in the hole of multi-holed jet or porous spinneret.
As exemplary and preferably, in the present invention, described hydrogel stoste is prepared by the following method and obtains: by carboxymethyl Shitosan, amide-containing monomer are added to the water with poly-(methyl) ethyl acrylate, stir, and after deaeration, prepare hydrogel Stoste, wherein, carboxymethyl chitosan, amide-containing monomer are 100: 2~5: 3~5 with the weight ratio of poly-(methyl) ethyl acrylate. Described amide-containing monomer such as can select Methacrylamide, N-butoxy methyl acrylamide N, N-dimethyl allene acyl Amine, N, N-acrylamide, N, N-dimethyl-to styrene sulfonamide, N, N-dimethylaminoethylacryl acyl Amine, N, N-diethylaminoethyl etc..Utilize this hydrogel stoste use the present invention aquagel fibre equipment and The fracture strength of aquagel fibre prepared by technique can reach 2.5~3.5cN/dtex, elongation at break can reach 1000% with On, inhaling pure water multiplying power can be to 80~150g/g, compared with the aquagel fibre prepared only with carboxymethyl chitosan stoste, disconnected Resistance to spalling and elongation at break all can be enhanced about more than once, and the non-woven fabrics that the aquagel fibre prepared is made can be rapid Absorb moisture in blood, make the haemocyte in blood condense in wound surface, block broken blood vessels, such that it is able to reach fast short stopping The effect of blood.
For the ordinary skill in the art, the present invention is simply exemplarily described by specific embodiment, it is clear that this Invention implements and is not subject to the restrictions described above, as long as the method design that have employed the present invention is various with what technical scheme was carried out The improvement of unsubstantiality, or the most improved design by the present invention and technical scheme directly apply to other occasion, all at this Within bright protection domain.

Claims (6)

1. an aquagel fibre produces equipment, it is characterised in that including: raw material tank, drainage pipe, spinning appts, irradiation fill Put, transmit crawler belt and pressue device;Described raw material tank is used for containing hydrogel stoste, and described drainage pipe is L-shaped and includes Vertical duct and horizontal pipeline, the free end of wherein said vertical duct is connected with the bottom of described raw material tank, described horizontal pipeline Be internally provided with pressue device, and the free end of described horizontal pipeline is provided with spinning appts;Described irradiation devices are band Having the arc pipe of ultraviolet light, described spinning head to be arranged in the first end of described arc pipe, described transmission crawler belt is arranged on institute State near the second end of arc pipe.
Aquagel fibre the most according to claim 1 produces equipment, it is characterised in that: described spinning appts is porous spinneret Head or porous spinneret.
Aquagel fibre the most according to claim 1 produces equipment, it is characterised in that: it is provided with on described arc pipe and follows Ring cooling water pipeline.
4. utilizing aquagel fibre described in any one of claim 1~3 to produce equipment and prepare a technique for aquagel fibre, it is special Levy and be to comprise the following steps:
(1) ready hydrogel stoste is contained in described raw material tank;
(2) described hydrogel stoste is entered in horizontal pressue device by drainage pipe after stirring;
(3) described hydrogel stoste is sprayed by spinning appts after pressurization, and enters in irradiation devices, through hardening with radiation After shaping, form aquagel fibre through transmitting crawling traction.
Technique the most according to claim 4, it is characterised in that: described aquagel fibre is single fiber finished product.
Technique the most according to claim 4, it is characterised in that: arrange in the hole of described multi-holed jet or porous spinneret Having fiber, the product obtained is hydrogel covered fiber.
CN201610505034.5A 2016-06-30 2016-06-30 Hydrogel fiber production technology and equipment Pending CN105926056A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610505034.5A CN105926056A (en) 2016-06-30 2016-06-30 Hydrogel fiber production technology and equipment

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610505034.5A CN105926056A (en) 2016-06-30 2016-06-30 Hydrogel fiber production technology and equipment

Publications (1)

Publication Number Publication Date
CN105926056A true CN105926056A (en) 2016-09-07

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CN201610505034.5A Pending CN105926056A (en) 2016-06-30 2016-06-30 Hydrogel fiber production technology and equipment

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106498516A (en) * 2016-12-15 2017-03-15 江苏大学 The wheeled gel spinning machine that a kind of multistation is automatically adjusted
CN106964303A (en) * 2017-04-21 2017-07-21 北京健康广济生物技术有限公司 Hydrogel production technology and device
CN115894084A (en) * 2022-11-10 2023-04-04 福建省德化非凡陶瓷有限公司 Dehua high-white porcelain decorated by tortoise back textures and preparation process thereof

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101161696A (en) * 2007-09-27 2008-04-16 北京师范大学 Hydrogel and method for preparing same
JP4326612B2 (en) * 1997-12-10 2009-09-09 株式会社日本触媒 Method for producing particulate water-absorbing resin
CN102657892A (en) * 2012-04-16 2012-09-12 古元安 Preparation method of hydrogel dressing
CN102698313A (en) * 2012-01-11 2012-10-03 北京大学 Nano-silver antibacterial hydrogel and preparation method thereof
US20160177002A1 (en) * 2013-08-01 2016-06-23 Intellisiv Ltd. Hydrogel fibers and preparation thereof

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP4326612B2 (en) * 1997-12-10 2009-09-09 株式会社日本触媒 Method for producing particulate water-absorbing resin
CN101161696A (en) * 2007-09-27 2008-04-16 北京师范大学 Hydrogel and method for preparing same
CN102698313A (en) * 2012-01-11 2012-10-03 北京大学 Nano-silver antibacterial hydrogel and preparation method thereof
CN102657892A (en) * 2012-04-16 2012-09-12 古元安 Preparation method of hydrogel dressing
US20160177002A1 (en) * 2013-08-01 2016-06-23 Intellisiv Ltd. Hydrogel fibers and preparation thereof

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106498516A (en) * 2016-12-15 2017-03-15 江苏大学 The wheeled gel spinning machine that a kind of multistation is automatically adjusted
CN106498516B (en) * 2016-12-15 2018-06-26 江苏大学 A kind of wheeled gel spinning machine of multistation automatic adjustment
CN106964303A (en) * 2017-04-21 2017-07-21 北京健康广济生物技术有限公司 Hydrogel production technology and device
CN115894084A (en) * 2022-11-10 2023-04-04 福建省德化非凡陶瓷有限公司 Dehua high-white porcelain decorated by tortoise back textures and preparation process thereof
CN115894084B (en) * 2022-11-10 2023-09-19 福建省德化非凡陶瓷有限公司 Texalized high-whiteness porcelain decorated by tortoise back texture and preparation process thereof

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Application publication date: 20160907