CN105860205A - Tube for sputtering unit cooling and preparation method for tube - Google Patents
Tube for sputtering unit cooling and preparation method for tube Download PDFInfo
- Publication number
- CN105860205A CN105860205A CN201610266360.5A CN201610266360A CN105860205A CN 105860205 A CN105860205 A CN 105860205A CN 201610266360 A CN201610266360 A CN 201610266360A CN 105860205 A CN105860205 A CN 105860205A
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- Prior art keywords
- preparation
- consumption
- cooling
- weight portion
- tube
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L23/00—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
- C08L23/02—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers not modified by chemical after-treatment
- C08L23/04—Homopolymers or copolymers of ethene
- C08L23/06—Polyethene
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2203/00—Applications
- C08L2203/18—Applications used for pipes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Materials For Medical Uses (AREA)
Abstract
The invention discloses a tube for sputtering unit cooling and a preparation method for the tube. The preparation method comprises the following steps: mixing polyethylene, polyvinyl chloride, phenolic resin, titanium dioxide, calcium carbonate, a toughening agent and a defoaming agent to form a mixture M; and fusing the mixture M and adding the fused mixture M into a mould for cooling and forming, thereby obtaining the tube for sputtering unit cooling. The raw materials cooperate with one another, so that the prepared cooling tube has excellent high temperature resistance and toughness; and meanwhile, the method for preparing the cooling tube is simple, and the raw materials are easily available.
Description
Technical field
The present invention relates to the preparation of cooling tube, in particular it relates to the preparation method of sputtering unit cooling pipe.
Background technology
In coating film on glass technique, vacuum coating is a kind of common method, and it is mainly in vacuum chamber
The atom of material is isolated the surface getting to glass from heating source.The vacuum coating of glass is to spatter
Carry out in penetrating unit, according to the technology needs of plated film, operationally, the side plate of sputtering unit and base plate
Being required for carrying out cooling process, due to sputtering unit operationally, its internal temperature is higher, transports cold
But the cooling tube of liquid needs higher tolerable temperature and toughness guarantee it will not be subject in sputtering unit
To high temperature deformation.
Summary of the invention
It is an object of the invention to provide a kind of sputtering unit cooling pipe and preparation method thereof, the cooling prepared
Higher tolerable temperature and toughness is possessed with pipe.
To achieve these goals, the invention provides the preparation method of a kind of sputtering unit cooling pipe,
Wherein, described preparation method includes:
(1) by polyethylene, polrvinyl chloride, phenolic resin, titanium dioxide, calcium carbonate, toughener with disappear
Infusion is mixed to form mixture M；
(2) described mixture M is melted, and add cooling molding in mould, obtain described sputtering single
Unit's cooling pipe, wherein,
Relative to the polyethylene of 100 weight portions, the consumption of described polrvinyl chloride is 20-30 weight portion, institute
The consumption stating phenolic resin is 10-18 weight portion, and the consumption of described titanium dioxide is 1-10 weight portion, described
The consumption of calcium carbonate is 2-15 weight portion, and the consumption of described toughener is 2-6 weight portion, described defoamer
Consumption be 0.1-1 weight portion.
Present invention also offers a kind of sputtering unit cooling pipe, wherein, described sputtering unit cooling is managed
Prepared by above-mentioned preparation method.
By technique scheme, the invention provides the preparation method of a kind of sputtering unit cooling pipe,
Wherein, described preparation method includes: by polyethylene, polrvinyl chloride, phenolic resin, titanium dioxide, carbonic acid
Calcium, toughener and defoamer are mixed to form mixture M；Described mixture M is melted, and adds mould
Tool cools down molding, obtains described sputtering unit cooling pipe, by the synergism between each raw material,
Make the cooling tube prepared possess excellent heat-resisting ability and toughness, meanwhile, be used for preparing this cooling
The method of pipe is simple, and raw material is easy to get.
Other features and advantages of the present invention will be described in detail in detailed description of the invention part subsequently.
Detailed description of the invention
Hereinafter the detailed description of the invention of the present invention is described in detail.It should be appreciated that this place is retouched
The detailed description of the invention stated is merely to illustrate and explains the present invention, is not limited to the present invention.
The invention provides the preparation method of a kind of sputtering unit cooling pipe, wherein, described preparation method
Including: by polyethylene, polrvinyl chloride, phenolic resin, titanium dioxide, calcium carbonate, toughener and defoamer
It is mixed to form mixture M；Described mixture M is melted, and adds cooling molding in mould, obtain
Described sputtering unit cooling is managed, wherein, relative to the polyethylene of 100 weight portions, described polrvinyl chloride
Consumption be 20-30 weight portion, the consumption of described phenolic resin is 10-18 weight portion, described titanium dioxide
Consumption be 1-10 weight portion, the consumption of described calcium carbonate is 2-15 weight portion, the use of described toughener
Amount is 2-6 weight portion, and the consumption of described defoamer is 0.1-1 weight portion.By the association between each raw material
Same-action so that the cooling tube prepared possesses excellent heat-resisting ability and toughness, meanwhile, is used for making
The method of this cooling tube standby is simple, and raw material is easy to get.
So that the cooling tube prepared possesses higher toughness, described toughener is polybutadiene rubber
One or more in glue, butyl rubber and nitrile rubber.
So that mixing will not produce more foam between raw material, affect the internal structure of cooling tube,
Described defoamer is polypropylene glycerol aether, polyoxyethylene polyoxypropylene glycerin ether and polydimethylsiloxane
In one or more.
So that the cooling tube prepared possesses more excellent heat-resisting ability and toughness, described polyethylene
Weight average molecular weight be 8000-12000, the weight average molecular weight of described polrvinyl chloride is 7000-9000.
So that raw material can be the most melted, described melted temperature is 270-290 DEG C, the melting time
For 10-20min.
In order to the most quickly cool down, and saving cooling power consumption, described cooling uses the mode of water-cooled, and
The temperature of cooling water is 10-15 DEG C.
Present invention also offers a kind of sputtering unit cooling pipe, wherein, described sputtering unit cooling is managed
Prepared by above-mentioned preparation method.
Hereinafter will be described the present invention by embodiment.
Embodiment 1
By 100g polyethylene (weight average molecular weight is 8000), (weight average molecular weight is 20g polrvinyl chloride
7000), 10g phenolic resin, 1g titanium dioxide, 2g calcium carbonate, 2g toughener and the mixing of 0.1g defoamer
Form mixture M；By melted for described mixture M (melted temperature is 270 DEG C, and the time is 10min),
And add cooling molding in mould, obtain described sputtering unit cooling pipe A1.
Embodiment 2
By 100g polyethylene (weight average molecular weight is 12000), (weight average molecular weight is 30g polrvinyl chloride
9000), 18g phenolic resin, 10g titanium dioxide, 15g calcium carbonate, 6g toughener and 1g defoamer are mixed
Close and form mixture M；(melted temperature is 290 DEG C, and the time is by melted for described mixture M
20min), and add cooling molding in mould, obtain described sputtering unit cooling pipe A2.
Embodiment 3
By 100g polyethylene (weight average molecular weight is 10000), (weight average molecular weight is 25g polrvinyl chloride
8000), 15g phenolic resin, 5g titanium dioxide, 10g calcium carbonate, 4g toughener and 0.5g defoamer are mixed
Close and form mixture M；(melted temperature is 280 DEG C, and the time is by melted for described mixture M
15min), and add cooling molding in mould, obtain described sputtering unit cooling pipe A3.
Comparative example 1
Being prepared according to the mode of embodiment 1, except for the difference that, the consumption of polyethylene is 100g, described
The consumption of polrvinyl chloride is 10g, and the consumption of described phenolic resin is 5g, and the consumption of described titanium dioxide is
0.4g, the consumption of described calcium carbonate is 1g, and the consumption of described toughener is 1g, the consumption of described defoamer
For 0.05g, obtain described sputtering unit cooling pipe D1.
Comparative example 2
Being prepared according to the mode of embodiment 1, except for the difference that, the consumption of polyethylene is 100g, described
The consumption of polrvinyl chloride is 40g, and the consumption of described phenolic resin is 25g, and the consumption of described titanium dioxide is
15g, the consumption of described calcium carbonate is 20g, and the consumption of described toughener is 8g, the use of described defoamer
Amount is 2g, obtains described sputtering unit cooling pipe D2.
Table 1
| Embodiment is numbered | The highest tolerable temperature (DEG C) | Toughness (J/m^3) |
| A1 | 120 | 12 |
| A2 | 125 | 15 |
| A3 | 124 | 16 |
| D1 | 90 | 6 |
| D2 | 98 | 7 |
By upper table it can be seen that the cooling pipe A1-A3's prepared within the scope of the invention is the highest
Tolerable temperature and toughness are higher than outside the scope of the invention cooling pipe D1 and D2 prepared, the most permissible
Realize cooling and manage excellent resistance to elevated temperatures and toughness.
The preferred embodiment of the present invention described in detail above, but, the present invention is not limited to above-mentioned reality
Execute the detail in mode, in the technology concept of the present invention, can be to the technical side of the present invention
Case carries out multiple simple variant, and these simple variant belong to protection scope of the present invention.
It is further to note that each the concrete technology described in above-mentioned detailed description of the invention is special
Levy, in the case of reconcilable, can be combined by any suitable means, in order to avoid need not
The repetition wanted, various possible compound modes are illustrated by the present invention the most separately.
Additionally, combination in any can also be carried out between the various different embodiment of the present invention, as long as its
Without prejudice to the thought of the present invention, it should be considered as content disclosed in this invention equally.
Claims (8)
1. the preparation method of a sputtering unit cooling pipe, it is characterised in that described preparation method bag
Include:
(1) by polyethylene, polrvinyl chloride, phenolic resin, titanium dioxide, calcium carbonate, toughener with disappear
Infusion is mixed to form mixture M；
(2) described mixture M is melted, and add cooling molding in mould, obtain described sputtering single
Unit's cooling pipe, wherein,
Relative to the polyethylene of 100 weight portions, the consumption of described polrvinyl chloride is 20-30 weight portion, institute
The consumption stating phenolic resin is 10-18 weight portion, and the consumption of described titanium dioxide is 1-10 weight portion, described
The consumption of calcium carbonate is 2-15 weight portion, and the consumption of described toughener is 2-6 weight portion, described defoamer
Consumption be 0.1-1 weight portion.
Preparation method the most according to claim 1, wherein, described toughener is polybutadiene rubber
One or more in glue, butyl rubber and nitrile rubber.
Preparation method the most according to claim 1, wherein, described defoamer is that polyoxypropylene is sweet
One or more in oil ether, polyoxyethylene polyoxypropylene glycerin ether and polydimethylsiloxane.
Preparation method the most according to claim 1, wherein, the weight average molecular weight of described polyethylene
For 8000-12000.
Preparation method the most according to claim 1, wherein, the Weight-average molecular of described polrvinyl chloride
Amount is 7000-9000.
Preparation method the most according to claim 1, wherein, described melted temperature is 270-290
DEG C, the melting time is 10-20min.
Preparation method the most according to claim 1, wherein, described cooling uses the mode of water-cooled,
And the temperature of cooling water is 10-15 DEG C.
8. a sputtering unit cooling pipe, it is characterised in that described sputtering unit cooling Guan Youquan
Profit requires in 1-7 that the preparation method described in any one prepares.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610266360.5A CN105860205A (en) | 2016-04-27 | 2016-04-27 | Tube for sputtering unit cooling and preparation method for tube |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610266360.5A CN105860205A (en) | 2016-04-27 | 2016-04-27 | Tube for sputtering unit cooling and preparation method for tube |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105860205A true CN105860205A (en) | 2016-08-17 |
Family
ID=56628343
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610266360.5A Pending CN105860205A (en) | 2016-04-27 | 2016-04-27 | Tube for sputtering unit cooling and preparation method for tube |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108384091A (en) * | 2018-02-26 | 2018-08-10 | 佛山杰致信息科技有限公司 | A kind of Environmentally-frieantibacterial antibacterial PE plastics and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102002181A (en) * | 2010-12-23 | 2011-04-06 | 南京聚隆科技股份有限公司 | High-toughness and high-strength polyethylene composite material and preparation method thereof |
| CN104194218A (en) * | 2014-09-01 | 2014-12-10 | 康泰塑胶科技集团有限公司 | Polyethylene-polyvinyl chloride blend-modified tube and preparation method thereof |
-
2016
- 2016-04-27 CN CN201610266360.5A patent/CN105860205A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102002181A (en) * | 2010-12-23 | 2011-04-06 | 南京聚隆科技股份有限公司 | High-toughness and high-strength polyethylene composite material and preparation method thereof |
| CN104194218A (en) * | 2014-09-01 | 2014-12-10 | 康泰塑胶科技集团有限公司 | Polyethylene-polyvinyl chloride blend-modified tube and preparation method thereof |
Non-Patent Citations (3)
| Title |
|---|
| 张巧玲等主编: "《化工工艺学》", 31 July 2015, ，国防工业出版社 * |
| 本书编写组编: "《石油和石化工业概述》", 31 July 2010, 中国石化出版社 * |
| 李玉瑛主编: "《高分子物理及化学》", 31 May 1995, 化学工业出版社， * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108384091A (en) * | 2018-02-26 | 2018-08-10 | 佛山杰致信息科技有限公司 | A kind of Environmentally-frieantibacterial antibacterial PE plastics and preparation method thereof |
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Application publication date: 20160817 |