CN105858749B - A kind of dedicated sewage-treating agent of livestock and poultry cultivation and preparation method thereof - Google Patents
A kind of dedicated sewage-treating agent of livestock and poultry cultivation and preparation method thereof Download PDFInfo
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- CN105858749B CN105858749B CN201610394701.7A CN201610394701A CN105858749B CN 105858749 B CN105858749 B CN 105858749B CN 201610394701 A CN201610394701 A CN 201610394701A CN 105858749 B CN105858749 B CN 105858749B
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- 244000144972 livestock Species 0.000 title claims abstract description 46
- 244000144977 poultry Species 0.000 title claims abstract description 45
- 238000002360 preparation method Methods 0.000 title claims abstract description 18
- 238000012364 cultivation method Methods 0.000 title abstract description 5
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 41
- 235000017166 Bambusa arundinacea Nutrition 0.000 claims abstract description 17
- 235000017491 Bambusa tulda Nutrition 0.000 claims abstract description 17
- 241001330002 Bambuseae Species 0.000 claims abstract description 17
- 235000015334 Phyllostachys viridis Nutrition 0.000 claims abstract description 17
- 239000011425 bamboo Substances 0.000 claims abstract description 17
- 239000003610 charcoal Substances 0.000 claims abstract description 17
- 238000000034 method Methods 0.000 claims abstract description 16
- VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 claims abstract description 13
- 229940075529 glyceryl stearate Drugs 0.000 claims abstract description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 13
- 229920001353 Dextrin Polymers 0.000 claims abstract description 12
- 239000004375 Dextrin Substances 0.000 claims abstract description 12
- 235000019425 dextrin Nutrition 0.000 claims abstract description 12
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical class O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 claims description 43
- 239000000440 bentonite Substances 0.000 claims description 34
- 229910000278 bentonite Inorganic materials 0.000 claims description 34
- 239000000203 mixture Substances 0.000 claims description 28
- 239000000843 powder Substances 0.000 claims description 24
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 18
- 238000001035 drying Methods 0.000 claims description 18
- 238000002525 ultrasonication Methods 0.000 claims description 14
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 12
- 239000002002 slurry Substances 0.000 claims description 9
- 230000035484 reaction time Effects 0.000 claims description 8
- 238000012545 processing Methods 0.000 claims description 7
- 238000003756 stirring Methods 0.000 claims description 7
- CPELXLSAUQHCOX-UHFFFAOYSA-M Bromide Chemical compound [Br-] CPELXLSAUQHCOX-UHFFFAOYSA-M 0.000 claims description 6
- VVQNEPGJFQJSBK-UHFFFAOYSA-N Methyl methacrylate Chemical compound COC(=O)C(C)=C VVQNEPGJFQJSBK-UHFFFAOYSA-N 0.000 claims description 6
- YDEXUEFDPVHGHE-GGMCWBHBSA-L disodium;(2r)-3-(2-hydroxy-3-methoxyphenyl)-2-[2-methoxy-4-(3-sulfonatopropyl)phenoxy]propane-1-sulfonate Chemical compound [Na+].[Na+].COC1=CC=CC(C[C@H](CS([O-])(=O)=O)OC=2C(=CC(CCCS([O-])(=O)=O)=CC=2)OC)=C1O YDEXUEFDPVHGHE-GGMCWBHBSA-L 0.000 claims description 6
- 239000000377 silicon dioxide Substances 0.000 claims description 6
- GCLGEJMYGQKIIW-UHFFFAOYSA-H sodium hexametaphosphate Chemical compound [Na]OP1(=O)OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])O1 GCLGEJMYGQKIIW-UHFFFAOYSA-H 0.000 claims description 6
- 239000002689 soil Substances 0.000 claims description 6
- 239000002202 Polyethylene glycol Substances 0.000 claims description 5
- 238000001914 filtration Methods 0.000 claims description 5
- 229920001223 polyethylene glycol Polymers 0.000 claims description 5
- 238000001291 vacuum drying Methods 0.000 claims description 5
- 229920002873 Polyethylenimine Polymers 0.000 claims description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims 1
- 150000001412 amines Chemical class 0.000 claims 1
- 229910052708 sodium Inorganic materials 0.000 claims 1
- 239000011734 sodium Substances 0.000 claims 1
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 6
- XKMRRTOUMJRJIA-UHFFFAOYSA-N ammonia nh3 Chemical compound N.N XKMRRTOUMJRJIA-UHFFFAOYSA-N 0.000 abstract description 4
- 229910021645 metal ion Inorganic materials 0.000 abstract description 4
- 239000000126 substance Substances 0.000 abstract description 3
- 239000010865 sewage Substances 0.000 description 7
- -1 Alkene imines Chemical class 0.000 description 4
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- 239000002351 wastewater Substances 0.000 description 3
- 230000000052 comparative effect Effects 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 210000003608 fece Anatomy 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000009395 breeding Methods 0.000 description 1
- 230000001488 breeding effect Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000010304 firing Methods 0.000 description 1
- 239000003673 groundwater Substances 0.000 description 1
- 239000010842 industrial wastewater Substances 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 229910000162 sodium phosphate Inorganic materials 0.000 description 1
- 239000001488 sodium phosphate Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000002352 surface water Substances 0.000 description 1
- RYFMWSXOAZQYPI-UHFFFAOYSA-K trisodium phosphate Chemical compound [Na+].[Na+].[Na+].[O-]P([O-])([O-])=O RYFMWSXOAZQYPI-UHFFFAOYSA-K 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
Abstract
The invention discloses dedicated sewage-treating agents of a kind of livestock and poultry cultivation and preparation method thereof, the dedicated sewage-treating agent of livestock and poultry cultivation, according to the component of parts by weight are as follows: 45-55 parts of modified alta-mud, 20-30 parts of bamboo charcoal, 5-8 parts of glyceryl stearate and 1-2 parts of dextrin.The present invention enables to the physical and chemical index of the dedicated sewage-treating agent of livestock and poultry cultivation to reach GB18918-2002 standard, and effectively reduces COD, BOD, SS, ammonia-nitrogen content and metal ion content；Treatment process is simple, and dosage is few, and treatment effect is good, and performance is stablized, and effluent quality is good, can significantly reduce the cost of water process, has good economic benefit and extensive social benefit.
Description
Technical field
The present invention relates to a kind of sewage-treating agent technical field, the dedicated sewage-treating agent of specifically a kind of livestock and poultry cultivation and
Preparation method.
Background technique
According to pertinent literature, former National Environmental Environmental Protection Administration is to national 23 provinces (area), market scale livestock and poultry cultivations
Industry pollution situation sample investigation shows that national feces of livestock and poultry and sewage yield are more than 20,000,000,000 tons, is industrial solid castoff
2.4 times of yield, feces of livestock and poultry COD (COD) is considerably beyond China's industrial wastewater and sanitary sewage COD discharge amount
The sum of.Pollution from livestock and poultry has become the third-largest pollution sources after industrial pollution, domestic pollution, becomes agricultural side of China
One of the main reason for face is polluted.The sewage of high concentration is discharged into rivers and lakes, causes the continuous of surface water quality and groundwater quality
Deteriorate, directly endangers the health of people, also seriously constrain the development of cultivation industry.Livestock breeding wastewater has typical
" three high " feature, COD are up to 3000-12000mg/L, and ammonia nitrogen is up to 800-2200mg/L, the exceeded decades of times of SS, and waste water composition is answered
Miscellaneous, water quality and quantity fluctuation is greatly.As state sewage emission standard increasingly updates, how high-concentration culture waste water reaches discharge standard
Problem is more prominent.
Summary of the invention
The purpose of the present invention is to provide dedicated sewage-treating agents of a kind of livestock and poultry cultivation and preparation method thereof, on solving
State the problem of proposing in background technique.
To achieve the above object, the invention provides the following technical scheme:
A kind of dedicated sewage-treating agent of livestock and poultry cultivation, according to the component of parts by weight are as follows: 45-55 parts of modified alta-mud, bamboo
20-30 parts of charcoal, 5-8 parts of glyceryl stearate and 1-2 parts of dextrin, the method for preparing modified bentonite are as follows:
(1) bentonite original soil is added in rotary kiln, 38min is fired under the conditions of 970 DEG C of temperature, is ground into after kiln discharge
40-50 mesh bentonite fine powder；
(2) the resulting bentonite fine powder of step (1) is taken to carry out vacuum drying treatment 12h, be subsequently placed at calgon and
2-4h is impregnated in sodium lignin sulfonate, so that bentonite fine powder is sufficiently impregnated, low temperature drying is carried out after filtering；
(3) the bentonite fine powder after taking low temperature drying obtained by step (2) is added in polymeric kettle, then successively adds poly- second
Alkene imines, polyethylene glycol, azobisisoheptonitrile, nano silica, methanol, methyl methacrylate and 4 bromide,
Reaction temperature is 53-62 DEG C, and reaction time 1-2h obtains modified alta-mud.
As a further solution of the present invention: in the method for preparing modified bentonite step (1), in 970 DEG C of conditions
Lower firing 38min is ground into 45 mesh bentonite fine powders after kiln discharge.
As a further solution of the present invention: in the method for preparing modified bentonite step (2), being subsequently placed at six partially
3h is impregnated in sodium phosphate and sodium lignin sulfonate.
As a further solution of the present invention: in the method for preparing modified bentonite step (3), reaction temperature 58
DEG C, reaction time 1.5h.
A kind of preparation method of the dedicated sewage-treating agent of livestock and poultry cultivation, specific steps are as follows:
(1) firstly, adding water to obtain mixture slurry into modified alta-mud, ultrasonication, ultrasonication are then carried out
Temperature be 110-120 DEG C, time 30-60min obtains mixture；
(2) then, mixture and bamboo charcoal, glyceryl stearate and dextrin are subjected to ice bath and mix stirring, speed of agitator is
300-400r/min then carries out low temperature drying at a temperature of microencapsulation processing is placed in 2 DEG C -6 DEG C, it is dedicated to obtain livestock and poultry cultivation
Sewage-treating agent.
As a further solution of the present invention: the temperature of ultrasonication is 115 DEG C in step (1), time 45min.
As a further solution of the present invention: speed of agitator is 350r/min in step (2).
Compared with prior art, the beneficial effects of the present invention are:
The present invention enables to the physical and chemical index of the dedicated sewage-treating agent of livestock and poultry cultivation to reach GB18918-2002 standard,
And effectively reduce COD, BOD, SS and metal ion content；Treatment process is simple, and dosage is few, and treatment effect is good, performance
Stablize, effluent quality is good, can significantly reduce the cost of water process, has good economic benefit and extensive society's effect
Benefit.
Specific embodiment
Below in conjunction with the embodiment of the present invention, technical scheme in the embodiment of the invention is clearly and completely described,
Obviously, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based in the present invention
Embodiment, every other embodiment obtained by those of ordinary skill in the art without making creative efforts, all
Belong to the scope of protection of the invention.
Embodiment 1
A kind of dedicated sewage-treating agent of livestock and poultry cultivation, according to the component of parts by weight are as follows: 45 parts of modified alta-mud, bamboo charcoal 20
Part, 5 parts of glyceryl stearate and 1 part of dextrin, the method for preparing modified bentonite are as follows:
(1) bentonite original soil is added in rotary kiln, 38min is fired under the conditions of 970 DEG C of temperature, is ground into 40 after kiln discharge
Mesh bentonite fine powder；
(2) the resulting bentonite fine powder of step (1) is taken to carry out vacuum drying treatment 12h, be subsequently placed at calgon and
2h is impregnated in sodium lignin sulfonate, so that bentonite fine powder is sufficiently impregnated, low temperature drying is carried out after filtering；
(3) the bentonite fine powder after taking low temperature drying obtained by step (2) is added in polymeric kettle, then successively adds poly- second
Alkene imines, polyethylene glycol, azobisisoheptonitrile, nano silica, methanol, methyl methacrylate and 4 bromide,
Reaction temperature is 53 DEG C, and reaction time 1h obtains modified alta-mud.
A kind of preparation method of the dedicated sewage-treating agent of livestock and poultry cultivation, specific steps are as follows:
(1) firstly, adding water to obtain mixture slurry into modified alta-mud, ultrasonication, ultrasonication are then carried out
Temperature be 110 DEG C, time 30min obtains mixture；
(2) then, mixture and bamboo charcoal, glyceryl stearate and dextrin are subjected to ice bath and mix stirring, speed of agitator is
300r/min then carries out low temperature drying at a temperature of microencapsulation processing is placed in 2 DEG C, obtains at the dedicated sewage of livestock and poultry cultivation
Manage agent.
Embodiment 2
A kind of dedicated sewage-treating agent of livestock and poultry cultivation, according to the component of parts by weight are as follows: 50 parts of modified alta-mud, bamboo charcoal 25
Part, 8 parts of glyceryl stearate and 2 parts of dextrin, the method for preparing modified bentonite are as follows:
(1) bentonite original soil is added in rotary kiln, 38min is fired under the conditions of 970 DEG C of temperature, is ground into 45 after kiln discharge
Mesh bentonite fine powder；
(2) the resulting bentonite fine powder of step (1) is taken to carry out vacuum drying treatment 12h, be subsequently placed at calgon and
3h is impregnated in sodium lignin sulfonate, so that bentonite fine powder is sufficiently impregnated, low temperature drying is carried out after filtering；
(3) the bentonite fine powder after taking low temperature drying obtained by step (2) is added in polymeric kettle, then successively adds poly- second
Alkene imines, polyethylene glycol, azobisisoheptonitrile, nano silica, methanol, methyl methacrylate and 4 bromide,
Reaction temperature is 58 DEG C, and reaction time 1.5h obtains modified alta-mud.
A kind of preparation method of the dedicated sewage-treating agent of livestock and poultry cultivation, specific steps are as follows:
(1) firstly, adding water to obtain mixture slurry into modified alta-mud, ultrasonication, ultrasonication are then carried out
Temperature be 115 DEG C, time 45min obtains mixture；
(2) then, mixture and bamboo charcoal, glyceryl stearate and dextrin are subjected to ice bath and mix stirring, speed of agitator is
350r/min then carries out low temperature drying at a temperature of microencapsulation processing is placed in 4 DEG C, obtains at the dedicated sewage of livestock and poultry cultivation
Manage agent.
Embodiment 3
A kind of dedicated sewage-treating agent of livestock and poultry cultivation, according to the component of parts by weight are as follows: 55 parts of modified alta-mud, bamboo charcoal 30
Part, 8 parts of glyceryl stearate and 2 parts of dextrin, the method for preparing modified bentonite are as follows:
(1) bentonite original soil is added in rotary kiln, 38min is fired under the conditions of 970 DEG C of temperature, is ground into 50 after kiln discharge
Mesh bentonite fine powder；
(2) the resulting bentonite fine powder of step (1) is taken to carry out vacuum drying treatment 12h, be subsequently placed at calgon and
4h is impregnated in sodium lignin sulfonate, so that bentonite fine powder is sufficiently impregnated, low temperature drying is carried out after filtering；
(3) the bentonite fine powder after taking low temperature drying obtained by step (2) is added in polymeric kettle, then successively adds poly- second
Alkene imines, polyethylene glycol, azobisisoheptonitrile, nano silica, methanol, methyl methacrylate and 4 bromide,
Reaction temperature is 62 DEG C, and reaction time 2h obtains modified alta-mud.
A kind of preparation method of the dedicated sewage-treating agent of livestock and poultry cultivation, specific steps are as follows:
(1) firstly, adding water to obtain mixture slurry into modified alta-mud, ultrasonication, ultrasonication are then carried out
Temperature be 120 DEG C, time 60min obtains mixture；
(2) then, mixture and bamboo charcoal, glyceryl stearate and dextrin are subjected to ice bath and mix stirring, speed of agitator is
400r/min then carries out low temperature drying at a temperature of microencapsulation processing is placed in 6 DEG C, obtains at the dedicated sewage of livestock and poultry cultivation
Manage agent.
Comparative example 1
A kind of dedicated sewage-treating agent of livestock and poultry cultivation, according to the component of parts by weight are as follows: 50 parts of bentonite, 25 parts of bamboo charcoal.
A kind of preparation method of the dedicated sewage-treating agent of livestock and poultry cultivation, specific steps are as follows:
(1) firstly, adding water to obtain mixture slurry into bentonite, ultrasonication, the temperature of ultrasonication are then carried out
Degree is 115 DEG C, and time 45min obtains mixture；
(2) then, mixture and bamboo charcoal are subjected to ice bath and mix stirring, speed of agitator 350r/min is then carried out micro-
Low temperature drying at a temperature of encapsulated processing is placed in 4 DEG C, obtains the dedicated sewage-treating agent of livestock and poultry cultivation.
Comparative example 2
A kind of dedicated sewage-treating agent of livestock and poultry cultivation, according to the component of parts by weight are as follows: 50 parts of bentonite, 25 parts of bamboo charcoal.
A kind of preparation method of the dedicated sewage-treating agent of livestock and poultry cultivation, specific steps are as follows:
Into bentonite and bamboo charcoal plus water obtains mixture slurry, low temperature drying at a temperature of being subsequently placed at 4 DEG C, obtains livestock and poultry and supports
Grow dedicated sewage-treating agent.
A kind of dedicated sewage-treating agent of livestock and poultry cultivation, according to the component of parts by weight are as follows: 50 parts of modified alta-mud, bamboo charcoal 25
Part, 8 parts of glyceryl stearate and 2 parts of dextrin, the method for preparing modified bentonite are as follows:
(1) bentonite original soil is added in rotary kiln, 38min is fired under the conditions of 970 DEG C of temperature, is ground into 45 after kiln discharge
Mesh bentonite fine powder；
(2) it takes the resulting bentonite fine powder of step (1) to be added in polymeric kettle, then successively adds polyethyleneimine, gathers
Ethylene glycol, azobisisoheptonitrile, nano silica, methanol, methyl methacrylate and 4 bromide, reaction temperature are
58 DEG C, reaction time 1.5h obtains modified alta-mud.
A kind of preparation method of the dedicated sewage-treating agent of livestock and poultry cultivation, specific steps are as follows:
Into modified alta-mud plus water obtains mixture slurry, then by mixture slurry and bamboo charcoal, glyceryl stearate and paste
The row ice bath that progresses greatly mixes stirring, and speed of agitator 400r/min then carries out low temperature at a temperature of microencapsulation processing is placed in 4 DEG C
Drying, obtains the dedicated sewage-treating agent of livestock and poultry cultivation.
Test experience
Embodiment 1, embodiment 2, embodiment 3 and contrast sample 1 are weighed respectively, contrast sample 2, each 1kg of contrast sample 3 add
Enter into the dedicated sewage-treating agent of livestock and poultry cultivation of 20kg, temperature control is stirred continuously 1h at 25 DEG C, respectively with COD, BOD, SS,
Ammonia-nitrogen content, metal ion content test the effect of the dedicated sewage-treating agent of livestock and poultry cultivation of the invention as evaluation criterion
Fruit, test result chart 1.
Table 1
It can be seen that the dedicated sewage-treating agent of livestock and poultry cultivation of the invention, there is preferably significant place compared with the control group
Effect is managed, the present invention enables to the physical and chemical index of the dedicated sewage-treating agent of livestock and poultry cultivation to reach GB18918-2002 standard
(can achieve level-one B standard or more), and effectively reduce COD, BOD, SS, ammonia-nitrogen content and metal ion content；Handle work
Skill is simple, and dosage is few, and treatment effect is good, and performance is stablized, and effluent quality is good, can significantly reduce the cost of water process,
With good economic benefit and extensive social benefit.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie
In the case where without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
Which point say from the point of view of, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended
Claim rather than above description limit, it is intended that the institute that will be fallen within the meaning and scope of the equivalent elements of the claims
It changes and is included within the present invention.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
The other embodiments being understood that.
Claims (7)
1. a kind of dedicated sewage-treating agent of livestock and poultry cultivation, according to the component of parts by weight are as follows: 45-55 parts of modified alta-mud, bamboo charcoal
20-30 parts, 5-8 parts of glyceryl stearate and 1-2 parts of dextrin, which is characterized in that the method for preparing modified bentonite are as follows:
(1) bentonite original soil is added in rotary kiln, 38min is fired under the conditions of 970 DEG C of temperature, is ground into 40-50 after kiln discharge
Mesh bentonite fine powder；
(2) it takes the resulting bentonite fine powder of step (1) to carry out vacuum drying treatment 12h, is subsequently placed at calgon and wooden
2-4h is impregnated in plain sodium sulfonate, so that bentonite fine powder is sufficiently impregnated, low temperature drying is carried out after filtering；
(3) the bentonite fine powder after taking low temperature drying obtained by step (2) is added in polymeric kettle, then successively adds polyethyleneimine
Amine, polyethylene glycol, azobisisoheptonitrile, nano silica, methanol, methyl methacrylate and 4 bromide, reaction
Temperature is 53-62 DEG C, and reaction time 1-2h obtains modified alta-mud.
2. the dedicated sewage-treating agent of livestock and poultry cultivation according to claim 1, which is characterized in that the modified alta-mud
In preparation method step (1), 38min is fired under the conditions of 970 DEG C, and 45 mesh bentonite fine powders are ground into after kiln discharge.
3. the dedicated sewage-treating agent of livestock and poultry cultivation according to claim 1, which is characterized in that the modified alta-mud
In preparation method step (2), it is subsequently placed in calgon and sodium lignin sulfonate and impregnates 3h.
4. the dedicated sewage-treating agent of livestock and poultry cultivation according to claim 1, which is characterized in that the modified alta-mud
In preparation method step (3), reaction temperature is 58 DEG C, reaction time 1.5h.
5. a kind of preparation method of the dedicated sewage-treating agent of livestock and poultry cultivation as described in claim 1-4 is any, feature exist
In specific steps are as follows:
(1) firstly, adding water to obtain mixture slurry into modified alta-mud, ultrasonication, the temperature of ultrasonication are then carried out
Degree is 110-120 DEG C, and time 30-60min obtains mixture；
(2) then, mixture and bamboo charcoal, glyceryl stearate and dextrin are subjected to ice bath and mix stirring, speed of agitator 300-
400r/min then carries out low temperature drying at a temperature of microencapsulation processing is placed in 2 DEG C -6 DEG C, obtains the dedicated dirt of livestock and poultry cultivation
Water treatment agent.
6. the preparation method of the dedicated sewage-treating agent of livestock and poultry cultivation according to claim 5, which is characterized in that step
(1) temperature of ultrasonication is 115 DEG C in, time 45min.
7. the preparation method of the dedicated sewage-treating agent of livestock and poultry cultivation according to claim 5, which is characterized in that step
(2) speed of agitator is 350r/min in.
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| CN201811155851.8A CN109250769A (en) | 2016-05-31 | 2016-05-31 | A kind of dedicated sewage-treating agent of livestock and poultry cultivation and preparation method thereof |
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| CN107098425A (en) * | 2017-05-05 | 2017-08-29 | 中科众沃生态科技（武汉）有限公司 | A kind of microcapsules water purification agent and preparation method thereof |
| CN109368759A (en) * | 2018-12-25 | 2019-02-22 | 重庆市沃利克环保设备有限公司 | A kind of sewage-treating agent and preparation method thereof for coating material production |
| WO2022110091A1 (en) * | 2020-11-29 | 2022-06-02 | 南京溧水高新创业投资管理有限公司 | Wastewater treatment agent and preparation method therefor |
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|---|---|---|---|---|
| DK1021241T3 (en) * | 1997-10-06 | 2001-12-27 | Adalbert Raps Stiftung | Process for producing a powdered product from a liquid substance or a liquid substance mixture |
| CN100545095C (en) * | 2003-12-11 | 2009-09-30 | 李伟 | A kind of sewage-treating agent |
| CN101530723A (en) * | 2009-04-17 | 2009-09-16 | 北京中新国能环保科技有限公司 | A method for reducing the energy consumption of flue gas desulfurization process system and a nano-lubricant |
| GB2482834B (en) * | 2009-05-12 | 2015-02-11 | Council Scient Ind Res | Clay nanocomposite forming microcapsule useful for guest encapsulation and process thereof |
| CN101712730B (en) * | 2009-05-13 | 2011-07-27 | 北京瑞仕邦精细化工技术有限公司 | Preparation method of water-soluble polymer dispersion |
| CN101717141B (en) * | 2009-12-01 | 2013-07-03 | 暨南大学 | Organic-inorganic in-situ composite flocculant and preparation method thereof |
| CN101992132B (en) * | 2010-11-25 | 2012-06-06 | 同济大学 | Ion exchange waste water denitrification material and preparation method thereof |
| CN104761109B (en) * | 2015-03-19 | 2016-12-07 | 郑州市少林滤材有限公司 | A kind of environment friendly light haydite firming agent and preparation method thereof |
| CN104785226B (en) * | 2015-04-15 | 2017-04-26 | 陕西科技大学 | Glass powder enhanced Zr modification montmorillonite honeycomb block chromium sorbent and preparation method thereof |
-
2016
- 2016-05-31 CN CN201811155851.8A patent/CN109250769A/en not_active Withdrawn
- 2016-05-31 CN CN201610394701.7A patent/CN105858749B/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| CN105858749A (en) | 2016-08-17 |
| CN109250769A (en) | 2019-01-22 |
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