CN105908494A - Composite anti-microbial finishing agent and application thereof to wool products - Google Patents
Composite anti-microbial finishing agent and application thereof to wool products Download PDFInfo
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- CN105908494A CN105908494A CN201610332826.7A CN201610332826A CN105908494A CN 105908494 A CN105908494 A CN 105908494A CN 201610332826 A CN201610332826 A CN 201610332826A CN 105908494 A CN105908494 A CN 105908494A
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- Prior art keywords
- finishing agent
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- antibacterial finishing
- composite antibacterial
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Classifications
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/144—Alcohols; Metal alcoholates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
- D06M13/203—Unsaturated carboxylic acids; Anhydrides, halides or salts thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/244—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus
- D06M13/248—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus with compounds containing sulfur
- D06M13/256—Sulfonated compounds esters thereof, e.g. sultones
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/53—Polyethers
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/10—Animal fibres
- D06M2101/12—Keratin fibres or silk
Abstract
The invention provides a composite anti-microbial finishing agent and application thereof to wool products. The composite anti-microbial finishing agent comprises the following components: 20-35 parts of mugwort extract, 35-55 parts of sodium alkyl benzene sulfonate,30-45 parts of sorbitan ester, 5-10 parts of rosin-polythylene oxide ester, 8-12 parts of polyethylene laurate, 3-6 parts of isopropyl alcohol and 2-3 parts of potassium sorbate. When the composite anti-microbial finishing agent prepared herein is used to wool products, growth of staphylococcus aureus, escherichia coli and aspergillus flavus can be remarkably inhibited.
Description
Technical field
The invention belongs to plant extraction liquid antibacterial applications field, particularly to a kind of composite antibacterial finishing agent
And the application on wool product.
Background technology
Science and technology develops rapidly now, is bringing the most simultaneously, also result in ring
Environment pollution and deterioration, correspondingly caused the hazardous events of various therapeutic microorganism, and people are raw in addition
The raising that running water is flat, the most increasingly payes attention to self health care and environmental protection, and woollen sweater is people's warps
Often a kind of sweater of dress, has heat-preserving function more more preferable than other sweaters, in daily life
In play very important role, therefore, the woollen sweater antibacterial finishing agent of exploitation environment-friendly type very must
Want.
It is the perennial wild herb of composite family artemisia that argy wormwood is also referred to as tarragon grass.Argy wormwood is in China's tradition
Medicine is used as medicine with leaf.The medicinal part of argy wormwood is tarragon, and the medicinal function of tarragon derives from contained therein
The chemical composition of chemical substance argy wormwood after deliberation mainly has volatile oil, flavones, eudesmane, triterpenes
And trace chemical elements etc., biennial wormwood extract has good antibacterial action, and due to directly from planting
Thing extracts, it is not necessary to through chemical treatment, nontoxic, harmless, to skin without allergy and carcinogenicity,
There is preferable degradability and Environmental compatibility, its active ingredient be affixed on woollen sweater, it is possible to
Play skin care, the physical and mental health of the effect of antibacterial deodourizing, beneficially people.Argy wormwood belongs to renewable
Resource, wide material sources, there is not the exhausted problem of resource.
Biennial wormwood extract is highlighted the antibacterial of felon herb raffinate as medicinal application in field of medicaments
Property, but felon herb raffinate is applied to wool product finishing agent and has no relevant report.
Summary of the invention
It is an object of the invention to provide a kind of containing plant extraction liquid antimicrobial component, natural, to human body
Nonhazardous, the composite antibacterial finishing agent of environmentally safe.
It is a further object to provide this composite antibacterial finishing agent application on wool product.
The present invention provides a kind of composite antibacterial finishing agent, it is characterised in that: component includes: argy wormwood is extracted
Liquid 20～35 parts, sodium alkyl benzene sulfonate 3～5 parts, sorbitan ester 5～10 parts, rosin acid gather
Oxygen vinyl acetate 5～10 parts, laurate polyoxyethylene ester 8～12 parts, isopropanol 3～6 parts, sorb
Acid potassium 2～3 parts.
Described composite antibacterial finishing agent, it prepares, including:
(1) preparation of felon herb raffinate: weigh the argy wormwood that portion crushes, joins in extractor,
Add the ethanol water that mass fraction is 60% of 6 times, be heated to 80 DEG C while stirring, backflow
Extracting 1.5h, will concentrate at refluxing extraction solution 100 DEG C, the concentration of concentrate is concentrated into solid content matter
Amount mark is 35%～48%.
(2) the compound preparation of antibacterial finishing agent: by sodium alkyl benzene sulfonate 3～5 parts, anhydrous sorbitol
Ester 5～10 parts, polyoxylethylene abietate 5～10 parts, laurate polyoxyethylene ester 8～12 parts,
Isopropanol 3～6 parts, potassium sorbate 2～3 parts add to felon herb raffinate 20～35 parts, are heated to
85～90 DEG C, recombination reaction 3～4h.
Preferably, the mass concentration of the argy wormwood active ingredient of described composite antibacterial finishing agent be 15%～
25%.
The present invention provides the application on wool product of a kind of composite antibacterial finishing agent, and its feature exists
In: the application on woollen sweater or worsted shirt of the composite antibacterial finishing agent.
Preferably, described composite antibacterial finishing agent and woollen sweater amount ratio are mass ratio 1:5:.
Preferably, first, woollen sweater is used industrial washing of drum type washing machine, remove residual on clothing
Dust, the rear water injecting 40-50 DEG C adds composite antibacterial finishing agent simultaneously, and bath raio is 1:10-20,
The process time is 30-40min, and pH value is 6-7.
Preferably, described composite antibacterial finishing agent and worsted shirt amount ratio are mass ratio 2:5.
Preferably, first, by the industrial washing of drum type washing machine of worsted shirt, remove on clothing residual
The dust stayed, the rear water injecting 40-50 DEG C adds composite antibacterial finishing agent simultaneously, and bath raio is
1:10-20, the process time is 30-40min, and pH value is 7-8.
The beneficial effects of the present invention is: the composite antibacterial finishing agent prepared has good suppression
The function of the growth of staphylococcus aureus, Escherichia coli and aspergillus flavus.Arrangement through the present invention
The common wool product that agent processed is through test, and the inhibiting rate of staphylococcus aureus can reach
More than 96%, colibacillary inhibiting rate can reach more than 90%, and colibacillary inhibiting rate is permissible
Reach more than 95%, there is good fungistatic effect.
Detailed description of the invention
Below by specific embodiment, the present invention is described further, but embodiment is not limiting as this
The protection domain of invention.
Embodiment 1
Weigh the argy wormwood 5kg that portion crushes, join in extractor, add the mass fraction of 6 times
It is the ethanol water of 60%, is heated to 80 DEG C while stirring, refluxing extraction 1.5h, backflow is carried
Taking and concentrate at solution 100 DEG C, it is 35% that the concentration of concentrate is concentrated into solid content mass fraction.
By sodium alkyl benzene sulfonate 3 parts, sorbitan ester 5 parts, polyoxylethylene abietate 5 parts,
Laurate polyoxyethylene ester 8 parts, isopropanol 3 parts, potassium sorbate 2 parts add to felon herb raffinate
20 parts, it is heated to 85 DEG C, recombination reaction 3h.
Described composite antibacterial finishing agent and woollen sweater amount ratio are mass ratio 1:5:.
Woollen sweater is used industrial washing of drum type washing machine, removes the dust of residual on clothing, rear injection 40 DEG C
Water add composite antibacterial finishing agent simultaneously, bath raio is 1:10, and the process time is 30min, pH value
For 6-7.
Described composite antibacterial finishing agent and worsted shirt amount ratio are mass ratio 2:5.
By the industrial washing of drum type washing machine of worsted shirt, remove the dust of residual on clothing, inject afterwards
The water of 40 DEG C adds composite antibacterial finishing agent simultaneously, and bath raio is 1:10, and the process time is 30min, pH
Value is 7-8.
Embodiment 2
(1) preparation of felon herb raffinate: weigh the argy wormwood 5kg that portion crushes, join extractor
In, add the ethanol water that mass fraction is 60% of 6 times, be heated to 80 DEG C while stirring,
Refluxing extraction 1.5h, will concentrate at refluxing extraction solution 100 DEG C, and the concentration of concentrate is concentrated into and admittedly contains
Amount mass fraction is 40%.
(2) the compound preparation of antibacterial finishing agent: by sodium alkyl benzene sulfonate 4 parts, sorbitan ester 6
Part, polyoxylethylene abietate 7 parts, laurate polyoxyethylene ester 10 parts, isopropanol 5 parts, mountain
Potassium sorbate 3 parts adds to felon herb raffinate 30 parts, is heated to 90 DEG C, recombination reaction 4h.
Described composite antibacterial finishing agent and woollen sweater amount ratio are mass ratio 1:5:.
Woollen sweater is used industrial washing of drum type washing machine, removes the dust of residual on clothing, inject afterwards
The water of 45 DEG C adds composite antibacterial finishing agent simultaneously, and bath raio is 1:15, and the process time is 35min,
PH value is 6-7.
Preferably, described composite antibacterial finishing agent and worsted shirt amount ratio are mass ratio 2:5.
Preferably, first, by the industrial washing of drum type washing machine of worsted shirt, remove on clothing residual
The dust stayed, the rear water injecting 45 DEG C adds composite antibacterial finishing agent simultaneously, and bath raio is 1:15,
The process time is 30min, and pH value is 7-8.
Embodiment 3
(1) preparation of felon herb raffinate: weigh the argy wormwood 5kg that portion crushes, join extractor
In, add the ethanol water that mass fraction is 60% of 6 times, be heated to 80 DEG C while stirring,
Refluxing extraction 1.5h, will concentrate at refluxing extraction solution 100 DEG C, and the concentration of concentrate is concentrated into and admittedly contains
Amount mass fraction is 48%.
(2) the compound preparation of antibacterial finishing agent: by sodium alkyl benzene sulfonate 5 parts, sorbitan ester 10
Part, polyoxylethylene abietate 10 parts, laurate polyoxyethylene ester 12 parts, isopropanol 6 parts,
Potassium sorbate 3 parts adds to felon herb raffinate 35 parts, is heated to 90 DEG C, recombination reaction 4h.
Described composite antibacterial finishing agent and woollen sweater amount ratio are mass ratio 1:5.
Woollen sweater is used industrial washing of drum type washing machine, removes the dust of residual on clothing, rear injection 50 DEG C
Water add composite antibacterial finishing agent simultaneously, bath raio is 1:20, and the process time is 40min, pH value
For 6-7.
Described composite antibacterial finishing agent and worsted shirt amount ratio are mass ratio 2:5.
By the industrial washing of drum type washing machine of worsted shirt, remove the dust of residual on clothing, inject afterwards
The water of 50 DEG C adds composite antibacterial finishing agent simultaneously, and bath raio is 1:20, and the process time is 40min,
PH value is 7-8.
Embodiment 4
(1) preparation of felon herb raffinate: weigh the argy wormwood 5kg that portion crushes, join extractor
In, add the ethanol water that mass fraction is 60% of 6 times, be heated to 80 DEG C while stirring,
Refluxing extraction 1.5h, will concentrate at refluxing extraction solution 100 DEG C, and the concentration of concentrate is concentrated into and admittedly contains
Amount mass fraction is 45%.
(2) the compound preparation of antibacterial finishing agent: by sodium alkyl benzene sulfonate 5 parts, sorbitan ester 8
Part, polyoxylethylene abietate 8 parts, laurate polyoxyethylene ester 10 parts, isopropanol 4 parts, mountain
Potassium sorbate 3 parts adds to felon herb raffinate 30 parts, is heated to 90 DEG C, recombination reaction 3.5h.
Described composite antibacterial finishing agent and woollen sweater amount ratio are mass ratio 1:5:.
Woollen sweater is used industrial washing of drum type washing machine, removes the dust of residual on clothing, rear injection 40-50 DEG C
Water add composite antibacterial finishing agent simultaneously, bath raio is 1:18, and the process time is 35min, pH value
It is 6.
Preferably, described composite antibacterial finishing agent and worsted shirt amount ratio are mass ratio 2:5.
Preferably, first, by the industrial washing of drum type washing machine of worsted shirt, remove on clothing residual
The dust stayed, the rear water injecting 45 DEG C adds composite antibacterial finishing agent simultaneously, and bath raio is 1:16,
The process time is 35min, and pH value is 8.
Woollen sweater after the arrangement of embodiment 1-4 finishing agent and the fungistatic effect such as table of worsted shirt
Shown in 1 to table 3:
Table 1 staphylococcus aureus bacteriostasis rate
Table 2 Escherichia coli bacteriostasis rate
| Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | |
| Woollen sweater | 93 | 92 | 91 | 90 |
| Worsted shirt | 94 | 92 | 93 | 91 |
Table 3 aspergillus flavus bacteriostasis rate
| Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | |
| Woollen sweater | 97 | 95.3 | 96.2 | 95.5 |
| Worsted shirt | 96 | 95.8 | 95.5 | 96.4 |
It should be noted that above example is only in order to illustrate technical scheme and unrestricted.
Although being described in detail the present invention with reference to preferred embodiment, those of ordinary skill in the art should
Work as understanding, the technical scheme of invention can be modified or equivalent, without deviating from the present invention
The scope of technical scheme, it all should be contained in scope of the presently claimed invention.
Claims (7)
1. a composite antibacterial finishing agent, it is characterised in that: component includes: felon herb raffinate 20～35 parts, sodium alkyl benzene sulfonate 3～5 parts, sorbitan ester 5～10 parts, polyoxylethylene abietate 5～10 parts, laurate polyoxyethylene ester 8～12 parts, isopropanol 3～6 parts, potassium sorbate 2～3 parts.
2. a kind of composite antibacterial finishing agent as claimed in claim 1, it is characterised in that: the mass concentration of the argy wormwood active ingredient of described composite antibacterial finishing agent is 15%～25%.
3. the application on wool product of a kind of composite antibacterial finishing agent as described in claim 1-2, it is characterised in that: the application on woollen sweater or worsted shirt of the composite antibacterial finishing agent.
A kind of composite antibacterial finishing agent the most as claimed in claim 3 application on wool product, it is characterised in that: described composite antibacterial finishing agent and woollen sweater amount ratio are mass ratio 1:5.
A kind of composite antibacterial finishing agent the most as claimed in claim 4 application on wool product, it is characterized in that: first, woollen sweater is used industrial washing of drum type washing machine, remove the dust of residual on clothing, the rear water injecting 40-50 DEG C adds composite antibacterial finishing agent simultaneously; bath raio is 1:10-20, and the process time is 30-40min, and pH value is 6-7.
A kind of composite antibacterial finishing agent the most as claimed in claim 3 application on wool product, it is characterised in that: described composite antibacterial finishing agent and worsted shirt amount ratio are mass ratio 2:5.
A kind of composite antibacterial finishing agent the most as claimed in claim 6 application on wool product, it is characterized in that: first, by the industrial washing of drum type washing machine of worsted shirt, remove the dust of residual on clothing, the rear water injecting 40-50 DEG C adds composite antibacterial finishing agent simultaneously; bath raio is 1:10-20, and the process time is 30-40min, and pH value is 7-8.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610332826.7A CN105908494A (en) | 2016-05-19 | 2016-05-19 | Composite anti-microbial finishing agent and application thereof to wool products |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610332826.7A CN105908494A (en) | 2016-05-19 | 2016-05-19 | Composite anti-microbial finishing agent and application thereof to wool products |
Publications (1)
| Publication Number | Publication Date |
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| CN105908494A true CN105908494A (en) | 2016-08-31 |
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ID=56748304
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| CN201610332826.7A Pending CN105908494A (en) | 2016-05-19 | 2016-05-19 | Composite anti-microbial finishing agent and application thereof to wool products |
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Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20070054819A1 (en) * | 2004-02-20 | 2007-03-08 | Shulong Li | Carpet treated for resistance to odors and contaminants and method |
| CN101884450A (en) * | 2009-05-12 | 2010-11-17 | 苗广伟 | Disposable health-care deodorized insole |
| CN103422351A (en) * | 2013-08-02 | 2013-12-04 | 吴江市七都镇庙港雅迪针织制衣厂 | Woolen sweater treating liquid containing abietic acid polyoxyethylene ester |
| CN103422343A (en) * | 2013-08-02 | 2013-12-04 | 吴江市七都镇庙港雅迪针织制衣厂 | Woolen sweater treating liquid with potassium myristate |
| CN103451926A (en) * | 2012-06-05 | 2013-12-18 | 太仓协大申泰羊毛衫有限公司 | Moth-proofing finishing technique of woollen sweater |
| CN104894858A (en) * | 2015-05-21 | 2015-09-09 | 青岛德翕拓创高新技术有限公司 | Wool fabric sterilization treating agent |
-
2016
- 2016-05-19 CN CN201610332826.7A patent/CN105908494A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20070054819A1 (en) * | 2004-02-20 | 2007-03-08 | Shulong Li | Carpet treated for resistance to odors and contaminants and method |
| CN101884450A (en) * | 2009-05-12 | 2010-11-17 | 苗广伟 | Disposable health-care deodorized insole |
| CN103451926A (en) * | 2012-06-05 | 2013-12-18 | 太仓协大申泰羊毛衫有限公司 | Moth-proofing finishing technique of woollen sweater |
| CN103422351A (en) * | 2013-08-02 | 2013-12-04 | 吴江市七都镇庙港雅迪针织制衣厂 | Woolen sweater treating liquid containing abietic acid polyoxyethylene ester |
| CN103422343A (en) * | 2013-08-02 | 2013-12-04 | 吴江市七都镇庙港雅迪针织制衣厂 | Woolen sweater treating liquid with potassium myristate |
| CN104894858A (en) * | 2015-05-21 | 2015-09-09 | 青岛德翕拓创高新技术有限公司 | Wool fabric sterilization treating agent |
Non-Patent Citations (3)
| Title |
|---|
| 楼之岑等: "《常用中药材品种整理和质量研究 北方编 第1册》", 30 September 1995, 北京医科大学、中国协和医科大学联合出版社 * |
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Application publication date: 20160831 |