CN105838161A - Interior decoration coating of high adhesion antimicrobial container and preparation method thereof - Google Patents
Interior decoration coating of high adhesion antimicrobial container and preparation method thereof Download PDFInfo
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- CN105838161A CN105838161A CN201610338443.0A CN201610338443A CN105838161A CN 105838161 A CN105838161 A CN 105838161A CN 201610338443 A CN201610338443 A CN 201610338443A CN 105838161 A CN105838161 A CN 105838161A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D127/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Coating compositions based on derivatives of such polymers
- C09D127/02—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Coating compositions based on derivatives of such polymers not modified by chemical after-treatment
- C09D127/12—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Coating compositions based on derivatives of such polymers not modified by chemical after-treatment containing fluorine atoms
- C09D127/18—Homopolymers or copolymers of tetrafluoroethene
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/14—Paints containing biocides, e.g. fungicides, insecticides or pesticides
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/14—Polymer mixtures characterised by other features containing polymeric additives characterised by shape
- C08L2205/16—Fibres; Fibrils
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Plant Pathology (AREA)
- Paints Or Removers (AREA)
Abstract
The invention discloses an interior decoration coating of a high adhesion antimicrobial container. The interior decoration coating of the high adhesion antimicrobial container is prepared from the following raw materials in parts by weight: polytetrafluoroethylene resin, coumarone resin, coconut alcohol, bamboo fibers, carbon black, dimethylolbutyric acid, 80-mesh medical stone powder, acrylonitrile, potassium persulfate, sodium chloride, rosin pentaerythritol ester, ammonium molybdate, dimethyl fumarate, dodecanol ester, polydimethylsiloxane, methanol, glycerol and butyl acetate anhydrous. The invention further discloses a preparation method of the coating. The coating prepared by the invention has strong adhesion and good antibacterial effect. Furthermore, the coating prepared by the invention is safe in use, wide and high in raw material availability, simple and feasible in manufacturing method and suitable for fields of packaging industries requiring high antibacterial properties and abrasion resistance.
Description
Technical field
The invention belongs to paint field, be specifically related to a kind of high adhesion force antibacterial container interior paint and preparation method thereof.
Background technology
Container, as a kind of efficient, economic and special use the large cargo box-shaped container of being easy to mechanically actuated and transport, because of one chest of its profile rubber, can transport with packaging again in groups, therefore referred to as container.According to holding freight kind, container can be divided into again the plurality of classes such as plain edition, liquid type, automobile type, frozen type, preservation type.Container is mainly prepared from by iron and steel, aluminum, light-alloy, fiberglass, fiber-reinforced plastic (FRP), plywood etc., the most topmost is prepared from by iron and steel, aluminum.In order to reduce internal container due to water, the impact of corrosive substance, generally protective coating can be coated at internal container.And container is in use, goods can produce phase mutual friction or extruding to inner wall of container, and the common protective coating of internal container is easy to come off and reduce its protection to container;Additionally, internal container also easily breed bacteria and affect safe handling, these antibacterial grown not easy cleanings are removed, the most inconvenient especially for some van containers.Accordingly, it would be desirable to a kind of high adhesion force antibacterial container interior paint of preparation, with the more preferable application demand of satisfied reality.
Summary of the invention
At least one of present invention prior art problem to be solved, it is provided that a kind of high adhesion force antibacterial container interior paint and preparation method thereof.
In order to solve above-mentioned technical problem, the present invention is achieved by the following technical solutions:
The present invention provides a kind of high adhesion force antibacterial container interior paint, it is prepared from by the raw material of following weight portion: polyflon 42-56 part, coumarone indene resin 15-21 part, coconut alcohol 8-14 part, bamboo fibre 3-7 part, white carbon black 4-9 part, dimethylolpropionic acid 3-10 part, 80 mesh wheat metal plate stone powder 2-6 parts, acrylonitrile 3-6 part, potassium peroxydisulfate 3-9 part, sodium chloride 5-8 part, pentalyn 2-8 part, ammonium molybdate 1-5 part, dimethyl fumarate 4-10 part, Lauryl Alcohol ester 6-12 part, polydimethylsiloxane 2-5 part, methanol 46-58 part, glycerol 21-35 part, Glacial acetic acid butyl ester 10-22 part.
Preferably, described high adhesion force antibacterial container interior paint, is prepared from by the raw material of following weight portion: polyflon 47 parts, coumarone indene resin 16 parts, coconut alcohol 9 parts, bamboo fibre 5 parts, white carbon black 6 parts, dimethylolpropionic acid 7 parts, 80 mesh wheat metal plate stone powders 5 parts, acrylonitrile 4 parts, potassium peroxydisulfate 7 parts, 6 parts of sodium chloride, pentalyn 5 parts, ammonium molybdate 2 parts, dimethyl fumarate 6 parts, Lauryl Alcohol ester 9 parts, polydimethylsiloxane 3 parts, methanol 48 parts, glycerol 29 parts, Glacial acetic acid butyl ester 15 parts.
Preferably, described high adhesion force antibacterial container interior paint, is prepared from by the raw material of following weight portion: polyflon 53 parts, coumarone indene resin 19 parts, coconut alcohol 11 parts, bamboo fibre 4 parts, white carbon black 4 parts, dimethylolpropionic acid 5 parts, 80 mesh wheat metal plate stone powders 4 parts, acrylonitrile 3 parts, potassium peroxydisulfate 8 parts, 5 parts of sodium chloride, pentalyn 7 parts, ammonium molybdate 3 parts, dimethyl fumarate 8 parts, Lauryl Alcohol ester 10 parts, polydimethylsiloxane 4 parts, methanol 53 parts, glycerol 23 parts, Glacial acetic acid butyl ester 18 parts.
The preparation method of above-mentioned high adhesion force antibacterial container interior paint, comprises the following steps:
(1) each component raw material is weighed by following weight;
(2) methanol weighed, glycerol, Glacial acetic acid butyl ester are added in blender, adding polyflon, coumarone indene resin, coconut alcohol, acrylonitrile, sodium chloride, dimethyl fumarate, dimethylolpropionic acid, Lauryl Alcohol ester, at a temperature of 40-52 DEG C, stir 15-40min with mixing speed for 1100-1800rpm;
(3) it is subsequently adding bamboo fibre, white carbon black, 80 mesh wheat metal plate stone powders, ammonium molybdate, is warming up to 60-78 DEG C, stirs 20-45min with mixing speed for 400-800rpm;
(4) it is cooled to 40-52 DEG C, adds remaining raw material, stir for 200-350rpm with mixing speed;
(5) through 100 mesh silk screen filter after having stirred, it is cooled to room temperature, obtains described container interior paint.
Preferably, in described step (2) at a temperature of 47 DEG C, 20min is stirred with mixing speed for 1500rpm.
Described step is warming up to 72 DEG C in (3), stirs 30min with mixing speed for 560rpm.
Described step is cooled to 46 DEG C in (4), stirs with mixing speed for 260rpm.
Owing to have employed above technical scheme, present invention have the beneficial effect that
The adhesive force of the coating prepared by the present invention is strong, and its adhesive force test grade is zero level;And good anti-bacterial effect, it is up to more than 94.2% to the antibiotic rate of staphylococcus aureus, colibacillary antibiotic rate is up to more than 95.4%.Additionally, the coating prepared by the present invention uses safety, raw material sources are extensively easy to get, manufacture method simple possible, be suitable for packaging industry and antibiotic property and wearability are required high field.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is described in further detail.Following example are used for illustrating the present invention, but are not limited to the scope of the present invention.
Embodiment one
The preparation method of a kind of high adhesion force antibacterial container interior paint, comprises the following steps:
(1) each component raw material is weighed by following weight: polyflon 42 parts, coumarone indene resin 15 parts, coconut alcohol 8 parts, bamboo fibre 3 parts, white carbon black 4 parts, dimethylolpropionic acid 3 parts, 80 mesh wheat metal plate stone powders 2 parts, acrylonitrile 3 parts, potassium peroxydisulfate 3 parts, 5 parts of sodium chloride, pentalyn 2 parts, ammonium molybdate 1 part, dimethyl fumarate 4 parts, Lauryl Alcohol ester 6 parts, polydimethylsiloxane 2 parts, methanol 46 parts, glycerol 21 parts, Glacial acetic acid butyl ester 10 parts;
(2) methanol weighed, glycerol, Glacial acetic acid butyl ester are added in blender, adding polyflon, coumarone indene resin, coconut alcohol, acrylonitrile, sodium chloride, dimethyl fumarate, dimethylolpropionic acid, Lauryl Alcohol ester, at a temperature of 40 DEG C, stir 15min with mixing speed for 1100rpm;
(3) it is subsequently adding bamboo fibre, white carbon black, 80 mesh wheat metal plate stone powders, ammonium molybdate, is warming up to 60 DEG C, stirs 20min with mixing speed for 400rpm;
(4) it is cooled to 40 DEG C, adds remaining raw material, stir for 200rpm with mixing speed;
(5) through 100 mesh silk screen filter after having stirred, it is cooled to room temperature, obtains described container interior paint.
Embodiment two
The preparation method of a kind of high adhesion force antibacterial container interior paint, comprises the following steps:
(1) each component raw material is weighed by following weight: polyflon 56 parts, coumarone indene resin 21 parts, coconut alcohol 14 parts, bamboo fibre 7 parts, white carbon black 9 parts, dimethylolpropionic acid 10 parts, 80 mesh wheat metal plate stone powders 6 parts, acrylonitrile 6 parts, potassium peroxydisulfate 9 parts, 8 parts of sodium chloride, pentalyn 8 parts, ammonium molybdate 5 parts, dimethyl fumarate 10 parts, Lauryl Alcohol ester 12 parts, polydimethylsiloxane 5 parts, methanol 58 parts, glycerol 35 parts, Glacial acetic acid butyl ester 22 parts;
(2) methanol weighed, glycerol, Glacial acetic acid butyl ester are added in blender, adding polyflon, coumarone indene resin, coconut alcohol, acrylonitrile, sodium chloride, dimethyl fumarate, dimethylolpropionic acid, Lauryl Alcohol ester, at a temperature of 52 DEG C, stir 40min with mixing speed for 1800rpm;
(3) it is subsequently adding bamboo fibre, white carbon black, 80 mesh wheat metal plate stone powders, ammonium molybdate, is warming up to 78 DEG C, stirs 45min with mixing speed for 800rpm;
(4) it is cooled to 52 DEG C, adds remaining raw material, stir for 350rpm with mixing speed;
(5) through 100 mesh silk screen filter after having stirred, it is cooled to room temperature, obtains described container interior paint.
Embodiment three
The preparation method of a kind of high adhesion force antibacterial container interior paint, comprises the following steps:
(1) each component raw material is weighed by following weight: polyflon 49 parts, coumarone indene resin 18 parts, coconut alcohol 11 parts, bamboo fibre 5 parts, white carbon black 6 parts, dimethylolpropionic acid 7 parts, 80 mesh wheat metal plate stone powders 4 parts, acrylonitrile 4 parts, potassium peroxydisulfate 6 parts, 6 parts of sodium chloride, pentalyn 5 parts, ammonium molybdate 3 parts, dimethyl fumarate 7 parts, Lauryl Alcohol ester 9 parts, polydimethylsiloxane 3 parts, methanol 52 parts, glycerol 28 parts, Glacial acetic acid butyl ester 16 parts;
(2) methanol weighed, glycerol, Glacial acetic acid butyl ester are added in blender, adding polyflon, coumarone indene resin, coconut alcohol, acrylonitrile, sodium chloride, dimethyl fumarate, dimethylolpropionic acid, Lauryl Alcohol ester, at a temperature of 46 DEG C, stir 32min with mixing speed for 1450rpm;
(3) it is subsequently adding bamboo fibre, white carbon black, 80 mesh wheat metal plate stone powders, ammonium molybdate, is warming up to 69 DEG C, stirs 32min with mixing speed for 600rpm;
(4) it is cooled to 46 DEG C, adds remaining raw material, stir for 270rpm with mixing speed;
(5) through 100 mesh silk screen filter after having stirred, it is cooled to room temperature, obtains described container interior paint.
Embodiment four
The preparation method of a kind of high adhesion force antibacterial container interior paint, comprises the following steps:
(1) each component raw material is weighed by following weight: polyflon 47 parts, coumarone indene resin 16 parts, coconut alcohol 9 parts, bamboo fibre 5 parts, white carbon black 6 parts, dimethylolpropionic acid 7 parts, 80 mesh wheat metal plate stone powders 5 parts, acrylonitrile 4 parts, potassium peroxydisulfate 7 parts, 6 parts of sodium chloride, pentalyn 5 parts, ammonium molybdate 2 parts, dimethyl fumarate 6 parts, Lauryl Alcohol ester 9 parts, polydimethylsiloxane 3 parts, methanol 48 parts, glycerol 29 parts, Glacial acetic acid butyl ester 15 parts;
(2) methanol weighed, glycerol, Glacial acetic acid butyl ester are added in blender, adding polyflon, coumarone indene resin, coconut alcohol, acrylonitrile, sodium chloride, dimethyl fumarate, dimethylolpropionic acid, Lauryl Alcohol ester, at a temperature of 47 DEG C, stir 20min with mixing speed for 1500rpm;
(3) it is subsequently adding bamboo fibre, white carbon black, 80 mesh wheat metal plate stone powders, ammonium molybdate, is warming up to 72 DEG C, stirs 30min with mixing speed for 560rpm;
(4) it is cooled to 46 DEG C, adds remaining raw material, stir for 260rpm with mixing speed;
(5) through 100 mesh silk screen filter after having stirred, it is cooled to room temperature, obtains described container interior paint.
Embodiment five
The preparation method of a kind of high adhesion force antibacterial container interior paint, comprises the following steps:
(1) each component raw material is weighed by following weight: polyflon 53 parts, coumarone indene resin 19 parts, coconut alcohol 11 parts, bamboo fibre 4 parts, white carbon black 4 parts, dimethylolpropionic acid 5 parts, 80 mesh wheat metal plate stone powders 4 parts, acrylonitrile 3 parts, potassium peroxydisulfate 8 parts, 5 parts of sodium chloride, pentalyn 7 parts, ammonium molybdate 3 parts, dimethyl fumarate 8 parts, Lauryl Alcohol ester 10 parts, polydimethylsiloxane 4 parts, methanol 53 parts, glycerol 23 parts, Glacial acetic acid butyl ester 18 parts;
(2) methanol weighed, glycerol, Glacial acetic acid butyl ester are added in blender, adding polyflon, coumarone indene resin, coconut alcohol, acrylonitrile, sodium chloride, dimethyl fumarate, dimethylolpropionic acid, Lauryl Alcohol ester, at a temperature of 47 DEG C, stir 20min with mixing speed for 1500rpm;
(3) it is subsequently adding bamboo fibre, white carbon black, 80 mesh wheat metal plate stone powders, ammonium molybdate, is warming up to 72 DEG C, stirs 30min with mixing speed for 560rpm;
(4) it is cooled to 46 DEG C, adds remaining raw material, stir for 260rpm with mixing speed;
(5) through 100 mesh silk screen filter after having stirred, it is cooled to room temperature, obtains described container interior paint.
Comparative example one
This comparative example is in place of the difference of embodiment two, and without white carbon black, pentalyn and Lauryl Alcohol ester, other guide keeps constant.
Comparative example two
This comparative example is in place of the difference of embodiment two, and without wheat metal plate stone powder, dimethyl fumarate and potassium peroxydisulfate, other guide keeps constant.
Test case
Being coated on substrate by the coating of above-mentioned preparation, carry out properties test according to industry testing standard, its test result is as shown in the table:
As seen from the above table, the adhesive force of the coating prepared by the present invention is strong, and its adhesive force test grade is zero level;And good anti-bacterial effect, it is up to more than 94.2% to the antibiotic rate of staphylococcus aureus, colibacillary antibiotic rate is up to more than 95.4%.Additionally, the coating prepared by the present invention uses safety, raw material sources are extensively easy to get, manufacture method simple possible, be suitable for packaging industry and antibiotic property and wearability are required high field.
Claims (7)
1. a high adhesion force antibacterial container interior paint, it is characterized in that, it is prepared from by the raw material of following weight portion: polyflon 42-56 part, coumarone indene resin 15-21 part, coconut alcohol 8-14 part, bamboo fibre 3-7 part, white carbon black 4-9 part, dimethylolpropionic acid 3-10 part, 80 mesh wheat metal plate stone powder 2-6 parts, acrylonitrile 3-6 part, potassium peroxydisulfate 3-9 part, sodium chloride 5-8 part, pentalyn 2-8 part, ammonium molybdate 1-5 part, dimethyl fumarate 4-10 part, Lauryl Alcohol ester 6-12 part, polydimethylsiloxane 2-5 part, methanol 46-58 part, glycerol 21-35 part, Glacial acetic acid butyl ester 10-22 part.
High adhesion force the most according to claim 1 antibacterial container interior paint, it is characterized in that, the raw material of following weight portion be prepared from: polyflon 47 parts, coumarone indene resin 16 parts, coconut alcohol 9 parts, bamboo fibre 5 parts, white carbon black 6 parts, dimethylolpropionic acid 7 parts, 80 mesh wheat metal plate stone powders 5 parts, acrylonitrile 4 parts, potassium peroxydisulfate 7 parts, 6 parts of sodium chloride, pentalyn 5 parts, ammonium molybdate 2 parts, dimethyl fumarate 6 parts, Lauryl Alcohol ester 9 parts, polydimethylsiloxane 3 parts, methanol 48 parts, glycerol 29 parts, Glacial acetic acid butyl ester 15 parts.
High adhesion force the most according to claim 1 antibacterial container interior paint, it is characterized in that, the raw material of following weight portion be prepared from: polyflon 53 parts, coumarone indene resin 19 parts, coconut alcohol 11 parts, bamboo fibre 4 parts, white carbon black 4 parts, dimethylolpropionic acid 5 parts, 80 mesh wheat metal plate stone powders 4 parts, acrylonitrile 3 parts, potassium peroxydisulfate 8 parts, 5 parts of sodium chloride, pentalyn 7 parts, ammonium molybdate 3 parts, dimethyl fumarate 8 parts, Lauryl Alcohol ester 10 parts, polydimethylsiloxane 4 parts, methanol 53 parts, glycerol 23 parts, Glacial acetic acid butyl ester 18 parts.
4. the preparation method of the high adhesion force antibacterial container interior paint as described in any one of claim 1-3, it is characterised in that comprise the following steps:
(1) each component raw material is weighed by following weight;
(2) methanol weighed, glycerol, Glacial acetic acid butyl ester are added in blender, adding polyflon, coumarone indene resin, coconut alcohol, acrylonitrile, sodium chloride, dimethyl fumarate, dimethylolpropionic acid, Lauryl Alcohol ester, at a temperature of 40-52 DEG C, stir 15-40min with mixing speed for 1100-1800rpm;
(3) it is subsequently adding bamboo fibre, white carbon black, 80 mesh wheat metal plate stone powders, ammonium molybdate, is warming up to 60-78 DEG C, stirs 20-45min with mixing speed for 400-800rpm;
(4) it is cooled to 40-52 DEG C, adds remaining raw material, stir for 200-350rpm with mixing speed;
(5) through 100 mesh silk screen filter after having stirred, it is cooled to room temperature, obtains described container interior paint.
The preparation method of high adhesion force the most according to claim 4 antibacterial container interior paint, it is characterised in that in described step (2) at a temperature of 47 DEG C, stir 20min with mixing speed for 1500rpm.
The preparation method of high adhesion force the most according to claim 4 antibacterial container interior paint, it is characterised in that described step is warming up to 72 DEG C in (3), stirs 30min with mixing speed for 560rpm.
The preparation method of high adhesion force the most according to claim 4 antibacterial container interior paint, it is characterised in that described step is cooled to 46 DEG C in (4), stirs with mixing speed for 260rpm.
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Cited By (1)
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CN113943500A (en) * | 2021-11-24 | 2022-01-18 | 安徽固瑞特新材料科技有限公司 | Modified pyrolytic carbon black and preparation method and application thereof |
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Application publication date: 20160810 |
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