CN105888604A - Method applicable to repeatedly transforming stratum nearby shaft of low-pressure gas field old well to complete permanent blocking - Google Patents

Method applicable to repeatedly transforming stratum nearby shaft of low-pressure gas field old well to complete permanent blocking Download PDF

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Publication number
CN105888604A
CN105888604A CN201610229259.2A CN201610229259A CN105888604A CN 105888604 A CN105888604 A CN 105888604A CN 201610229259 A CN201610229259 A CN 201610229259A CN 105888604 A CN105888604 A CN 105888604A
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China
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well
gas
cement
reserves
wellbore formation
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CN201610229259.2A
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CN105888604B (en
Inventor
高伟
李宪文
马旭
张燕明
来轩昂
周长静
肖元相
马占国
何明舫
郝瑞芬
丁勇
史华
叶亮
胡阳明
毕曼
李喆
问晓勇
李楼楼
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China Petroleum and Natural Gas Co Ltd
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China Petroleum and Natural Gas Co Ltd
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    • EFIXED CONSTRUCTIONS
    • E21EARTH OR ROCK DRILLING; MINING
    • E21BEARTH OR ROCK DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
    • E21B33/00Sealing or packing boreholes or wells
    • E21B33/10Sealing or packing boreholes or wells in the borehole
    • E21B33/13Methods or devices for cementing, for plugging holes, crevices or the like
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09KMATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K8/00Compositions for drilling of boreholes or wells; Compositions for treating boreholes or wells, e.g. for completion or for remedial operations
    • C09K8/42Compositions for cementing, e.g. for cementing casings into boreholes; Compositions for plugging, e.g. for killing wells
    • C09K8/426Compositions for cementing, e.g. for cementing casings into boreholes; Compositions for plugging, e.g. for killing wells for plugging
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09KMATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K8/00Compositions for drilling of boreholes or wells; Compositions for treating boreholes or wells, e.g. for completion or for remedial operations
    • C09K8/42Compositions for cementing, e.g. for cementing casings into boreholes; Compositions for plugging, e.g. for killing wells
    • C09K8/46Compositions for cementing, e.g. for cementing casings into boreholes; Compositions for plugging, e.g. for killing wells containing inorganic binders, e.g. Portland cement

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  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Geology (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Mining & Mineral Resources (AREA)
  • Physics & Mathematics (AREA)
  • Environmental & Geological Engineering (AREA)
  • Fluid Mechanics (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Inorganic Chemistry (AREA)
  • Consolidation Of Soil By Introduction Of Solidifying Substances Into Soil (AREA)
  • Filling Or Discharging Of Gas Storage Vessels (AREA)

Abstract

The invention provides a method applicable to repeatedly transforming a stratum nearby a shaft of a low-pressure gas field old well to complete permanent blocking. The method is characterized by mixing micro-grade resin with cement before repeated transformation, pumping a mixture of the micro-grade resin and the cement into the stratum nearby the shaft, and permanently blocking holes and cracks in a low-pressure voidage zone around the old well. According to the method applicable to repeatedly transforming the stratum nearby the shaft of the low-pressure gas field old well to complete the permanent blocking, provided by the invention, the micro-grade resin and the cement are mixed, and the mixture of the micro-grade resin, and the cement is pumped into the stratum around the shaft before refracturing; since the particle diameter of ultrafine plugging agent particles is smaller and the ultrafine plugging agent particles have good fluidity and good penetrability, the ultrafine plugging agent particles can permeate into the holes of a reservoir stratum so as to permanently block the holes and the cracks in the low-pressure voidage zone around the old well, leakage of fracturing liquid to the stratum is slowed down, and the fracture making efficiency of the fracturing liquid is increased.

Description

A kind of it is applicable to the method that the old well in low pressure gas field repeats to transform the permanent closure of nearly wellbore formation
Technical field
The invention belongs to low pressure and low permeability breathe freely stimulation technology field, field, be specifically related to a kind of be applicable to the method that the old well in low pressure gas field repeats to transform the permanent closure of nearly wellbore formation.
Background technology
Along with gas field development degree continuous intensification, low yield inefficient well ratio increases year by year, and stable yields situation is increasingly serious.For improving well yield, excavating Oil/gas Well productive potentialities, selected part main layer sand body is grown, reservoir properties is good, accumulating condition is excellent, but refracturing transformation carried out by the Production development old well poor compared with offset well.Different from the transformation of new well, old well is due to long-term production, nearly pit shaft area stratum energy is in debt, cause well killing fluid and fracturing fluid wastage in work progress big, not only reservoir caused secondary injury, and liquid to make seam efficiency low, fracture extension is apart from limited, after transformation, the discharge opeing cycle is long, discharge opeing weak effect, does not reaches expection transformation target.
At present Changqing oilfields repeats transformation for the old well of low-pressure gas well, blocks up well killing fluid temporarily only with Low Damage to prevent well killing fluid leak-off, but application DeGrain, it is impossible to effectively solving practical problems.Repeat to transform stratum permanent block up design method to this end, need the old well in a kind of gas field of invention badly, can complete, to the low pressure deficit district permanent closure of reservoir around pit shaft, to meet the old well in current gas field and repeat to transform the urgent needs of anti-filter potentiation with existing fracturing unit.
Summary of the invention
It is an object of the invention to overcome prior art in the old well of low-pressure gas well repeats transformation, well killing fluid and fracturing fluid wastage are big, do not reach a difficult problem for expection transformation target.
For this, the invention provides and a kind of be applicable to the method that the old well in low pressure gas field repeats to transform the permanent closure of nearly wellbore formation, by micron order resin and cement mixture before repeating to transform, pump in nearly wellbore formation after mixture, by the permanent closure of low pressure deficit district's hole and crack around old well.
Micron order resin is determined by gas well recovery percent of reserves with cement mixed ratio:
1) when gas well recovery percent of reserves is less than 30%, the weight ratio of resin and cement is 1:9;
2) when gas well recovery percent of reserves is less than 60% more than 30%, the weight ratio of resin and cement is 2:8;
3) when gas well recovery percent of reserves is more than 60%, the weight ratio of resin and cement is 3:7.
After micron order resin and cement mixture, injection rate is determined by gas well recovery percent of reserves and gas pay thickness;
1) when gas well recovery percent of reserves is less than 30%, injection rate is every meter of gas pay thickness 8.0m3
2) when gas well recovery percent of reserves is less than 60% more than 30%, injection rate is every meter of gas pay thickness 12m3
3) when gas well recovery percent of reserves is more than 60%, injection rate is every meter of gas pay thickness 15m3
Described gas well recovery percent of reserves can the amount of adopting ratio calculation with the amount of adopting and reality.
Described micron order resin particle diameter is 3.0-12.0 μm.
A kind of it is applicable to the method that the old well in low pressure gas field repeats to transform the permanent closure of nearly wellbore formation, comprises the following steps:
Step 1) determines micron order resin and cement mixed ratio and injection rate according to gas well recovery percent of reserves and gas pay thickness;
Step 2) it is pumped in nearly wellbore formation after micron order resin and cement mixture;
Step 3) closing well Hou Ning;
Step 4) nitrogen pressure testing 30MPa, pressure measurement is dropped 30 minutes, if 30 minutes pressure is dropped by less than 0.5MPa, is shown that nearly wellbore formation blocks successfully, proceed step 5);If nearly wellbore formation closure is unsuccessful, then repeat step 2) and step 3);
After step 5) closure is qualified, to interval of interest again perforation;
Step 6) refracturing is transformed.
Step 2) in after micron order resin and cement mixture pump displacement control at 1-2m3Within/min.
The described closing well Hou Ning time is not less than 7 days.
Described micron order resin relative molecular mass is 3000-4000.
The invention has the beneficial effects as follows:
This of present invention offer is applicable to the method that the old well in low pressure gas field repeats to transform the permanent closure of nearly wellbore formation, use micron order resin and cement mixture, pump in pit shaft surrounding formation before refracturing, owing to ultra-fine blocking agent grain diameter is little, there is good mobility and penetrance, it is possible to infiltrate through in reservoir pore space, by the permanent closure of low pressure deficit district's hole and crack around old well, slowing down fracturing fluid leak-off in stratum, that improves fracturing fluid makes seam efficiency.
It is described in further details below in conjunction with accompanying drawing.
Accompanying drawing explanation
Fig. 1 is nearly wellbore formation pressure schematic diagram before gas well is gone into operation;
Fig. 2 is nearly wellbore formation pressure schematic diagram after gas well is gone into operation;
Fig. 3 is that micron order resin and cement mixture are injected nearly pit shaft area, closure pit shaft low pressure deficit district stratum schematic diagram by the inventive method.
Detailed description of the invention
Embodiment 1:
Present embodiments provide and a kind of be applicable to the method that the old well in low pressure gas field repeats to transform the permanent closure of nearly wellbore formation, by micron order resin and cement mixture before repeating to transform, pump in nearly wellbore formation after mixture, by the permanent closure of low pressure deficit district's hole and crack around old well.
Know-why: by means of micron order resin, pump in pit shaft surrounding formation before refracturing, owing to ultra-fine blocking agent grain diameter is little, there is good mobility and penetrance, can infiltrate through in reservoir pore space, by the permanent closure of low pressure deficit district's hole and crack around old well, slowing down fracturing fluid leak-off in stratum, that improves fracturing fluid makes seam efficiency.
Embodiment 2:
On the basis of embodiment 1, a kind of it is applicable to the method that the old well in low pressure gas field repeats to transform the permanent closure of nearly wellbore formation, comprises the following steps:
Step 1) determines micron order resin and cement mixed ratio and injection rate according to gas well recovery percent of reserves and gas pay thickness;
Step 2) it is pumped in nearly wellbore formation after micron order resin and cement mixture;
Step 3) closing well Hou Ning;
Step 4) nitrogen pressure testing 30MPa, pressure measurement is dropped 30 minutes, if 30 minutes pressure is dropped by less than 0.5MPa, is shown that nearly wellbore formation blocks successfully, proceed step 5);If nearly wellbore formation closure is unsuccessful, then repeat step 2) and step 3);
After step 5) closure is qualified, to interval of interest again perforation;
Step 6) refracturing is transformed.
Owing to the Sulige gas field main force of Soviet Union gas pay is low porosity and low permeability reservoir, reservoir permeability is less than 1mD, little on the impact of resin material usage ratio, and this research mainly determines resin and superfine cement amount ratio with gas well recovery percent of reserves and gas pay thickness.Recovery percent of reserves can the amount of adopting calculate with reality with the amount of adopting the most.
Micron order resin is determined by gas well recovery percent of reserves with cement mixed ratio:
1) when gas well recovery percent of reserves is less than 30%, the weight ratio of resin and cement is 1:9;
2) when gas well recovery percent of reserves is less than 60% more than 30%, the weight ratio of resin and cement is 2:8;
3) when gas well recovery percent of reserves is more than 60%, the weight ratio of resin and cement is 3:7.
After micron order resin and cement mixture, injection rate is determined by gas well recovery percent of reserves and gas pay thickness;
1) when gas well recovery percent of reserves is less than 30%, injection rate is every meter of gas pay thickness 8.0m3
2) when gas well recovery percent of reserves is less than 60% more than 30%, injection rate is every meter of gas pay thickness 12m3
3) when gas well recovery percent of reserves is more than 60%, injection rate is every meter of gas pay thickness 15m3
Wherein, step 2) in after micron order resin and cement mixture pump displacement control at 1-2m3Within/min.
In step 3), the closing well Hou Ning time is not less than 7 days.
The micron order resin used in the present embodiment is the three-dimensional unlimited polymer network of a kind of solidification that the cross-linking reaction between a kind of amino curing agent and a kind of epoxide produces, and its molecular structure is as follows.
This micron order resin particle diameter is 3.0-12.0 μm, and relative molecular mass is 3000-4000.Owing to its grain diameter is little, having good mobility and penetrance, it is possible to infiltrate through (0.1-15um is shouted in Changqing Gas Fields reservoir hole) in reservoir pore space, have stronger resistance to compression, anti-permeability performance, intensity is high, and means of press seals ability is strong (1000psi/ foot).Traditional cements can be entered or region that superfine cement all cannot arrive, it is possible to realize the permanent closure to reservoir.This system consumption is few, low cost, and operational procedure is simple, it is easy to operation.There is a following features:
(1) Solid Free can penetrate micron order hole;
(2) infinited-valued logic under Newtonian fluid-liquid condition;
(3) bond by force can anti-high pressure (23MPa/m);
(4) resist chemical (acid/CO2);
(5) complementary with cement;
(6) contamination resistance is strong (overcoming insufficient mud to replace);
(7) compatible good (including water);
(8) high-ductility (deformation can reach 20%);
(9) high intensity and can boring;
(10) high resiliency, when testing in the environmental test stove at 162 °F (72 ° of C), resin material can be at 12500psi(86MPa) pressure under remain in that high resiliency.
Embodiment 3:
On-the-spot application example:
XX gas field is positioned at Depression Area, the southeast, XX basin XX rift slope belt, and main force's gas pay is glutenite, more densely, buries deep, and temperature is high, and pressure is high.Since exploitation in 2009, at pit shaft oil jacket and skill set, there is many places leak source, owing to annular space is with pressure and gas well pressure high, use traditional cements or superfine cement operation repeatedly to process and still cannot solve.
Within 2015, introduce micron order resin first, formulate site operation scheme and carry out on-the-spot test, use resin material and cement with 2:8 ratio mixture, implement closure operation.
Work progress:
(1) transport resin plugging material is to well site;
(2) mixture micron order resin and cement;
(3) mixture compound system pump 20m3, displacement control is at 1-2m3Within/min;
(4) cementing truck and construction pipeline are cleaned;
(5) wait solidifying being not less than 7 days;
(6) nitrogen pressure testing 30MPa.
On July 27th, 2015,17:00 scene nitrogen car group is to 5-1/2, and " carrying out pressure testing in Tao, pump truck suppresses 30MPa, voltage stabilizing 15 minutes, and pressure is qualified, returns out without gas at skill set valve, and nitrogen pressure testing is qualified, blocks successfully.As it is shown in figure 1, before not going into operation, strata pressure is original formation pressure, and stress is respectively to homogenizing;After operation, stress field changes, and along with the continuous growth of recovery time, nearly pit shaft area pressure is gradually reduced, and the pressure drop of biggest principal stress direction is apparently higher than minimum principal stress direction, as shown in Figure 2;Fig. 3 is that micron order resin and cement mixture are injected nearly pit shaft area, closure pit shaft low pressure deficit district stratum schematic diagram, makes up the pressure drop brought because of long-term production, reduces and repeat to transform fluid loss.
Carrying out refracturing transformation afterwards, construction main-process stream is as follows:
Drifting → well-flushing → pressure testing → perforation → fracturing tubing string → fracturing reform → open flow and discharge opeing → seek product
1) drifting: drift size gauge tool external diameter 115mm, length 1500mm, passes to artificial bottom of a well.
2) well-flushing: flushing fluid uses clear water, well-flushing discharge capacity is less than 1.0m3/ min, consumption specifically calculates according to casing volume, returns out flushing fluid content of impurities and is not more than 0.2%.
3) pressure testing: clear water pressure testing 30.0MPa, within 30 minutes, pressure is dropped by less than 0.5MPa.
4) perforation: use SYD-102 rifle, 127 bullets, carry out perforating job by " perforating design (advice note) ", emissivity more than 95%, Perforation Density 16 holes/m, 60 ° of perforation phase angle.Perforated interval error is less than 20cm, tightly notes well head, prevent blowout during perforation.
5) fracturing reform: for improving the secondary transformation degree of reservoir, fracturing string uses the construction of full well Ф 88.39mm oil pipe, and operational discharge capacity controls at 3.0-4.0m3/min.Return row for liquid after improving pressure to lead and sand phenomenon is told in control, add the measures such as fiber at construction pad stage companion's fluid injection nitrogen and mulling liquid.
6) open flow and discharge opeing: after modification measures terminates, drives a well for 20-40 minute, and the open flow initial stage uses Ф 3-8mm oil nozzle to control open flow, discharge capacity 100-200-300l/min.During open flow discharge opeing, sleeve gate is closed, accurate recording tubing pressure and casing pressure, and liquid measure is discharged in metering.If can not blowing, use other draining mode timely induced flow discharge opeing such as liquid nitrogen gaslift.
7) seeking product: oil, set pressure are in a basic balance, tubing pressure time rising value is less than 0.05MPa in 24 hours, proceeds to ask product or air water to reach to be pressed into formation breakdown liquid measure more than 80%, and Cl with going out well array liquid measure-Content undulating value in 3 days seeks product less than turning after 5%.Generating method uses " one point method ".
Exemplified as above is only the illustration to the present invention, is not intended that the restriction to protection scope of the present invention, within the every and same or analogous design of the present invention belongs to protection scope of the present invention.The method that the present embodiment describes the most in detail belongs to the common knowledge of the industry, describes the most one by one.

Claims (9)

1. one kind is applicable to the method that the old well in low pressure gas field repeats to transform the permanent closure of nearly wellbore formation, it is characterized in that: by micron order resin and cement mixture before repeating to transform, pump in nearly wellbore formation after mixture, by the permanent closure of low pressure deficit district's hole and crack around old well.
The most according to claim 1 a kind of it is applicable to the method that the old well in low pressure gas field repeats to transform the permanent closure of nearly wellbore formation, it is characterised in that: micron order resin is determined by gas well recovery percent of reserves with cement mixed ratio;
1) when gas well recovery percent of reserves is less than 30%, the weight ratio of resin and cement is 1:9;
2) when gas well recovery percent of reserves is less than 60% more than 30%, the weight ratio of resin and cement is 2:8;
3) when gas well recovery percent of reserves is more than 60%, the weight ratio of resin and cement is 3:7.
The most according to claim 1 a kind of it is applicable to the method that the old well in low pressure gas field repeats to transform the permanent closure of nearly wellbore formation, it is characterised in that: after micron order resin and cement mixture, injection rate is determined by gas well recovery percent of reserves and gas pay thickness;
1) when gas well recovery percent of reserves is less than 30%, injection rate is every meter of gas pay thickness 8.0m3
2) when gas well recovery percent of reserves is less than 60% more than 30%, injection rate is every meter of gas pay thickness 12m3
3) when gas well recovery percent of reserves is more than 60%, injection rate is every meter of gas pay thickness 15m3
4. it is applicable to, according to a kind of described in Claims 2 or 3, the method that the old well in low pressure gas field repeats to transform the permanent closure of nearly wellbore formation, it is characterised in that: described gas well recovery percent of reserves can the amount of adopting ratio calculation with the amount of adopting and reality.
The most according to claim 2 a kind of it is applicable to the method that the old well in low pressure gas field repeats to transform the permanent closure of nearly wellbore formation, it is characterised in that: described micron order resin particle diameter is 3.0-12.0 μm.
The most according to claim 2 a kind of it is applicable to the method that the old well in low pressure gas field repeats to transform the permanent closure of nearly wellbore formation, it is characterised in that comprise the following steps:
Step 1) determines micron order resin and cement mixed ratio and injection rate according to gas well recovery percent of reserves and gas pay thickness;
Step 2) it is pumped in nearly wellbore formation after micron order resin and cement mixture;
Step 3) closing well Hou Ning;
Step 4) nitrogen pressure testing 30MPa, pressure measurement is dropped 30 minutes, if 30 minutes pressure is dropped by less than 0.5MPa, is shown that nearly wellbore formation blocks successfully, proceed step 5);If nearly wellbore formation closure is unsuccessful, then repeat step 2) and step 3);
After step 5) closure is qualified, to interval of interest again perforation;
Step 6) refracturing is transformed.
The most according to claim 6 a kind of be applicable to the method that the old well in low pressure gas field repeats to transform the permanent closure of nearly wellbore formation, it is characterised in that: step 2) in after micron order resin and cement mixture pump displacement control at 1-2m3Within/min.
The most according to claim 6 a kind of it is applicable to the method that the old well in low pressure gas field repeats to transform the permanent closure of nearly wellbore formation, it is characterised in that: the described closing well Hou Ning time is not less than 7 days.
The most according to claim 2 a kind of it is applicable to the method that the old well in low pressure gas field repeats to transform the permanent closure of nearly wellbore formation, it is characterised in that: described micron order resin relative molecular mass is 3000-4000.
CN201610229259.2A 2016-04-14 2016-04-14 A kind of old well in low pressure gas field that is suitable for repeats to transform the method that nearly wellbore formation permanently blocks Active CN105888604B (en)

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CN107989589A (en) * 2017-11-28 2018-05-04 青海九0六工程勘察设计院 A kind of method of heat exchange efficiency after raising hot dry rock pressure break
CN109138954A (en) * 2018-08-29 2019-01-04 中国石油大学(北京) A kind of refracturing method of Unconventional gas
CN111155952A (en) * 2019-12-30 2020-05-15 山西晋城无烟煤矿业集团有限责任公司 Method for recycling abandoned coal bed gas well in goaf

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Publication number Priority date Publication date Assignee Title
CN107989589A (en) * 2017-11-28 2018-05-04 青海九0六工程勘察设计院 A kind of method of heat exchange efficiency after raising hot dry rock pressure break
CN107989589B (en) * 2017-11-28 2019-12-03 青海九0六工程勘察设计院 A method of improving heat exchange efficiency after hot dry rock pressure break
CN109138954A (en) * 2018-08-29 2019-01-04 中国石油大学(北京) A kind of refracturing method of Unconventional gas
CN111155952A (en) * 2019-12-30 2020-05-15 山西晋城无烟煤矿业集团有限责任公司 Method for recycling abandoned coal bed gas well in goaf

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