CN105817185B - A kind of rotary gas feed distributor suitable for heterophase reactor - Google Patents

A kind of rotary gas feed distributor suitable for heterophase reactor Download PDF

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Publication number
CN105817185B
CN105817185B CN201610189223.6A CN201610189223A CN105817185B CN 105817185 B CN105817185 B CN 105817185B CN 201610189223 A CN201610189223 A CN 201610189223A CN 105817185 B CN105817185 B CN 105817185B
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China
Prior art keywords
air inlet
inlet pipe
main air
nozzle
gas
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CN201610189223.6A
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Chinese (zh)
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CN105817185A (en
Inventor
罗明生
孙永伟
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Beijing Institute of Petrochemical Technology
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Beijing Institute of Petrochemical Technology
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Priority to CN201610189223.6A priority Critical patent/CN105817185B/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/20Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium
    • B01J8/22Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium gas being introduced into the liquid
    • B01J8/222Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium gas being introduced into the liquid in the presence of a rotating device only
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/1818Feeding of the fluidising gas
    • B01J8/1827Feeding of the fluidising gas the fluidising gas being a reactant
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2/00Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon
    • C10G2/30Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen
    • C10G2/32Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen with the use of catalysts
    • C10G2/34Apparatus, reactors
    • C10G2/342Apparatus, reactors with moving solid catalysts
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00796Details of the reactor or of the particulate material
    • B01J2208/00893Feeding means for the reactants
    • B01J2208/00902Nozzle-type feeding elements
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00796Details of the reactor or of the particulate material
    • B01J2208/00893Feeding means for the reactants
    • B01J2208/00911Sparger-type feeding elements

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Combustion & Propulsion (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • General Chemical & Material Sciences (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)

Abstract

The invention discloses a kind of rotary gas feed distributors suitable for heterophase reactor, the distributor includes main air inlet pipe, rotary joint, tiltedly charging distribution arms, lateral nozzle and longitudinal nozzle, the main air inlet pipe is located at the central position of the distributor, and cylinder structure vertical penetrates through entire distributor;The rotary joint is located at the centre of the main air inlet pipe, and can rotate freely;The rotary joint can remain stationary as the lower part of the main air inlet pipe, but the top of the main air inlet pipe can rotate freely;The charging distribution arms are connected and communicate with the top of the main air inlet pipe, and the oblique lateral nozzle and longitudinal nozzle are located in the charging distribution arms;When there is gas ejection in the longitudinal nozzle, the gas of ejection generates cornering force, pushes the rotation of the top of the charging distribution arms and the main air inlet pipe.The distributor can improve the uniformity of gas distribution, reduce the abrasion to catalyst, improve reaction efficiency.

Description

A kind of rotary gas feed distributor suitable for heterophase reactor
Technical field
The present invention relates to technical field of chemical more particularly to a kind of rotary gas suitable for heterophase reactor into Expect distributor.
Background technology
At present, in slurry reactor, gas raw material enters gas distributor by main air inlet pipe, in air inlet In the case of pressure stability, gas will be dispersed into charging distributor pipe, and enter slurry bed system eventually by the trepanning on distributor pipe Reactor drives the slurries (liquid and solid catalyst) in reactor to move and generation F- T synthesis is anti-under catalyst action Should, the fluid product of generation, which is separated by filtration, leaves reactor.
But slurry reactor of the prior art, entire gas distributor are not active, lead to unstripped gas It is unevenly distributed in the reactor, the undercompounding of gas and catalyst so that part generates high temperature, and catalyst abrasion is tight Weight.
Invention content
The object of the present invention is to provide a kind of rotary gas feed distributor suitable for heterophase reactor, the distributors The uniformity of gas distribution can be improved, reduces the abrasion to catalyst, improves reaction efficiency.
A kind of rotary gas feed distributor suitable for heterophase reactor, the distributor include main air inlet pipe, rotation Adapter, tiltedly charging distribution arms, lateral nozzle and longitudinal nozzle, wherein:
The main air inlet pipe is located at the central position of the distributor, the cylinder entire distribution of structure vertical perforation Device;
The rotary joint is located at the centre of the main air inlet pipe, and can rotate freely;
The rotary joint can remain stationary as the lower part of the main air inlet pipe, but the top of the main air inlet pipe can be freely Rotation;
The charging distribution arms are connected and communicate with the top of the main air inlet pipe, and the oblique lateral nozzle and longitudinal direction are sprayed Mouth is located in the charging distribution arms;
When having gas ejection in the oblique lateral nozzle and longitudinal nozzle, the gas of ejection generates thrust, described in promotion The top of charging distribution arms and the main air inlet pipe rotates counterclockwise.
As seen from the above technical solution provided by the invention, which can improve the uniformity of gas distribution, The abrasion to catalyst is reduced, reaction efficiency is improved, available for the F-T synthetic reactions based on paste state bed reactor.
Description of the drawings
In order to illustrate the technical solution of the embodiments of the present invention more clearly, required use in being described below to embodiment Attached drawing be briefly described, it should be apparent that, the accompanying drawings in the following description is only some embodiments of the present invention, for this For the those of ordinary skill in field, without creative efforts, other are can also be obtained according to these attached drawings Attached drawing.
The structure that Fig. 1 is provided by the embodiment of the present invention suitable for the rotary gas feed distributor of heterophase reactor is shown It is intended to;
The side that Fig. 2 is provided by the embodiment of the present invention suitable for the rotary gas feed distributor of heterophase reactor shows It is intended to.
Specific embodiment
With reference to the attached drawing in the embodiment of the present invention, the technical solution in the embodiment of the present invention is carried out clear, complete Ground describes, it is clear that described embodiment is only part of the embodiment of the present invention, instead of all the embodiments.Based on this The embodiment of invention, the every other implementation that those of ordinary skill in the art are obtained without making creative work Example, belongs to protection scope of the present invention.
The embodiment of the present invention is described in further detail below in conjunction with attached drawing, is implemented as shown in Figure 1 for the present invention Example provides suitable for heterophase reactor rotary gas feed distributor structure diagram, the distributor including lead into Tracheae 1, rotary joint 2, tiltedly charging distribution arms 3, lateral nozzle 4 and longitudinal nozzle 5, wherein:
The main air inlet pipe 1 is located at the central position of the distributor, the cylinder entire distribution of structure vertical perforation Device;
The rotary joint 2 is located at the centre of the main air inlet pipe 1, and the effect of the rotary joint 2 is can be in inside Under conditions of having liquid medium, and it can rotate freely;
The rotary joint 2 can remain stationary as the lower part of the main air inlet pipe 1, but the top energy of the main air inlet pipe 1 It rotates freely;
The charging distribution arms 3 are connected and communicate with the top of the main air inlet pipe 1, the oblique lateral nozzle 4 and indulge It is located in the charging distribution arms 3 to nozzle 5;
When having gas ejection in the oblique lateral nozzle 4 and longitudinal nozzle 5, the gas of ejection generates thrust, pushes institute The top for stating charging distribution arms 3 and the main air inlet pipe 1 rotates counterclockwise.
In addition, charging distribution arms is pushed to rotate using the unstrpped gas that tiltedly lateral nozzle 4 is discharged, so as to drive charging point After cloth branch pipe 3 and its exhaust outlet rotation, unstripped gas is more uniform from exhaust outlet discharge distribution, so as to make the mixed of gas and catalyst Conjunction is more abundant, the problem of improving reaction efficiency, avoid hot-spot, alleviates the abrasion of catalyst.
In the specific implementation, the upper connection of the distributor uses self sealing structure, and use stainless steel or engineering plastics It makes.
The side schematic view of the gas feed distributor is illustrated in figure 2, as can be seen from Figure:The tiltedly gas of transverse direction nozzle 4 Body injection direction is 45 degree of obliquely downward of horizontal direction, and the gas injection direction of longitudinal nozzle 5 is vertical downward direction.
Meanwhile during realization, the gas discharged in oblique transverse direction nozzle 4 and longitudinal nozzle 5 will not be fixed at one Position is moved with the rotation of charging distribution arms 3, when distribution arms 3 rotate to different location, oblique transverse direction 4 He of nozzle Longitudinal nozzle 5 also can discharge gas in corresponding position.
In conclusion the distributor that the embodiment of the present invention is provided can improve the uniformity of gas distribution, reduce to urging The abrasion of agent improves reaction efficiency.
The foregoing is only a preferred embodiment of the present invention, but protection scope of the present invention be not limited thereto, Any one skilled in the art is in the technical scope of present disclosure, the change or replacement that can readily occur in, It should be covered by the protection scope of the present invention.Therefore, protection scope of the present invention should be with the protection model of claims Subject to enclosing.

Claims (4)

1. a kind of rotary gas feed distributor suitable for heterophase reactor, which is characterized in that the distributor includes master Air inlet pipe, rotary joint, tiltedly charging distribution arms, lateral nozzle and longitudinal nozzle, wherein:
The main air inlet pipe is located at the central position of the distributor, and cylinder structure vertical penetrates through entire distributor;
The rotary joint is located at the centre of the main air inlet pipe, and can rotate freely;
The rotary joint can remain stationary as the lower part of the main air inlet pipe, but the top of the main air inlet pipe can freely revolve Turn;
The charging distribution arms are connected and communicate with the top of the main air inlet pipe, the oblique lateral nozzle and longitudinal nozzle position In in the charging distribution arms;
When having gas ejection in the oblique lateral nozzle and longitudinal nozzle, the gas of ejection generates thrust, pushes the charging The top of distribution arms and the main air inlet pipe rotates counterclockwise;
Further, the gas injection direction of the oblique lateral nozzle is 45 degree of obliquely downward of horizontal direction, and the longitudinal direction is sprayed The gas injection direction of mouth is vertical downward direction.
2. it is suitable for the rotary gas feed distributor of heterophase reactor according to claim 1, which is characterized in that
The charging distribution arms is pushed to rotate, and then drive the charging distribution using the unstrpped gas of oblique lateral nozzle discharge Branch pipe and its nozzle rotation.
3. it is suitable for the rotary gas feed distributor of heterophase reactor according to claim 1, which is characterized in that
The rotary joint of the distributor uses self sealing structure, and is made of stainless steel or engineering plastics.
4. it is suitable for the rotary gas feed distributor of heterophase reactor according to claim 1, which is characterized in that
The gas discharged in the oblique lateral nozzle and longitudinal nozzle will not be a fixed position, with charging distribution arms Rotation and move.
CN201610189223.6A 2016-03-29 2016-03-29 A kind of rotary gas feed distributor suitable for heterophase reactor Active CN105817185B (en)

Priority Applications (1)

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CN201610189223.6A CN105817185B (en) 2016-03-29 2016-03-29 A kind of rotary gas feed distributor suitable for heterophase reactor

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Application Number Priority Date Filing Date Title
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CN105817185B true CN105817185B (en) 2018-07-03

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CN107979009A (en) * 2017-12-29 2018-05-01 天津宇拓电源有限公司 Three-phase voltage collector distribution transformer box
CN108465315A (en) * 2018-05-07 2018-08-31 河南省中原大化集团有限责任公司 High pressure is passivated air compressor unit blowdown separating and reclaiming device and application process
CN110523262A (en) * 2019-08-12 2019-12-03 芜湖职业技术学院 A kind of biological filter deodorizing device
CN112546974B (en) * 2019-09-26 2022-10-11 中国石油化工股份有限公司 Fluidized bed reactor for preparing olefin from methanol
CN110787629B (en) * 2019-12-09 2022-02-08 安徽顺达环保科技股份有限公司 Cement kiln high temperature high dust SCR denitrification facility

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US4646637A (en) * 1985-12-26 1987-03-03 Cloots Henry R Method and apparatus for fluidized bed combustion
CN201127855Y (en) * 2007-11-07 2008-10-08 浙江工业大学 Concentric ring type cross flow type high gravity field swinging bed device
CN101618304B (en) * 2008-07-04 2011-09-21 中国石油化工股份有限公司 Esterification reactor
CN202113844U (en) * 2011-06-15 2012-01-18 北京工业大学 Gas-liquid-phase reaction unit with gas in rotary pulsation distribution
CN202478904U (en) * 2012-02-24 2012-10-10 刘小可 Gas distributor and gas-liquid-solid three-phase reactor

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