CN105866168A - Identification method and apparatus for lower matrix material of coating - Google Patents

Identification method and apparatus for lower matrix material of coating Download PDF

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Publication number
CN105866168A
CN105866168A CN201610176997.5A CN201610176997A CN105866168A CN 105866168 A CN105866168 A CN 105866168A CN 201610176997 A CN201610176997 A CN 201610176997A CN 105866168 A CN105866168 A CN 105866168A
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target
logarithm
temperature
lowering curve
temperature lowering
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CN105866168B (en
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陈大鹏
李晓丽
张小龙
武敬力
张亚洲
雷浩
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Beijing Institute of Environmental Features
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Beijing Institute of Environmental Features
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N25/00Investigating or analyzing materials by the use of thermal means
    • G01N25/20Investigating or analyzing materials by the use of thermal means by investigating the development of heat, i.e. calorimetry, e.g. by measuring specific heat, by measuring thermal conductivity
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01JMEASUREMENT OF INTENSITY, VELOCITY, SPECTRAL CONTENT, POLARISATION, PHASE OR PULSE CHARACTERISTICS OF INFRARED, VISIBLE OR ULTRAVIOLET LIGHT; COLORIMETRY; RADIATION PYROMETRY
    • G01J5/00Radiation pyrometry, e.g. infrared or optical thermometry
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01JMEASUREMENT OF INTENSITY, VELOCITY, SPECTRAL CONTENT, POLARISATION, PHASE OR PULSE CHARACTERISTICS OF INFRARED, VISIBLE OR ULTRAVIOLET LIGHT; COLORIMETRY; RADIATION PYROMETRY
    • G01J5/00Radiation pyrometry, e.g. infrared or optical thermometry
    • G01J2005/0077Imaging

Abstract

The invention discloses an identification method for a lower matrix material of a coating. The method comprises the following steps: exciting a first target of a coated coating by using light pulse and acquiring an infrared thermogram sequence by using a thermal infrared imager; for any point of the first target, acquiring temperature-time data of the point and then acquiring the logarithmic cooling curve of the point; calculating the slop of the logarithmic cooling curve and then calculating the separation characteristic value of the point; acquiring the separation characteristic value of each point of the first target; acquiring the surface gray scale graph of the first target; acquiring the surface gray scale graph of each target of a plurality of targets; and identifying the matrix material of the plurality of targets according to the surface gray scale graph. The method provided by the invention can detect and identify the lower matrix material of the coating by analyzing the separation degree of the logarithmic cooling curves of different matrixes and the coating.

Description

The discrimination method of a kind of coating lower substrate material and device
Technical field
The present invention relates to infrared characteristic fields of measurement, particularly relate to the discriminating side of a kind of coating lower substrate material Method and device.
Background technology
Coating paint-on technique be widely used in Aero-Space, mechanical engineering, information technology, microelectric technique, The fields such as optical Information science, the quality of coating coating directly affects its actual application.Coating quality detection has A lot of means, infrared thermal imaging is one of them.Infrared thermal imaging is an emerging technology, with tradition Detection method compare, this technical speed is fast, noncontact, pollution-free.But the infra-red radiation due to target Only relevant with the material behavior in its surface tens micron thickness, thus scribble the matrix material of same coating Material often shows identical in infrared image, and under simple analysis target thermal equilibrium state, a certain moment is infrared Characteristic is difficult to effectively detect it and identify.
Therefore, need discrimination method and the device of a kind of coating lower substrate material badly, utilize controlled, effective Motivator breaks coating material thermal balance, and the heat of inverting inner material is carried out in the warm field changed by research Physical attribute.
Summary of the invention
The present invention provides a kind of and carries out what coating lower substrate material differentiated based on light pulse excitation infrared thermal imaging Method and device, by analyzing the separation degree of different matrix and coating logarithm temperature lowering curve, exploitation is corresponding Data processing algorithm, it is achieved the detection of coating lower substrate material and identification.
One aspect of the present invention provides the discrimination method of a kind of coating lower substrate material, including step: S1. utilizes The first object surface being coated with application layer is encouraged by light pulse, gathers first object by thermal infrared imager The infrared information on surface, obtains infrared thermal imagery graphic sequence;S2. for any point on first object surface, root According to the Temperature-time data of described this point of Infrared Thermogram retrieval, should by Temperature-time data acquisition The logarithm temperature lowering curve of point;S3. calculate the slope of described logarithm temperature lowering curve, and lower the temperature according to described logarithm Slope of a curve calculates the separation characteristic values of this point;S4. repeat step S1-S3, obtain first object surface The separation characteristic values of every bit;According to the separation characteristic values of first object surface every bit, obtain the first mesh Mark surface gray-scale figure;S5. for the second target, the 3rd target ... each target in N target, repeat Step S1-S4, it is thus achieved that the surface gray-scale figure of described each target;N number of mesh is differentiated according to surface gray-scale figure Target matrix material;Wherein, N is the integer more than 1.
Preferably, by the logarithm temperature lowering curve of this point of Temperature-time data acquisition particularly as follows: to temperature- Time data carries out background subtraction process, normalized, process of taking the logarithm, and obtains logarithm temperature lowering curve.
Preferably, described normalized is: obtain the maximum temperature values in Temperature-time data, according to Temperature-time data are normalized by maximum temperature values;Described taking the logarithm is processed as Temperature-time Temperature, time in data take the logarithm respectively.
Preferably, the slope calculating described logarithm temperature lowering curve includes:
S31. the very first time value meeting the first preset rules and the second time value are chosen, by logarithm cooling song The line acquisition the first temperature value corresponding to very first time value, the second temperature value corresponding to the second time value;
S32. the slope of logarithm temperature lowering curve is calculated according to formula 1;
Wherein, k is the slope of logarithm temperature lowering curve, and a is very first time value, and m is the second time value, b Being the first temperature value, n is the second temperature value;B=f (a), n=f (m), y=f (x) are logarithm temperature lowering curve.
Preferably, the first preset rules is particularly as follows: very first time value and the difference of the second time value are not less than pre- If interval.
Preferably, calculate the separation characteristic values of this point according to the slope of described logarithm temperature lowering curve to include:
S33. the M group data the earliest after being collected in light pulse excitation in logarithm temperature lowering curve are intended Conjunction obtains coating slope;
S34. using the difference of the slope of logarithm temperature lowering curve and coating slope as the separation characteristic values of this point;
Wherein, M is the positive integer less than 15.
Preferably, at the described separation characteristic values according to first object surface every bit, first object is obtained Before the gray-scale figure of surface, step S4 also includes: pre-set the corresponding relation of separation characteristic values and grey decision-making.
Preferably, differentiate that the matrix material of N number of target is particularly as follows: according to N number of mesh according to surface gray-scale figure Mark surface gray-scale figure directly distinguishes the matrix material of each target;Or by each for target surface each in N number of target The separation characteristic values of point compares with the separation characteristic values of standard specimen, determines the matrix material of each target.
Preferably, described standard specimen is for pre-setting, and the separation characteristic values of described standard specimen is according to step Rapid S1-S4 obtains.
Another aspect of the present invention provides the identification device of a kind of coating lower substrate material, including:
Information acquisition unit, each object table in utilizing light pulse to the N number of target being coated with application layer Face is encouraged, and is gathered the infrared information of each target surface by thermal infrared imager, obtains each target Infrared thermal imagery graphic sequence;
Logarithm temperature lowering curve acquiring unit, for every according to each target surface of Infrared Thermogram retrieval The Temperature-time data of a bit, Temperature-time data are carried out background subtraction process, maximum normalized, Take the logarithm and after processing, obtain the logarithm temperature lowering curve of described every bit;
Separation characteristic values computing unit, for utilizing two-point method to calculate the logarithm temperature lowering curve of described every bit Slope, and the slope of logarithm temperature lowering curve is separated as described every bit with the difference of coating slope Eigenvalue;
Gray-scale figure acquiring unit, is used for the separation characteristic values according to described every bit and the separation pre-set The corresponding relation of eigenvalue and grey decision-making, obtains the surface gray-scale figure of each target in N number of target;
Matrix material discriminating unit, for differentiating the matrix material of N number of target according to surface gray-scale figure;
Wherein, coating slope is to the M the earliest being collected in logarithm temperature lowering curve after light pulse excitation Group data are fitted obtaining, and M is the positive integer less than 15, and N is the integer more than 1.
What the present invention provided carries out, based on light pulse excitation infrared thermal imaging, the side that coating lower substrate material differentiates Method and device, by analyzing the separation degree of different matrix and coating logarithm temperature lowering curve, exploitation is corresponding Data processing algorithm, it is achieved the detection of coating lower substrate material and identification.
Accompanying drawing explanation
Fig. 1 is the discrimination method schematic diagram of the coating lower substrate material of the present invention;
Fig. 2 is the identification device schematic diagram of the coating lower substrate material of the present invention;
Fig. 3 is different matrix logarithm temperature lowering curve separation schematic diagram.
Detailed description of the invention
For making the purpose of the present invention, technical scheme and advantage clearer, develop simultaneously referring to the drawings Going out preferred embodiment, the present invention is described in more detail.However, it is necessary to explanation, in description The many details listed be only used to make reader one or more aspects of the present invention are had one thorough Understand, the aspects of the invention can also be realized even without these specific details.
Light pulse excitation is a kind of effective means detecting coating coating quality and thickness, but in prior art Do not utilize the research that the ermal physics attribute of coating material surface lower substrate is differentiated by this technology.This Bright it is considered that utilize light pulse controlled, effective excitation to break coating material thermal balance, by analyzing Different matrix and the separation degree of coating logarithm temperature lowering curve, develop corresponding data processing algorithm, it is possible to Realize detection and the identification of coating lower substrate material.
Fig. 1 shows the discrimination method of the coating lower substrate material of the present invention, as shown in Figure 1:
In step S1, light pulse is utilized to encourage, the first object surface being coated with application layer by infrared Thermal imaging system gathers the infrared information on first object surface, obtains infrared thermal imagery graphic sequence.
Infrared thermal imagery graphic sequence is made up of the multiframe Infrared Thermogram arranged according to acquisition time sequencing, The frame number of Infrared Thermogram is the most, and test result is the most accurate.Infrared Thermogram is collected in light pulse to painting After the first object surface of application layer is encouraged.
It follows that in step S2, for any point on first object surface, according to infrared thermal imagery graphic sequence Obtain the Temperature-time data of this point, by the logarithm temperature lowering curve of this point of Temperature-time data acquisition.
Level-time data according to infrared thermal imagery graphic sequence is obtained in that Temperature-time data.
In a preferred embodiment of the invention, had by the logarithm temperature lowering curve of this point of Temperature-time data acquisition Body is: Temperature-time data carry out background subtraction process, normalized, process of taking the logarithm, and it is right to obtain Number temperature lowering curve.
Background subtraction processes and is specially Temperature-time data subtracting background data, it is thus achieved that do not comprise background information Target data.
It is preferred that in a preferred embodiment of the invention, normalized is: obtain Temperature-time data In maximum temperature values, according to maximum temperature values, Temperature-time data are normalized;Take the logarithm It is processed as the temperature in Temperature-time data, time are taken the logarithm respectively.
Then, in step S3, the slope of logarithm temperature lowering curve is calculated, and oblique according to logarithm temperature lowering curve Rate calculates the separation characteristic values of this point.
As a preferred version, the slope calculating logarithm temperature lowering curve can include performing process as follows:
First, in step S31, choose the very first time value meeting the first preset rules and the second time value, The first temperature value corresponding to very first time value is obtained, corresponding to the second time value by logarithm temperature lowering curve The second temperature value;
Then, in step S32, the slope of logarithm temperature lowering curve is calculated according to formula 1;
Wherein, k is the slope of logarithm temperature lowering curve, and a is very first time value, and m is the second time value, b Being the first temperature value, n is the second temperature value;B=f (a), n=f (m), y=f (x) are logarithm temperature lowering curve.
Logarithm temperature lowering curve can reflect the heat conductivility of target substrate material.
In a preferred embodiment of the invention, the first preset rules particularly as follows: the very first time value with the second time The difference of value is not less than predetermined interval.If very first time value is the least with the difference of the second time value, thus calculate Slope just cannot reflect the complete information of logarithm temperature lowering curve, therefore the two must keep certain intervals.
It is preferred that in a preferred embodiment of the invention, calculate this point according to the slope of logarithm temperature lowering curve Separation characteristic values execution specific as follows:
First, in step S33, to the M the earliest being collected in logarithm temperature lowering curve after light pulse excitation Group data are fitted obtaining coating slope;
Then, in step S34, using the difference of the slope of logarithm temperature lowering curve and coating slope as this point Separation characteristic values;
Wherein, M is the positive integer less than 15
Data in logarithm temperature lowering curve i.e. Temperature-time data carry out background subtraction process, normalized, Take the logarithm and process the data generated;Coating slope is the slope of coating logarithm temperature lowering curve.
M group data the earliest after being collected in light pulse excitation may be considered light pulse without coating and Basal body interface, the data produced when propagating the most in the coating, it is possible to the heat conductivility of sign coating, therefore with Its matching coating slope.
Above-mentioned separation characteristic values can reflect the separation degree of matrix and coating heat conductivility, different separation Eigenvalue can represent the matrix of different materials, therefore using it as the Main Means of matrix material discriminating.Point If representing that the matrix material capacity of heat transmission is more than coating from eigenvalue negative value, if on the occasion of representing that matrix is relative Coating is thermal resistance medium.
It follows that in step S4, repeat step S1-S3, obtain the separation of first object surface every bit Eigenvalue;According to the separation characteristic values of first object surface every bit, obtain first object surface gray-scale figure.
As a preferred version, at the separation characteristic values according to first object surface every bit, obtain Before one target surface gray-scale figure, step S4 can also include performing process as follows: pre-sets separation spy Value indicative and the corresponding relation of grey decision-making.
The separation characteristic values of target surface is converted to gray-scale figure, it is possible to show different matrix material intuitively Difference, and then realize the discriminating of matrix material.
Then, in step S5, for the second target, the 3rd target ... each target in N target, Repeat step S1-S4, it is thus achieved that the surface gray-scale figure of each target;N number of mesh is differentiated according to surface gray-scale figure Target matrix material;
Wherein, N is the integer more than 1.
In a preferred embodiment of the invention, differentiate that the matrix material of N number of target is concrete according to surface gray-scale figure For: the matrix material of each target is directly distinguished according to N number of target surface gray-scale figure;Or by N number of target Each separation characteristic values of target surface each point compares with the separation characteristic values of standard specimen, determines each target Matrix material.
As a preferred version, standard specimen for pre-setting, the separation characteristic values of standard specimen according to Step S1-S4 obtains.
The present invention is achieved in detection and the identification of coating lower substrate material.
Fig. 2 shows the identification device of the coating lower substrate material of the present invention, as in figure 2 it is shown, described dress Put and include: information acquisition unit 11, logarithm temperature lowering curve acquiring unit 12, separation characteristic values computing unit 13, gray-scale figure acquiring unit 14, matrix material discriminating unit 15.
Information acquisition unit 11, each target in utilizing light pulse to the N number of target being coated with application layer Surface is encouraged, and is gathered the infrared information of each target surface by thermal infrared imager, obtains each mesh Target infrared thermal imagery graphic sequence;
Logarithm temperature lowering curve acquiring unit 12, for according to each target surface of Infrared Thermogram retrieval Temperature-time data are carried out at background subtraction process, maximum normalization by the Temperature-time data of every bit The logarithm temperature lowering curve of every bit is obtained after reason, process of taking the logarithm;
Separation characteristic values computing unit 13, for utilizing the logarithm temperature lowering curve of two-point method calculating every bit Slope, and using the difference of the slope of logarithm temperature lowering curve and coating slope as the separation characteristic values of every bit;
Gray-scale figure acquiring unit 14, is used for the separation characteristic values according to every bit and the separation spy pre-set The corresponding relation of value indicative and grey decision-making, obtains the surface gray-scale figure of each target in N number of target;
Matrix material discriminating unit 15, for differentiating the matrix material of N number of target according to surface gray-scale figure;
Wherein, coating slope is to the M group data being collected in logarithm temperature lowering curve after light pulse excitation Being fitted obtaining, M is the positive integer less than 15, and N is the integer more than 1.
Fig. 3 is different matrix logarithm temperature lowering curve separation schematic diagram, and the matrix material 1 in figure is black plastics, 2 is fiberglass, and 3 is carbon fiber, and 4 is aluminum, and 5 is steel.It can be seen that different matrix material is right Number temperature lowering curve creates significantly separation, is conducive to thus carrying out the discriminating of different matrix material.Curve 3, The theoretical log temperature lowering curve that empty oblique line is coating between 4, slope is-0.5.
The discrimination method of the coating lower substrate material that the present invention provides and device can be by analyzing different matrix Separation degree with coating logarithm temperature lowering curve, it is achieved the detection of coating lower substrate material and identification.Simultaneously It is easy to design, is suitable in engineer applied promoting.
One of ordinary skill in the art will appreciate that all or part of step realizing in above-described embodiment method The program that can be by completes to instruct relevant hardware, and this program can be stored in a computer-readable Take in storage medium, such as: ROM/RAM, magnetic disc, CD etc..
The above is only the preferred embodiment of the present invention, it is noted that general for the art For logical technical staff, under the premise without departing from the principles of the invention, it is also possible to make some improvement and profit Decorations, these improvements and modifications also should be regarded as protection scope of the present invention.

Claims (10)

1. the discrimination method of a coating lower substrate material, it is characterised in that include step:
S1. utilize light pulse that the first object surface being coated with application layer is encouraged, adopted by thermal infrared imager The infrared information on collection first object surface, obtains infrared thermal imagery graphic sequence;
S2. for any point on first object surface, according to the temperature of described this point of Infrared Thermogram retrieval Degree-time data, by the logarithm temperature lowering curve of this point of Temperature-time data acquisition;
S3. calculate the slope of described logarithm temperature lowering curve, and calculate according to the slope of described logarithm temperature lowering curve The separation characteristic values of this point;
S4. repeat step S1-S3, obtain the separation characteristic values of first object surface every bit;According to first The separation characteristic values of target surface every bit, obtains first object surface gray-scale figure;
S5. for the second target, the 3rd target ... each target in N target, step S1-S4 is repeated, Obtain the surface gray-scale figure of described each target;The matrix material of N number of target is differentiated according to surface gray-scale figure;
Wherein, N is the integer more than 1.
2. the method for claim 1, it is characterised in that by this point of Temperature-time data acquisition Logarithm temperature lowering curve particularly as follows: Temperature-time data are carried out background subtraction process, normalized, take Logarithm process, obtains logarithm temperature lowering curve.
3. method as claimed in claim 2, it is characterised in that described normalized is: obtain temperature Temperature-time data are normalized place according to maximum temperature values by the maximum temperature values in degree-time data Reason;Described taking the logarithm is processed as taking the logarithm the temperature in Temperature-time data, time respectively.
4. method as claimed in claim 3, it is characterised in that calculate the oblique of described logarithm temperature lowering curve Rate includes:
S31. the very first time value meeting the first preset rules and the second time value are chosen, by logarithm cooling song The line acquisition the first temperature value corresponding to very first time value, the second temperature value corresponding to the second time value;
S32. the slope of logarithm temperature lowering curve is calculated according to formula 1;
Wherein, k is the slope of logarithm temperature lowering curve, and a is very first time value, and m is the second time value, b Being the first temperature value, n is the second temperature value;B=f (a), n=f (m), y=f (x) are logarithm temperature lowering curve.
5. method as claimed in claim 4, it is characterised in that the first preset rules is particularly as follows: first Time value is not less than predetermined interval with the difference of the second time value.
6. method as claimed in claim 5, it is characterised in that oblique according to described logarithm temperature lowering curve Rate calculates the separation characteristic values of this point and includes:
S33. the M group data the earliest after being collected in light pulse excitation in logarithm temperature lowering curve are intended Conjunction obtains coating slope;
S34. using the difference of the slope of logarithm temperature lowering curve and coating slope as the separation characteristic values of this point;
Wherein, M is the positive integer less than 15.
7. method as claimed in claim 6, it is characterised in that described every according to first object surface The separation characteristic values of a bit, before obtaining first object surface gray-scale figure, step S4 also includes:
Pre-set the corresponding relation of separation characteristic values and grey decision-making.
8. method as claimed in claim 7, it is characterised in that differentiate N number of mesh according to surface gray-scale figure Target matrix material particularly as follows:
The matrix material of each target is directly distinguished according to N number of target surface gray-scale figure;Or
Separation characteristic values by the separation characteristic values of target surface each point each in N number of target Yu standard specimen Relatively, the matrix material of each target is determined.
9. method as claimed in claim 8, it is characterised in that described standard specimen for pre-setting, The separation characteristic values of described standard specimen obtains according to step S1-S4.
10. the identification device of a coating lower substrate material, it is characterised in that including:
Information acquisition unit, each object table in utilizing light pulse to the N number of target being coated with application layer Face is encouraged, and is gathered the infrared information of each target surface by thermal infrared imager, obtains each target Infrared thermal imagery graphic sequence;
Logarithm temperature lowering curve acquiring unit, for every according to each target surface of Infrared Thermogram retrieval The Temperature-time data of a bit, Temperature-time data are carried out background subtraction process, maximum normalized, Take the logarithm and after processing, obtain the logarithm temperature lowering curve of described every bit;
Separation characteristic values computing unit, for utilizing two-point method to calculate the logarithm temperature lowering curve of described every bit Slope, and the slope of logarithm temperature lowering curve is separated as described every bit with the difference of coating slope Eigenvalue;
Gray-scale figure acquiring unit, is used for the separation characteristic values according to described every bit and the separation pre-set The corresponding relation of eigenvalue and grey decision-making, obtains the surface gray-scale figure of each target in N number of target;
Matrix material discriminating unit, for differentiating the matrix material of N number of target according to surface gray-scale figure;
Wherein, coating slope is to the M the earliest being collected in logarithm temperature lowering curve after light pulse excitation Group data are fitted obtaining, and M is the positive integer less than 15, and N is the integer more than 1.
CN201610176997.5A 2016-03-25 2016-03-25 A kind of discrimination method and device of coating lower substrate material Active CN105866168B (en)

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