CN105875686A - Copper base-containing non-stick barbecue mat made from polytetrafluoroethylene, and manufacturing method of non-stick barbecue mat - Google Patents
Copper base-containing non-stick barbecue mat made from polytetrafluoroethylene, and manufacturing method of non-stick barbecue mat Download PDFInfo
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- CN105875686A CN105875686A CN201610221477.1A CN201610221477A CN105875686A CN 105875686 A CN105875686 A CN 105875686A CN 201610221477 A CN201610221477 A CN 201610221477A CN 105875686 A CN105875686 A CN 105875686A
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- politef
- barbecue
- copper powder
- mat
- stick
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- A—HUMAN NECESSITIES
- A21—BAKING; EDIBLE DOUGHS
- A21B—BAKERS' OVENS; MACHINES OR EQUIPMENT FOR BAKING
- A21B3/00—Parts or accessories of ovens
-
- A—HUMAN NECESSITIES
- A21—BAKING; EDIBLE DOUGHS
- A21B—BAKERS' OVENS; MACHINES OR EQUIPMENT FOR BAKING
- A21B3/00—Parts or accessories of ovens
- A21B3/15—Baking sheets; Baking boards
-
- D—TEXTILES; PAPER
- D03—WEAVING
- D03D—WOVEN FABRICS; METHODS OF WEAVING; LOOMS
- D03D13/00—Woven fabrics characterised by the special disposition of the warp or weft threads, e.g. with curved weft threads, with discontinuous warp threads, with diagonal warp or weft
-
- D—TEXTILES; PAPER
- D03—WEAVING
- D03D—WOVEN FABRICS; METHODS OF WEAVING; LOOMS
- D03D15/00—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used
-
- D—TEXTILES; PAPER
- D03—WEAVING
- D03D—WOVEN FABRICS; METHODS OF WEAVING; LOOMS
- D03D15/00—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used
- D03D15/20—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the material of the fibres or filaments constituting the yarns or threads
- D03D15/242—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the material of the fibres or filaments constituting the yarns or threads inorganic, e.g. basalt
- D03D15/267—Glass
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Food Science & Technology (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Baking, Grill, Roasting (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
Abstract
The invention relates to a copper base-containing non-stick barbecue mat made from polytetrafluoroethylene. The non-stick barbecue mat is fiber cloth formed by dipping high-performance glass fiber cloth by taking polytetrafluoroethylene resin dispersion liquid and polytetrafluoroethylene resin suspension containing 0.05-10 percent by weight of copper powder as raw materials; the non-stick barbecue mat product prepared from the polytetrafluoroethylene has antibacterial, bactericidal and bacteriostatic functions. The copper base-containing non-stick barbecue mat made from the polytetrafluoroethylene has the advantages that (1) a polytetrafluoroethylene coating contains a certain amount of copper, so that the non-stick barbecue mat has the antibacterial, bactericidal and bacteriostatic functions and an odor removal function; (2) the surface of the barbecue mat is non-stick and is coated with polytetrafluoroethylene, thus being very smooth and not easy to stick to food; (3) the non-stick barbecue mat is easy to clean, and is dried in the air after being washed by clear water; (4) the non-stick barbecue mat has heat resistance, and can be continuously used in an environment of -70 DECG to 260 DEG C; (5) the non-stick barbecue mat is long in service life and can be repeatedly used for a plurality times. Therefore, the copper base-containing non-stick barbecue mat made from the polytetrafluoroethylene is massively used for baking foods such as vegetables, meats and seafood on a charcoal fire barbecue oven, an electric oven, a baking oven or a microwave oven.
Description
Technical field
The present invention relates to a kind of formula of the not viscous barbecue pad of the politef containing cuprio with antibiotic and sterilizing taste removal effect and preparation method thereof.
Background technology
Politef is the macromolecular compound in molecular backbone containing fluorine atom, owing in molecule, C-F key has high dissociation energy, and fluorine atom high electronegativity and screen effect, make it have high and low temperature resistance and the chemical stability of excellence, and there is good dielectric properties, non-adhesive, low abrasiveness, weatherability, noninflammability and lubricity, it is the macromolecular material that a kind of performance is the most excellent.
Glass fibre is the inorganic non-metallic material of a kind of excellent performance, and its advantage is insulation, heat-resisting, anticorrosive, and mechanical strength is high, and its filament diameter is several micron to twenties micron, and every bundle fiber precursor is all made up of hundreds of the most thousands of monofilament.
By politef and glass fabric and copper powder three be composited containing cuprio, there is the viscous barbecue pad of the politef of antibiotic and sterilizing taste removal effect and preparation method is not also having corresponding document to report at present.
Summary of the invention
A kind of not viscous barbecue pad of the politef containing cuprio with antibiotic and sterilizing taste removal effect of purpose of the present invention research and development.
The above-mentioned technical problem of the present invention is mainly addressed by following proposal: the not viscous barbecue pad of a kind of politef containing cuprio, politef, glass fabric and copper powder three are composited.
As preferably, the not viscous barbecue pad of the described politef containing cuprio is by percentage by weight 0.01～the copper powder of 6%；Percentage by weight 5～the politef of 60%；Percentage by weight 20～90% glass fabric three be composited.
As preferably, described politef is tetrafluoraoethylene-hexafluoropropylene copolymer FEP, polytrifluorochloroethylene PCTFE, Kynoar PVDF, polyvinyl fluoride PVF, ethylene-chlorotrifluoro-ethylene copolymer E-CTFE, ethylene-tetrafluoroethylene copolymer E-TFE, tetrafluoroethylene-perfluoroalkyl vinyl ether copolymer Teflon PFA, vinylidene-chlorotrifluoroethylene VDF-CTFE, hexafluoropropylene (HFP)/tetrafluoroethylene (TFE)-perfluoroalkyl vinyl ether copolymer Teflon EPE, one or more in perfluorinated sulfonic resin XR resin and vinylidene-hexafluoro-isobutene copolymer CM-I resin.
As preferably, described glass fibre is alkali-free glass fibre, medium-alkali glass fibre or high-strength glass fibre, and wherein glass fiber diameter is 5～25 microns；The weavy grain of glass fabric is plain weave, twill, satin weave, rib-loop or basket, and the grammes per square metre of glass fabric is 20～1000.
As preferably, described copper powder includes cathode copper i.e. pure copper powder or red copper powder, alloy copper powder, atomized copper powder or cupric oxide powder, and copper powder particle size is 100 mesh～2 microns.
Another technical scheme of the present invention is to provide the manufacture method of the not viscous barbecue pad of a kind of politef containing cuprio, comprise the steps: that copper powder is inserted to fill in the mixing drum that solids content is 60% polyflon dispersion liquid B by (1) to stir 2～8 hours, temperature controls at 20～25 DEG C, makes containing the polyflon suspending liquid A that percentage by weight is 0.05%～10% copper powder；(2) the most first glass fabric be impregnated in and then the polyflon dispersion liquid B that solids content is 60% picks up dry, sinter at a certain temperature, repeated impregnations drying and sintering operation 0～3 times；(3) what the glass fabric through step (2) impregnated in prepared by above-mentioned steps (1) the most again is dry containing then picking up in the polyflon suspending liquid A that percentage by weight is 0.05%～10% copper powder, sinter at a certain temperature, repeated impregnations drying and sintering operation 1～3 times；(4) it is 60% dry for then picking up in polyflon dispersion liquid B for the glass fabric through step (2) and (3) then soaking again stain in solids content, it is sintered, repeated impregnations--being dried--sintering circuit 0 to 3 times at a certain temperature；Thus making intermediate layer is glass fabric, the membranaceous cloth of politef/glass fabric of the outer layer polytetrafluorethylecoatings coatings containing 0.01%～6% percentage by weight copper powder；(5) then will make intermediate layer through step (2) (3) and (4) is glass fabric, the membranaceous cloth of politef/glass fabric of the outer layer polytetrafluorethylecoatings coatings containing 0.01%～6% percentage by weight copper powder is divided into long strip type cloth, and cut into the tablet of definite shape as required, then tablet is carried out chamfering and edge sealing processes, make the not viscous barbecue pad of politef containing cuprio with antibiotic and sterilizing taste removal effect.
As preferably, in the impregnation drying sintering circuit in described step (2), (3) and (4), baking temperature controls at 90～100 DEG C, and sintering temperature controls at 370～390 DEG C.
As preferably, in described step (2), (3) and (4), sintering uses vertical consecutive sintering furnace or horizontal continuous fritting furnace, and sintering time controlled at 2～10 minutes；Process velocity controls at 0.5～6 m/min.
As preferably, in described step (2) and (4), its dipping--being dried--is when sintering circuit number of times is 0, i.e. without step (2) and (4), only through step (3).
As another preferably, to make intermediate layer through step (2) (3) and (4) is glass fabric, the membranaceous cloth of politef/glass fabric of the outer layer polytetrafluorethylecoatings coatings containing copper powder is divided into long strip type cloth, and cut into the tablet of definite shape as required, then tablet is carried out chamfering and edge sealing processes.
Compared with prior art, the viscous barbecue pad of politef that present invention research and development have antibiotic and sterilizing taste removal effect containing cuprio is with polyflon dispersion liquid and to contain the polyflon suspension of 0.05%～10% (weight percent content) copper powder as raw material, the fiber cloth of dipping high-performance glass fiber cloth, is a kind of politef not viscous barbecue pad product with antibiotic and sterilizing and bacteriostasis.Have the advantage that (1) because containing the copper of certain content in polytetrafluorethylecoatings coatings, thus have that antibiotic and sterilizing is antibacterial and taste removal effect；(2) non-stick, surface-coated has politef, and surface is the most smooth, is difficult to cling food；(3) easy to clean, rinse well with clear water, dry；(4) thermostability, persistently can use in the environment of-70～260 DEG C；(4) service life is long, can repeated multiple times use.Therefore charcoal oven it is largely used to, baking vegetable meat seafood food in electric oven, baking box, microwave oven.
Detailed description of the invention
It is further discussed below the present invention below in conjunction with embodiment, but the present invention should not be limited by the examples.
It is as follows that the not viscous barbecue of a kind of politef containing cuprio pads its making step:
(1) copper powder is inserted fill in the mixing drum that solids content is 60% polyflon dispersion liquid B stir 2～8 hours, temperature controls at 20～25 DEG C, makes containing the polyflon suspending liquid A that percentage by weight is 0.05%～10% copper powder；(2) the most first glass fabric be impregnated in and then the polyflon dispersion liquid B that solids content is 60% picks up dry, sinter at a certain temperature, repeated impregnations drying and sintering operation 0～3 times；(3) what the glass fabric through step (2) impregnated in prepared by above-mentioned steps (1) the most again is dry containing then picking up in the polyflon suspending liquid A that percentage by weight is 0.05%～10% copper powder, sinter at a certain temperature, repeated impregnations drying and sintering operation 1～3 times；(4) it is 60% dry for then picking up in polyflon dispersion liquid B for the glass fabric through step (2) and (3) then soaking again stain in solids content, it is sintered, repeated impregnations--being dried--sintering circuit 0 to 3 times at a certain temperature；Thus making intermediate layer is glass fabric, the membranaceous cloth of politef/glass fabric of the outer layer polytetrafluorethylecoatings coatings containing 0.01%～6% percentage by weight copper powder；(5) then will make intermediate layer through step (2) (3) and (4) is glass fabric, the membranaceous cloth of politef/glass fabric of the outer layer polytetrafluorethylecoatings coatings containing 0.01%～6% percentage by weight copper powder is divided into long strip type cloth, and cut into the tablet of definite shape as required, then tablet is carried out chamfering and edge sealing processes, make the not viscous barbecue pad of politef containing cuprio with antibiotic and sterilizing taste removal effect.
Embodiment 1
It is as follows that the not viscous barbecue of a kind of politef containing cuprio pads its making step:
(1) is moistened in Hengshui, Sichuan metal dust company limited produce pure copper powder, granularity is 800 mesh, insert in the mixing drum filling the polyflon dispersion liquid B that solids content is 60%, and add additive, dispersed with stirring 2 to 8 hours, make the polyflon suspending liquid A containing 5% (weight percent content) copper powder, and filter with 80 mesh stainless steel meshs；And storage temperature is 20～25 DEG C of standby paintings in indoor；.
(2) SFN-1H polyflon dispersion liquid (solids content is about the 60%) B that Zhong Hao Chenguang Research Institute of Chemical Industry produces is used；
(3) the G75 Weave type electronic-grade glass yarn (single fiber diameter is 9um, and line density is 68.7Tex) that glass fabric uses Chongqing Polycomp International Corporation to produce is the glass fabric that raw material is made into；
(4) sintering furnace uses autonomous Design and the vertical three Room continuous fritting furnaces of production, and this sintering furnace is wide 2.5 meters, high 12 meters；
(5) the most first glass fabric be impregnated in polyflon dispersion liquid B (solids content is 60%) then picks up dry, sinter at a certain temperature, baking temperature controls at 90～100 DEG C, and sintering temperature controls at 370～390 DEG C；Sintering time controlled at 2～10 minutes；Process velocity controls at 0.5～6 m/min, repeated impregnations drying and sintering operation 2 times；
(6) the most again the glass fabric through step (5) be impregnated in the polyflon suspending liquid A containing 5% (weight percent content) copper powder prepared by above-mentioned steps (1) then picks up dry, sinter at a certain temperature, baking temperature controls at 90～100 DEG C, and sintering temperature controls at 370～390 DEG C；Sintering time controlled at 2～10 minutes；Process velocity controls at 0.5～6 m/min, repeated impregnations--being dried--sintering circuit 2 times；
(6) then the glass fabric through step (5) and (6) is soaked again stain and then pick up dry in polyflon dispersion liquid (solids content is 60%) B, it is sintered at a certain temperature, baking temperature controls at 90～100 DEG C, and sintering temperature controls at 370～390 DEG C；Sintering time controlled at 2～10 minutes；Process velocity controls at 0.5～6 m/min, repeated impregnations--being dried--sintering circuit 2 times；Thus making intermediate layer is glass fabric, the membranaceous cloth of politef/glass fabric of the outer layer polytetrafluorethylecoatings coatings containing a certain amount of copper powder (1% weight percent content)；
(7) will make intermediate layer through step (2) (3) and (4) is glass fabric, the membranaceous cloth of politef/glass fabric of the outer layer polytetrafluorethylecoatings coatings containing a certain amount of copper powder (0.01% to 6% weight percent content) is divided into long strip type cloth, and cut into definite shape as required, then tablet is carried out chamfering and edge sealing processes.
Containing cuprio, there is the copper that the viscous barbecue pad of politef of antibiotic and sterilizing taste removal effect contains 1% (percentage by weight) by finally prepare after above-mentioned steps, the politef of the glass fibre each 34% of 55% (percentage by weight), has antibiotic and sterilizing and taste removal effect.
It is an object of the invention to invent a kind of not viscous barbecue of politef containing cuprio with antibiotic and sterilizing taste removal effect, it is with polyflon dispersion liquid and to contain the polyflon suspension of 0.05% to 10% (weight percent content) copper powder as raw material, the fiber cloth of dipping high-performance glass fiber cloth, is a kind of politef not viscous barbecue pad product with antibiotic and sterilizing and bacteriostasis.Have the advantage that (1) because containing the copper of certain content in polytetrafluorethylecoatings coatings, thus have that antibiotic and sterilizing is antibacterial and taste removal effect；(2) non-stick, surface-coated has politef, and surface is the most smooth, is difficult to cling food；(3) easy to clean, rinse well with clear water, dry；(4) thermostability, persistently can use in the environment of-70～260 DEG C；(4) service life is long, can repeated multiple times use.Therefore baking vegetable meat seafood food in charcoal oven, electric oven, baking box, microwave oven it is largely used to.
Finally it is pointed out that above example is only the more representational example of the present invention.Obviously, technical scheme is not limited to above-described embodiment, it is also possible to have many variations.All deformation that those of ordinary skill in the art can directly derive from present disclosure or associate, are all considered as protection scope of the present invention.
Claims (10)
1. the not viscous barbecue pad of the politef containing cuprio, it is characterised in that by politef, glass fibers
Dimension cloth and copper powder three are composited.
The not viscous barbecue pad of a kind of politef containing cuprio the most according to claim 1, it is characterised in that
By percentage by weight 0.01～the copper powder of 6%；Percentage by weight 5～the politef of 60%；Percentage by weight
20～90% glass fabric three be composited.
The not viscous barbecue pad of a kind of politef containing cuprio the most according to claim 1, it is characterised in that
Described politef is tetrafluoraoethylene-hexafluoropropylene copolymer FEP, polytrifluorochloroethylene PCTFE, poly-partially
Fluorothene PVDF, polyvinyl fluoride PVF, ethylene-chlorotrifluoro-ethylene copolymer E-CTFE, ethylene-tetrafluoro second
Alkene copolymer E-TFE, tetrafluoroethylene-perfluoroalkyl vinyl ether copolymer Teflon PFA, vinylidene-three
Fluorine vinyl chloride copolymer VDF-CTFE, hexafluoropropylene (HFP)/tetrafluoroethylene (TFE)-perfluoroalkyl vinyl ether copolymer
Teflon EPE, perfluorinated sulfonic resin XR resin and vinylidene-hexafluoro-isobutene copolymer CM-I resin
In one or more.
The not viscous barbecue pad of a kind of politef containing cuprio the most according to claim 1, it is characterised in that
Described glass fibre is alkali-free glass fibre, medium-alkali glass fibre or high-strength glass fibre, wherein glass fibre
A diameter of 5～25 microns；The weavy grain of glass fabric is plain weave, twill, satin weave, rib-loop or basket,
The grammes per square metre of glass fabric is 20～1000.
The not viscous barbecue pad of a kind of politef containing cuprio the most according to claim 1, it is characterised in that
Described copper powder includes cathode copper i.e. pure copper powder or red copper powder, alloy copper powder, atomized copper powder or cupric oxide powder,
Copper powder particle size is 100 mesh～2 microns.
6. a manufacture method for the not viscous barbecue pad of the politef containing cuprio described in claim 1-5, its feature
It is, comprises the steps: that copper powder is inserted that to fill solids content be that 60% polyflon divides by (1)
Dissipating in the mixing drum of liquid B and stir 2～8 hours, temperature controls, at 20～25 DEG C, to make containing weight percent
Than the polyflon suspending liquid A being 0.05%～10% copper powder；(2) the most first by glass fabric
Impregnated in then the polyflon dispersion liquid B that solids content is 60% picks up dry, at a constant temperature
The lower sintering of degree, repeated impregnations drying and sintering operation 0～3 times；(3) the most again will be through the glass of step (2)
What glass fiber cloth impregnated in prepared by above-mentioned steps (1) is the poly-of 0.05%～10% copper powder containing percentage by weight
Then picking up dry in TFE suspending liquid A, sinter at a certain temperature, repeated impregnations is dried
Sintering circuit 1～3 times；(4) then the glass fabric through step (2) and (3) is soaked again stain in
Solids content is 60% dry for then picking up in polyflon dispersion liquid B, enters at a certain temperature
Row sintering, repeated impregnations--being dried--sintering circuit 0 to 3 times；Thus making intermediate layer is glass fabric,
Politef/the glass fabric of the outer layer polytetrafluorethylecoatings coatings containing 0.01%～6% percentage by weight copper powder
Membranaceous cloth；(5) then will make intermediate layer through step (2) (3) and (4) is glass fabric,
Politef/the glass fabric of the outer layer polytetrafluorethylecoatings coatings containing 0.01%～6% percentage by weight copper powder
Membranaceous cloth is divided into long strip type cloth, and cuts into the tablet of definite shape as required, then by sheet
Shape thing carries out chamfering and edge sealing processes, and makes and has the politef of antibiotic and sterilizing taste removal effect not containing cuprio
Viscous barbecue pad.
The manufacture method of the not viscous barbecue pad of a kind of politef containing cuprio the most according to claim 6, its
It is characterised by: in the impregnation drying sintering circuit in described step (2), (3) and (4), is dried temperature
Degree controls at 90～100 DEG C, and sintering temperature controls at 370～390 DEG C.
The manufacture method of the not viscous barbecue pad of a kind of politef containing cuprio the most according to claim 6, its
Being characterised by: in described step (2), (3) and (4), sintering uses vertical consecutive sintering furnace or crouches
Formula continuous fritting furnace, sintering time controlled at 2～10 minutes；Process velocity controls at 0.5～6 m/min.
The manufacture method of the not viscous barbecue pad of a kind of politef containing cuprio the most according to claim 6, its
Being characterised by: in described step (2) and (4), its dipping--being dried--is when sintering circuit number of times is 0, i.e.
Without step (2) and (4), only through step (3).
The manufacture method of the not viscous barbecue pad of a kind of politef containing cuprio the most according to claim 6,
It is characterized in that: will make intermediate layer through step (2) (3) and (4) is glass fabric, and outer layer contains
The membranaceous cloth of politef/glass fabric of the polytetrafluorethylecoatings coatings of copper powder is divided into long strip type cloth,
And cut into the tablet of definite shape as required, then tablet is carried out chamfering and edge sealing processes.
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| CN201610221477.1A CN105875686A (en) | 2016-04-11 | 2016-04-11 | Copper base-containing non-stick barbecue mat made from polytetrafluoroethylene, and manufacturing method of non-stick barbecue mat |
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| CN201610221477.1A CN105875686A (en) | 2016-04-11 | 2016-04-11 | Copper base-containing non-stick barbecue mat made from polytetrafluoroethylene, and manufacturing method of non-stick barbecue mat |
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| CN202680347U (en) * | 2012-08-07 | 2013-01-23 | 桐乡市科力复合材料有限公司 | Barbecue pad |
| CN104250929A (en) * | 2013-06-28 | 2014-12-31 | 曹建林 | Teflon glass fiber cloth film material |
| CN104911911A (en) * | 2015-05-20 | 2015-09-16 | 赵国平 | Teflon glass fiber gridding cloth production technology |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| JPS5889629A (en) * | 1981-11-25 | 1983-05-28 | Yokohama Rubber Co Ltd:The | Fiber-reinforced plastic compound |
| JPS5889630A (en) * | 1981-11-25 | 1983-05-28 | Yokohama Rubber Co Ltd:The | Fiber-reinforced plastic composition |
| CN101463562A (en) * | 2009-01-09 | 2009-06-24 | 薛艳艳 | Preparation of fluoro-resin emulsion dipping agent and preparation of coated fabric |
| CN101768811A (en) * | 2010-02-05 | 2010-07-07 | 东华大学 | Method for preparing polytetrafluoroethylene-based three-dimensional orthogonal composite material |
| CN102641120A (en) * | 2012-05-21 | 2012-08-22 | 重庆帅能科技有限公司 | Nonmetal wrist band making method |
| CN202680347U (en) * | 2012-08-07 | 2013-01-23 | 桐乡市科力复合材料有限公司 | Barbecue pad |
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Application publication date: 20160824 |
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