CN105842103A - Tobacco moisture retention performance test method - Google Patents

Tobacco moisture retention performance test method Download PDF

Info

Publication number
CN105842103A
CN105842103A CN201610160015.3A CN201610160015A CN105842103A CN 105842103 A CN105842103 A CN 105842103A CN 201610160015 A CN201610160015 A CN 201610160015A CN 105842103 A CN105842103 A CN 105842103A
Authority
CN
China
Prior art keywords
moisture
sample
tobacco
moisture content
time
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201610160015.3A
Other languages
Chinese (zh)
Other versions
CN105842103B (en
Inventor
楼佳颖
沙云菲
吴达
朱云
张乾
刘百战
严逸凯
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shanghai Tobacco Group Co Ltd
Original Assignee
Shanghai Tobacco Group Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shanghai Tobacco Group Co Ltd filed Critical Shanghai Tobacco Group Co Ltd
Priority to CN201610160015.3A priority Critical patent/CN105842103B/en
Publication of CN105842103A publication Critical patent/CN105842103A/en
Application granted granted Critical
Publication of CN105842103B publication Critical patent/CN105842103B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N5/00Analysing materials by weighing, e.g. weighing small particles separated from a gas or liquid
    • G01N5/02Analysing materials by weighing, e.g. weighing small particles separated from a gas or liquid by absorbing or adsorbing components of a material and determining change of weight of the adsorbent, e.g. determining moisture content
    • G01N5/025Analysing materials by weighing, e.g. weighing small particles separated from a gas or liquid by absorbing or adsorbing components of a material and determining change of weight of the adsorbent, e.g. determining moisture content for determining moisture content

Abstract

The invention provides a tobacco moisture retention performance test method which comprises the steps of sample preprocessing, sample weight dynamic testing and data acquisition, dry base moisture rate calculation and moisture loss curve drawing, moisture ratio calculation and data fitting, and calculation of the moisture retention index and the average moisture loss rate or calculation of the average moisture loss rate at specific moisture ratio and the moisture retention index. The invention provides the tobacco moisture retention performance test and evaluation method which is used for solving the problems in the prior art that the tobacco shred moisture retention performance cannot be rapidly, simply, accurately and comprehensively tested and evaluated. Based on a fact that the tobacco physical moisture retention performance has relatively strong correlation with thermodynamics and kinetics indexes, the moisture retention evaluation method takes thermodynamic and kinetic indexes into account simultaneously, so that the tobacco physical moisture retention performance is more comprehensively and scientifically evaluated.

Description

A kind of method of testing of humid keeping performance of tobacco
Technical field
The present invention relates to Field of Tobacco, specifically disclose the method for testing of a kind of humid keeping performance of tobacco.
Background technology
The humid keeping performance of Medicated cigarette is in close relations with cigarette quality, and improving Medicated cigarette physics humid keeping performance is to improve Medicated cigarette sense organ to relax One of important channel of appropriateness.During Medicated cigarette humectation is studied, the most quickly, easy, accurately to tobacco shred humid keeping performance Carry out test and evaluation and become the problem needing solution badly.2008, Hu Jun et al. invented the side that tobacco moisture percentage is measured continuously Method and device thereof, utilize this device can be continuously monitored tobacco moisture percentage, thus compares different humectant humid keeping performances Difference.What Bao Jiang in 2009 et al. has invented tobacco moisture percentage test glove box, measures tobacco shred and initiates moisture content;At constant temperature and humidity The glove box of environment is measured tobacco shred weight and change thereof;Measured value is carried out record, according to initial moisture content and example weight Change release tobacco shred instant moisture content, form the data point of a series of tobacco shred instant moisture content relative time;Make tobacco shred Instant moisture content time graph, according to slope and the contrast of the equilibrium moisture content in later stage of the early stage of this curve, compares Nicotiana tabacum L. and protects Profit agent humectation effect nuance.2011, Wu Da et al. utilized dynamic water adsorption analysis systematic study tobacco shred at dry ring The dynamic law of moisture loss in border, draw moisture in cut tobacco scatter and disappear early stage moisture content of drying base and the square root of time between deposit At preferable linear dependence, by t tobacco shred moisture content of drying base MtValue is to t0.5Make rectilinear, from the slope of gained straight line Obtain rate constants k value, and in this, as the foundation of test humid keeping performance of tobacco, can be used for investigating tobacco humectant performance and cigarette Grass humectant screening etc..2013, Hu Jun et al. disclosed a kind of method evaluating humid keeping performance of tobacco, utilizes tobacco moisture percentage Measurement apparatus is measured tobacco sample tobacco shred weight in constant environment and is gone forward side by side over time line nonlinearity matching, by kinetics Index i.e. solves the average rate-of-loss of coolant value of wet (moisture absorption) as the foundation evaluating tobacco sample humid keeping performance.
Medicated cigarette physics humid keeping performance can be divided into two aspects of thermodynamics and kinetics.In Thermodynamic Criteria in sector application relatively For being " equilibrium moisture content " widely, it is key factor and the basis affecting Medicated cigarette physics humid keeping performance, is Medicated cigarette dehydration Endogenous cause of ill, reflects the inherent moisture holding capacity of Medicated cigarette.Dynamics index is mainly Medicated cigarette moisture loss speed or half-life, and it is thing Reason humid keeping performance the most directly embodies.In dry area, if cigarette moisture declines too fast, quickly become dry, easily disappeared Expense person causes the impression that humid keeping performance is not good enough.Therefore, investigate Nicotiana tabacum L. physics humid keeping performance and should take into account thermodynamics and kinetics simultaneously Index.
Summary of the invention
It is an object of the invention to overcome the defect of prior art, it is provided that the new test side of a kind of humid keeping performance of tobacco Method, overcomes in prior art the test and evaluation to humid keeping performance of tobacco can not take into account the defect of thermodynamics and kinetics.
In order to realize object above and other purposes, the present invention is by including that techniques below scheme realizes:
The invention discloses a kind of humid keeping performance of tobacco method of testing, comprise the following steps:
1) sample pre-treatments: Nicotiana tabacum L. will be weighed and as sample and balance 48~72h;
2) example weight dynamic test and data acquisition: sample is placed in Medicated cigarette humectation test equipment, the temperature of equipment With relative humidity set to presumptive test value, being continually changing of t weighs sample quality m in time, and records result;
3) moisture content of drying base calculates and dehydration curve plotting: according to the data of sample quality m t in time change, uses baking oven Method obtains butt quality m of sampleDryAnd calculate moisture content of drying base q, draw sample moisture content of drying base q t change curve in time;Its In,mtFor the quality of sample, m after baking time t in an ovenDryQuality after drying for sample;
4) moisture is than calculating and data matching: moisture during calculating acquisition t is than MR, whereinIts In, qtFor the moisture content of drying base that t is corresponding, q0For initial moisture content of drying base, qeFor final moisture content of drying base;
5) data matching with specific moisture than lower corresponding time tMRCalculate: moisture corresponding for time t is compared MRtSubstitute into MR =exp (-ktd) matching in equation, obtain constant k and d;And according to formulaCalculate specific moisture more right than lower The time answered;
6) average percentage of water loss v or specific moisture than under average rate-of-loss of coolant vMR:
Wherein, k and d is constant, t0For initial time section, t is the t time Section, q0Moisture content of drying base for initial time;qeFor final moisture content of drying base;
q0Moisture content of drying base for initial time;qeFor final moisture content of drying base, tMRFor Reach the time period that moisture is more corresponding than MR;
7) calculating of humectation index M RI:OrOrWhereinFor The t of several same sampleMRMeansigma methods,Q for several same sampleeMeansigma methods,V flat for several same sample Average.
Preferably, step 1) in the temperature of balance be 20~25 DEG C, equilibrium humidity is 55~65%.
Preferably, step 1) in balance be to carry out in standard environment, standard environment is RH=60%, T=22 DEG C.
Preferably, step 2) described in Medicated cigarette humectation test equipment be dynamic water analyze system DVS, tobacco moisture percentage survey Trial work casing or dynamic water analyze the one in climate box.
Preferably, step 2) in the temperature of equipment be 20~25 DEG C;Equipment humidity is 30~40%;The number of described data At least 50.
Step 3) described in Oven Method be to use prior art is tested in tobacco business the baking oven that moisture content of drying base is conventional Method is tested, and wherein, in Oven Method, oven temperature is 100 DEG C, and drying time is 2h.
Preferably, step 6) in tMRBe MR be the time corresponding to 0.367 or 0.5.
Preferably, described step 6) described in vMRBe MR be the average rate-of-loss of coolant corresponding to 0.367 or 0.5.
Preferably, step 7) in, described humectation indexOrOr It is average rate-of-loss of coolant corresponding when being 0.367 for MR,It it is average rate-of-loss of coolant corresponding when being 0.5 for MR.
The invention also discloses the method as described above purposes on test humid keeping performance of tobacco.
As it has been described above, humid keeping performance of tobacco method of testing of the present invention, have the advantages that
This humid keeping performance of tobacco test and evaluation method, it is achieved that reduce test period to greatest extent, decrease centre Link and manual operation error, substantially increase automaticity, and have employed degree of fitting more preferable drying model PAGE equation Carrying out data process, devise and can directly characterize the humectation index that Nicotiana tabacum L. physics humid keeping performance is good and bad, this index is taken into account simultaneously Affect kinetic factor and the Thermodynamics of humid keeping performance, compare current industry with single index to evaluate humid keeping performance of tobacco More science is with comprehensively, and this evaluation index is applicable to the test data of all kinds of humectation test equipment.The method is in current industry Main flow humectation tests equipment such as: dynamic water analyzes system DVS, tobacco moisture percentage test glove box, dynamic water analysis weather Casees etc. are the most applicable.Humectation index is the biggest, and humid keeping performance is the best.
The present invention provides a kind of humid keeping performance of tobacco test and evaluation method, is used for solving that prior art lacks energy fast Fast, easy, precisely, all sidedly tobacco shred humid keeping performance to be carried out test and evaluation problem.Physics humid keeping performance in view of Nicotiana tabacum L. All there are stronger dependency, humectation evaluation methodology to take into account thermodynamics and kinetics index with thermodynamics, dynamics index simultaneously, from And more fully and scientifically to Nicotiana tabacum L. physics humid keeping performance be evaluated.
Humid keeping performance of tobacco test and evaluation method disclosed in the present invention overcome many disadvantages of the prior art and Creative.
Accompanying drawing explanation
Fig. 1 is the schematic flow sheet of humid keeping performance of tobacco evaluation methodology of the present invention.
Fig. 2 is the moisture content of drying base time dependent dehydration curve chart in the embodiment of the present invention 1 method.
Fig. 3 is the moisture content of drying base time dependent dehydration curve chart of tobacco sample in embodiment 2 method in the present invention.
Fig. 4 is the moisture content of drying base time dependent dehydration curve chart of tobacco sample in the embodiment of the present invention 3 method.
Fig. 5 is the moisture content of drying base time dependent dehydration curve chart of tobacco sample in the embodiment of the present invention 4 method.
Detailed description of the invention
The present invention is expanded on further below in conjunction with embodiment.Should be understood that embodiment is merely to illustrate the present invention, and unrestricted The scope of the present invention.
Refer to Fig. 1 to Fig. 5.It should be noted that the diagram provided in the present embodiment illustrates this most in a schematic way The basic conception of invention, the most graphic in package count time only display with relevant assembly in the present invention rather than is implemented according to reality Mesh, shape and size are drawn, and during its actual enforcement, the kenel of each assembly, quantity and ratio can be a kind of random change, and its Assembly layout kenel is likely to increasingly complex.
As it is shown in figure 1, humid keeping performance of tobacco evaluation methodology of the present invention, comprise the following steps:
1) weigh a certain amount of tobacco sample to be positioned in the planchet of known quality;Wherein, the Functionality, quality and appealing design of tobacco sample Electing 1.0000g~20.0000g as, and be preferably 22 DEG C ± 1 DEG C under standard environment, relative humidity is 60% ± 1% balance 48 ~72h;
2) by the ambient temperature in humectation test equipment and relative humidity set to presumptive test value, change the most in time Change quality m weighing tobacco samplet, time interval is preferably 0 second~300 seconds, and records each weighing result, is accurate to 0.0001g, obtains tobacco sample quality corresponding for time t, sample quality unit be the unit of g, t be min;
3) derive the delta data of sample quality m t in time in humectation test equipment, use Oven Method to record Nicotiana tabacum L. sample Weight m of product, calculates moisture content of drying base q, moisture content of drying basemtFor the quality of t sample, mDry Quality after drying for sample, obtains the moisture content of drying base data over time of sample and draws dehydration curve chart.Quality m Unit be g, the unit of moisture content of drying base q is %, and the unit of time t is min;
4) according to step 3) moisture that records, it is calculated moisture ratio corresponding for time tWherein qtFor The moisture content of drying base that time t is corresponding, q0For initial moisture content of drying base, qeFor final moisture content of drying base, unit is %;
5) carry out models fitting investigation by lot of experimental data, find that moisture more meets PAGE side than the relation with the time Journey MR=exp (-ktd), data are fitted and try to achieve reach specify moisture than the corresponding timetMR The biggest, the dehydration of tobacco sample is the slowest, tMRThe least, the dehydration of tobacco sample is the fastest;
6) by k, d, q0And qeValue substitutes intoOrIn, obtain spy Fixing time or average rate-of-loss of coolant v of tobacco sample under dedicated half-life, v is the biggest, and the dehydration of tobacco sample is the fastest, and v is the least, The dehydration of tobacco sample is the slowest;
7) by 5) the dynamics index t that obtainsMROr 6) average rate-of-loss of coolant v of dynamics index that obtains and Thermodynamic Criteria qeIt is added after normalization respectively and obtains humectation index (MRI).Wherein, average rate-of-loss of coolant and humid keeping performance are negative correlation, therefore should Adding negative sign before Xiang, humectation index is the biggest, and humid keeping performance is the best.
OrOr
This humid keeping performance of tobacco method of testing utilizes the humectation test equipment research tobacco shred that can arrange temperature and relative humidity The dynamic law of moisture loss in dry environment, result shows that the moisture in moisture in cut tobacco dispersion process is than the pass with the time System meets PAGE equation, is fitted obtaining corresponding parameter by data with the equation, calculates the average mistake under dedicated half-life Water speed is as evaluation index, and final moisture content of drying base is as another evaluation index, by two indices normalization and be added To humectation index.This method is suitable for all kinds of humectation test equipment, the most scientific and reasonable compared to tradition evaluation methodology result.
The specific embodiment of above-mentioned humid keeping performance of tobacco method of testing is as follows.
Embodiment 1
1) preparation of samples: weigh 12g tobacco sample respectively and be placed in the planchet of known quality, the title of tobacco sample and Sequence number is as shown in table 1;
Table 1 tobacco sample title table
Sequence number Tobacco sample title
1 Cut tobacco 1
2 Cut tobacco 2
3 Cut tobacco 3
4 Swollen silk 1
5 Swollen silk 2
6 Swollen silk 3
7 Stem 1
8 Stem 2
9 Stem 3
2) tobacco sample balances 48 hours in standard environment;Described standard environment is RH=60%, T=22 DEG C;
3) moisture content of drying base dynamic test: preset dynamic water and analyze in climate box the temperature of air ambient with relative Humidity 22 DEG C and 40% respectively, and set every 20s sample quality of record, quality is accurate to 0.0001g;It is sequentially placed into 9 Bring into operation after tobacco sample, run and be automatically stopped to 15h, obtain tobacco sample quality m corresponding for time tt;Oven Method obtains To moisture content of drying base q corresponding for sample time tt, the moisture content of drying base q of tobacco sampletHomologous thread such as Fig. 2 institute with time t Show;
4) data calculate: calculate the moisture ratio in each moment and carry out PAGE equation MR=exp (-ktd) matching, try to achieve k, The value of d, substitutes into PAGE Equation for Calculating each sample at the time t corresponding to MR=0.3670.367, and do according to the final of each sample Base moisture content, calculates 9 sample water proportions by subtraction respectively and is down to the time needed for 0.367 and the meansigma methods of final moisture content of drying base, Substitute intoIt is calculated the humectation index of each sample.
Table 23 grows tobacco sample average rate-of-loss of coolant, final moisture content of drying base and humectation index
Shown by table 2 data, cut tobacco, swollen silk and stem under RH=40% dry environment corresponding to MR=0.367 time Between be respectively 94.17min, 66.09min and 63.63min (3 Duplicate Samples are averaged, lower with).Cut tobacco, swollen silk and stem are Whole moisture content of drying base difference 8.95%, 8.82% and 9.93%.Finally being calculated respective humectation index cut tobacco is 2.23, swollen Silk is 1.84, and stem is 1.93, and the relative standard deviation between Duplicate Samples is less.Therefore, the humid keeping performance of cut tobacco is best, secondly For stem and swollen silk.
Embodiment 2
1) preparation of samples: weigh 1g tobacco shred blank control sample respectively and the different humectant of interpolation obtains tobacco sample and is placed in Knowing in the planchet of quality and test one by one, title and the sequence number of tobacco sample are as shown in table 3;
Table 3 tobacco sample title table
Sequence number Tobacco sample title
1 Tobacco shred blank
2 Tobacco shred+humectant 1
3 Tobacco shred+humectant 2
4 Tobacco shred+humectant 3
2) tobacco sample balances 48 hours in standard environment;Described standard environment is RH=60%, T=22 DEG C.
3) moisture content of drying base dynamic test: set dynamic water tester (DVS) temperature and relative humidity respectively 22 DEG C and 30%, do not have 1min to record a sample quality, quality is accurate to 0.000001g, is automatically stopped entrance and dries journey after running 15h Sequence, obtains tobacco sample quality m corresponding for time ttAnd final mass i.e. butt weight mDry;Butt corresponding for calculating time t contains Water rate qt, the moisture content of drying base q of tobacco sampletWith the homologous thread of time t as shown in Figure 3;
4) data calculate: calculate the moisture ratio in each moment and carry out PAGE equation MR=exp (-ktd) matching, try to achieve k, d Value, substitutes into PAGE Equation for Calculating each sample at the time t corresponding to MR=0.3670.367, byObtain Moisture is down to the average rate-of-loss of coolant during 0.367 than by 1, and according to the final moisture content of drying base of each sample, calculates 4 respectively Meansigma methods v of sample average rate-of-loss of coolant and the meansigma methods of final moisture content of drying baseSubstitute intoCalculate Obtain the humectation index of each sample.
44 kinds of tobacco sample v of table0.367, final moisture content of drying base and humectation index
Being shown by table 4 data, the humid keeping performance of tobacco shred is all had castering action, 3 kinds of humectants all to have at low humidity by humectant Environment slows down rate-of-loss of coolant, and improves the effect of final moisture content of drying base, the wherein humectation best results of humectant 2.
Embodiment 3
1) preparation of samples: weigh 10g stem blank sample respectively and with the addition of the stem sample of humectant and be placed in known In the planchet of quality, title and the sequence number of tobacco sample are as shown in table 5;;
Table 5 tobacco sample title table
Sequence number Tobacco sample title
1 Stem blank
2 Stem+humectant 1
3 Stem+humectant 2
4 Stem+humectant 3
2) tobacco sample balances 48 hours in standard environment;
3) moisture content of drying base dynamic test: preset the temperature of climate box air ambient and relative humidity respectively 22 DEG C and 40%, and set every 20s sample quality of record, quality is accurate to 0.0001g;Start after being sequentially placed into 4 tobacco samples Run, run and be automatically stopped to 48h, obtain tobacco sample quality m corresponding for time tt;Oven Method obtains sample time t pair The moisture content of drying base q answeredt, the moisture content of drying base q of tobacco sampletWith the homologous thread of time t as shown in Figure 4;
4) data calculate: calculate the moisture ratio in each moment and carry out PAGE equation MR=exp (-ktd) matching, try to achieve k, The value of d, substitutes into PAGE Equation for Calculating each sample at the time t corresponding to MR=0.50.5, byObtain Moisture is down to the average rate-of-loss of coolant during 0.5 than by 1, and according to the final moisture content of drying base of each sample, calculates 4 samples respectively The meansigma methods of the average rate-of-loss of coolant of productAnd the meansigma methods of final moisture content of drying baseSubstitute intoCalculate Humectation index to each sample.
64 kinds of stem sample v of table0.5, final moisture content of drying base and humectation index
Table 6 data show, the humid keeping performance of stem is all had castering action, 3 kinds of humectants all to have at low humidity ring by humectant Slowing down the effect of rate-of-loss of coolant in border, wherein humectant 1 and humectant 2 have an effect improving moisture content of drying base, and humectant 3 Humectation most pronounced effects.
Embodiment 4
1) preparation of samples: take 16 finished cigarettes and tear tobacco shred (a~j) open and tile afterwards in the planchet being placed in known quality;
2) tobacco sample balances 48 hours in standard environment;
3) moisture content of drying base dynamic test: preset the temperature of climate box air ambient and relative humidity respectively 22 DEG C and 40%, and set every 20s sample quality of record, quality is accurate to 0.0001g;Start after being sequentially placed into 10 tobacco samples Run, run and be automatically stopped to 48h, obtain tobacco sample quality m corresponding for time tt;Oven Method obtains sample time t pair The moisture content of drying base q answeredt, the moisture content of drying base q of tobacco sampletWith the homologous thread of time t as shown in Figure 5;
4) data calculate: calculate the moisture ratio in each moment and carry out PAGE equation MR=exp (-ktd) matching, try to achieve k, The value of d, by k, d, q0, qeValue substitute intoIn, the average dehydration speed of 90min before calculating sample Rate v, and according to the final moisture content of drying base of each sample, the meansigma methods of the average rate-of-loss of coolant of 90min before 10 samples of calculating respectivelyAnd the meansigma methods of final moisture content of drying baseSubstitute intoThe humectation being calculated each sample refers to Number.
7 10 kinds of cigarette rags sample v of table90min, final moisture content of drying base and humectation index go
By table 7 data, the humectation index of 10 cigarette rags samples is ranked up from high to low, its humid keeping performance Have excellent to bad for d, j, c, g, h, f, b, a, i, e.
In sum, humid keeping performance of tobacco evaluation methodology of the present invention, combined by index big to thermodynamics and dynamics two Close to consider to devise and can directly characterize the humectation index that humid keeping performance is good and bad, science and directly perceived, applied widely.
The above, only presently preferred embodiments of the present invention, not any formal and substantial to present invention restriction, It should be pointed out that, for those skilled in the art, on the premise of without departing from the inventive method, also can make Some improvement and supplement, these improve and supplement also should be regarded as protection scope of the present invention.All those skilled in the art, Without departing from the spirit and scope of the present invention, make when available disclosed above technology contents a little more The equivalent variations moved, modify and develop, is the Equivalent embodiments of the present invention;Meanwhile, all substantial technological pair according to the present invention The change of any equivalent variations that above-described embodiment is made, modify and develop, all still fall within the scope of technical scheme In.

Claims (8)

1. a humid keeping performance of tobacco method of testing, comprises the following steps:
1) sample pre-treatments: Nicotiana tabacum L. will be weighed and as sample and balance 48~72h;
2) example weight dynamic test and data acquisition: sample is placed in Medicated cigarette humectation test equipment, the temperature of equipment and phase To humidity set to presumptive test value, being continually changing of t weighs sample quality m in time, and records result;
3) moisture content of drying base calculates and dehydration curve plotting: according to the data of sample quality m t in time change, uses Oven Method Obtain butt quality m of sampleDryAnd calculating moisture content of drying base q, the dehydration drawing sample moisture content of drying base q t in time change is bent Line;Wherein,Mt is the quality of sample, m after baking time t in an ovenDryAfter drying for sample Quality;
4) moisture is than calculating: moisture during calculating acquisition t is than MR, whereinWherein, qtFor t pair The moisture content of drying base answered, q0For initial moisture content of drying base, qeFor final moisture content of drying base;
5) data matching with specific moisture than lower corresponding time tMRCalculating: moisture corresponding for time t is substituted into MR=than MR exp(-ktd) matching in equation, obtain constant k and d, and according to formulaCalculate specific moisture than lower correspondence Time;
6) average percentage of water loss v or specific moisture than under average rate-of-loss of coolant vMR:
Wherein, k and d is constant, t0For initial time section, t is the t time period, q0 Moisture content of drying base for initial time;qeFor final moisture content of drying base;
q0Moisture content of drying base for initial time;qeFor final moisture content of drying base, tMRFor reaching The time period that moisture is more corresponding than MR;
7) calculating of humectation index M RI:OrOrWhereinFor several phases T with sampleMRMeansigma methods,Q for several same sampleeMeansigma methods,Meansigma methods for the v of several same sample.
2. as claimed in claim 1 method, it is characterised in that: step 1) in the temperature of balance be 20~25 DEG C, equilibrium humidity is 55~65%.
3. as claimed in claim 1 method, it is characterised in that: step 2) described in Medicated cigarette humectation test equipment be that dynamic water is divided Analysis system DVS, tobacco moisture percentage test glove box or dynamic water analyze the one in climate box.
4. as claimed in claim 1 method, it is characterised in that: step 2) in the temperature of equipment be 20~25 DEG C;Equipment humidity is 30~40%;The number of described data is at least 50.
5. as claimed in claim 1 method, it is characterised in that: step 6) in tMRBe MR be corresponding to 0.367 or 0.5 time Between.
6. as claimed in claim 1 method, it is characterised in that: described step 6) described in vMRBe MR be corresponding to 0.367 or 0.5 Average rate-of-loss of coolant.
7. method as claimed in claim 1, it is characterised in that: step 7) in, described humectation indexOrOr It is average rate-of-loss of coolant corresponding when being 0.367 for MR,Be MR be 0.5 Time corresponding average rate-of-loss of coolant.
8. the purposes on test humid keeping performance of tobacco of the method as described in as arbitrary in claim 1~7.
CN201610160015.3A 2016-03-21 2016-03-21 A kind of test method of humid keeping performance of tobacco Active CN105842103B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610160015.3A CN105842103B (en) 2016-03-21 2016-03-21 A kind of test method of humid keeping performance of tobacco

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610160015.3A CN105842103B (en) 2016-03-21 2016-03-21 A kind of test method of humid keeping performance of tobacco

Publications (2)

Publication Number Publication Date
CN105842103A true CN105842103A (en) 2016-08-10
CN105842103B CN105842103B (en) 2018-09-25

Family

ID=56587617

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610160015.3A Active CN105842103B (en) 2016-03-21 2016-03-21 A kind of test method of humid keeping performance of tobacco

Country Status (1)

Country Link
CN (1) CN105842103B (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107490658A (en) * 2017-09-11 2017-12-19 云南中烟工业有限责任公司 A kind of evaluation method of cigarette humid keeping performance
CN111189974A (en) * 2020-01-07 2020-05-22 云南中烟工业有限责任公司 Method for evaluating moisture-proof and moisture-retaining performance of package
CN111474290A (en) * 2020-04-29 2020-07-31 上海烟草集团有限责任公司 Method for measuring protein content in tobacco
CN112989554A (en) * 2020-12-31 2021-06-18 北京石油化工学院 Method, device and equipment for acquiring moisture content ratio of agricultural products based on different drying stages

Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5470874A (en) * 1994-10-14 1995-11-28 Lerner; Sheldon Ascorbic acid and proanthocyanidine composition for topical application to human skin
JP4053799B2 (en) * 2002-03-19 2008-02-27 三井化学ポリウレタン株式会社 Polyol, production method thereof, polyurethane resin or foam obtained from the polyol
CN102128763A (en) * 2010-11-16 2011-07-20 上海烟草集团有限责任公司 Method for testing humid keeping performance of tobacco
CN102636407A (en) * 2012-04-10 2012-08-15 广西中烟工业有限责任公司 Tobacco physical humectation performance testing method
CN103105341A (en) * 2013-01-31 2013-05-15 中国烟草总公司郑州烟草研究院 Method for evaluating humidity keeping performance of tobacco
CN103471957A (en) * 2013-09-25 2013-12-25 上海烟草集团有限责任公司 Tobacco moisture-retaining performance test method
CN103760062A (en) * 2014-02-14 2014-04-30 江苏中烟工业有限责任公司 Method for evaluating humidifying performance of tobacco humectant
CN103776720A (en) * 2014-02-14 2014-05-07 江苏中烟工业有限责任公司 Evaluation method for moisture keeping performance of cigarette raw materials
CN104013094A (en) * 2014-06-26 2014-09-03 福建中烟工业有限责任公司 Additive for improving quality of CO2 expanded cut tobacco and application of additive in cigarettes
CN104634693A (en) * 2015-01-15 2015-05-20 华环国际烟草有限公司 Method for obtaining drying characteristic parameter of blend-threshed tobacco leaves in redrying technology

Patent Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5470874A (en) * 1994-10-14 1995-11-28 Lerner; Sheldon Ascorbic acid and proanthocyanidine composition for topical application to human skin
JP4053799B2 (en) * 2002-03-19 2008-02-27 三井化学ポリウレタン株式会社 Polyol, production method thereof, polyurethane resin or foam obtained from the polyol
CN102128763A (en) * 2010-11-16 2011-07-20 上海烟草集团有限责任公司 Method for testing humid keeping performance of tobacco
CN102636407A (en) * 2012-04-10 2012-08-15 广西中烟工业有限责任公司 Tobacco physical humectation performance testing method
CN103105341A (en) * 2013-01-31 2013-05-15 中国烟草总公司郑州烟草研究院 Method for evaluating humidity keeping performance of tobacco
CN103471957A (en) * 2013-09-25 2013-12-25 上海烟草集团有限责任公司 Tobacco moisture-retaining performance test method
CN103760062A (en) * 2014-02-14 2014-04-30 江苏中烟工业有限责任公司 Method for evaluating humidifying performance of tobacco humectant
CN103776720A (en) * 2014-02-14 2014-05-07 江苏中烟工业有限责任公司 Evaluation method for moisture keeping performance of cigarette raw materials
CN104013094A (en) * 2014-06-26 2014-09-03 福建中烟工业有限责任公司 Additive for improving quality of CO2 expanded cut tobacco and application of additive in cigarettes
CN104634693A (en) * 2015-01-15 2015-05-20 华环国际烟草有限公司 Method for obtaining drying characteristic parameter of blend-threshed tobacco leaves in redrying technology

Non-Patent Citations (9)

* Cited by examiner, † Cited by third party
Title
W. K. ZHU .ETC: "Effect of two-stage dehydration on retention of characteristic flavor components of flue-cured tobacco in rotary dryer", 《DRYING TECHNOLOGY》 *
何保江 等: "烟草保润性能测试方法", 《烟草工艺》 *
张安丰 等: "烟草保润性的研究进展", 《轻工科技》 *
张峻松等: "不同烟草原料物理保润性能影响因素研究", 《轻工学报》 *
张蓉 等: "烟草保润剂分析方法研究进展", 《云南化工》 *
曾世通 等: "烟叶保润性能影响因素研究", 《烟草化学》 *
楼佳颖 等: "不同卷烟原料物理保润机理研究", 《中国烟草学报》 *
楼佳颖 等: "动态水分吸附分析系统在烟草中的应用", 《烟草化学》 *
马林 等: "烟草自身保润性能", 《广东化工》 *

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107490658A (en) * 2017-09-11 2017-12-19 云南中烟工业有限责任公司 A kind of evaluation method of cigarette humid keeping performance
CN107490658B (en) * 2017-09-11 2019-07-16 云南中烟工业有限责任公司 A kind of evaluation method of cigarette humid keeping performance
CN111189974A (en) * 2020-01-07 2020-05-22 云南中烟工业有限责任公司 Method for evaluating moisture-proof and moisture-retaining performance of package
CN111474290A (en) * 2020-04-29 2020-07-31 上海烟草集团有限责任公司 Method for measuring protein content in tobacco
CN112989554A (en) * 2020-12-31 2021-06-18 北京石油化工学院 Method, device and equipment for acquiring moisture content ratio of agricultural products based on different drying stages
CN112989554B (en) * 2020-12-31 2023-06-30 北京石油化工学院 Agricultural product water ratio acquisition method, device and equipment based on different drying stages

Also Published As

Publication number Publication date
CN105842103B (en) 2018-09-25

Similar Documents

Publication Publication Date Title
CN105842103A (en) Tobacco moisture retention performance test method
JP5231683B2 (en) Method for measuring moisture retention of tobacco
CN103471957A (en) Tobacco moisture-retaining performance test method
Barr et al. Use of change-point detection for friction–velocity threshold evaluation in eddy-covariance studies
Jost et al. High-resolution simulations of the last glacial maximum climate over Europe: a solution to discrepancies with continental palaeoclimatic reconstructions?
Langford et al. Eddy-covariance data with low signal-to-noise ratio: time-lag determination, uncertainties and limit of detection
CN103760061B (en) A kind of evaluation method of humidity preservation property of cigarette
CN102221511B (en) Method for testing moisture adsorption-desorption performance of tobacco leaf
CN103776720B (en) A kind of evaluation method of cigarette raw material humid keeping performance
CN101131344A (en) Method for on-line measuring drying property of tobacco and kinetic analysis
CN103105341A (en) Method for evaluating humidity keeping performance of tobacco
CN105942567A (en) Method and device used for cigarette formula classification and management
CN101685092B (en) Method for judging alcoholization quality of flue-cured tobacco by pH detection value of tobacco leaf
Yoshimori et al. Fixed anvil temperature feedback: Positive, zero, or negative?
CN105092789A (en) Analysis method for tobacco leaf style characteristic variation trend in lamina aging process
CN105699239A (en) Method for analyzing moisture retention ability of tobaccos and tobacco products by aid of near-infrared spectral models
CN103868957B (en) A kind of method evaluating beating and double roasting operation sheet cigarette organoleptic quality stability
Fan et al. Comments on “Do ultrafine cloud condensation nuclei invigorate deep convection?”
CN106769619A (en) Pipe tobacco roller drying processes intensity decision method and system
CN104899424A (en) Microscopic feature based method for objectively testing ripeness and leaf structure of flue-cured tobacco leaves
Fu et al. Improvements in simulating the relationship between ENSO and East Asian summer rainfall in the CMIP5 models
CN109916971B (en) Rapid nondestructive testing method for fresh tobacco moisture based on capacitor
CN111610117A (en) Method for rapidly measuring moisture content of sheet for heating cigarette
CN105787518A (en) Near infrared spectrum pretreatment method based on null-space projection
Lindholm et al. Effects of climate on the growth of Scots pine in the Saimaa lake district, south-eastern Finland, in the southern part of the boreal forest belt

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant