CN105880044A - Cyclone centrifugal separation method and equipment - Google Patents

Cyclone centrifugal separation method and equipment Download PDF

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Publication number
CN105880044A
CN105880044A CN201410751233.5A CN201410751233A CN105880044A CN 105880044 A CN105880044 A CN 105880044A CN 201410751233 A CN201410751233 A CN 201410751233A CN 105880044 A CN105880044 A CN 105880044A
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China
Prior art keywords
cylinder
light substance
discharge pipe
cyclone
centrifugal separation
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Pending
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CN201410751233.5A
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Chinese (zh)
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刘英聚
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Individual
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Individual
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Priority to CN201410751233.5A priority Critical patent/CN105880044A/en
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Abstract

The invention discloses a cyclone centrifugal separation method, and belongs to the technical field of petroleum chemical engineering, beneficiation, two-phase separation and environmental protecting equipment. The cyclone centrifugal separation method is characterized by comprising feeding, light medium emission and heavy medium emission, and is characterized by adopting 2-10 cyclone feeding and constant speed/acceleration two-section centrifugal separation; a light medium is leaded out from the center of the upper part; each quadrant of materials rotates with high speed through multiple cyclone feeding; and the centrifugal force being thousand times of the gravity is generated through further acceleration to perform two-phase separation. The invention further provides feeding pipe, cyclone and light medium emission pipe equipment for realizing the method. The equipment is high in efficiency, high in separation efficiency and used for process two-phase or multi-phase separation.

Description

A kind of eddy flow centrifugal separation method and equipment
Technical field
The invention belongs to petrochemical industry, ore dressing, two-phase laminated flow, environmental protection technical field, particularly to centrifugal point of a kind of eddy flow From method and apparatus.
Background technology
A lot of industrial process or be in technique and need or the equipment that is in runs and needs or be in environmental protection and need to relate to two-phase or multiphase and separate. Typical two-phase laminated flow process has gas to separate with catalyst fines, gas-liquid separation, water and separating of oil, water or oily thin with catalyst Powder separation etc..
It is designed with catalyst fines recvery facility with reactor, the regenerator of catalyst fines fluidization operation, generally uses whirlwind Separator.The reactor of device, the regenerator such as catalytic cracking (FCC), methanol-to-olefins (MTO) generally use PV type whirlwind at present Separator or other modified model cyclone separator, be made up of inlet tube, cylinder, cone cylinder, ash bucket and dipleg, it is characterized in that containing thin Powder gas tangentially enters cylinder from 1 entrance, is rotated into row centrifugation in cylinder, cone cylinder, reclaims fine powder and falls into Ash bucket is discharged through dipleg, purifies gas and discharges from central upper portion exhaustor through device interior center stream.Conventional cyclones is only 1 gas access, when device diameters is bigger there is obvious current gradient (reducing successively) in 4 quadrants, and this will make equipment imitate Rate reduces and causes gas-solid disngaging efficiency to reduce.The device such as catalytic cracking, methanol-to-olefins is additionally provided with three-stage cyclone separator, closely Within several years, develop " willy-willy " formula three to revolve, make three-stage cyclone separator structure significantly simplify, be easy to manufacture and safeguard.Many institutes Known three-stage cyclone separator carries out ultra acelerator fine particle gas solid separation, and " willy-willy " separator relative diameter is relatively big and only has 1 gas access, its gas-solid disngaging efficiency the highest (general only about 80%).
Gas-liquid two-phase separates the most universal, and process gas medium is cooled to 40 DEG C of entrance gs-oil separators, at oil gas Separator carries out air-liquid natural subsidence separation, it is commonly known that natural subsidence separation efficiency is the highest, it is desirable to strict technical process If gas band liquid seriously will affect normal operating, need to arrange high efficiency separation equipment as supplementing and to ensure process optimization.
A lot of technical processs also have fresh water (FW) or sewage to discharge, and the gas medium containing steam cycle is condensed is cooled to 40 DEG C of entrance oil gas Separator, carries out oil gas, liquid phase oil product and water natural subsidence at gs-oil separator and separates, and water is discharged through point water bag.Due to a point water Inclusion amasss little, natural subsidence separation therefore inefficient, discharges water often band Chuck Steak, on the one hand causes product to lose, the opposing party In the face of lower procedure adversely affects, as the sewage more containing light oil enters sewage stripping device, in addition to affecting normal operating, Also can cause safety problem.It is thus desirable to the separating of oil equipment of High-efficient Water.The example of another 1 oil-water separation is catalysis, coking plant divides Evaporate top pumparound oil often band water, cause fractionating column top salt crust, affect fractionating column normal operating.Some devices are provided with Drain sump, employing natural subsidence separation equipment volume is big, separation efficiency is the highest.Need online high efficiency oil-water separation equipment by tower top It is properly functioning that the moisture content that circulating reflux oil carries effectively removes guarantee device.
Catalytic cracking unit circulation slurry oil contains catalyst fines, when level of catalyst fines height except increasing recycle oil stock pump, changing Outside hot equipment attrition also can increase circulation slurry oil scaling, coking tendency, affect heat transmission equipment heat-transfer effect, equipment life and Fractionating system safe operation.Downstream user can be affected during externally extracting oil level of catalyst fines height use, owing to slurry oil viscosity is big, Temperature height conventional equipment separating catalyst fine powder is abnormal difficult.It is thus desirable in special online high efficiency separation equipment removing circulation slurry oil Catalyst fines or reduce circulation slurry oil in level of catalyst fines.Methanol-to-olefins device technique process produces a large amount of moisture content, Reaction gas, water vapour carry a small amount of catalyst fines and flow out together, carry out chilled water (chw) and wash after heat exchange is lowered the temperature, most of water vapor Condensing and wash the catalyst fines carried, fresh water (FW), a small amount of oil and catalyst fines are discharged together, need to separate through high-efficiency three-phase Equipment processes.
Summary of the invention
It is an object of the present invention to provide a kind of eddy flow centrifugal separation method, having superpower centrifugal force, can to realize efficient gas, liquid, solid biphase Or three phase centrifugation separates.
The technical solution adopted for the present invention to solve the technical problems is: include that charging, light substance are discharged, dense media is discharged, its Feature is: use 2~10 bursts of eddy flow chargings, uses constant speed, accelerates two-part centrifugation, and draws light Jie in central upper portion Matter;The charging of multiply eddy flow makes system all quadrants all in high speed rotating, enters through further speeding up the centrifugal force producing thousand times of gravity Row two-phase laminated flow.
A kind of Rotational flow centrifugal separation device, including cylinder, cone cylinder housing, feed pipe, light substance discharge pipe, dense media discharge pipe, Cyclone, circular cylindrical shell top is ellipsoidal head structure or slab construction, and cone cylinder upper end is connected with cylinder lower end, lower end and dense medium Matter discharge pipe connects;Cylinder top arranges feed pipe, single or multiple runner cyclone, light substance discharge pipe, and feed pipe is in 1 Heart feed pipe or 1 bushing type feed pipe, from up to down reach cylinder interior and be connected with multiple flow passages cyclone;Feed pipe or 2~ 10 straight cutting feed pipes, its lower end reaches cylinder interior respectively and is connected with single channel cyclone;Light substance discharge pipe is that center is gently situated between Matter discharge pipe or bushing type light substance discharge pipe, its lower end edge axis reaches cylinder interior or is connected with cylinder upper end.
Further, it is also possible at bushing type feed pipe and straight cutting feed pipe entrance, horn mouth is set.
Further, it is also possible at light substance discharge pipe end opening, taper guide grid is set.
Further, it is also possible to be provided above feed space at cylinder, straight cutting feed pipe upper end inserts into the inner;Can also be above cylinder Arranging light substance surge drum, its lower end is connected with light substance discharge pipe upper end.
Further, it is also possible to arrange dense media surge drum below cone cylinder, its upper end is connected with cone cylinder lower end, its lower end and dense medium Matter discharge pipe connects.
Further, it is also possible to multiple stage Rotational flow centrifugal separation device is arranged on an enclosure.
Innovative point of the present invention and good effect:
Innovative point of the present invention is: uses 2~10 bursts of eddy flow chargings, uses constant speed, accelerates two-part centrifugation, and on top Light substance is drawn at center;The charging of multiply eddy flow makes system all quadrants all in high speed rotating, produces thousand times of weights through further speeding up The centrifugal force of power carries out two-phase laminated flow.
Good effect of the present invention is: 1, use the charging of multiply eddy flow, forms strength rotational flow and accelerate to produce thousand times through cone cylinder in cylinder Gravity centrifugal force, 4 quadrants of equipment are in high (4 the quadrants existence substantially streams of conventional centrifugal equipment of high speed rotating-device efficiency Speed gradient), use center light substance discharge pipe to discharge light substance-separation efficiency from its upper side center high.2, this equipment tool Having self-cleaning function, cylinder, cone cylinder wall are washed away to be washed away by the impurity such as mud and are taken out of by dense media to bottom by rotating fluid, therefore It is particularly suited for the high liquid-liquid diphase of impurity content to separate.
Accompanying drawing explanation
Fig. 1 is a kind of eddy flow centrifugal separation method and equipment schematic diagram.
1A-light substance outlet, 2-charging aperture, 3-central feed tube, 4-multiple flow passages cyclone, 5-cylinder, 6-cone cylinder, 8-dense medium Matter discharge pipe, 10-light substance surge drum, 11-light substance exports.
Fig. 2 is another kind of eddy flow centrifugal separation method and equipment schematic diagram.
1A-light substance outlet, 3B-straight cutting feed pipe, 4A-single channel cyclone, 5-cylinder, 6-cone cylinder, 8-dense media is discharged Pipe, 10-light substance surge drum, 11-light substance exports
Fig. 3 is another kind of eddy flow centrifugal separation method and equipment schematic diagram.
1-light substance center discharge pipe, 3A-bushing type feed pipe, 4-multiple flow passages cyclone, 5-cylinder, 6-cone cylinder, 7-dense media Surge drum, 8-dense media discharge pipe.
Fig. 4 is another kind of eddy flow centrifugal separation method and equipment schematic diagram.
1-light substance center discharge pipe, 3B-straight cutting feed pipe, 4A-single channel cyclone, 5-cylinder, 6-cone cylinder, 7-dense media is received Collection cylinder, 8-dense media discharge pipe.,
Fig. 5 is another kind of eddy flow centrifugal separation method and equipment schematic diagram.
1-light substance center discharge pipe, 2-charging aperture, 3B-straight cutting feed pipe, 4A-single channel cyclone, 5-cylinder, 6-cone cylinder, 7-dense media surge drum, 8-dense media discharge pipe, 9-feed space, 10-feed space dividing plate.
Detailed description of the invention
See that Fig. 1, light substance surge drum 10 lower end are connected with cylinder 5 upper end through light substance outlet 1A, light substance surge drum 10 Upper end is provided with light substance outlet 11;Central feed tube 3 from up to down reaches cylinder 5 inside along central axis (to be recommended with multiple flow passages 2~4) cyclone 4 connects, and central feed tube 3 upper end is connected with charging aperture 2;Cone cylinder 6 lower end is connected with dense media discharge pipe 8, Upper end is connected with cylinder 5 lower end.
See that Fig. 2, light substance surge drum 10 lower end are connected with cylinder 5 upper end through light substance outlet 1A, light substance surge drum 10 Upper end is provided with light substance outlet 11;2~4 straight cutting feed pipe 3B are uniformly distributed along 5 sections of gardens of cylinder, and from up to down reach circle Cylinder 5 is internal to be connected with 2~4 single channel cyclone 4A;Cone cylinder 6 lower end is connected with dense media discharge pipe 8, upper end and cylinder 5 lower ends connect.
See that Fig. 3, bushing type feed pipe 3A from up to down reach cylinder 5 inside and multiple flow passages (recommending 2~4) rotation along central axis Stream device 4 connects, and light substance center discharge pipe 1 upwards passes along central axis is bottom-up through bushing type feed pipe 3A;Cone cylinder 6 Upper end is connected with cylinder 5 lower end, and cone cylinder 6 lower end is connected with dense media surge drum 7, dense media surge drum 7 lower end and dense media Discharge pipe 8 connects.
Seeing Fig. 4,2~4 straight cutting feed pipe 3B are uniformly distributed along 5 sections of gardens of cylinder, and from up to down reach cylinder 5 internal with 2~ 4 single channel cyclone 4A connect;Light substance center discharge pipe 1 from up to down reaches inside cylinder 5 along central axis;Cone cylinder 6 upper ends are connected with cylinder 5 lower end, and cone cylinder 6 lower end is connected with dense media surge drum 7, dense media surge drum 7 lower end and dense medium Matter discharge pipe 8 connects.
See Fig. 5, feed space dividing plate 10 is set inside cylinder 5, above it, form feed space 9.2~4 straight cutting feed pipe 3B It is uniformly distributed along 5 sections of gardens of cylinder, and from up to down reaches cylinder 5 inside and 2~4 single channels rotations through feed space dividing plate 10 Stream device 4A connects, and straight cutting feed pipe 3B upper end reaches feed space 9;Light substance center discharge pipe 1 is along central axis from up to down Cylinder 5 is reached internal through feed space 9 top board and feed space dividing plate 10;Cone cylinder 6 upper end is connected with cylinder 5 lower end, cone cylinder 6 Lower end is connected with dense media surge drum 7, and dense media surge drum 7 lower end is connected with dense media discharge pipe 8.
See Fig. 1, Fig. 2, two-phase medium such as water oil mixture from charging aperture 2, central feed tube 3 enter multiple flow passages (recommend 2~ 4) cyclone 4 (Fig. 2 enters 2~4 single channel cyclone 4A through 2~4 straight cutting feed pipe 3B), then multiply eddy flow tangent line Direction is flowed out and is formed strength rotational flow in cylinder 5, accelerates to produce thousand times of gravity centrifugal forces, water under centrifugal action through cone cylinder 6 To barrel concentration, oil in center set, pressure and buoyancy oil flow up and enter light substance collection through light substance outlet 1A Cylinder 10 is also discharged through light substance outlet 11.Water flows downward under gravity and pressure effect and discharges through dense media discharge pipe 8.
See Fig. 3, two-phase medium such as gas-solid mixture or gas-liquid mixture, enter multiple flow passages from bushing type feed pipe 3A and (recommend 2~4) cyclone 4, then multiply eddy flow tangential direction flows out and forms strength rotational flow in cylinder 5, accelerates generation thousand through cone cylinder 6 Times gravity centrifugal force, under centrifugal action solid particle or liquid concentrate to barrel, gas in center set, at pressure and floating Under power effect, gas enters from discharge suitable for reading from light substance center discharge pipe 1 end opening.Solid particle (concentrated phase) or liquid at gravity and Pressure effect is dirty to bottom dense media surge drum 7, discharges through dense media discharge pipe 8.
See Fig. 4, Fig. 5, two-phase medium such as gas-solid mixture or gas-liquid mixture, from 2~4 straight cutting feed pipe 3B enter 2~ 4 single channel cyclone 4A (Fig. 5 first enters feed space 9 through charging aperture 2), then multiply eddy flow tangential direction flows out at cylinder 5 Interior formation strength rotational flow, accelerates to produce thousand times of gravity centrifugal forces through cone cylinder 6, and under centrifugal action, solid particle or liquid are to cylinder Wall concentration, gas are in center set, and under pressure and buoyancy, gas enters from suitable for reading from light substance center discharge pipe 1 end opening Discharge.Solid particle (concentrated phase) or liquid are dirty to bottom dense media surge drum 7 at gravity and pressure effect, discharge through dense media Pipe 8 is discharged.

Claims (7)

1. an eddy flow centrifugal separation method, including charging, light substance discharge, dense media discharge, it is characterized in that: use 2~ 10 bursts of eddy flow chargings, use constant speed, accelerate two-part centrifugation, and draw light substance in central upper portion;Multiply eddy flow feeds Make system all quadrants all in high speed rotating, carry out two-phase laminated flow through further speeding up the centrifugal force producing thousand times of gravity.
2. a Rotational flow centrifugal separation device, discharges including cylinder, cone cylinder housing, feed pipe, light substance discharge pipe, dense media Pipe, cyclone, circular cylindrical shell top is ellipsoidal head structure or slab construction, and cone cylinder upper end is connected with cylinder lower end, lower end and Dense media discharge pipe connects;Cylinder top arranges feed pipe, single or multiple runner cyclone, light substance discharge pipe, and feed pipe is 1 Root central feed tube or 1 bushing type feed pipe, from up to down reach cylinder interior and be connected with multiple flow passages cyclone;Feed pipe or Being 2~10 straight cutting feed pipes, its lower end reaches cylinder interior respectively and is connected with single channel cyclone;During light substance discharge pipe is Heart light substance discharge pipe or bushing type light substance discharge pipe, its lower end edge axis reaches cylinder interior or is connected with cylinder upper end.
Rotational flow centrifugal separation device the most according to claim 1, is characterized in that: can also be at bushing type feed pipe and straight cutting Feed pipe entrance arranges horn mouth.
Rotational flow centrifugal separation device the most according to claim 1, is characterized in that: can also set at light substance discharge pipe end opening Put taper guide grid.
Rotational flow centrifugal separation device the most according to claim 1, is characterized in that: can also be provided above feed space at cylinder, Straight cutting feed pipe upper end inserts into the inner;Light substance surge drum can also be provided above, on its lower end and light substance discharge pipe at cylinder End connects.
Rotational flow centrifugal separation device the most according to claim 1, is characterized in that: can also arrange dense media below cone cylinder Surge drum, its upper end is connected with cone cylinder lower end, and its lower end is connected with dense media discharge pipe.
Rotational flow centrifugal separation device the most according to claim 1, is characterized in that: can also multiple stage eddy flow centrifugation be set For being arranged on an enclosure.
CN201410751233.5A 2014-12-10 2014-12-10 Cyclone centrifugal separation method and equipment Pending CN105880044A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201410751233.5A CN105880044A (en) 2014-12-10 2014-12-10 Cyclone centrifugal separation method and equipment

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201410751233.5A CN105880044A (en) 2014-12-10 2014-12-10 Cyclone centrifugal separation method and equipment

Publications (1)

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CN105880044A true CN105880044A (en) 2016-08-24

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106398779A (en) * 2016-10-26 2017-02-15 航天长征化学工程股份有限公司 Synthetic gas washing, dedusting and dewatering system
CN106520217A (en) * 2016-10-26 2017-03-22 航天长征化学工程股份有限公司 Dust removal dehydration tower

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106398779A (en) * 2016-10-26 2017-02-15 航天长征化学工程股份有限公司 Synthetic gas washing, dedusting and dewatering system
CN106520217A (en) * 2016-10-26 2017-03-22 航天长征化学工程股份有限公司 Dust removal dehydration tower

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Application publication date: 20160824